CA2573759A1 - Method of purifying a dispersion of ionic fluoropolymer - Google Patents

Method of purifying a dispersion of ionic fluoropolymer Download PDF

Info

Publication number
CA2573759A1
CA2573759A1 CA002573759A CA2573759A CA2573759A1 CA 2573759 A1 CA2573759 A1 CA 2573759A1 CA 002573759 A CA002573759 A CA 002573759A CA 2573759 A CA2573759 A CA 2573759A CA 2573759 A1 CA2573759 A1 CA 2573759A1
Authority
CA
Canada
Prior art keywords
dispersion
exchanged
ionic fluoropolymer
ionic
fluoropolymer
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Abandoned
Application number
CA002573759A
Other languages
English (en)
French (fr)
Inventor
Klaus Hintzer
Kai H. Lochhaas
Tanja Zeif
Steven J. Hamrock
H. Todd Freemyer
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
3M Innovative Properties Co
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Publication of CA2573759A1 publication Critical patent/CA2573759A1/en
Abandoned legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F6/00Post-polymerisation treatments
    • C08F6/14Treatment of polymer emulsions
    • C08F6/16Purification
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F14/00Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen
    • C08F14/18Monomers containing fluorine
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F214/00Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen
    • C08F214/18Monomers containing fluorine
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/30Hydrogen technology
    • Y02E60/50Fuel cells

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
CA002573759A 2004-07-19 2005-07-11 Method of purifying a dispersion of ionic fluoropolymer Abandoned CA2573759A1 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US10/894,090 US7304101B2 (en) 2004-07-19 2004-07-19 Method of purifying a dispersion of ionic fluoropolymer
US10/894,090 2004-07-19
PCT/US2005/024415 WO2006019652A1 (en) 2004-07-19 2005-07-11 Method of purifying a dispersion of ionic fluoropolymer

Publications (1)

Publication Number Publication Date
CA2573759A1 true CA2573759A1 (en) 2006-02-23

Family

ID=34981699

Family Applications (1)

Application Number Title Priority Date Filing Date
CA002573759A Abandoned CA2573759A1 (en) 2004-07-19 2005-07-11 Method of purifying a dispersion of ionic fluoropolymer

Country Status (8)

Country Link
US (1) US7304101B2 (enExample)
EP (1) EP1769010A1 (enExample)
JP (1) JP2008506834A (enExample)
KR (1) KR20070044018A (enExample)
CN (1) CN100532407C (enExample)
CA (1) CA2573759A1 (enExample)
TW (1) TW200619233A (enExample)
WO (1) WO2006019652A1 (enExample)

Families Citing this family (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20070015937A1 (en) * 2005-07-15 2007-01-18 3M Innovative Properties Company Process for recovery of fluorinated carboxylic acid surfactants from exhaust gas
US20080015304A1 (en) 2006-07-13 2008-01-17 Klaus Hintzer Aqueous emulsion polymerization process for producing fluoropolymers
GB2430437A (en) * 2005-09-27 2007-03-28 3M Innovative Properties Co Method of making a fluoropolymer
EP1845116A1 (en) * 2006-04-11 2007-10-17 Solvay Solexis S.p.A. Fluoropolymer dispersion purification
US20100022702A1 (en) * 2006-12-12 2010-01-28 Chen Lisa P Thermally stable fluoropolymers
US20080264864A1 (en) 2007-04-27 2008-10-30 3M Innovative Properties Company PROCESS FOR REMOVING FLUORINATED EMULSIFIER FROM FLUOROPOLMER DISPERSIONS USING AN ANION-EXCHANGE RESIN AND A pH-DEPENDENT SURFACTANT AND FLUOROPOLYMER DISPERSIONS CONTAINING A pH-DEPENDENT SURFACTANT
JP5119854B2 (ja) * 2007-10-22 2013-01-16 ダイキン工業株式会社 含フッ素ポリマー分散体及び含フッ素ポリマー分散体製造方法
JP2009170412A (ja) * 2007-12-18 2009-07-30 Sumitomo Chemical Co Ltd 高分子電解質の精製方法
US9217045B2 (en) 2008-12-11 2015-12-22 Solvay Specialty Polymers Italy S.P.A. Purification of fluoroionomer compositions
CN102459361B (zh) 2009-06-12 2019-07-05 索尔维索莱克西斯公司 具有低表面张力、低液体粘度以及高固体含量的氟代离聚物分散体
JP5605460B2 (ja) * 2012-05-23 2014-10-15 ダイキン工業株式会社 含フッ素ポリマー水性分散体の製造方法及び精製含フッ素ポリマー水性分散体
JP5978762B2 (ja) * 2012-05-23 2016-08-24 ダイキン工業株式会社 含フッ素ポリマー水性分散体の製造方法及び精製含フッ素ポリマー水性分散体
WO2017038824A1 (ja) * 2015-08-31 2017-03-09 旭硝子株式会社 液状組成物の製造方法、触媒層形成用塗工液の製造方法および膜電極接合体の製造方法
JP6819596B2 (ja) * 2015-08-31 2021-01-27 Agc株式会社 液状組成物の製造方法、触媒層形成用塗工液の製造方法および膜電極接合体の製造方法
EP3353221B1 (en) * 2015-09-23 2023-06-07 3M Innovative Properties Company Method of making a copolymer of tetrafluoroethylene having sulfonyl pendant groups
US11377510B2 (en) 2017-09-14 2022-07-05 3M Innovative Properties Company Fluorinated copolymer and compositions and articles including the same
KR102482452B1 (ko) * 2017-09-28 2022-12-29 삼성디스플레이 주식회사 유기 재료 정제 조성물 및 이를 이용한 유기 재료 정제 방법
CN107858140B (zh) * 2017-10-25 2021-01-01 中国石油天然气股份有限公司 一种耐酸型泡沫防窜剂及其制备方法
CN114651351B (zh) * 2019-12-12 2025-01-28 庄信万丰氢能科技有限公司 电催化剂油墨
KR20220119048A (ko) 2019-12-20 2022-08-26 쓰리엠 이노베이티브 프로퍼티즈 컴파니 플루오르화 공중합체 및 이를 포함하는 조성물 및 물품
US20230090482A1 (en) 2020-04-09 2023-03-23 3M Innovative Properties Company Composite including fluorinated polymer and salt nanoparticles and articles including the same
CN111495108B (zh) * 2020-04-22 2022-03-15 浙江利化新材料科技有限公司 一种六氟环氧丙烷的分离纯化方法及所用吸附剂
KR102305504B1 (ko) * 2020-05-22 2021-09-27 주식회사 유라마 유기발광소재(oled) 정제용 이온성액체의 재사용을 위한 정제방법
WO2023057926A1 (en) 2021-10-07 2023-04-13 3M Innovative Properties Company Composite including fluorinated polymer and lithium fluoride nanoparticles and articles including the same

Family Cites Families (45)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3624053A (en) * 1963-06-24 1971-11-30 Du Pont Trifluorovinyl sulfonic acid polymers
GB1034197A (en) 1963-09-13 1966-06-29 Du Pont Sulphonic acid derivatives of fluorocarbon vinyl ethers, and polymers thereof
US3282875A (en) * 1964-07-22 1966-11-01 Du Pont Fluorocarbon vinyl ether polymers
US3993614A (en) * 1969-07-14 1976-11-23 Minnesota Mining And Manufacturing Company Sulfonated aromatic polyisocyanates and preparation of stable anionic polyurethane or polyurea latices therefor
JPS5349090A (en) * 1976-10-15 1978-05-04 Asahi Glass Co Ltd Preparation of fluorinated plymer containing ion exchange group
DE2903981A1 (de) * 1979-02-02 1980-08-07 Hoechst Ag Rueckgewinnung fluorierter emulgatorsaeuren aus basischen anionenaustauschern
DE2908001C2 (de) * 1979-03-01 1981-02-19 Hoechst Ag, 6000 Frankfurt Verfahren zur Herstellung konzentrierter Dispersionen von Fluorpolymeren
JPS5645911A (en) * 1979-09-25 1981-04-25 Asahi Glass Co Ltd Production of ion-exchangeable fluorinated polymer
US4358545A (en) * 1980-06-11 1982-11-09 The Dow Chemical Company Sulfonic acid electrolytic cell having flourinated polymer membrane with hydration product less than 22,000
US4433082A (en) * 1981-05-01 1984-02-21 E. I. Du Pont De Nemours And Company Process for making liquid composition of perfluorinated ion exchange polymer, and product thereof
US4940525A (en) * 1987-05-08 1990-07-10 The Dow Chemical Company Low equivalent weight sulfonic fluoropolymers
US5286843A (en) * 1992-05-22 1994-02-15 Rohm And Haas Company Process for improving water-whitening resistance of pressure sensitive adhesives
WO1994003503A2 (en) 1992-07-30 1994-02-17 Imperial Chemical Industries Plc Fluorinated polymers
US5310765A (en) * 1993-03-03 1994-05-10 E. I. Du Pont De Nemours And Company Process for hydrolysis of ion exchange membranes
DE4402694A1 (de) * 1993-06-02 1995-08-03 Hoechst Ag Verfahren zur Rückgewinnung von fluorierten Carbonsäuren
US5608022A (en) * 1993-10-12 1997-03-04 Asahi Kasei Kogyo Kabushiki Kaisha Perfluorocarbon copolymer containing functional groups and a method for producing it
US6156451A (en) * 1994-11-10 2000-12-05 E. I. Du Pont De Nemours And Company Process for making composite ion exchange membranes
US5936060A (en) * 1996-11-25 1999-08-10 E. I. Du Pont De Nemours And Company Perfluoroelastomer composition having improved processability
EP0968196B1 (fr) * 1997-07-25 2004-10-27 Acep Inc. Composes ioniques perfluorovinyliques et leur utilisation dans des materiaux conducteurs
US6025092A (en) * 1998-02-13 2000-02-15 E. I. Du Pont De Nemours And Company Fluorinated ionomers and their uses
DE19824614A1 (de) * 1998-06-02 1999-12-09 Dyneon Gmbh Verfahren zur Rückgewinnung von fluorierten Alkansäuren aus Abwässern
DE19824615A1 (de) * 1998-06-02 1999-12-09 Dyneon Gmbh Verfahren zur Rückgewinnung von fluorierten Alkansäuren aus Abwässern
DE19857111A1 (de) 1998-12-11 2000-06-15 Dyneon Gmbh Wäßrige Dispersionen von Fluorpolymeren
JP2002538235A (ja) * 1999-03-02 2002-11-12 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー フッ素化コポリマーのフリーラジカル重合方法
DE19932771A1 (de) * 1999-07-14 2001-01-18 Dyneon Gmbh Verfahren zur Eluierung fluorierter Emulgatoren
DE19933696A1 (de) * 1999-07-17 2001-01-18 Dyneon Gmbh Verfahren zur Rückgewinnung fluorierter Emulgatoren aus wässrigen Phasen
DE19953285A1 (de) * 1999-11-05 2001-05-10 Dyneon Gmbh Verfahren zur Rückgewinnung fluorierter Emulgatoren
US6720360B1 (en) * 2000-02-01 2004-04-13 3M Innovative Properties Company Ultra-clean fluoropolymers
US6593416B2 (en) * 2000-02-01 2003-07-15 3M Innovative Properties Company Fluoropolymers
JP4759782B2 (ja) * 2000-02-16 2011-08-31 ダイキン工業株式会社 フッ素系アイオノマーの精製・濃縮方法
EP1283225B1 (en) 2000-02-16 2006-05-03 Daikin Industries, Ltd. Process for producing fluoroionomer, method for purification and concentration of the ionomer, and method of film formation
US6733914B1 (en) * 2000-02-18 2004-05-11 Ion Power, Inc. Fuel cell membranes
US6610465B2 (en) * 2001-04-11 2003-08-26 Clariant Finance (Bvi) Limited Process for producing film forming resins for photoresist compositions
US6713567B2 (en) * 2001-07-13 2004-03-30 E. I. Du Pont De Nemours And Company Method for forming fluorinated ionomers
EP1427788B1 (en) 2001-09-05 2014-05-21 3M Innovative Properties Company Fluoropolymer dispersion containing no or little low molecular weight fluorinated surfactant
CN1571808A (zh) * 2001-10-15 2005-01-26 纳幕尔杜邦公司 通过原位聚合制备的用于燃料电池的固体聚合物薄膜
EP1364972B1 (en) * 2002-05-22 2006-08-30 3M Innovative Properties Company Process for reducing the amount of fluorinated surfactant in aqueous fluoropolymer dispersions
CA2490136C (en) 2002-06-17 2009-08-18 Daikin Industries, Ltd. Fluoropolymer dispersion and process for producing fluoropolymer dispersion
US20040107869A1 (en) * 2002-12-10 2004-06-10 3M Innovative Properties Company Catalyst ink
US6624328B1 (en) * 2002-12-17 2003-09-23 3M Innovative Properties Company Preparation of perfluorinated vinyl ethers having a sulfonyl fluoride end-group
US7348088B2 (en) * 2002-12-19 2008-03-25 3M Innovative Properties Company Polymer electrolyte membrane
ATE502062T1 (de) 2003-10-24 2011-04-15 3M Innovative Properties Co Wässrige dispersionen von polytetrafluorethylenteilchen
US7265162B2 (en) * 2003-11-13 2007-09-04 3M Innovative Properties Company Bromine, chlorine or iodine functional polymer electrolytes crosslinked by e-beam
EP1533325B1 (en) * 2003-11-17 2011-10-19 3M Innovative Properties Company Aqueous dispersions of polytetrafluoroethylene having a low amount of fluorinated surfactant
US7060738B2 (en) * 2003-12-11 2006-06-13 3M Innovative Properties Company Polymer electrolytes crosslinked by ultraviolet radiation

Also Published As

Publication number Publication date
US20060014886A1 (en) 2006-01-19
CN1989160A (zh) 2007-06-27
JP2008506834A (ja) 2008-03-06
WO2006019652A1 (en) 2006-02-23
EP1769010A1 (en) 2007-04-04
CN100532407C (zh) 2009-08-26
KR20070044018A (ko) 2007-04-26
US7304101B2 (en) 2007-12-04
TW200619233A (en) 2006-06-16

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Legal Events

Date Code Title Description
FZDE Discontinued