CA3016924A1 - Method for producing nickel powder - Google Patents
Method for producing nickel powder Download PDFInfo
- Publication number
- CA3016924A1 CA3016924A1 CA3016924A CA3016924A CA3016924A1 CA 3016924 A1 CA3016924 A1 CA 3016924A1 CA 3016924 A CA3016924 A CA 3016924A CA 3016924 A CA3016924 A CA 3016924A CA 3016924 A1 CA3016924 A1 CA 3016924A1
- Authority
- CA
- Canada
- Prior art keywords
- nickel
- nickel powder
- slurry
- precipitate
- seed crystals
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Abandoned
Links
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 title claims abstract description 168
- 238000004519 manufacturing process Methods 0.000 title abstract description 12
- 229910052759 nickel Inorganic materials 0.000 claims abstract description 58
- 239000013078 crystal Substances 0.000 claims abstract description 29
- 238000006243 chemical reaction Methods 0.000 claims abstract description 28
- 238000000034 method Methods 0.000 claims abstract description 24
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims abstract description 21
- 239000002244 precipitate Substances 0.000 claims abstract description 15
- 150000002500 ions Chemical class 0.000 claims abstract description 4
- 239000002002 slurry Substances 0.000 claims description 33
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims description 13
- 239000007792 gaseous phase Substances 0.000 claims description 9
- 239000002270 dispersing agent Substances 0.000 claims description 8
- 239000002245 particle Substances 0.000 claims description 7
- 239000007791 liquid phase Substances 0.000 claims description 6
- 238000007664 blowing Methods 0.000 claims description 5
- 239000001257 hydrogen Substances 0.000 claims description 5
- 229910052739 hydrogen Inorganic materials 0.000 claims description 5
- 229920000058 polyacrylate Polymers 0.000 claims description 3
- 150000003839 salts Chemical class 0.000 claims description 3
- LGQLOGILCSXPEA-UHFFFAOYSA-L nickel sulfate Chemical compound [Ni+2].[O-]S([O-])(=O)=O LGQLOGILCSXPEA-UHFFFAOYSA-L 0.000 abstract description 5
- 229910000363 nickel(II) sulfate Inorganic materials 0.000 abstract description 5
- 239000011268 mixed slurry Substances 0.000 abstract 2
- 239000000243 solution Substances 0.000 description 30
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 6
- 230000000694 effects Effects 0.000 description 6
- 229920001495 poly(sodium acrylate) polymer Polymers 0.000 description 4
- 239000000843 powder Substances 0.000 description 4
- NNMHYFLPFNGQFZ-UHFFFAOYSA-M sodium polyacrylate Chemical compound [Na+].[O-]C(=O)C=C NNMHYFLPFNGQFZ-UHFFFAOYSA-M 0.000 description 4
- 239000003638 chemical reducing agent Substances 0.000 description 3
- 239000011259 mixed solution Substances 0.000 description 3
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 2
- OAKJQQAXSVQMHS-UHFFFAOYSA-N Hydrazine Chemical compound NN OAKJQQAXSVQMHS-UHFFFAOYSA-N 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 229910021529 ammonia Inorganic materials 0.000 description 2
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 description 2
- 229910052921 ammonium sulfate Inorganic materials 0.000 description 2
- 235000011130 ammonium sulphate Nutrition 0.000 description 2
- 238000000889 atomisation Methods 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 239000006185 dispersion Substances 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 238000005979 thermal decomposition reaction Methods 0.000 description 2
- VEQPNABPJHWNSG-UHFFFAOYSA-N Nickel(2+) Chemical compound [Ni+2] VEQPNABPJHWNSG-UHFFFAOYSA-N 0.000 description 1
- UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 description 1
- -1 adding Chemical compound 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 239000003985 ceramic capacitor Substances 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 229910017052 cobalt Inorganic materials 0.000 description 1
- 239000010941 cobalt Substances 0.000 description 1
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000010419 fine particle Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 238000009854 hydrometallurgy Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000013462 industrial intermediate Substances 0.000 description 1
- 238000005342 ion exchange Methods 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 229910001453 nickel ion Inorganic materials 0.000 description 1
- 229910000480 nickel oxide Inorganic materials 0.000 description 1
- 229910000008 nickel(II) carbonate Inorganic materials 0.000 description 1
- ZULUUIKRFGGGTL-UHFFFAOYSA-L nickel(ii) carbonate Chemical compound [Ni+2].[O-]C([O-])=O ZULUUIKRFGGGTL-UHFFFAOYSA-L 0.000 description 1
- BFDHFSHZJLFAMC-UHFFFAOYSA-L nickel(ii) hydroxide Chemical compound [OH-].[OH-].[Ni+2] BFDHFSHZJLFAMC-UHFFFAOYSA-L 0.000 description 1
- GNRSAWUEBMWBQH-UHFFFAOYSA-N oxonickel Chemical compound [Ni]=O GNRSAWUEBMWBQH-UHFFFAOYSA-N 0.000 description 1
- 238000004663 powder metallurgy Methods 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F9/00—Making metallic powder or suspensions thereof
- B22F9/16—Making metallic powder or suspensions thereof using chemical processes
- B22F9/18—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds
- B22F9/24—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds starting from liquid metal compounds, e.g. solutions
- B22F9/26—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds starting from liquid metal compounds, e.g. solutions using gaseous reductors
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
- B22F1/05—Metallic powder characterised by the size or surface area of the particles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F9/00—Making metallic powder or suspensions thereof
- B22F9/16—Making metallic powder or suspensions thereof using chemical processes
- B22F9/18—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds
- B22F9/24—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds starting from liquid metal compounds, e.g. solutions
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F2201/00—Treatment under specific atmosphere
- B22F2201/01—Reducing atmosphere
- B22F2201/013—Hydrogen
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F2301/00—Metallic composition of the powder or its coating
- B22F2301/15—Nickel or cobalt
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F2304/00—Physical aspects of the powder
- B22F2304/10—Micron size particles, i.e. above 1 micrometer up to 500 micrometer
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F2999/00—Aspects linked to processes or compositions used in powder metallurgy
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Metal Powder And Suspensions Thereof (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Powder Metallurgy (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2016038185A JP2017155265A (ja) | 2016-02-29 | 2016-02-29 | ニッケル粉の製造方法 |
| JP2016-038185 | 2016-02-29 | ||
| PCT/JP2017/004499 WO2017150105A1 (ja) | 2016-02-29 | 2017-02-08 | ニッケル粉の製造方法 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA3016924A1 true CA3016924A1 (en) | 2017-09-08 |
Family
ID=59743801
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA3016924A Abandoned CA3016924A1 (en) | 2016-02-29 | 2017-02-08 | Method for producing nickel powder |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US20210197266A1 (cg-RX-API-DMAC7.html) |
| EP (1) | EP3424625A4 (cg-RX-API-DMAC7.html) |
| JP (1) | JP2017155265A (cg-RX-API-DMAC7.html) |
| CN (1) | CN108698131A (cg-RX-API-DMAC7.html) |
| AU (1) | AU2017227099A1 (cg-RX-API-DMAC7.html) |
| CA (1) | CA3016924A1 (cg-RX-API-DMAC7.html) |
| PH (1) | PH12018501840A1 (cg-RX-API-DMAC7.html) |
| WO (1) | WO2017150105A1 (cg-RX-API-DMAC7.html) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP7007650B2 (ja) * | 2018-07-31 | 2022-01-24 | 住友金属鉱山株式会社 | ニッケル粉の製造方法 |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA2359347A1 (en) | 2001-10-18 | 2003-04-18 | Cesur Celik | Laminated ceramic capacitor internal electrode material |
| KR101014158B1 (ko) | 2002-08-28 | 2011-02-14 | 도호 티타늄 가부시키가이샤 | 금속 니켈 분말 및 그 제조 방법 |
| JP2009079239A (ja) * | 2007-09-25 | 2009-04-16 | Sumitomo Electric Ind Ltd | ニッケル粉末、またはニッケルを主成分とする合金粉末およびその製造方法、導電性ペースト、並びに積層セラミックコンデンサ |
| CN101428349B (zh) * | 2008-07-29 | 2011-06-22 | 张建玲 | 一种镍钴金属粉末的制备方法 |
| JP5407495B2 (ja) | 2009-04-02 | 2014-02-05 | 住友電気工業株式会社 | 金属粉末および金属粉末製造方法、導電性ペースト、並びに積層セラミックコンデンサ |
| JP5828923B2 (ja) * | 2014-01-30 | 2015-12-09 | 国立大学法人高知大学 | ニッケル粉の製造方法 |
| JP5881091B2 (ja) * | 2014-02-17 | 2016-03-09 | 住友金属鉱山株式会社 | ニッケル粉の製造方法 |
| CA2939809C (en) * | 2014-02-21 | 2017-08-22 | Kochi University, National University Corporation | Method for producing nickel powder |
| JP6442298B2 (ja) * | 2014-03-26 | 2018-12-19 | 国立大学法人高知大学 | ニッケル粉の製造方法 |
| JP5796696B1 (ja) * | 2015-01-22 | 2015-10-21 | 住友金属鉱山株式会社 | ニッケル粉の製造方法 |
| JP6610425B2 (ja) * | 2015-08-31 | 2019-11-27 | 住友金属鉱山株式会社 | ニッケル粉の製造方法 |
-
2016
- 2016-02-29 JP JP2016038185A patent/JP2017155265A/ja active Pending
-
2017
- 2017-02-08 CN CN201780013765.0A patent/CN108698131A/zh active Pending
- 2017-02-08 CA CA3016924A patent/CA3016924A1/en not_active Abandoned
- 2017-02-08 EP EP17759576.6A patent/EP3424625A4/en not_active Withdrawn
- 2017-02-08 WO PCT/JP2017/004499 patent/WO2017150105A1/ja not_active Ceased
- 2017-02-08 AU AU2017227099A patent/AU2017227099A1/en not_active Abandoned
- 2017-02-08 US US16/080,363 patent/US20210197266A1/en not_active Abandoned
-
2018
- 2018-08-29 PH PH12018501840A patent/PH12018501840A1/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| EP3424625A4 (en) | 2019-11-20 |
| WO2017150105A1 (ja) | 2017-09-08 |
| US20210197266A1 (en) | 2021-07-01 |
| CN108698131A (zh) | 2018-10-23 |
| JP2017155265A (ja) | 2017-09-07 |
| EP3424625A1 (en) | 2019-01-09 |
| PH12018501840A1 (en) | 2019-05-15 |
| AU2017227099A1 (en) | 2018-09-13 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FZDE | Discontinued |
Effective date: 20210219 |