CA1269995C - PREPARATION OF 2-HYDROXY-METHYLTHIOBUTYRIC ACID LIQUID - Google Patents
PREPARATION OF 2-HYDROXY-METHYLTHIOBUTYRIC ACID LIQUIDInfo
- Publication number
- CA1269995C CA1269995C CA467698A CA467698A CA1269995C CA 1269995 C CA1269995 C CA 1269995C CA 467698 A CA467698 A CA 467698A CA 467698 A CA467698 A CA 467698A CA 1269995 C CA1269995 C CA 1269995C
- Authority
- CA
- Canada
- Prior art keywords
- hydroxy
- methylthiobutyric acid
- acid
- preparation
- methylthiobutyric
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000000034 method Methods 0.000 title abstract 3
- 238000002360 preparation method Methods 0.000 title abstract 3
- SOGMDUPYAJRSJA-UHFFFAOYSA-N 2-hydroxy-2-methylbutanethioic s-acid Chemical compound CCC(C)(O)C(S)=O SOGMDUPYAJRSJA-UHFFFAOYSA-N 0.000 title abstract 2
- 239000007788 liquid Substances 0.000 title abstract 2
- PICCHNWCTUUCAQ-UHFFFAOYSA-N 2-hydroxypentanethioic s-acid Chemical compound CCCC(O)C(O)=S PICCHNWCTUUCAQ-UHFFFAOYSA-N 0.000 abstract 5
- 238000000605 extraction Methods 0.000 abstract 3
- VWWOJJANXYSACS-UHFFFAOYSA-N 2-hydroxy-4-methylsulfanylbutanenitrile Chemical compound CSCCC(O)C#N VWWOJJANXYSACS-UHFFFAOYSA-N 0.000 abstract 2
- 239000002253 acid Substances 0.000 abstract 2
- DOLNLDKZJKDWLS-UHFFFAOYSA-N 2-hydroxypentanethioamide Chemical compound CCCC(O)C(N)=S DOLNLDKZJKDWLS-UHFFFAOYSA-N 0.000 abstract 1
- 238000009835 boiling Methods 0.000 abstract 1
- 229910052500 inorganic mineral Inorganic materials 0.000 abstract 1
- 230000014759 maintenance of location Effects 0.000 abstract 1
- 239000011707 mineral Substances 0.000 abstract 1
- 239000012074 organic phase Substances 0.000 abstract 1
- 238000000926 separation method Methods 0.000 abstract 1
- 239000007787 solid Substances 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
- 238000001256 steam distillation Methods 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C319/00—Preparation of thiols, sulfides, hydropolysulfides or polysulfides
- C07C319/14—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides
- C07C319/20—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides by reactions not involving the formation of sulfide groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C319/00—Preparation of thiols, sulfides, hydropolysulfides or polysulfides
- C07C319/26—Separation; Purification; Stabilisation; Use of additives
- C07C319/28—Separation; Purification
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CA467698A CA1269995C (en) | 1983-11-14 | 1984-11-13 | PREPARATION OF 2-HYDROXY-METHYLTHIOBUTYRIC ACID LIQUID |
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US55123183A | 1983-11-14 | 1983-11-14 | |
| US551,231 | 1983-11-14 | ||
| CA467698A CA1269995C (en) | 1983-11-14 | 1984-11-13 | PREPARATION OF 2-HYDROXY-METHYLTHIOBUTYRIC ACID LIQUID |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CA1269995A CA1269995A (en) | 1990-06-05 |
| CA1269995C true CA1269995C (en) | 1990-06-05 |
Family
ID=24200399
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA467698A Expired CA1269995C (en) | 1983-11-14 | 1984-11-13 | PREPARATION OF 2-HYDROXY-METHYLTHIOBUTYRIC ACID LIQUID |
Country Status (5)
| Country | Link |
|---|---|
| EP (1) | EP0143100B1 (ref) |
| JP (1) | JPS60166661A (ref) |
| AT (1) | ATE28747T1 (ref) |
| CA (1) | CA1269995C (ref) |
| DE (1) | DE3465194D1 (ref) |
Families Citing this family (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| ES2005784A6 (es) * | 1988-02-22 | 1989-03-16 | Desarrollo Tecnico Ind S A Soc | Un procedimiento para preparar soluciones acuosas de acido 2-hidroxi-4-metil-tiobutirico. |
| MY109603A (en) * | 1992-05-21 | 1997-03-31 | Daicel Chem | Process for producing 2-hydroxy-4-methylthiobutanoic acid |
| DE4428608C1 (de) * | 1994-08-12 | 1996-02-29 | Degussa | Verfahren zur Gewinnung von 2-Hydroxy-4-methylthiobuttersäure (MHA) |
| JPH11508876A (ja) | 1995-06-07 | 1999-08-03 | ノーバス インターナショナル インコーポレイテッド | ２−ヒドロキシ−４−メチルチオブタン酸又はその塩を製造するための連続加水分解法 |
| US5856567A (en) * | 1995-06-07 | 1999-01-05 | Novus International, Inc. | Continuous hydrolysis process for preparing 2-hydroxy-4-methylthiobutanioc acid or salts thereof |
| DE19548538C2 (de) * | 1995-12-23 | 1997-12-18 | Degussa | Verfahren zur Gewinnung von 2-Hydroxy-4-methylthiobuttersäure (MHA) |
| FR2780969B1 (fr) * | 1998-07-10 | 2000-08-18 | Rhone Poulenc Nutrition Animal | Procede de separation de l'acide hydroxymethylthiobutyrique |
| JP4517474B2 (ja) * | 2000-07-25 | 2010-08-04 | 住友化学株式会社 | ２−ヒドロキシ−４−メチルチオブタン酸の製造方法 |
| JP4517486B2 (ja) * | 2000-09-25 | 2010-08-04 | 住友化学株式会社 | ２−ヒドロキシ−４−メチルチオブタンニトリルの製造方法 |
| JP4517520B2 (ja) * | 2001-02-27 | 2010-08-04 | 住友化学株式会社 | ２−ヒドロキシ−４−メチルチオブタン酸の製造方法 |
| DE10316110A1 (de) * | 2003-04-09 | 2004-10-28 | Degussa Ag | Verfahren zur Herstellung von 2-Hydroxy-4-methylthio-buttersäure Ammoniumsalz |
| JP4696496B2 (ja) * | 2004-08-18 | 2011-06-08 | 住友化学株式会社 | ２−ヒドロキシ−４−メチルチオ酪酸の製造方法 |
| JP2007238553A (ja) * | 2006-03-10 | 2007-09-20 | Sumitomo Chemical Co Ltd | ２−ヒドロキシ−４−メチルチオブタン酸の製造方法および製造装置 |
| EP3656760A1 (de) | 2018-11-21 | 2020-05-27 | Evonik Operations GmbH | Lagerstabile form von 3-methylthiopropionaldehyd |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2975192A (en) * | 1959-11-09 | 1961-03-14 | Monsanto Chemicals | Methionine analogues |
| BE611435A (fr) * | 1960-12-14 | 1962-06-12 | Stamicarbon | Procédé de préparation de sels métalliques d'acide alpha-hydroxy- gamma -méthylmercaptobutyrique |
-
1984
- 1984-11-13 CA CA467698A patent/CA1269995C/en not_active Expired
- 1984-11-13 AT AT84870151T patent/ATE28747T1/de not_active IP Right Cessation
- 1984-11-13 EP EP84870151A patent/EP0143100B1/en not_active Expired
- 1984-11-13 JP JP59239324A patent/JPS60166661A/ja active Granted
- 1984-11-13 DE DE8484870151T patent/DE3465194D1/de not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0430948B2 (ref) | 1992-05-25 |
| CA1269995A (en) | 1990-06-05 |
| EP0143100A2 (en) | 1985-05-29 |
| DE3465194D1 (en) | 1987-09-10 |
| EP0143100A3 (en) | 1985-06-26 |
| EP0143100B1 (en) | 1987-08-05 |
| JPS60166661A (ja) | 1985-08-29 |
| ATE28747T1 (de) | 1987-08-15 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MKEX | Expiry | ||
| MKEX | Expiry |
Effective date: 20070605 |