CA1102795A - Method of isolating polar lipids from a mixture of polar and non-polar cereal lipids - Google Patents
Method of isolating polar lipids from a mixture of polar and non-polar cereal lipidsInfo
- Publication number
- CA1102795A CA1102795A CA309,300A CA309300A CA1102795A CA 1102795 A CA1102795 A CA 1102795A CA 309300 A CA309300 A CA 309300A CA 1102795 A CA1102795 A CA 1102795A
- Authority
- CA
- Canada
- Prior art keywords
- polar
- lipids
- water
- mixture
- cereal
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 150000002632 lipids Chemical class 0.000 title claims abstract description 50
- 239000000203 mixture Substances 0.000 title claims abstract description 30
- 235000013339 cereals Nutrition 0.000 title claims abstract description 12
- 238000000034 method Methods 0.000 title claims description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 31
- 238000000926 separation method Methods 0.000 claims abstract description 11
- 230000005484 gravity Effects 0.000 claims abstract description 6
- 238000002156 mixing Methods 0.000 claims abstract description 3
- 150000003839 salts Chemical class 0.000 claims description 4
- -1 halogen salt Chemical class 0.000 claims description 3
- 229910052783 alkali metal Inorganic materials 0.000 claims description 2
- 150000001340 alkali metals Chemical class 0.000 claims description 2
- 229910052736 halogen Inorganic materials 0.000 claims description 2
- 239000012071 phase Substances 0.000 abstract description 23
- 235000008429 bread Nutrition 0.000 abstract description 8
- 239000000654 additive Substances 0.000 abstract description 6
- 230000000996 additive effect Effects 0.000 abstract description 6
- 239000008346 aqueous phase Substances 0.000 abstract description 2
- 239000000543 intermediate Substances 0.000 abstract 1
- 235000013312 flour Nutrition 0.000 description 8
- 241000209140 Triticum Species 0.000 description 7
- 235000021307 Triticum Nutrition 0.000 description 7
- 238000000605 extraction Methods 0.000 description 4
- 230000000694 effects Effects 0.000 description 3
- 239000003995 emulsifying agent Substances 0.000 description 3
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical group CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 2
- 229920002472 Starch Polymers 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 239000012153 distilled water Substances 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 238000002955 isolation Methods 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000003960 organic solvent Substances 0.000 description 2
- 150000003904 phospholipids Chemical class 0.000 description 2
- 150000003626 triacylglycerols Chemical class 0.000 description 2
- IIZPXYDJLKNOIY-JXPKJXOSSA-N 1-palmitoyl-2-arachidonoyl-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCC\C=C/C\C=C/C\C=C/C\C=C/CCCCC IIZPXYDJLKNOIY-JXPKJXOSSA-N 0.000 description 1
- 235000007319 Avena orientalis Nutrition 0.000 description 1
- 244000075850 Avena orientalis Species 0.000 description 1
- JIEJACFVMGPCON-UHFFFAOYSA-N CCCCCCCCCCCCCCCCCCCC(C(=O)C(C)O)(C(=O)O)O Chemical class CCCCCCCCCCCCCCCCCCCC(C(=O)C(C)O)(C(=O)O)O JIEJACFVMGPCON-UHFFFAOYSA-N 0.000 description 1
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- 108010068370 Glutens Proteins 0.000 description 1
- 240000005979 Hordeum vulgare Species 0.000 description 1
- 235000007340 Hordeum vulgare Nutrition 0.000 description 1
- 241000209056 Secale Species 0.000 description 1
- 235000007238 Secale cereale Nutrition 0.000 description 1
- 229930182558 Sterol Natural products 0.000 description 1
- 235000019714 Triticale Nutrition 0.000 description 1
- 240000008042 Zea mays Species 0.000 description 1
- 235000016383 Zea mays subsp huehuetenangensis Nutrition 0.000 description 1
- 235000002017 Zea mays subsp mays Nutrition 0.000 description 1
- OGBUMNBNEWYMNJ-UHFFFAOYSA-N batilol Chemical class CCCCCCCCCCCCCCCCCCOCC(O)CO OGBUMNBNEWYMNJ-UHFFFAOYSA-N 0.000 description 1
- ASGJEMPQQVNTGO-UHFFFAOYSA-N benzene chloroform Chemical compound C(Cl)(Cl)Cl.C1=CC=CC=C1.C1=CC=CC=C1 ASGJEMPQQVNTGO-UHFFFAOYSA-N 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 230000002844 continuous effect Effects 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- IDGUHHHQCWSQLU-UHFFFAOYSA-N ethanol;hydrate Chemical compound O.CCO IDGUHHHQCWSQLU-UHFFFAOYSA-N 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 239000000295 fuel oil Substances 0.000 description 1
- 235000021312 gluten Nutrition 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000008240 homogeneous mixture Substances 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 239000000787 lecithin Substances 0.000 description 1
- 229940067606 lecithin Drugs 0.000 description 1
- 235000010445 lecithin Nutrition 0.000 description 1
- 235000009973 maize Nutrition 0.000 description 1
- 235000013575 mashed potatoes Nutrition 0.000 description 1
- 238000003801 milling Methods 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 235000018102 proteins Nutrition 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- YNOVLNPSBVENJC-UHFFFAOYSA-M sodium 2-hydroxy-2-(2-hydroxypropanoyl)henicosanoate Chemical compound C(CCCCCCCCCCCCCCCCC)CC(C(=O)[O-])(O)C(C(O)C)=O.[Na+] YNOVLNPSBVENJC-UHFFFAOYSA-M 0.000 description 1
- MGWJZJGAXWOTDN-UHFFFAOYSA-M sodium decan-1-ol octanoate hydrate Chemical compound O.[Na+].CCCCCCCC([O-])=O.CCCCCCCCCCO MGWJZJGAXWOTDN-UHFFFAOYSA-M 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 235000003702 sterols Nutrition 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 238000004809 thin layer chromatography Methods 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
- 229940100445 wheat starch Drugs 0.000 description 1
- 241000228158 x Triticosecale Species 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B7/00—Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils
-
- A—HUMAN NECESSITIES
- A21—BAKING; EDIBLE DOUGHS
- A21D—TREATMENT OF FLOUR OR DOUGH FOR BAKING, e.g. BY ADDITION OF MATERIALS; BAKING; BAKERY PRODUCTS
- A21D2/00—Treatment of flour or dough by adding materials thereto before or during baking
- A21D2/08—Treatment of flour or dough by adding materials thereto before or during baking by adding organic substances
- A21D2/14—Organic oxygen compounds
- A21D2/16—Fatty acid esters
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Food Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Bakery Products And Manufacturing Methods Therefor (AREA)
- Fats And Perfumes (AREA)
- Compounds Of Unknown Constitution (AREA)
- Cereal-Derived Products (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SE77-09374-8 | 1977-08-19 | ||
| SE7709374A SE417441B (sv) | 1977-08-19 | 1977-08-19 | Forfarande for att isolera polera lipider ur en blandning av polera och opolera cerealiclipider genom blandning med vatten och derpa foljande tyngdkraftsseparation |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA1102795A true CA1102795A (en) | 1981-06-09 |
Family
ID=20332052
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA309,300A Expired CA1102795A (en) | 1977-08-19 | 1978-08-14 | Method of isolating polar lipids from a mixture of polar and non-polar cereal lipids |
Country Status (7)
| Country | Link |
|---|---|
| JP (1) | JPS5452003A (enExample) |
| AU (1) | AU522378B2 (enExample) |
| CA (1) | CA1102795A (enExample) |
| DE (1) | DE2834999A1 (enExample) |
| FI (1) | FI782477A7 (enExample) |
| FR (1) | FR2400552A1 (enExample) |
| SE (1) | SE417441B (enExample) |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2003089620A2 (en) | 2002-04-19 | 2003-10-30 | Diversa Corporation | Phospholipases, nucleic acids encoding them and methods for making and using them |
| WO2006009676A2 (en) | 2004-06-16 | 2006-01-26 | Diversa Corporation | Compositions and methods for enzymatic decolorization of chlorophyll |
| WO2008036863A2 (en) | 2006-09-21 | 2008-03-27 | Verenium Corporation | Phospholipases, nucleic acids encoding them and methods for making and using them |
| EP2216403A2 (en) | 2006-02-02 | 2010-08-11 | Verenium Corporation | Esterases and related nucleic acids and methods |
| WO2011046812A1 (en) | 2009-10-16 | 2011-04-21 | Verenium Corporation | Phospholipases, nucleic acids encoding them and methods for making and using them |
| WO2011046815A1 (en) | 2009-10-16 | 2011-04-21 | Bunge Oils, Inc. | Oil degumming methods |
| EP2853593A1 (en) | 2003-03-07 | 2015-04-01 | DSM IP Assets B.V. | Hydrolases, nucleic acids encoding them and mehods for making and using them |
| US9017990B2 (en) | 2004-09-10 | 2015-04-28 | Dsm Ip Assets B.V. | Methods for enzymatic decolorization of chlorophyll |
| EP3190182A1 (en) | 2004-03-08 | 2017-07-12 | DSM IP Assets B.V. | Phospholipases, nucleic acids encoding them and methods for making and using them |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2676936B1 (fr) * | 1991-05-27 | 1993-11-05 | Inocosm Laboratoires | Procede de separation d'un compose riche en glycolipides lysophospholipides shingolipides et ceramides d'origine vegetale, ainsi que produits cosmetiques obtenus par la mise en óoeuvre de ce procede. |
| ES2135756T3 (es) * | 1994-08-16 | 1999-11-01 | Frische Gmbh | Procedimiento para la obtencion de productos nativos no solubles en agua a partir de mezclas de sustancias con ayuda de la fuerza centrifuga. |
| WO1997010050A1 (en) * | 1995-09-14 | 1997-03-20 | Unilever N.V. | Surface-active composition |
| FR2836335B1 (fr) * | 2002-02-27 | 2004-12-03 | Intersnack Knabber Geback Gmbh | Flocons deshydrates a base d'amidon comprenant 0,05 % de glycolipide(s) |
| WO2010104444A1 (en) | 2009-03-11 | 2010-09-16 | Swedish Oat Fiber Ab | Method for separating neutral and polar lipids and an oil rich in polar lipids |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1469392A (fr) * | 1965-02-20 | 1967-02-10 | Inst Przemyslu Tluszczowego | Procédé continu de démucilagination des huiles végétales et de production de lécithine à partir des boues de phosphatides obtenues, et dispositif de mise en oeuvre de ce procédé |
| DE1923971B1 (de) * | 1969-05-10 | 1970-11-26 | Heinz Schumacher | Verfahren und Vorrichtung zur Entschleimung von pflanzlichen OElen |
-
1977
- 1977-08-19 SE SE7709374A patent/SE417441B/sv not_active IP Right Cessation
-
1978
- 1978-08-04 AU AU38631/78A patent/AU522378B2/en not_active Expired
- 1978-08-10 DE DE19782834999 patent/DE2834999A1/de active Granted
- 1978-08-14 CA CA309,300A patent/CA1102795A/en not_active Expired
- 1978-08-14 FI FI782477A patent/FI782477A7/fi unknown
- 1978-08-17 FR FR7824047A patent/FR2400552A1/fr active Granted
- 1978-08-18 JP JP10136578A patent/JPS5452003A/ja active Granted
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2003089620A2 (en) | 2002-04-19 | 2003-10-30 | Diversa Corporation | Phospholipases, nucleic acids encoding them and methods for making and using them |
| EP2298871A1 (en) | 2002-04-19 | 2011-03-23 | Verenium Corporation | Phospholipases, nucleic acids encoding them and methods for making and using them |
| EP2853593A1 (en) | 2003-03-07 | 2015-04-01 | DSM IP Assets B.V. | Hydrolases, nucleic acids encoding them and mehods for making and using them |
| EP3190182A1 (en) | 2004-03-08 | 2017-07-12 | DSM IP Assets B.V. | Phospholipases, nucleic acids encoding them and methods for making and using them |
| WO2006009676A2 (en) | 2004-06-16 | 2006-01-26 | Diversa Corporation | Compositions and methods for enzymatic decolorization of chlorophyll |
| EP2468853A1 (en) | 2004-06-16 | 2012-06-27 | Verenium Corporation | Composition and methods for enzymatic decolorization of chlorophyll |
| US9017990B2 (en) | 2004-09-10 | 2015-04-28 | Dsm Ip Assets B.V. | Methods for enzymatic decolorization of chlorophyll |
| EP2216403A2 (en) | 2006-02-02 | 2010-08-11 | Verenium Corporation | Esterases and related nucleic acids and methods |
| WO2008036863A2 (en) | 2006-09-21 | 2008-03-27 | Verenium Corporation | Phospholipases, nucleic acids encoding them and methods for making and using them |
| WO2011046812A1 (en) | 2009-10-16 | 2011-04-21 | Verenium Corporation | Phospholipases, nucleic acids encoding them and methods for making and using them |
| WO2011046815A1 (en) | 2009-10-16 | 2011-04-21 | Bunge Oils, Inc. | Oil degumming methods |
| US9512382B2 (en) | 2009-10-16 | 2016-12-06 | Bunge Global Innovation, Llc | Oil degumming methods |
Also Published As
| Publication number | Publication date |
|---|---|
| SE417441B (sv) | 1981-03-16 |
| JPS626558B2 (enExample) | 1987-02-12 |
| JPS5452003A (en) | 1979-04-24 |
| AU522378B2 (en) | 1982-06-03 |
| AU3863178A (en) | 1980-02-07 |
| SE7709374L (sv) | 1979-02-20 |
| DE2834999A1 (de) | 1979-03-01 |
| FI782477A7 (fi) | 1979-02-20 |
| FR2400552B1 (enExample) | 1983-08-05 |
| DE2834999C2 (enExample) | 1989-04-20 |
| FR2400552A1 (fr) | 1979-03-16 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MKEX | Expiry |