CA2950379C - Urea composition and method for producing same - Google Patents

Urea composition and method for producing same Download PDF

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Publication number
CA2950379C
CA2950379C CA2950379A CA2950379A CA2950379C CA 2950379 C CA2950379 C CA 2950379C CA 2950379 A CA2950379 A CA 2950379A CA 2950379 A CA2950379 A CA 2950379A CA 2950379 C CA2950379 C CA 2950379C
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CA
Canada
Prior art keywords
urea
composition
component
iii
particulate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CA2950379A
Other languages
English (en)
French (fr)
Other versions
CA2950379A1 (en
Inventor
Thomas KRAWCZYK
Matthias Potthoff
Luc Vanmarcke
Erik Alexander Bijpost
Alexander Maslow
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
ThyssenKrupp AG
Uhde Fertilizer Technology BV
Original Assignee
ThyssenKrupp AG
Uhde Fertilizer Technology BV
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
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Publication of CA2950379A1 publication Critical patent/CA2950379A1/en
Application granted granted Critical
Publication of CA2950379C publication Critical patent/CA2950379C/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23K—FODDER
    • A23K20/00—Accessory food factors for animal feeding-stuffs
    • A23K20/10—Organic substances
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23K—FODDER
    • A23K40/00—Shaping or working-up of animal feeding-stuffs
    • A23K40/10—Shaping or working-up of animal feeding-stuffs by agglomeration; by granulation, e.g. making powders
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23K—FODDER
    • A23K50/00—Feeding-stuffs specially adapted for particular animals
    • A23K50/10—Feeding-stuffs specially adapted for particular animals for ruminants
    • A23K50/15—Feeding-stuffs specially adapted for particular animals for ruminants containing substances which are metabolically converted to proteins, e.g. ammonium salts or urea
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K31/00—Medicinal preparations containing organic active ingredients
    • A61K31/16—Amides, e.g. hydroxamic acids
    • A61K31/17—Amides, e.g. hydroxamic acids having the group >N—C(O)—N< or >N—C(S)—N<, e.g. urea, thiourea, carmustine
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K47/00—Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
    • A61K47/06—Organic compounds, e.g. natural or synthetic hydrocarbons, polyolefins, mineral oil, petrolatum or ozokerite
    • A61K47/08—Organic compounds, e.g. natural or synthetic hydrocarbons, polyolefins, mineral oil, petrolatum or ozokerite containing oxygen, e.g. ethers, acetals, ketones, quinones, aldehydes, peroxides
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K47/00—Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
    • A61K47/06—Organic compounds, e.g. natural or synthetic hydrocarbons, polyolefins, mineral oil, petrolatum or ozokerite
    • A61K47/08—Organic compounds, e.g. natural or synthetic hydrocarbons, polyolefins, mineral oil, petrolatum or ozokerite containing oxygen, e.g. ethers, acetals, ketones, quinones, aldehydes, peroxides
    • A61K47/12—Carboxylic acids; Salts or anhydrides thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K47/00—Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
    • A61K47/30—Macromolecular organic or inorganic compounds, e.g. inorganic polyphosphates
    • A61K47/32—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds, e.g. carbomers, poly(meth)acrylates, or polyvinyl pyrrolidone
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K47/00—Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
    • A61K47/30—Macromolecular organic or inorganic compounds, e.g. inorganic polyphosphates
    • A61K47/34—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polyesters, polyamino acids, polysiloxanes, polyphosphazines, copolymers of polyalkylene glycol or poloxamers
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K9/00—Medicinal preparations characterised by special physical form
    • A61K9/0012—Galenical forms characterised by the site of application
    • A61K9/0053—Mouth and digestive tract, i.e. intraoral and peroral administration
    • A61K9/0056—Mouth soluble or dispersible forms; Suckable, eatable, chewable coherent forms; Forms rapidly disintegrating in the mouth; Lozenges; Lollipops; Bite capsules; Baked products; Baits or other oral forms for animals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
    • B01J2/003—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic followed by coating of the granules
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
    • B01J2/16—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by suspending the powder material in a gas, e.g. in fluidised beds or as a falling curtain
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05C—NITROGENOUS FERTILISERS
    • C05C9/00—Fertilisers containing urea or urea compounds
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05C—NITROGENOUS FERTILISERS
    • C05C9/00—Fertilisers containing urea or urea compounds
    • C05C9/005—Post-treatment
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G5/00—Fertilisers characterised by their form
    • C05G5/10—Solid or semi-solid fertilisers, e.g. powders
    • C05G5/12—Granules or flakes
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C273/00—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
    • C07C273/02—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds
    • C07C273/14—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00—Processes of treating or compounding macromolecular substances
    • C08J3/12—Powdering or granulating
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2339/00—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a single or double bond to nitrogen or by a heterocyclic ring containing nitrogen; Derivatives of such polymers
    • C08J2339/02—Homopolymers or copolymers of vinylamine
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2379/00—Characterised by the use of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing nitrogen with or without oxygen, or carbon only, not provided for in groups C08J2361/00 - C08J2377/00
    • C08J2379/02—Polyamines
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2439/00—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a single or double bond to nitrogen or by a heterocyclic ring containing nitrogen; Derivatives of such polymers
    • C08J2439/02—Homopolymers or copolymers of vinylamine
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2479/00—Characterised by the use of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing nitrogen with or without oxygen, or carbon only, not provided for in groups C08J2461/00 - C08J2477/00
    • C08J2479/02—Polyamines

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Organic Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Veterinary Medicine (AREA)
  • Medicinal Chemistry (AREA)
  • Animal Behavior & Ethology (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Epidemiology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Zoology (AREA)
  • Food Science & Technology (AREA)
  • Animal Husbandry (AREA)
  • Pest Control & Pesticides (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • General Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Birds (AREA)
  • Nutrition Science (AREA)
  • Physiology (AREA)
  • Proteomics, Peptides & Aminoacids (AREA)
  • Fertilizers (AREA)
  • Fodder In General (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
CA2950379A 2014-06-20 2015-06-17 Urea composition and method for producing same Active CA2950379C (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE102014108703.8A DE102014108703A1 (de) 2014-06-20 2014-06-20 Harnstoffzusammensetzung und Verfahren zu ihrer Herstellung
DE102014108703.8 2014-06-20
PCT/EP2015/063599 WO2015193377A1 (de) 2014-06-20 2015-06-17 Harnstoffzusammensetzung und verfahren zu ihrer herstellung

Publications (2)

Publication Number Publication Date
CA2950379A1 CA2950379A1 (en) 2015-12-23
CA2950379C true CA2950379C (en) 2020-04-21

Family

ID=53524731

Family Applications (1)

Application Number Title Priority Date Filing Date
CA2950379A Active CA2950379C (en) 2014-06-20 2015-06-17 Urea composition and method for producing same

Country Status (11)

Country Link
US (1) US10106469B2 (enExample)
EP (1) EP3157889B1 (enExample)
JP (1) JP6530771B2 (enExample)
CN (1) CN106458782B (enExample)
CA (1) CA2950379C (enExample)
DE (1) DE102014108703A1 (enExample)
EA (1) EA032215B1 (enExample)
MY (1) MY177438A (enExample)
PL (1) PL3157889T3 (enExample)
SA (1) SA516380533B1 (enExample)
WO (1) WO2015193377A1 (enExample)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3112332A1 (en) 2015-07-03 2017-01-04 Casale SA Method for producing solid urea by granulation
DE102015122070A1 (de) * 2015-12-17 2017-06-22 Thyssenkrupp Ag Harnstoffhaltige Düngemittel und Verfahren zu ihrer Herstellung
LT3484601T (lt) * 2016-07-15 2021-04-26 Thyssenkrupp Fertilizer Technology Gmbh Karbamido kompozicijos panaudojimas dyzelio išmetamųjų dujų skysčio gavimui
DE102017108842A1 (de) 2017-04-25 2018-10-25 Thyssenkrupp Ag Verfahren und Vorrichtung zur Herstellung von Harnstoff
DE102018215427A1 (de) * 2018-09-11 2020-03-12 Skw Stickstoffwerke Piesteritz Gmbh Pelletierter Harnstoff in zylindrischer Form als Schüttgut und Methode zur Herstellung davon
WO2020142707A1 (en) * 2019-01-03 2020-07-09 Aqua Yield Operations LLC Pamam dendrimers for fertilizer delivery
FR3162442A1 (fr) * 2024-05-27 2025-11-28 Snf Sa Composition adhésive de crépage

Family Cites Families (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR1021100A (fr) * 1949-07-20 1953-02-13 Basf Ag Procédé pour la production d'urée
GB1581761A (en) 1977-06-09 1980-12-17 Azote Sa Cie Neerlandaise Urea granulation
NO148744C (no) * 1977-09-19 1983-12-07 Norsk Hydro As Fremgangsmaate til fremstilling av urea med hoey mekanisk styrke
DE4131345A1 (de) * 1991-09-20 1993-03-25 Bayer Ag Granulate aus pulvrigen primaerpartikeln mit verbesserten verarbeitungseigenschaften
EP0701543A4 (en) 1993-05-07 1997-10-22 Univ New England METHOD FOR PACKING GRAINED FERTILIZER
DE19826570C2 (de) 1998-06-15 2002-10-31 Piesteritz Stickstoff Verfahren zur Herstellung von Harnstoff und Ammonsulfat enthaltenden Düngemittel-Granulaten
JP2001247392A (ja) * 2000-03-01 2001-09-11 Miyoshi Oil & Fat Co Ltd 徐放性肥料の製造方法及び徐放性肥料
JP4050052B2 (ja) * 2001-01-29 2008-02-20 三菱化学株式会社 被覆粒状肥料
US6884756B2 (en) * 2001-09-14 2005-04-26 The Andersons Agriservices, Inc. Water-dispersible pellets
WO2005040072A1 (en) * 2003-10-06 2005-05-06 Yara International Asa A method of improving the properties of urea granules
NO321761B1 (no) * 2004-06-30 2006-07-03 Yara Int Asa Fremgangsmate for a forbedre knusestyrke og redusere stovdannelse og tendens til kaking av urea, partikler, og anvendelse av karbohydrater og eventuelt polyvinylforbindelser som additiv til smeltet urea
FR2874008B1 (fr) * 2004-08-06 2007-02-23 Snf Sas Soc Par Actions Simpli Granules d'engrais et procede de fabrication
CN1279000C (zh) * 2004-11-16 2006-10-11 王威 高氮大颗粒尿素生产工艺
WO2006091077A1 (en) * 2005-01-14 2006-08-31 Yara International Asa Urea composition having reduced compressibility, caking and dust formation, and process for its preparation
NL1028019C2 (nl) * 2005-01-14 2006-07-17 Holland Novochem B V Werkwijze ter vervaardiging van minerale olie-vrije, vrijvloeiende granulaatdeeltjes van een plantenhulpstof.
EP2192099A1 (en) 2008-11-28 2010-06-02 Uhde Fertilizer Technology B.V. Urea granulation process with an acidic scrubbing system and the subsequent integration of ammonium salt into urea granules
CN101613244A (zh) * 2009-08-07 2009-12-30 中国-阿拉伯化肥有限公司 一种提高尿基肥成粒性能的方法

Also Published As

Publication number Publication date
PL3157889T3 (pl) 2020-05-18
EA201790049A1 (ru) 2017-04-28
EA032215B1 (ru) 2019-04-30
EP3157889B1 (de) 2019-11-20
CN106458782A (zh) 2017-02-22
MY177438A (en) 2020-09-15
DE102014108703A1 (de) 2015-12-24
JP2017524635A (ja) 2017-08-31
SA516380533B1 (ar) 2020-08-18
WO2015193377A1 (de) 2015-12-23
JP6530771B2 (ja) 2019-06-12
EP3157889A1 (de) 2017-04-26
CA2950379A1 (en) 2015-12-23
CN106458782B (zh) 2020-05-12
US10106469B2 (en) 2018-10-23
US20170190632A1 (en) 2017-07-06

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