CA1334619C - Process for the preparation of crystalline sodium silicates having a sheet structure - Google Patents
Process for the preparation of crystalline sodium silicates having a sheet structureInfo
- Publication number
- CA1334619C CA1334619C CA000565746A CA565746A CA1334619C CA 1334619 C CA1334619 C CA 1334619C CA 000565746 A CA000565746 A CA 000565746A CA 565746 A CA565746 A CA 565746A CA 1334619 C CA1334619 C CA 1334619C
- Authority
- CA
- Canada
- Prior art keywords
- sodium silicate
- spray
- weight
- rotary tubular
- zone
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000004115 Sodium Silicate Substances 0.000 title claims abstract description 36
- 238000002360 preparation method Methods 0.000 title claims abstract description 6
- 238000000034 method Methods 0.000 title claims description 21
- 235000019351 sodium silicates Nutrition 0.000 title abstract description 7
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims abstract description 49
- 229910052911 sodium silicate Inorganic materials 0.000 claims abstract description 29
- 235000019353 potassium silicate Nutrition 0.000 claims abstract description 20
- 239000000463 material Substances 0.000 claims abstract description 12
- 238000001694 spray drying Methods 0.000 claims abstract description 8
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 7
- KKCBUQHMOMHUOY-UHFFFAOYSA-N Na2O Inorganic materials [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 claims abstract description 4
- 229910052681 coesite Inorganic materials 0.000 claims abstract description 4
- 229910052906 cristobalite Inorganic materials 0.000 claims abstract description 4
- 229910052682 stishovite Inorganic materials 0.000 claims abstract description 4
- 229910052905 tridymite Inorganic materials 0.000 claims abstract description 4
- 239000000377 silicon dioxide Substances 0.000 claims abstract description 3
- 235000012239 silicon dioxide Nutrition 0.000 claims abstract description 3
- 238000010438 heat treatment Methods 0.000 claims description 6
- 230000000694 effects Effects 0.000 claims description 2
- 238000011084 recovery Methods 0.000 claims description 2
- 238000000137 annealing Methods 0.000 claims 2
- 238000002425 crystallisation Methods 0.000 claims 1
- 230000008025 crystallization Effects 0.000 claims 1
- 239000002245 particle Substances 0.000 claims 1
- 239000007787 solid Substances 0.000 abstract description 7
- 239000002912 waste gas Substances 0.000 abstract description 5
- 239000000243 solution Substances 0.000 description 14
- PMYUVOOOQDGQNW-UHFFFAOYSA-N hexasodium;trioxido(trioxidosilyloxy)silane Chemical compound [Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[O-][Si]([O-])([O-])O[Si]([O-])([O-])[O-] PMYUVOOOQDGQNW-UHFFFAOYSA-N 0.000 description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 9
- 239000007921 spray Substances 0.000 description 6
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 5
- 239000000047 product Substances 0.000 description 5
- 239000011734 sodium Substances 0.000 description 5
- 229910052708 sodium Inorganic materials 0.000 description 5
- DHMQDGOQFOQNFH-UHFFFAOYSA-N Glycine Chemical compound NCC(O)=O DHMQDGOQFOQNFH-UHFFFAOYSA-N 0.000 description 4
- 239000011777 magnesium Substances 0.000 description 4
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 description 3
- 230000000052 comparative effect Effects 0.000 description 3
- 239000013078 crystal Substances 0.000 description 3
- 239000007789 gas Substances 0.000 description 3
- 239000004471 Glycine Substances 0.000 description 2
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 2
- TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical compound [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- 239000011575 calcium Substances 0.000 description 2
- 229910052749 magnesium Inorganic materials 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 238000005507 spraying Methods 0.000 description 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 1
- 102000005701 Calcium-Binding Proteins Human genes 0.000 description 1
- 108010045403 Calcium-Binding Proteins Proteins 0.000 description 1
- 101100348017 Drosophila melanogaster Nazo gene Proteins 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000001110 calcium chloride Substances 0.000 description 1
- 229910001628 calcium chloride Inorganic materials 0.000 description 1
- 235000011148 calcium chloride Nutrition 0.000 description 1
- ZFXVRMSLJDYJCH-UHFFFAOYSA-N calcium magnesium Chemical compound [Mg].[Ca] ZFXVRMSLJDYJCH-UHFFFAOYSA-N 0.000 description 1
- 238000005341 cation exchange Methods 0.000 description 1
- MCWXGJITAZMZEV-UHFFFAOYSA-N dimethoate Chemical compound CNC(=O)CSP(=S)(OC)OC MCWXGJITAZMZEV-UHFFFAOYSA-N 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 229910001629 magnesium chloride Inorganic materials 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229910052615 phyllosilicate Inorganic materials 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
- 238000010079 rubber tapping Methods 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/20—Silicates
- C01B33/36—Silicates having base-exchange properties but not having molecular sieve properties
- C01B33/38—Layered base-exchange silicates, e.g. clays, micas or alkali metal silicates of kenyaite or magadiite type
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Silicates, Zeolites, And Molecular Sieves (AREA)
- Medicines Containing Material From Animals Or Micro-Organisms (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
- External Artificial Organs (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19873718350 DE3718350A1 (de) | 1987-06-01 | 1987-06-01 | Verfahren zur herstellung von kristallinen natriumsilikaten mit schichtstruktur |
| DEP3718350.8 | 1987-06-01 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA1334619C true CA1334619C (en) | 1995-03-07 |
Family
ID=6328822
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA000565746A Expired - Fee Related CA1334619C (en) | 1987-06-01 | 1988-05-03 | Process for the preparation of crystalline sodium silicates having a sheet structure |
Country Status (9)
| Country | Link |
|---|---|
| EP (1) | EP0293640B1 (enrdf_load_stackoverflow) |
| JP (1) | JPS63310717A (enrdf_load_stackoverflow) |
| AT (1) | ATE73737T1 (enrdf_load_stackoverflow) |
| CA (1) | CA1334619C (enrdf_load_stackoverflow) |
| DE (2) | DE3718350A1 (enrdf_load_stackoverflow) |
| DK (1) | DK167917B1 (enrdf_load_stackoverflow) |
| ES (1) | ES2031175T3 (enrdf_load_stackoverflow) |
| NO (1) | NO171671C (enrdf_load_stackoverflow) |
| PT (1) | PT87624B (enrdf_load_stackoverflow) |
Families Citing this family (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5229095A (en) * | 1989-10-25 | 1993-07-20 | Hoechst Aktiengesellschaft | Process for producing amorphous sodium silicate |
| US5236682A (en) * | 1989-10-25 | 1993-08-17 | Hoechst Aktiengesellschaft | Process for producing crystalline sodium silicates having a layered structure |
| CA2024966C (en) * | 1989-10-25 | 1995-07-18 | Gunther Schimmel | Process for producing sodium silicates |
| CA2025073C (en) * | 1989-10-25 | 1995-07-18 | Gunther Schimmel | Process for producing sodium silicates |
| DE4000705A1 (de) | 1990-01-12 | 1991-07-18 | Hoechst Ag | Verfahren zur herstellung von kristallinen natriumsilikaten |
| DE4102743A1 (de) * | 1991-01-30 | 1992-08-06 | Henkel Kgaa | Phosphatfreies reinigungsmittel |
| DE4107231A1 (de) * | 1991-03-07 | 1992-09-10 | Hoechst Ag | Verfahren zur herstellung von natriumsilikaten |
| DE4107230C2 (de) * | 1991-03-07 | 1995-04-06 | Hoechst Ag | Verfahren zur Herstellung von Natriumsilikaten |
| DE4142711A1 (de) * | 1991-12-21 | 1993-06-24 | Hoechst Ag | Verfahren zur herstellung von kristallinen natriumdisilikaten |
| KR0139976B1 (ko) * | 1994-05-31 | 1998-06-01 | 강박광 | 층상결정성 이규산나트륨의 제조방법 |
| US5567404A (en) * | 1994-05-31 | 1996-10-22 | Korea Research Institute Of Chemical Technology | Process for preparation of layered sodium silicate from anhydrous sodium silicate |
| DE4419744A1 (de) * | 1994-06-06 | 1995-12-07 | Henkel Kgaa | Drucklose Niedertemperatursynthese kristalliner Disilicate |
| US5614160A (en) * | 1994-06-10 | 1997-03-25 | Pq Corporation | Composite silicate materials |
| DE4421851A1 (de) * | 1994-06-22 | 1996-01-04 | Henkel Kgaa | Verfahren zur Niedertemperatursynthese kristalliner Disilicate-II |
| DE4421850A1 (de) * | 1994-06-22 | 1996-01-04 | Henkel Kgaa | Verfahren zur Niedertemperatursynthese kristalliner Disilicate-I |
| DE19707448C2 (de) * | 1997-02-25 | 1998-11-26 | Clariant Gmbh | Verfahren zur Herstellung von kristallinen Natriumsilikaten |
| DE19707449C1 (de) * | 1997-02-25 | 1998-04-09 | Clariant Gmbh | Verfahren zur Herstellung von kristallinen Natriumsilikaten |
| KR100280376B1 (ko) * | 1998-08-14 | 2001-02-01 | 김충섭 | 결정성 층상 이규산나트륨의 제조방법 |
| CN100340484C (zh) * | 2005-09-01 | 2007-10-03 | 成都长江通信有限公司 | 一种结晶二硅酸钠的制备方法 |
| JP2010512447A (ja) | 2006-12-11 | 2010-04-22 | ザ プロクター アンド ギャンブル カンパニー | 印刷フィルム上の画像の改善された視覚認知性 |
| US20080210265A1 (en) | 2007-03-01 | 2008-09-04 | Crawford Charles A | Coating removal composition |
| EP2484747A1 (en) | 2007-08-16 | 2012-08-08 | The Procter & Gamble Company | Process for making a detergent composition |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3875282A (en) * | 1973-04-30 | 1975-04-01 | Stauffer Chemical Co | Production of high bulk density spray dried hydrous sodium silicate |
| JPS6056484B2 (ja) * | 1977-07-20 | 1985-12-10 | 株式会社日立製作所 | 電気掃除機の除塵装置 |
| DE3413571A1 (de) * | 1984-04-11 | 1985-10-24 | Hoechst Ag, 6230 Frankfurt | Verwendung von kristallinen schichtfoermigen natriumsilikaten zur wasserenthaertung und verfahren zur wasserenthaertung |
| DE3417649A1 (de) * | 1984-05-12 | 1985-11-14 | Hoechst Ag, 6230 Frankfurt | Verfahren zur herstellung von kristallinen natriumsilikaten |
-
1987
- 1987-06-01 DE DE19873718350 patent/DE3718350A1/de not_active Withdrawn
-
1988
- 1988-05-03 CA CA000565746A patent/CA1334619C/en not_active Expired - Fee Related
- 1988-05-09 ES ES198888107429T patent/ES2031175T3/es not_active Expired - Lifetime
- 1988-05-09 EP EP88107429A patent/EP0293640B1/de not_active Expired - Lifetime
- 1988-05-09 AT AT88107429T patent/ATE73737T1/de not_active IP Right Cessation
- 1988-05-09 DE DE8888107429T patent/DE3869209D1/de not_active Expired - Lifetime
- 1988-05-30 JP JP63130498A patent/JPS63310717A/ja active Granted
- 1988-05-31 DK DK295488A patent/DK167917B1/da not_active IP Right Cessation
- 1988-05-31 NO NO882391A patent/NO171671C/no not_active IP Right Cessation
- 1988-05-31 PT PT87624A patent/PT87624B/pt not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| EP0293640A3 (en) | 1989-11-29 |
| DK295488A (da) | 1988-12-02 |
| NO171671B (no) | 1993-01-11 |
| NO882391D0 (no) | 1988-05-31 |
| DE3869209D1 (de) | 1992-04-23 |
| NO882391L (no) | 1988-12-02 |
| PT87624B (pt) | 1992-09-30 |
| DE3718350A1 (de) | 1988-12-22 |
| DE3869209T (enrdf_load_stackoverflow) | 1992-04-23 |
| ATE73737T1 (de) | 1992-04-15 |
| DK167917B1 (da) | 1994-01-03 |
| ES2031175T3 (es) | 1992-12-01 |
| JPS63310717A (ja) | 1988-12-19 |
| DK295488D0 (da) | 1988-05-31 |
| PT87624A (pt) | 1988-06-01 |
| EP0293640B1 (de) | 1992-03-18 |
| NO171671C (no) | 1993-04-28 |
| EP0293640A2 (de) | 1988-12-07 |
| JPH0566888B2 (enrdf_load_stackoverflow) | 1993-09-22 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MKLA | Lapsed |