CA2356303C - Procede de revelation structurale pour superalliages monocristallins - Google Patents
Procede de revelation structurale pour superalliages monocristallins Download PDFInfo
- Publication number
- CA2356303C CA2356303C CA2356303A CA2356303A CA2356303C CA 2356303 C CA2356303 C CA 2356303C CA 2356303 A CA2356303 A CA 2356303A CA 2356303 A CA2356303 A CA 2356303A CA 2356303 C CA2356303 C CA 2356303C
- Authority
- CA
- Canada
- Prior art keywords
- acid
- bath
- attack
- process according
- cathode
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000000034 method Methods 0.000 title claims abstract description 21
- 229910000601 superalloy Inorganic materials 0.000 title claims abstract description 20
- 238000001514 detection method Methods 0.000 title claims 2
- 239000002253 acid Substances 0.000 claims abstract description 23
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims abstract description 18
- 229910052707 ruthenium Inorganic materials 0.000 claims abstract description 11
- KJTLSVCANCCWHF-UHFFFAOYSA-N Ruthenium Chemical compound [Ru] KJTLSVCANCCWHF-UHFFFAOYSA-N 0.000 claims abstract description 10
- 229910052702 rhenium Inorganic materials 0.000 claims abstract description 10
- WUAPFZMCVAUBPE-UHFFFAOYSA-N rhenium atom Chemical compound [Re] WUAPFZMCVAUBPE-UHFFFAOYSA-N 0.000 claims abstract description 10
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims abstract description 9
- 238000007689 inspection Methods 0.000 claims abstract description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 18
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 16
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 8
- 229910052759 nickel Inorganic materials 0.000 claims description 8
- 239000000126 substance Substances 0.000 claims description 8
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 claims description 7
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 6
- 150000003333 secondary alcohols Chemical class 0.000 claims description 6
- 230000007547 defect Effects 0.000 claims description 5
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims description 4
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 claims description 3
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 claims description 3
- RBTARNINKXHZNM-UHFFFAOYSA-K iron trichloride Chemical compound Cl[Fe](Cl)Cl RBTARNINKXHZNM-UHFFFAOYSA-K 0.000 claims description 3
- 239000011975 tartaric acid Substances 0.000 claims description 3
- 235000002906 tartaric acid Nutrition 0.000 claims description 3
- 238000004140 cleaning Methods 0.000 claims description 2
- 238000007654 immersion Methods 0.000 claims 1
- 230000000007 visual effect Effects 0.000 claims 1
- 238000004061 bleaching Methods 0.000 abstract description 4
- 238000005530 etching Methods 0.000 abstract description 3
- 238000000866 electrolytic etching Methods 0.000 abstract 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 8
- 239000000470 constituent Substances 0.000 description 5
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 239000010935 stainless steel Substances 0.000 description 4
- 229910001220 stainless steel Inorganic materials 0.000 description 4
- 238000009826 distribution Methods 0.000 description 3
- 238000001035 drying Methods 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 238000011179 visual inspection Methods 0.000 description 3
- 229910045601 alloy Inorganic materials 0.000 description 2
- 239000000956 alloy Substances 0.000 description 2
- 239000008367 deionised water Substances 0.000 description 2
- 229910021641 deionized water Inorganic materials 0.000 description 2
- -1 ions chloride Chemical class 0.000 description 2
- 229910052742 iron Inorganic materials 0.000 description 2
- 229910003449 rhenium oxide Inorganic materials 0.000 description 2
- ROZSPJBPUVWBHW-UHFFFAOYSA-N [Ru]=O Chemical class [Ru]=O ROZSPJBPUVWBHW-UHFFFAOYSA-N 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229910052804 chromium Inorganic materials 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 229910052735 hafnium Inorganic materials 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 229910001092 metal group alloy Inorganic materials 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 229910052750 molybdenum Inorganic materials 0.000 description 1
- DYIZHKNUQPHNJY-UHFFFAOYSA-N oxorhenium Chemical compound [Re]=O DYIZHKNUQPHNJY-UHFFFAOYSA-N 0.000 description 1
- 230000002085 persistent effect Effects 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 239000003870 refractory metal Substances 0.000 description 1
- 229910001925 ruthenium oxide Inorganic materials 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 230000008023 solidification Effects 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 229910052715 tantalum Inorganic materials 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23F—NON-MECHANICAL REMOVAL OF METALLIC MATERIAL FROM SURFACE; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL; MULTI-STEP PROCESSES FOR SURFACE TREATMENT OF METALLIC MATERIAL INVOLVING AT LEAST ONE PROCESS PROVIDED FOR IN CLASS C23 AND AT LEAST ONE PROCESS COVERED BY SUBCLASS C21D OR C22F OR CLASS C25
- C23F1/00—Etching metallic material by chemical means
- C23F1/10—Etching compositions
- C23F1/14—Aqueous compositions
- C23F1/16—Acidic compositions
- C23F1/26—Acidic compositions for etching refractory metals
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25F—PROCESSES FOR THE ELECTROLYTIC REMOVAL OF MATERIALS FROM OBJECTS; APPARATUS THEREFOR
- C25F3/00—Electrolytic etching or polishing
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
- G01N1/32—Polishing; Etching
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/20—Metals
- G01N33/204—Structure thereof, e.g. crystal structure
- G01N33/2045—Defects
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Metallurgy (AREA)
- Electrochemistry (AREA)
- Food Science & Technology (AREA)
- Crystallography & Structural Chemistry (AREA)
- Medicinal Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Mechanical Engineering (AREA)
- ing And Chemical Polishing (AREA)
- Investigating And Analyzing Materials By Characteristic Methods (AREA)
- Turbine Rotor Nozzle Sealing (AREA)
- Cleaning And De-Greasing Of Metallic Materials By Chemical Methods (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
- Sampling And Sample Adjustment (AREA)
- Electroplating And Plating Baths Therefor (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR0010979A FR2813392B1 (fr) | 2000-08-28 | 2000-08-28 | Procede de revelation structurale pour superalliages monocristallins |
| FR0010979 | 2000-08-28 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CA2356303A1 CA2356303A1 (fr) | 2002-02-28 |
| CA2356303C true CA2356303C (fr) | 2011-09-27 |
Family
ID=8853757
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA2356303A Expired - Lifetime CA2356303C (fr) | 2000-08-28 | 2001-08-24 | Procede de revelation structurale pour superalliages monocristallins |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US6582585B2 (https=) |
| EP (1) | EP1184656B1 (https=) |
| JP (1) | JP4495888B2 (https=) |
| CA (1) | CA2356303C (https=) |
| FR (1) | FR2813392B1 (https=) |
| RU (1) | RU2268953C2 (https=) |
| UA (1) | UA72911C2 (https=) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB201200360D0 (en) * | 2012-01-11 | 2012-02-22 | Rolls Royce Plc | Component production method |
| JP2013160619A (ja) * | 2012-02-03 | 2013-08-19 | Mitsubishi Heavy Ind Ltd | 電解エッチング方法及び構造部材の保全方法 |
| CN105318109A (zh) * | 2014-06-30 | 2016-02-10 | 江苏大力城电气有限公司 | 一种恒力支吊架用连接卡扣 |
| EP4546365A3 (en) | 2015-11-24 | 2025-08-06 | Insulet Corporation | Wearable automated medication delivery system |
| FR3101643B1 (fr) | 2019-10-08 | 2022-05-06 | Safran | Piece d'aeronef en superalliage comprenant du rhenium et/ou du ruthenium et procede de fabrication associe |
Family Cites Families (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5424318B2 (https=) * | 1974-07-03 | 1979-08-20 | ||
| US4234397A (en) * | 1978-08-15 | 1980-11-18 | United Technologies Corporation | Nondestructive metallographic examination of gas turbine components |
| US4445988A (en) * | 1980-09-29 | 1984-05-01 | The United States Of America As Represented By The Department Of Energy | Micrographic detection of plastic deformation in nickel base alloys |
| SU1236007A1 (ru) * | 1983-05-23 | 1986-06-07 | Предприятие П/Я М-5612 | Способ обработки изделий из никел |
| US4548903A (en) * | 1984-03-30 | 1985-10-22 | The United States Of America As Represented By The Secretary Of The Air Force | Method to reveal microstructures in single phase alloys |
| US4801367A (en) * | 1984-12-31 | 1989-01-31 | White Cap Dental Company, Inc. | Apparatus for electro-etching |
| JPH01191056A (ja) * | 1988-01-26 | 1989-08-01 | Nippon Sheet Glass Co Ltd | ＺｎＳｅ単結晶の転位密度の測定方法 |
| JP2568637B2 (ja) * | 1988-07-19 | 1997-01-08 | 株式会社日立製作所 | 高温用機器の損傷検出法 |
| US5186796A (en) * | 1989-06-05 | 1993-02-16 | Stelco Inc. | Method and apparatus for electrolytic etching of metals |
| RU2023767C1 (ru) * | 1990-06-25 | 1994-11-30 | Шабанов Геннадий Дмитриевич | Раствор для электрохимического полирования металлов |
| JP3064107B2 (ja) * | 1992-07-16 | 2000-07-12 | 三菱重工業株式会社 | オーステナイト系耐熱鋼の高温損傷評価方法 |
| JP3661801B2 (ja) * | 1995-05-18 | 2005-06-22 | 同和鉱業株式会社 | Ｉｉ−ｖｉ 族化合物半導体単結晶体の転位密度測定方法 |
| AU5435198A (en) * | 1996-11-08 | 1998-05-29 | Mountain States Analytical, Inc. | Sample preparation for metals analysis using accelerated acid digestion (aad) |
| FR2780982B1 (fr) * | 1998-07-07 | 2000-09-08 | Onera (Off Nat Aerospatiale) | Superalliage monocristallin a base de nickel a haut solvus |
-
2000
- 2000-08-28 FR FR0010979A patent/FR2813392B1/fr not_active Expired - Lifetime
-
2001
- 2001-08-24 CA CA2356303A patent/CA2356303C/fr not_active Expired - Lifetime
- 2001-08-24 RU RU2001124267/02A patent/RU2268953C2/ru active
- 2001-08-27 UA UA2001085968A patent/UA72911C2/uk unknown
- 2001-08-27 EP EP01402233.9A patent/EP1184656B1/fr not_active Expired - Lifetime
- 2001-08-27 JP JP2001255635A patent/JP4495888B2/ja not_active Expired - Lifetime
- 2001-08-27 US US09/938,495 patent/US6582585B2/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| JP2002161399A (ja) | 2002-06-04 |
| EP1184656B1 (fr) | 2015-01-28 |
| JP4495888B2 (ja) | 2010-07-07 |
| CA2356303A1 (fr) | 2002-02-28 |
| US6582585B2 (en) | 2003-06-24 |
| FR2813392B1 (fr) | 2002-12-06 |
| US20020023846A1 (en) | 2002-02-28 |
| UA72911C2 (uk) | 2005-05-16 |
| RU2268953C2 (ru) | 2006-01-27 |
| EP1184656A1 (fr) | 2002-03-06 |
| FR2813392A1 (fr) | 2002-03-01 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EEER | Examination request | ||
| MKEX | Expiry |
Effective date: 20210824 |