CA2573759A1 - Method of purifying a dispersion of ionic fluoropolymer - Google Patents

Method of purifying a dispersion of ionic fluoropolymer Download PDF

Info

Publication number
CA2573759A1
CA2573759A1 CA002573759A CA2573759A CA2573759A1 CA 2573759 A1 CA2573759 A1 CA 2573759A1 CA 002573759 A CA002573759 A CA 002573759A CA 2573759 A CA2573759 A CA 2573759A CA 2573759 A1 CA2573759 A1 CA 2573759A1
Authority
CA
Canada
Prior art keywords
dispersion
exchanged
ionic fluoropolymer
ionic
fluoropolymer
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Abandoned
Application number
CA002573759A
Other languages
English (en)
French (fr)
Inventor
Klaus Hintzer
Kai H. Lochhaas
Tanja Zeif
Steven J. Hamrock
H. Todd Freemyer
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
3M Innovative Properties Co
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Publication of CA2573759A1 publication Critical patent/CA2573759A1/en
Abandoned legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F6/00—Post-polymerisation treatments
    • C08F6/14—Treatment of polymer emulsions
    • C08F6/16—Purification
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F14/00—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen
    • C08F14/18—Monomers containing fluorine
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F214/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen
    • C08F214/18—Monomers containing fluorine
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/30—Hydrogen technology
    • Y02E60/50—Fuel cells

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
CA002573759A 2004-07-19 2005-07-11 Method of purifying a dispersion of ionic fluoropolymer Abandoned CA2573759A1 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US10/894,090 US7304101B2 (en) 2004-07-19 2004-07-19 Method of purifying a dispersion of ionic fluoropolymer
US10/894,090 2004-07-19
PCT/US2005/024415 WO2006019652A1 (en) 2004-07-19 2005-07-11 Method of purifying a dispersion of ionic fluoropolymer

Publications (1)

Publication Number Publication Date
CA2573759A1 true CA2573759A1 (en) 2006-02-23

Family

ID=34981699

Family Applications (1)

Application Number Title Priority Date Filing Date
CA002573759A Abandoned CA2573759A1 (en) 2004-07-19 2005-07-11 Method of purifying a dispersion of ionic fluoropolymer

Country Status (8)

Country Link
US (1) US7304101B2 (OSRAM)
EP (1) EP1769010A1 (OSRAM)
JP (1) JP2008506834A (OSRAM)
KR (1) KR20070044018A (OSRAM)
CN (1) CN100532407C (OSRAM)
CA (1) CA2573759A1 (OSRAM)
TW (1) TW200619233A (OSRAM)
WO (1) WO2006019652A1 (OSRAM)

Families Citing this family (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20070015937A1 (en) * 2005-07-15 2007-01-18 3M Innovative Properties Company Process for recovery of fluorinated carboxylic acid surfactants from exhaust gas
US20080015304A1 (en) 2006-07-13 2008-01-17 Klaus Hintzer Aqueous emulsion polymerization process for producing fluoropolymers
GB2430437A (en) * 2005-09-27 2007-03-28 3M Innovative Properties Co Method of making a fluoropolymer
EP1845116A1 (en) * 2006-04-11 2007-10-17 Solvay Solexis S.p.A. Fluoropolymer dispersion purification
WO2008127461A2 (en) * 2006-12-12 2008-10-23 3M Innovative Properties Company Thermally stable fluoropolymers
US20080264864A1 (en) * 2007-04-27 2008-10-30 3M Innovative Properties Company PROCESS FOR REMOVING FLUORINATED EMULSIFIER FROM FLUOROPOLMER DISPERSIONS USING AN ANION-EXCHANGE RESIN AND A pH-DEPENDENT SURFACTANT AND FLUOROPOLYMER DISPERSIONS CONTAINING A pH-DEPENDENT SURFACTANT
JP5119854B2 (ja) * 2007-10-22 2013-01-16 ダイキン工業株式会社 含フッ素ポリマー分散体及び含フッ素ポリマー分散体製造方法
JP2009170412A (ja) * 2007-12-18 2009-07-30 Sumitomo Chemical Co Ltd 高分子電解質の精製方法
DK2376541T3 (da) * 2008-12-11 2013-01-28 Solvay Specialty Polymers It Oprensning af fluorionomer-sammensætninger
EP2440586B1 (en) 2009-06-12 2020-02-05 Solvay Specialty Polymers Italy S.p.A. Fluoroionomers dispersions having low surface tension, low liquid viscosity and high solid content
JP5978762B2 (ja) * 2012-05-23 2016-08-24 ダイキン工業株式会社 含フッ素ポリマー水性分散体の製造方法及び精製含フッ素ポリマー水性分散体
US9644055B2 (en) 2012-05-23 2017-05-09 Daikin Industries, Ltd. Method for producing aqueous fluorine-containing polymer dispersing element, and purified aqueous fluorine-containing polymer dispersing element
WO2017038827A1 (ja) * 2015-08-31 2017-03-09 旭硝子株式会社 液状組成物の製造方法、触媒層形成用塗工液の製造方法および膜電極接合体の製造方法
CN107949585B (zh) * 2015-08-31 2020-02-18 Ａｇｃ株式会社 液体组合物的制造方法、催化剂层形成用涂布液的制造方法及膜电极接合体的制造方法
EP3353221B1 (en) 2015-09-23 2023-06-07 3M Innovative Properties Company Method of making a copolymer of tetrafluoroethylene having sulfonyl pendant groups
JP2020534402A (ja) 2017-09-14 2020-11-26 スリーエム イノベイティブ プロパティズ カンパニー フルオロポリマー分散体、フルオロポリマー分散体を製造するための方法、触媒インク及びポリマー電解質膜
KR102482452B1 (ko) * 2017-09-28 2022-12-29 삼성디스플레이 주식회사 유기 재료 정제 조성물 및 이를 이용한 유기 재료 정제 방법
CN107858140B (zh) * 2017-10-25 2021-01-01 中国石油天然气股份有限公司 一种耐酸型泡沫防窜剂及其制备方法
CN114651351B (zh) * 2019-12-12 2025-01-28 庄信万丰氢能科技有限公司 电催化剂油墨
KR20220119048A (ko) 2019-12-20 2022-08-26 쓰리엠 이노베이티브 프로퍼티즈 컴파니 플루오르화 공중합체 및 이를 포함하는 조성물 및 물품
US20230090482A1 (en) 2020-04-09 2023-03-23 3M Innovative Properties Company Composite including fluorinated polymer and salt nanoparticles and articles including the same
CN111495108B (zh) * 2020-04-22 2022-03-15 浙江利化新材料科技有限公司 一种六氟环氧丙烷的分离纯化方法及所用吸附剂
KR102305504B1 (ko) * 2020-05-22 2021-09-27 주식회사 유라마 유기발광소재(oled) 정제용 이온성액체의 재사용을 위한 정제방법
US20250239638A1 (en) 2021-10-07 2025-07-24 3M Innovative Properties Company Composite including fluorinated polymer and lithium fluoride nanoparticles and articles including the same

Family Cites Families (45)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3624053A (en) * 1963-06-24 1971-11-30 Du Pont Trifluorovinyl sulfonic acid polymers
GB1034197A (en) 1963-09-13 1966-06-29 Du Pont Sulphonic acid derivatives of fluorocarbon vinyl ethers, and polymers thereof
US3282875A (en) * 1964-07-22 1966-11-01 Du Pont Fluorocarbon vinyl ether polymers
US3993614A (en) * 1969-07-14 1976-11-23 Minnesota Mining And Manufacturing Company Sulfonated aromatic polyisocyanates and preparation of stable anionic polyurethane or polyurea latices therefor
JPS5349090A (en) * 1976-10-15 1978-05-04 Asahi Glass Co Ltd Preparation of fluorinated plymer containing ion exchange group
DE2903981A1 (de) * 1979-02-02 1980-08-07 Hoechst Ag Rueckgewinnung fluorierter emulgatorsaeuren aus basischen anionenaustauschern
DE2908001C2 (de) * 1979-03-01 1981-02-19 Hoechst Ag, 6000 Frankfurt Verfahren zur Herstellung konzentrierter Dispersionen von Fluorpolymeren
JPS5645911A (en) * 1979-09-25 1981-04-25 Asahi Glass Co Ltd Production of ion-exchangeable fluorinated polymer
US4358545A (en) * 1980-06-11 1982-11-09 The Dow Chemical Company Sulfonic acid electrolytic cell having flourinated polymer membrane with hydration product less than 22,000
US4433082A (en) * 1981-05-01 1984-02-21 E. I. Du Pont De Nemours And Company Process for making liquid composition of perfluorinated ion exchange polymer, and product thereof
US4940525A (en) * 1987-05-08 1990-07-10 The Dow Chemical Company Low equivalent weight sulfonic fluoropolymers
US5286843A (en) * 1992-05-22 1994-02-15 Rohm And Haas Company Process for improving water-whitening resistance of pressure sensitive adhesives
JPH08500374A (ja) * 1992-07-30 1996-01-16 インペリアル・ケミカル・インダストリーズ・ピーエルシー フッ素化ポリマー
US5310765A (en) * 1993-03-03 1994-05-10 E. I. Du Pont De Nemours And Company Process for hydrolysis of ion exchange membranes
DE4402694A1 (de) * 1993-06-02 1995-08-03 Hoechst Ag Verfahren zur Rückgewinnung von fluorierten Carbonsäuren
CN1062873C (zh) * 1993-10-12 2001-03-07 旭化成工业株式会社 含官能团的全氟化碳共聚物及其制备方法
US6156451A (en) * 1994-11-10 2000-12-05 E. I. Du Pont De Nemours And Company Process for making composite ion exchange membranes
US5936060A (en) * 1996-11-25 1999-08-10 E. I. Du Pont De Nemours And Company Perfluoroelastomer composition having improved processability
JP4657390B2 (ja) * 1997-07-25 2011-03-23 アセップ・インク ペルフルオロビニルイオン化合物および重合体型のイオン電導体の成分、選択膜の成分または触媒の成分としてのそれらの使用
US6025092A (en) * 1998-02-13 2000-02-15 E. I. Du Pont De Nemours And Company Fluorinated ionomers and their uses
DE19824615A1 (de) * 1998-06-02 1999-12-09 Dyneon Gmbh Verfahren zur Rückgewinnung von fluorierten Alkansäuren aus Abwässern
DE19824614A1 (de) * 1998-06-02 1999-12-09 Dyneon Gmbh Verfahren zur Rückgewinnung von fluorierten Alkansäuren aus Abwässern
DE19857111A1 (de) * 1998-12-11 2000-06-15 Dyneon Gmbh Wäßrige Dispersionen von Fluorpolymeren
DE60016577T2 (de) * 1999-03-02 2005-11-24 E.I. Du Pont De Nemours And Co., Wilmington Radikalische polymerisationsmethode für fluorierte copolymere
DE19932771A1 (de) * 1999-07-14 2001-01-18 Dyneon Gmbh Verfahren zur Eluierung fluorierter Emulgatoren
DE19933696A1 (de) * 1999-07-17 2001-01-18 Dyneon Gmbh Verfahren zur Rückgewinnung fluorierter Emulgatoren aus wässrigen Phasen
DE19953285A1 (de) * 1999-11-05 2001-05-10 Dyneon Gmbh Verfahren zur Rückgewinnung fluorierter Emulgatoren
US6720360B1 (en) * 2000-02-01 2004-04-13 3M Innovative Properties Company Ultra-clean fluoropolymers
US6593416B2 (en) * 2000-02-01 2003-07-15 3M Innovative Properties Company Fluoropolymers
EP1283225B1 (en) 2000-02-16 2006-05-03 Daikin Industries, Ltd. Process for producing fluoroionomer, method for purification and concentration of the ionomer, and method of film formation
JP4759782B2 (ja) * 2000-02-16 2011-08-31 ダイキン工業株式会社 フッ素系アイオノマーの精製・濃縮方法
US6733914B1 (en) * 2000-02-18 2004-05-11 Ion Power, Inc. Fuel cell membranes
US6610465B2 (en) * 2001-04-11 2003-08-26 Clariant Finance (Bvi) Limited Process for producing film forming resins for photoresist compositions
US6713567B2 (en) * 2001-07-13 2004-03-30 E. I. Du Pont De Nemours And Company Method for forming fluorinated ionomers
KR20040044531A (ko) 2001-09-05 2004-05-28 쓰리엠 이노베이티브 프로퍼티즈 캄파니 저분자량 불소화 계면활성제를 거의 함유하지 않는플루오로중합체 분산액
TW589759B (en) * 2001-10-15 2004-06-01 Du Pont Fuel cell membranes
EP1364972B1 (en) * 2002-05-22 2006-08-30 3M Innovative Properties Company Process for reducing the amount of fluorinated surfactant in aqueous fluoropolymer dispersions
JP4123272B2 (ja) 2002-06-17 2008-07-23 ダイキン工業株式会社 含フッ素ポリマー分散体及び含フッ素ポリマー分散体製造方法
US20040107869A1 (en) * 2002-12-10 2004-06-10 3M Innovative Properties Company Catalyst ink
US6624328B1 (en) * 2002-12-17 2003-09-23 3M Innovative Properties Company Preparation of perfluorinated vinyl ethers having a sulfonyl fluoride end-group
US7348088B2 (en) * 2002-12-19 2008-03-25 3M Innovative Properties Company Polymer electrolyte membrane
ATE502062T1 (de) 2003-10-24 2011-04-15 3M Innovative Properties Co Wässrige dispersionen von polytetrafluorethylenteilchen
US7265162B2 (en) * 2003-11-13 2007-09-04 3M Innovative Properties Company Bromine, chlorine or iodine functional polymer electrolytes crosslinked by e-beam
ATE529451T1 (de) * 2003-11-17 2011-11-15 3M Innovative Properties Co Wässrige ptfe-dispersionen mit einem niedrigen gehalt an fluorierten emulgatoren
US7060738B2 (en) * 2003-12-11 2006-06-13 3M Innovative Properties Company Polymer electrolytes crosslinked by ultraviolet radiation

Also Published As

Publication number Publication date
EP1769010A1 (en) 2007-04-04
US20060014886A1 (en) 2006-01-19
WO2006019652A1 (en) 2006-02-23
CN1989160A (zh) 2007-06-27
KR20070044018A (ko) 2007-04-26
CN100532407C (zh) 2009-08-26
US7304101B2 (en) 2007-12-04
TW200619233A (en) 2006-06-16
JP2008506834A (ja) 2008-03-06

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Legal Events

Date Code Title Description
FZDE Discontinued