CA2772971C - Method for the separation of ammonia and carbon dioxide from aqueous solutions - Google Patents

Method for the separation of ammonia and carbon dioxide from aqueous solutions Download PDF

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Publication number
CA2772971C
CA2772971C CA2772971A CA2772971A CA2772971C CA 2772971 C CA2772971 C CA 2772971C CA 2772971 A CA2772971 A CA 2772971A CA 2772971 A CA2772971 A CA 2772971A CA 2772971 C CA2772971 C CA 2772971C
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CA
Canada
Prior art keywords
ammonia
aqueous solution
carbon dioxide
tons
day
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CA2772971A
Other languages
English (en)
French (fr)
Other versions
CA2772971A1 (en
Inventor
Paolo Casara
Alessandro Gianazza
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Saipem SpA
Original Assignee
Saipem SpA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Saipem SpA filed Critical Saipem SpA
Publication of CA2772971A1 publication Critical patent/CA2772971A1/en
Application granted granted Critical
Publication of CA2772971C publication Critical patent/CA2772971C/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/36—Pervaporation; Membrane distillation; Liquid permeation
    • B01D61/364—Membrane distillation
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00—Ammonia; Compounds thereof
    • C01C1/02—Preparation, purification or separation of ammonia
    • C01C1/10—Separation of ammonia from ammonia liquors, e.g. gas liquors
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/44—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis
    • C02F1/447—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis by membrane distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C273/00—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
    • C07C273/02—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds
    • C07C273/04—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds from carbon dioxide and ammonia
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2313/00—Details relating to membrane modules or apparatus
    • B01D2313/22—Cooling or heating elements
    • B01D2313/221—Heat exchangers
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/02—Treatment of water, waste water, or sewage by heating
    • C02F1/04—Treatment of water, waste water, or sewage by heating by distillation or evaporation
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/44—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2101/00—Nature of the contaminant
    • C02F2101/10—Inorganic compounds
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2101/00—Nature of the contaminant
    • C02F2101/10—Inorganic compounds
    • C02F2101/16—Nitrogen compounds, e.g. ammonia
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2103/00—Nature of the water, waste water, sewage or sludge to be treated
    • C02F2103/34—Nature of the water, waste water, sewage or sludge to be treated from industrial activities not provided for in groups C02F2103/12 - C02F2103/32
    • C02F2103/36—Nature of the water, waste water, sewage or sludge to be treated from industrial activities not provided for in groups C02F2103/12 - C02F2103/32 from the manufacture of organic compounds

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Water Supply & Treatment (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Environmental & Geological Engineering (AREA)
  • Hydrology & Water Resources (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Carbon And Carbon Compounds (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)
  • Physical Water Treatments (AREA)
CA2772971A 2009-09-09 2010-09-01 Method for the separation of ammonia and carbon dioxide from aqueous solutions Active CA2772971C (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
ITMI2009A001551A IT1395383B1 (it) 2009-09-09 2009-09-09 Metodo di separazione di ammoniaca e diossido di carbonio da soluzioni acquose
ITMI2009A001551 2009-09-09
PCT/EP2010/005609 WO2011029625A1 (en) 2009-09-09 2010-09-01 Method for the separation of ammonia and carbon dioxide from aqueous solutions

Publications (2)

Publication Number Publication Date
CA2772971A1 CA2772971A1 (en) 2011-03-17
CA2772971C true CA2772971C (en) 2018-05-22

Family

ID=42102137

Family Applications (1)

Application Number Title Priority Date Filing Date
CA2772971A Active CA2772971C (en) 2009-09-09 2010-09-01 Method for the separation of ammonia and carbon dioxide from aqueous solutions

Country Status (12)

Country Link
US (2) US9266745B2 (https=)
EP (1) EP2475617B1 (https=)
JP (1) JP5753170B2 (https=)
CN (1) CN102695675B (https=)
BR (1) BR112012005238B1 (https=)
CA (1) CA2772971C (https=)
EA (1) EA022152B1 (https=)
EG (1) EG26889A (https=)
IT (1) IT1395383B1 (https=)
MX (1) MX339596B (https=)
MY (1) MY162327A (https=)
WO (1) WO2011029625A1 (https=)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
IT1395383B1 (it) * 2009-09-09 2012-09-14 Saipem Spa Metodo di separazione di ammoniaca e diossido di carbonio da soluzioni acquose
CN102989319A (zh) * 2011-09-16 2013-03-27 中国科学院生态环境研究中心 一种微波强化膜蒸馏过程的装置及方法
CN103998115B (zh) * 2011-11-17 2015-11-25 义安理工学院 用于膜蒸馏应用的三层疏水-亲水膜
WO2013165245A1 (en) * 2012-05-03 2013-11-07 Stamicarbon B.V. Urea production plant
EP2690090A1 (en) * 2012-07-27 2014-01-29 Urea Casale SA Concentration of the urea solution in a process for the synthesis of urea
US20140263061A1 (en) * 2013-03-15 2014-09-18 Celgard, Llc Membrane contactors and systems for membrane distillation or ammonia removal and related methods
US10828606B2 (en) * 2017-10-25 2020-11-10 New Jersey Institute Of Technology Radiative treatment of liquids in desalination and other membrane processes
CN115893414B (zh) * 2022-11-28 2025-04-22 吉林卓创新材料有限公司 一种一氧化碳中微量氨气的去除方法
CN118526802B (zh) * 2024-05-27 2025-02-14 武汉大学 一种基于膜蒸馏的氨液回收固碳一体化系统及方法

Family Cites Families (26)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4424072A (en) * 1982-07-01 1984-01-03 Lerner Bernard J Prilling
IN169678B (https=) 1987-08-13 1991-11-30 Austral Pacific Fertilizers
US5256296A (en) * 1990-12-28 1993-10-26 Membrane Technology & Research Membrane process and apparatus for removing a component from a fluid stream
NL9401233A (nl) * 1994-03-25 1995-11-01 Tno Werkwijze voor membraangasabsorptie.
DE29510582U1 (de) * 1995-06-26 1995-09-07 Schmidt, Heinz Dietmar, Dipl.-Biologe, 21224 Rosengarten Vorrichtung zur Gewinnung von Ammoniak aus ammoniakhaltigen wäßrigen Flüssigkeiten
US5670053A (en) * 1995-08-07 1997-09-23 Zenon Environmental, Inc. Purification of gases from water using reverse osmosis
US5766479A (en) * 1995-08-07 1998-06-16 Zenon Environmental Inc. Production of high purity water using reverse osmosis
DE19704508A1 (de) * 1996-09-27 1998-08-13 Gore W L & Ass Gmbh Gasabsorption mit Membrankontaktoren
US20020014154A1 (en) * 1996-09-27 2002-02-07 Richard Witzko Separation of gaseous components from a gas stream with a liquid absorbent
US5876604A (en) * 1996-10-24 1999-03-02 Compact Membrane Systems, Inc Method of gasifying or degasifying a liquid
US6086768A (en) * 1998-09-08 2000-07-11 Porocrit L.L.C. Method for demulsification of emulsions containing dense gas and liquid and a surfactant
NL1012575C2 (nl) * 1999-07-12 2001-01-15 Continental Engineering B V Werkwijze ter bereiding van ureum.
JP2004148208A (ja) * 2002-10-30 2004-05-27 Mitsui Eng & Shipbuild Co Ltd 膜分離方法及びその装置
US7381858B2 (en) * 2004-01-30 2008-06-03 Bp Corporation North America Inc. Xylene process using perm-selective separations
EP1925355A1 (en) * 2006-10-31 2008-05-28 Nederlandse Organisatie voor toegepast- natuurwetenschappelijk onderzoek TNO Membrane distillation method for the purification of a liquid
ITMI20071029A1 (it) * 2007-05-22 2008-11-23 Snam Progetti Procedimento migliorato per la sintesi di urea
US8349130B2 (en) * 2007-07-26 2013-01-08 Fpinnovations Process for treating pulp mill condenstates using a hollow fiber contactor
ITMI20072206A1 (it) * 2007-11-21 2009-05-22 Snam Progetti Metodo per il recupero di ammoniaca da una corrente gassosa in un processo di sintesi di urea
US7871520B2 (en) * 2007-12-18 2011-01-18 Milton Roy Company High-temperature membrane distillation
TW201032887A (en) * 2009-01-13 2010-09-16 Saipem Spa Process for the recovery of ammonia from a gaseous stream
GB0901699D0 (en) * 2009-02-02 2009-03-11 Ntnu Technology Transfer As gas seperation membrane
IT1395127B1 (it) * 2009-07-30 2012-09-05 Saipem Spa Procedimento per il recupero di ammoniaca da una corrente gassosa
IT1395383B1 (it) * 2009-09-09 2012-09-14 Saipem Spa Metodo di separazione di ammoniaca e diossido di carbonio da soluzioni acquose
EP2386346A1 (en) * 2010-05-11 2011-11-16 Stamicarbon B.V. Process for the reduction of ammonia emissions in a urea manufacturing process
ITMI20110804A1 (it) * 2011-05-10 2012-11-11 Saipem Spa "processo ad alta resa per la sintesi dell'urea"
ITMI20120013A1 (it) * 2012-01-09 2013-07-10 Saipem Spa Procedimento per la sintesi di urea comprendente un flusso di passivazione a fondo stripper

Also Published As

Publication number Publication date
MY162327A (en) 2017-05-31
WO2011029625A1 (en) 2011-03-17
EA201290122A1 (ru) 2012-08-30
US20120228225A1 (en) 2012-09-13
EP2475617A1 (en) 2012-07-18
IT1395383B1 (it) 2012-09-14
MX339596B (es) 2016-06-01
US20160082394A1 (en) 2016-03-24
JP2013503913A (ja) 2013-02-04
JP5753170B2 (ja) 2015-07-22
US9669360B2 (en) 2017-06-06
CN102695675B (zh) 2015-04-15
EP2475617B1 (en) 2018-12-26
BR112012005238A2 (pt) 2020-09-24
EA022152B1 (ru) 2015-11-30
MX2012002999A (es) 2012-07-17
US9266745B2 (en) 2016-02-23
BR112012005238B1 (pt) 2021-03-30
CA2772971A1 (en) 2011-03-17
CN102695675A (zh) 2012-09-26
ITMI20091551A1 (it) 2011-03-10
EG26889A (en) 2014-11-19

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