CA1335334C - Flaked tantalum powder composition and methods for making same - Google Patents
Flaked tantalum powder composition and methods for making sameInfo
- Publication number
- CA1335334C CA1335334C CA000584421A CA584421A CA1335334C CA 1335334 C CA1335334 C CA 1335334C CA 000584421 A CA000584421 A CA 000584421A CA 584421 A CA584421 A CA 584421A CA 1335334 C CA1335334 C CA 1335334C
- Authority
- CA
- Canada
- Prior art keywords
- powder
- flakes
- tantalum
- flake
- flaked
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- GUVRBAGPIYLISA-UHFFFAOYSA-N tantalum atom Chemical compound [Ta] GUVRBAGPIYLISA-UHFFFAOYSA-N 0.000 title claims abstract description 199
- 238000000034 method Methods 0.000 title claims abstract description 71
- 239000000203 mixture Substances 0.000 title description 4
- 229910052715 tantalum Inorganic materials 0.000 claims abstract description 69
- 239000008188 pellet Substances 0.000 claims abstract description 53
- 239000000843 powder Substances 0.000 claims abstract description 52
- 239000003990 capacitor Substances 0.000 claims abstract description 24
- 230000008569 process Effects 0.000 claims abstract description 13
- 238000005549 size reduction Methods 0.000 claims description 14
- 238000006722 reduction reaction Methods 0.000 claims description 10
- 239000003638 chemical reducing agent Substances 0.000 claims description 9
- 238000004845 hydriding Methods 0.000 claims description 6
- 230000009969 flowable effect Effects 0.000 claims description 2
- 239000002245 particle Substances 0.000 abstract description 27
- 238000003825 pressing Methods 0.000 abstract description 2
- 238000009826 distribution Methods 0.000 description 14
- 238000005054 agglomeration Methods 0.000 description 10
- 230000002776 aggregation Effects 0.000 description 10
- 238000004519 manufacturing process Methods 0.000 description 8
- 239000002253 acid Substances 0.000 description 7
- 238000003801 milling Methods 0.000 description 7
- 238000005245 sintering Methods 0.000 description 7
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 6
- 239000012535 impurity Substances 0.000 description 6
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 5
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 5
- 239000001257 hydrogen Substances 0.000 description 5
- 229910052739 hydrogen Inorganic materials 0.000 description 5
- 239000000463 material Substances 0.000 description 5
- 238000012545 processing Methods 0.000 description 5
- 230000000717 retained effect Effects 0.000 description 5
- 239000011734 sodium Substances 0.000 description 5
- 229910052708 sodium Inorganic materials 0.000 description 5
- 238000010438 heat treatment Methods 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 238000010894 electron beam technology Methods 0.000 description 3
- 238000005259 measurement Methods 0.000 description 3
- 229910052757 nitrogen Inorganic materials 0.000 description 3
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 2
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 239000008367 deionised water Substances 0.000 description 2
- 229910021641 deionized water Inorganic materials 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 229910017604 nitric acid Inorganic materials 0.000 description 2
- 230000001590 oxidative effect Effects 0.000 description 2
- 238000012216 screening Methods 0.000 description 2
- 230000035945 sensitivity Effects 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 229910001220 stainless steel Inorganic materials 0.000 description 2
- 239000010935 stainless steel Substances 0.000 description 2
- 238000005303 weighing Methods 0.000 description 2
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- 238000002048 anodisation reaction Methods 0.000 description 1
- 238000007743 anodising Methods 0.000 description 1
- 229910052786 argon Inorganic materials 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000009694 cold isostatic pressing Methods 0.000 description 1
- 239000000356 contaminant Substances 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000001627 detrimental effect Effects 0.000 description 1
- -1 e.g. Substances 0.000 description 1
- 239000003792 electrolyte Substances 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000001000 micrograph Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 230000002093 peripheral effect Effects 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 238000011946 reduction process Methods 0.000 description 1
- 238000012552 review Methods 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
- H01G9/00—Electrolytic capacitors, rectifiers, detectors, switching devices, light-sensitive or temperature-sensitive devices; Processes of their manufacture
- H01G9/004—Details
- H01G9/04—Electrodes or formation of dielectric layers thereon
- H01G9/048—Electrodes or formation of dielectric layers thereon characterised by their structure
- H01G9/052—Sintered electrodes
- H01G9/0525—Powder therefor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
- B22F1/06—Metallic powder characterised by the shape of the particles
- B22F1/068—Flake-like particles
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C1/00—Making non-ferrous alloys
- C22C1/04—Making non-ferrous alloys by powder metallurgy
- C22C1/045—Alloys based on refractory metals
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S75/00—Specialized metallurgical processes, compositions for use therein, consolidated metal powder compositions, and loose metal particulate mixtures
- Y10S75/954—Producing flakes or crystals
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Power Engineering (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Microelectronics & Electronic Packaging (AREA)
- Nanotechnology (AREA)
- Manufacture Of Metal Powder And Suspensions Thereof (AREA)
- Powder Metallurgy (AREA)
- Conductive Materials (AREA)
Applications Claiming Priority (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US12670687A | 1987-11-30 | 1987-11-30 | |
| US126,706 | 1987-11-30 | ||
| US209,746 | 1988-06-21 | ||
| US07/209,746 US4940490A (en) | 1987-11-30 | 1988-06-21 | Tantalum powder |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA1335334C true CA1335334C (en) | 1995-04-25 |
Family
ID=26824953
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA000584421A Expired - Fee Related CA1335334C (en) | 1987-11-30 | 1988-11-29 | Flaked tantalum powder composition and methods for making same |
Country Status (8)
Families Citing this family (59)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5211741A (en) * | 1987-11-30 | 1993-05-18 | Cabot Corporation | Flaked tantalum powder |
| HK1001346A1 (en) * | 1990-05-17 | 1998-06-12 | Cabot Corporation | Method of producing high surface area low metal impurity tantalum powder |
| BR9508497A (pt) * | 1994-08-01 | 1997-12-23 | Kroftt Brakston International | Processos para produzir um material elementar ou uma liga do mesmo a partir de um halogeneto ou misturas do mesmo e para produzir continuamente um metal ou não metal ou uma liga do mesmo |
| US7435282B2 (en) | 1994-08-01 | 2008-10-14 | International Titanium Powder, Llc | Elemental material and alloy |
| US20030061907A1 (en) * | 1994-08-01 | 2003-04-03 | Kroftt-Brakston International, Inc. | Gel of elemental material or alloy and liquid metal and salt |
| US20030145682A1 (en) * | 1994-08-01 | 2003-08-07 | Kroftt-Brakston International, Inc. | Gel of elemental material or alloy and liquid metal and salt |
| US7445658B2 (en) | 1994-08-01 | 2008-11-04 | Uchicago Argonne, Llc | Titanium and titanium alloys |
| JP3434041B2 (ja) * | 1994-09-28 | 2003-08-04 | スタルクヴイテック株式会社 | タンタル粉末及びそれを用いた電解コンデンサ |
| US5993513A (en) | 1996-04-05 | 1999-11-30 | Cabot Corporation | Method for controlling the oxygen content in valve metal materials |
| US5954856A (en) * | 1996-04-25 | 1999-09-21 | Cabot Corporation | Method of making tantalum metal powder with controlled size distribution and products made therefrom |
| KR100484686B1 (ko) * | 1996-04-25 | 2005-06-16 | 캐보트 코포레이션 | 탄탈륨분말의크기조절방법,크기분포가조절된탄탈륨금속분말의제조방법및그로부터제조되는생성물 |
| US6165623A (en) | 1996-11-07 | 2000-12-26 | Cabot Corporation | Niobium powders and niobium electrolytic capacitors |
| WO1998037249A1 (de) | 1997-02-19 | 1998-08-27 | H.C. Starck Gmbh & Co. Kg | Tantalpulver, verfahren zu seiner herstellung, sowie daraus erhältliche sinteranoden |
| US6444008B1 (en) | 1998-03-19 | 2002-09-03 | Cabot Corporation | Paint and coating compositions containing tantalum and/or niobium powders |
| US6051044A (en) * | 1998-05-04 | 2000-04-18 | Cabot Corporation | Nitrided niobium powders and niobium electrolytic capacitors |
| CN105033283A (zh) * | 1998-05-06 | 2015-11-11 | H.C.施塔克公司 | 用气态镁还原有关氧化物制备的金属粉末 |
| US6576038B1 (en) * | 1998-05-22 | 2003-06-10 | Cabot Corporation | Method to agglomerate metal particles and metal particles having improved properties |
| CN100381234C (zh) | 1999-03-19 | 2008-04-16 | 卡伯特公司 | 通过研磨制备铌和其它金属粉末 |
| US6375704B1 (en) | 1999-05-12 | 2002-04-23 | Cabot Corporation | High capacitance niobium powders and electrolytic capacitor anodes |
| US7621977B2 (en) * | 2001-10-09 | 2009-11-24 | Cristal Us, Inc. | System and method of producing metals and alloys |
| UA79310C2 (en) * | 2002-09-07 | 2007-06-11 | Int Titanium Powder Llc | Methods for production of alloys or ceramics with the use of armstrong method and device for their realization |
| AU2003298572A1 (en) * | 2002-09-07 | 2004-04-19 | International Titanium Powder, Llc. | Filter cake treatment method |
| AU2003273279B2 (en) * | 2002-09-07 | 2007-05-03 | Cristal Us, Inc. | Process for separating ti from a ti slurry |
| US20060107790A1 (en) * | 2002-10-07 | 2006-05-25 | International Titanium Powder, Llc | System and method of producing metals and alloys |
| EP2455340A1 (en) | 2003-05-19 | 2012-05-23 | Cabot Corporation | Valve metal sub-oxide powders and capacitors and sintered anode bodies made therefrom |
| DE10331785B4 (de) * | 2003-07-11 | 2007-08-23 | H. C. Starck Gmbh & Co. Kg | Verfahren zur Herstellung feiner Metall-, Legierungs-und Verbundpulver |
| US20070180951A1 (en) * | 2003-09-03 | 2007-08-09 | Armstrong Donn R | Separation system, method and apparatus |
| JP2008504692A (ja) * | 2004-06-28 | 2008-02-14 | キャボット コーポレイション | 高キャパシタンスのタンタルフレークス及びその生産方法 |
| US20070017319A1 (en) | 2005-07-21 | 2007-01-25 | International Titanium Powder, Llc. | Titanium alloy |
| US20070079908A1 (en) | 2005-10-06 | 2007-04-12 | International Titanium Powder, Llc | Titanium boride |
| US8257463B2 (en) * | 2006-01-23 | 2012-09-04 | Avx Corporation | Capacitor anode formed from flake powder |
| WO2007130483A2 (en) | 2006-05-05 | 2007-11-15 | Cabot Corporation | Tantalum powder with smooth surface and methods of manufacturing same |
| US20080031766A1 (en) * | 2006-06-16 | 2008-02-07 | International Titanium Powder, Llc | Attrited titanium powder |
| GB0622463D0 (en) * | 2006-11-10 | 2006-12-20 | Avx Ltd | Powder modification in the manufacture of solid state capacitor anodes |
| US7753989B2 (en) * | 2006-12-22 | 2010-07-13 | Cristal Us, Inc. | Direct passivation of metal powder |
| US20080229880A1 (en) * | 2007-03-23 | 2008-09-25 | Reading Alloys, Inc. | Production of high-purity tantalum flake powder |
| US20080233420A1 (en) * | 2007-03-23 | 2008-09-25 | Mccracken Colin G | Production of high-purity tantalum flake powder |
| US9127333B2 (en) * | 2007-04-25 | 2015-09-08 | Lance Jacobsen | Liquid injection of VCL4 into superheated TiCL4 for the production of Ti-V alloy powder |
| EP2214853A4 (en) * | 2007-10-15 | 2013-05-22 | Hi Temp Specialty Metals Inc | PROCESS FOR PREPARING TANTALUM POWDER USING RECYCLED AGENTS AS AN EXISTING MATERIAL |
| US20100085685A1 (en) * | 2008-10-06 | 2010-04-08 | Avx Corporation | Capacitor Anode Formed From a Powder Containing Coarse Agglomerates and Fine Agglomerates |
| US8430944B2 (en) * | 2008-12-22 | 2013-04-30 | Global Advanced Metals, Usa, Inc. | Fine particle recovery methods for valve metal powders |
| US8687347B2 (en) | 2011-01-12 | 2014-04-01 | Avx Corporation | Planar anode for use in a wet electrolytic capacitor |
| CN105026078B (zh) * | 2013-03-13 | 2017-10-24 | 凯米特电子公司 | 低能量研磨以制备片状粉末 |
| US9312075B1 (en) | 2013-09-06 | 2016-04-12 | Greatbatch Ltd. | High voltage tantalum anode and method of manufacture |
| US9633796B2 (en) | 2013-09-06 | 2017-04-25 | Greatbatch Ltd. | High voltage tantalum anode and method of manufacture |
| USRE48439E1 (en) | 2013-09-06 | 2021-02-16 | Greatbatch Ltd. | High voltage tantalum anode and method of manufacture |
| MX379158B (es) | 2013-12-25 | 2025-03-11 | Ningxia Orient Tantalum Ind Co Ltd | Polvo de tantalo grado capacitor de alta capacitancia especifica con propiedades electricas mejoradas y proceso para hacer el mismo. |
| MX2017001990A (es) | 2014-08-20 | 2017-05-23 | Ningxia Orient Tantalum Ind Co Ltd | Polvo de tantalo compuesto y proceso para preparar el mismo y anodo capacitor preparado a partir del polvo de tantalo. |
| EP3496884B1 (en) | 2016-08-12 | 2021-06-16 | COMPOSITE MATERIALS TECHNOLOGY, Inc. | Electrolytic capacitor and method for improved electrolytic capacitor anodes |
| US10230110B2 (en) | 2016-09-01 | 2019-03-12 | Composite Materials Technology, Inc. | Nano-scale/nanostructured Si coating on valve metal substrate for LIB anodes |
| US20180144874A1 (en) | 2016-10-21 | 2018-05-24 | Global Advanced Metals, Usa, Inc. | Tantalum Powder, Anode, And Capacitor Including Same, And Manufacturing Methods Thereof |
| JP7432927B2 (ja) | 2018-03-05 | 2024-02-19 | グローバル アドバンスト メタルズ ユー．エス．エー．，インコーポレイティド | 球状粉末含有陽極及びコンデンサ |
| EP3746240A2 (en) | 2018-03-05 | 2020-12-09 | Global Advanced Metals USA, Inc. | Spherical tantalum powder, products containing the same, and methods of making the same |
| WO2019236160A2 (en) | 2018-03-05 | 2019-12-12 | Global Advanced Metals Usa, Inc. | Powder metallurgy sputtering targets and methods of producing same |
| US20220023942A1 (en) | 2018-12-12 | 2022-01-27 | Global Advanced Metals Usa, Inc. | Spherical Niobium Alloy Powder, Products Containing The Same, And Methods Of Making The Same |
| US12119186B2 (en) | 2020-04-03 | 2024-10-15 | Greatbatch Ltd. | Electrolytic capacitor having an anode formed from a tantalum powder with a relatively low specific charge |
| US11450486B2 (en) * | 2020-04-03 | 2022-09-20 | Greatbatch Ltd. | Electrolytic capacitor having a tantalum anode |
| CN112404439A (zh) * | 2020-11-18 | 2021-02-26 | 贵州振华电子信息产业技术研究有限公司 | 一种电容器用高压钽粉及其制备方法和电容器 |
| CN112620636B (zh) * | 2020-12-15 | 2021-09-03 | 江门富祥电子材料有限公司 | 一种耐高压片形钽粉的生产方法 |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CH460261A (de) * | 1965-05-26 | 1968-07-31 | Ciba Geigy | Verfahren zur Herstellung von Tantalpulver |
| US4017302A (en) * | 1976-02-04 | 1977-04-12 | Fansteel Inc. | Tantalum metal powder |
| US4486225A (en) * | 1982-06-07 | 1984-12-04 | Mpd Technology Corporation | Production of highly reflective metal flake |
| US4482374A (en) * | 1982-06-07 | 1984-11-13 | Mpd Technology Corporation | Production of electrically conductive metal flake |
| US4441927A (en) * | 1982-11-16 | 1984-04-10 | Cabot Corporation | Tantalum powder composition |
| US4555268A (en) * | 1984-12-18 | 1985-11-26 | Cabot Corporation | Method for improving handling properties of a flaked tantalum powder composition |
| US4740238A (en) * | 1987-03-26 | 1988-04-26 | Fansteel Inc. | Platelet-containing tantalum powders |
-
1988
- 1988-06-21 US US07/209,746 patent/US4940490A/en not_active Expired - Lifetime
- 1988-11-29 CA CA000584421A patent/CA1335334C/en not_active Expired - Fee Related
- 1988-11-30 DE DE3840361A patent/DE3840361A1/de active Granted
- 1988-11-30 JP JP63301135A patent/JP2713365B2/ja not_active Expired - Lifetime
- 1988-11-30 KR KR1019880015956A patent/KR910001727B1/ko not_active Expired
- 1988-11-30 FR FR888815708A patent/FR2625122B1/fr not_active Expired - Fee Related
- 1988-11-30 ES ES8803653A patent/ES2009419A6/es not_active Expired
- 1988-11-30 GB GB8827970A patent/GB2212817B/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| ES2009419A6 (es) | 1989-09-16 |
| DE3840361C2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1991-12-12 |
| KR890008870A (ko) | 1989-07-12 |
| US4940490A (en) | 1990-07-10 |
| FR2625122A1 (fr) | 1989-06-30 |
| FR2625122B1 (fr) | 1992-09-18 |
| JPH02125804A (ja) | 1990-05-14 |
| GB2212817A (en) | 1989-08-02 |
| GB8827970D0 (en) | 1989-01-05 |
| KR910001727B1 (ko) | 1991-03-22 |
| JP2713365B2 (ja) | 1998-02-16 |
| DE3840361A1 (de) | 1989-06-08 |
| GB2212817B (en) | 1992-01-02 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MKLA | Lapsed |