CA2684533A1

CA2684533A1 - Phosphate-free dishwasher detergent with excellent rinsing power

Phosphate-free dishwasher detergent with excellent rinsing power Download PDF

Info

Publication number: CA2684533A1
Authority: CA; Canada
Prior art keywords: acid; weight; branched; acids; component
Prior art date: 2007-04-25
Legal status : Abandoned

Application number

CA002684533A

Other languages

English (en)

French (fr)

Inventor

Juergen Tropsch

Current Assignee

BASF SE

Original Assignee

Individual

Priority date

2007-04-25

Filing date

2008-04-24

Publication date

2008-11-06

2008-04-24 Application filed by Individual filed Critical Individual

2008-11-06 Publication of CA2684533A1 publication Critical patent/CA2684533A1/en

Status Abandoned legal-status Critical Current

Links

239000003599 detergent Substances 0.000 title claims abstract description 56
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 37
229920000642 polymer Polymers 0.000 claims abstract description 33
238000000034 method Methods 0.000 claims abstract description 23
229920005646 polycarboxylate Polymers 0.000 claims abstract description 21
239000008139 complexing agent Substances 0.000 claims abstract description 13
239000000654 additive Substances 0.000 claims abstract description 10
238000005406 washing Methods 0.000 claims abstract description 10
230000000996 additive effect Effects 0.000 claims abstract description 7
239000000203 mixture Substances 0.000 claims description 91
239000002253 acid Substances 0.000 claims description 78
239000000178 monomer Substances 0.000 claims description 55
229920001577 copolymer Polymers 0.000 claims description 51
150000007513 acids Chemical class 0.000 claims description 50
102000004190 Enzymes Human genes 0.000 claims description 30
108090000790 Enzymes Proteins 0.000 claims description 30
150000003839 salts Chemical class 0.000 claims description 30
239000001257 hydrogen Substances 0.000 claims description 25
229910052739 hydrogen Inorganic materials 0.000 claims description 25
239000000126 substance Substances 0.000 claims description 25
125000002947 alkylene group Chemical group 0.000 claims description 23
CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 claims description 22
SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims description 20
NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 20
125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims description 16
238000009826 distribution Methods 0.000 claims description 15
239000003205 fragrance Substances 0.000 claims description 14
230000008569 process Effects 0.000 claims description 13
239000003381 stabilizer Substances 0.000 claims description 12
239000007844 bleaching agent Substances 0.000 claims description 11
229910052751 metal Inorganic materials 0.000 claims description 10
239000002184 metal Substances 0.000 claims description 10
239000004094 surface-active agent Substances 0.000 claims description 10
239000012190 activator Substances 0.000 claims description 9
230000007797 corrosion Effects 0.000 claims description 8
238000005260 corrosion Methods 0.000 claims description 8
125000004435 hydrogen atom Chemical class [H]* 0.000 claims description 8
239000000463 material Substances 0.000 claims description 8
150000003460 sulfonic acids Chemical class 0.000 claims description 8
239000006096 absorbing agent Substances 0.000 claims description 6
239000003963 antioxidant agent Substances 0.000 claims description 6
239000000975 dye Substances 0.000 claims description 6
125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 claims description 6
239000000945 filler Substances 0.000 claims description 6
239000011521 glass Substances 0.000 claims description 6
MGFYIUFZLHCRTH-UHFFFAOYSA-N nitrilotriacetic acid Chemical compound OC(=O)CN(CC(O)=O)CC(O)=O MGFYIUFZLHCRTH-UHFFFAOYSA-N 0.000 claims description 6
BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 claims description 6
XEEYSDHEOQHCDA-UHFFFAOYSA-N 2-methylprop-2-ene-1-sulfonic acid Chemical compound CC(=C)CS(O)(=O)=O XEEYSDHEOQHCDA-UHFFFAOYSA-N 0.000 claims description 4
238000012661 block copolymerization Methods 0.000 claims description 4
239000003112 inhibitor Substances 0.000 claims description 4
229920003023 plastic Polymers 0.000 claims description 4
239000004033 plastic Substances 0.000 claims description 4
125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 claims description 4
XMWLVXXYIYBETQ-UHFFFAOYSA-N 2-hydroxy-3-(2-methylprop-2-enoylamino)propane-1-sulfonic acid Chemical compound CC(=C)C(=O)NCC(O)CS(O)(=O)=O XMWLVXXYIYBETQ-UHFFFAOYSA-N 0.000 claims description 3
KOQQKLZTINXBAS-UHFFFAOYSA-N 2-hydroxy-3-prop-2-enoxypropane-1-sulfonic acid Chemical compound OS(=O)(=O)CC(O)COCC=C KOQQKLZTINXBAS-UHFFFAOYSA-N 0.000 claims description 3
VSSGDAWBDKMCMI-UHFFFAOYSA-N 2-methyl-2-(2-methylprop-2-enoylamino)propane-1-sulfonic acid Chemical compound CC(=C)C(=O)NC(C)(C)CS(O)(=O)=O VSSGDAWBDKMCMI-UHFFFAOYSA-N 0.000 claims description 3
AGBXYHCHUYARJY-UHFFFAOYSA-N 2-phenylethenesulfonic acid Chemical compound OS(=O)(=O)C=CC1=CC=CC=C1 AGBXYHCHUYARJY-UHFFFAOYSA-N 0.000 claims description 3
NYUTUWAFOUJLKI-UHFFFAOYSA-N 3-prop-2-enoyloxypropane-1-sulfonic acid Chemical compound OS(=O)(=O)CCCOC(=O)C=C NYUTUWAFOUJLKI-UHFFFAOYSA-N 0.000 claims description 3
UDPYEFRYPGXIAL-UHFFFAOYSA-N NC(=O)C(C)=CCS(O)(=O)=O Chemical compound NC(=O)C(C)=CCS(O)(=O)=O UDPYEFRYPGXIAL-UHFFFAOYSA-N 0.000 claims description 3
239000000919 ceramic Substances 0.000 claims description 3
ZHCGVAXFRLLEFW-UHFFFAOYSA-N 2-methyl-3-(prop-2-enoylamino)propane-1-sulfonic acid Chemical compound OS(=O)(=O)CC(C)CNC(=O)C=C ZHCGVAXFRLLEFW-UHFFFAOYSA-N 0.000 claims description 2
KFNGWPXYNSJXOP-UHFFFAOYSA-N 3-(2-methylprop-2-enoyloxy)propane-1-sulfonic acid Chemical compound CC(=C)C(=O)OCCCS(O)(=O)=O KFNGWPXYNSJXOP-UHFFFAOYSA-N 0.000 claims description 2
239000004606 Fillers/Extenders Substances 0.000 claims description 2
239000011230 binding agent Substances 0.000 claims description 2
229910001092 metal group alloy Inorganic materials 0.000 claims description 2
229910052573 porcelain Inorganic materials 0.000 claims description 2
UIIIBRHUICCMAI-UHFFFAOYSA-N prop-2-ene-1-sulfonic acid Chemical compound OS(=O)(=O)CC=C UIIIBRHUICCMAI-UHFFFAOYSA-N 0.000 claims description 2
229910052572 stoneware Inorganic materials 0.000 claims description 2
NLVXSWCKKBEXTG-UHFFFAOYSA-N vinylsulfonic acid Chemical compound OS(=O)(=O)C=C NLVXSWCKKBEXTG-UHFFFAOYSA-N 0.000 claims description 2
239000002023 wood Substances 0.000 claims description 2
125000004169 (C1-C6) alkyl group Chemical group 0.000 claims 1
125000003161 (C1-C6) alkylene group Chemical group 0.000 claims 1
YDJFNSJFJXJHBG-UHFFFAOYSA-N 2-carbamoylprop-2-ene-1-sulfonic acid Chemical compound NC(=O)C(=C)CS(O)(=O)=O YDJFNSJFJXJHBG-UHFFFAOYSA-N 0.000 claims 1
KCNKJCHARANTIP-SNAWJCMRSA-N allyl-{4-[3-(4-bromo-phenyl)-benzofuran-6-yloxy]-but-2-enyl}-methyl-amine Chemical group C=1OC2=CC(OC/C=C/CN(CC=C)C)=CC=C2C=1C1=CC=C(Br)C=C1 KCNKJCHARANTIP-SNAWJCMRSA-N 0.000 claims 1
239000003795 chemical substances by application Substances 0.000 abstract description 6
125000001273 sulfonato group Chemical group [O-]S(*)(=O)=O 0.000 abstract 1
150000001875 compounds Chemical class 0.000 description 36
-1 C6-alkyl radical Chemical class 0.000 description 35
229940088598 enzyme Drugs 0.000 description 29
IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 26
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 25
LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 16
108090001060 Lipase Proteins 0.000 description 16
102000004882 Lipase Human genes 0.000 description 16
239000004367 Lipase Substances 0.000 description 16
235000019421 lipase Nutrition 0.000 description 16
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 15
125000004432 carbon atom Chemical group C* 0.000 description 15
GOOHAUXETOMSMM-UHFFFAOYSA-N Propylene oxide Chemical compound CC1CO1 GOOHAUXETOMSMM-UHFFFAOYSA-N 0.000 description 13
150000002431 hydrogen Chemical class 0.000 description 13
239000000243 solution Substances 0.000 description 13
239000003054 catalyst Substances 0.000 description 12
238000004140 cleaning Methods 0.000 description 12
239000000047 product Substances 0.000 description 12
229920006395 saturated elastomer Polymers 0.000 description 12
VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 12
239000003921 oil Substances 0.000 description 11
235000019198 oils Nutrition 0.000 description 11
238000002360 preparation method Methods 0.000 description 11
150000003751 zinc Chemical class 0.000 description 11
NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 description 10
KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 10
239000003999 initiator Substances 0.000 description 10
125000000542 sulfonic acid group Chemical group 0.000 description 10
QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 9
108091005804 Peptidases Proteins 0.000 description 9
102000035195 Peptidases Human genes 0.000 description 9
150000001735 carboxylic acids Chemical class 0.000 description 9
CHQMHPLRPQMAMX-UHFFFAOYSA-L sodium persulfate Chemical compound [Na+].[Na+].[O-]S(=O)(=O)OOS([O-])(=O)=O CHQMHPLRPQMAMX-UHFFFAOYSA-L 0.000 description 9
239000010457 zeolite Substances 0.000 description 9
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 8
VZCYOOQTPOCHFL-OWOJBTEDSA-N Fumaric acid Chemical compound OC(=O)\C=C\C(O)=O VZCYOOQTPOCHFL-OWOJBTEDSA-N 0.000 description 8
FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 8
OFOBLEOULBTSOW-UHFFFAOYSA-N Propanedioic acid Natural products OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 8
239000004365 Protease Substances 0.000 description 8
238000006243 chemical reaction Methods 0.000 description 8
150000002148 esters Chemical class 0.000 description 8
LNTHITQWFMADLM-UHFFFAOYSA-N gallic acid Chemical compound OC(=O)C1=CC(O)=C(O)C(O)=C1 LNTHITQWFMADLM-UHFFFAOYSA-N 0.000 description 8
ZSIAUFGUXNUGDI-UHFFFAOYSA-N hexan-1-ol Chemical compound CCCCCCO ZSIAUFGUXNUGDI-UHFFFAOYSA-N 0.000 description 8
WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 8
229910052749 magnesium Inorganic materials 0.000 description 8
239000011777 magnesium Substances 0.000 description 8
VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 description 8
239000011976 maleic acid Substances 0.000 description 8
239000011734 sodium Substances 0.000 description 8
229920002245 Dextrose equivalent Polymers 0.000 description 7
BGRWYDHXPHLNKA-UHFFFAOYSA-N Tetraacetylethylenediamine Chemical compound CC(=O)N(C(C)=O)CCN(C(C)=O)C(C)=O BGRWYDHXPHLNKA-UHFFFAOYSA-N 0.000 description 7
229910021536 Zeolite Inorganic materials 0.000 description 7
150000001298 alcohols Chemical class 0.000 description 7
HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 7
239000012153 distilled water Substances 0.000 description 7
238000009472 formulation Methods 0.000 description 7
239000003446 ligand Substances 0.000 description 7
229920002451 polyvinyl alcohol Polymers 0.000 description 7
229910052708 sodium Inorganic materials 0.000 description 7
SYURNNNQIFDVCA-UHFFFAOYSA-N 2-propyloxirane Chemical compound CCCC1CO1 SYURNNNQIFDVCA-UHFFFAOYSA-N 0.000 description 6
108010065511 Amylases Proteins 0.000 description 6
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VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 6
RGHNJXZEOKUKBD-SQOUGZDYSA-N D-gluconic acid Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C(O)=O RGHNJXZEOKUKBD-SQOUGZDYSA-N 0.000 description 6
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 6
XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 6
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125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 6
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150000002763 monocarboxylic acids Chemical class 0.000 description 6
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235000021317 phosphate Nutrition 0.000 description 6
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238000006116 polymerization reaction Methods 0.000 description 6
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DBVJJBKOTRCVKF-UHFFFAOYSA-N Etidronic acid Chemical compound OP(=O)(O)C(O)(C)P(O)(O)=O DBVJJBKOTRCVKF-UHFFFAOYSA-N 0.000 description 5
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239000007864 aqueous solution Substances 0.000 description 5
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WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 description 5
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239000004382 Amylase Substances 0.000 description 4
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