CA1070903A - Liquid preparations of reactive dyestuffs - Google Patents
Liquid preparations of reactive dyestuffsInfo
- Publication number
- CA1070903A CA1070903A CA224,031A CA224031A CA1070903A CA 1070903 A CA1070903 A CA 1070903A CA 224031 A CA224031 A CA 224031A CA 1070903 A CA1070903 A CA 1070903A
- Authority
- CA
- Canada
- Prior art keywords
- weight
- dyestuff
- parts
- formula
- solution
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000002360 preparation method Methods 0.000 title claims abstract description 69
- 239000007788 liquid Substances 0.000 title claims abstract description 8
- 239000000975 dye Substances 0.000 claims abstract description 223
- 238000004043 dyeing Methods 0.000 claims abstract description 90
- 238000000034 method Methods 0.000 claims abstract description 40
- 230000008569 process Effects 0.000 claims abstract description 16
- 239000000126 substance Substances 0.000 claims abstract description 12
- 239000002253 acid Substances 0.000 claims abstract description 6
- 239000004952 Polyamide Substances 0.000 claims abstract description 3
- 239000002657 fibrous material Substances 0.000 claims abstract description 3
- 229920002647 polyamide Polymers 0.000 claims abstract description 3
- 210000002268 wool Anatomy 0.000 claims abstract description 3
- 239000000203 mixture Substances 0.000 claims description 28
- 229910021538 borax Chemical class 0.000 claims description 10
- 235000010339 sodium tetraborate Nutrition 0.000 claims description 10
- BSVBQGMMJUBVOD-UHFFFAOYSA-N trisodium borate Chemical class [Na+].[Na+].[Na+].[O-]B([O-])[O-] BSVBQGMMJUBVOD-UHFFFAOYSA-N 0.000 claims description 10
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 6
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical class OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 6
- 229910052708 sodium Inorganic materials 0.000 claims description 6
- 239000011734 sodium Substances 0.000 claims description 5
- 239000000835 fiber Substances 0.000 claims description 4
- SCVFZCLFOSHCOH-UHFFFAOYSA-M potassium acetate Chemical compound [K+].CC([O-])=O SCVFZCLFOSHCOH-UHFFFAOYSA-M 0.000 claims description 4
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims description 3
- 239000003795 chemical substances by application Substances 0.000 claims description 3
- 159000000001 potassium salts Chemical class 0.000 claims description 3
- 235000011056 potassium acetate Nutrition 0.000 claims description 2
- 239000004627 regenerated cellulose Substances 0.000 claims description 2
- 239000001632 sodium acetate Substances 0.000 claims description 2
- 235000017281 sodium acetate Nutrition 0.000 claims description 2
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical class [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 claims 1
- 238000004040 coloring Methods 0.000 claims 1
- LWYJTCLDMYROHH-UHFFFAOYSA-M potassium;furan-2-carboxylate Chemical compound [K+].[O-]C(=O)C1=CC=CO1 LWYJTCLDMYROHH-UHFFFAOYSA-M 0.000 claims 1
- HDCRDACZYDHUQX-UHFFFAOYSA-M sodium;furan-2-carboxylate Chemical compound [Na+].[O-]C(=O)C1=CC=CO1 HDCRDACZYDHUQX-UHFFFAOYSA-M 0.000 claims 1
- 238000007639 printing Methods 0.000 abstract description 53
- 229920002678 cellulose Polymers 0.000 abstract description 2
- 239000001913 cellulose Substances 0.000 abstract description 2
- 239000000243 solution Substances 0.000 description 100
- 239000000843 powder Substances 0.000 description 52
- 230000015572 biosynthetic process Effects 0.000 description 32
- 238000003786 synthesis reaction Methods 0.000 description 29
- 230000000875 corresponding effect Effects 0.000 description 25
- 229920000742 Cotton Polymers 0.000 description 24
- 230000008878 coupling Effects 0.000 description 24
- 238000010168 coupling process Methods 0.000 description 24
- 238000005859 coupling reaction Methods 0.000 description 24
- 238000003756 stirring Methods 0.000 description 24
- 238000009472 formulation Methods 0.000 description 23
- 239000007864 aqueous solution Substances 0.000 description 19
- 238000001694 spray drying Methods 0.000 description 17
- 239000007858 starting material Substances 0.000 description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 13
- 150000003839 salts Chemical class 0.000 description 12
- 238000006243 chemical reaction Methods 0.000 description 8
- 238000006193 diazotization reaction Methods 0.000 description 7
- 238000004821 distillation Methods 0.000 description 5
- 239000000428 dust Substances 0.000 description 5
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical class OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 4
- 230000009918 complex formation Effects 0.000 description 4
- -1 alkali metal salts Chemical class 0.000 description 3
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 2
- 229910019142 PO4 Inorganic materials 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-L Phosphate ion(2-) Chemical compound OP([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-L 0.000 description 2
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 2
- 239000012752 auxiliary agent Substances 0.000 description 2
- OSGAYBCDTDRGGQ-UHFFFAOYSA-L calcium sulfate Chemical compound [Ca+2].[O-]S([O-])(=O)=O OSGAYBCDTDRGGQ-UHFFFAOYSA-L 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 125000000896 monocarboxylic acid group Chemical group 0.000 description 2
- 239000010452 phosphate Substances 0.000 description 2
- 229910052938 sodium sulfate Inorganic materials 0.000 description 2
- 235000011152 sodium sulphate Nutrition 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- 239000000758 substrate Substances 0.000 description 2
- 239000002351 wastewater Substances 0.000 description 2
- 238000005303 weighing Methods 0.000 description 2
- 229920003043 Cellulose fiber Polymers 0.000 description 1
- QXNVGIXVLWOKEQ-UHFFFAOYSA-N Disodium Chemical compound [Na][Na] QXNVGIXVLWOKEQ-UHFFFAOYSA-N 0.000 description 1
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 1
- 229910006069 SO3H Inorganic materials 0.000 description 1
- LEHOTFFKMJEONL-UHFFFAOYSA-N Uric Acid Chemical compound N1C(=O)NC(=O)C2=C1NC(=O)N2 LEHOTFFKMJEONL-UHFFFAOYSA-N 0.000 description 1
- TVWHNULVHGKJHS-UHFFFAOYSA-N Uric acid Natural products N1C(=O)NC(=O)C2NC(=O)NC21 TVWHNULVHGKJHS-UHFFFAOYSA-N 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 229910052783 alkali metal Inorganic materials 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 239000008366 buffered solution Substances 0.000 description 1
- 229910000019 calcium carbonate Inorganic materials 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000002844 continuous effect Effects 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 238000001599 direct drying Methods 0.000 description 1
- AFOSIXZFDONLBT-UHFFFAOYSA-N divinyl sulfone Chemical group C=CS(=O)(=O)C=C AFOSIXZFDONLBT-UHFFFAOYSA-N 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000032050 esterification Effects 0.000 description 1
- 238000005886 esterification reaction Methods 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 125000001145 hydrido group Chemical group *[H] 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 230000002427 irreversible effect Effects 0.000 description 1
- 239000012669 liquid formulation Substances 0.000 description 1
- 239000002480 mineral oil Substances 0.000 description 1
- 235000010446 mineral oil Nutrition 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 229940039748 oxalate Drugs 0.000 description 1
- 239000000985 reactive dye Substances 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- IOVGROKTTNBUGK-SJCJKPOMSA-N ritodrine Chemical compound N([C@@H](C)[C@H](O)C=1C=CC(O)=CC=1)CCC1=CC=C(O)C=C1 IOVGROKTTNBUGK-SJCJKPOMSA-N 0.000 description 1
- 235000015424 sodium Nutrition 0.000 description 1
- 159000000000 sodium salts Chemical class 0.000 description 1
- RBWSWDPRDBEWCR-RKJRWTFHSA-N sodium;(2r)-2-[(2r)-3,4-dihydroxy-5-oxo-2h-furan-2-yl]-2-hydroxyethanolate Chemical compound [Na+].[O-]C[C@@H](O)[C@H]1OC(=O)C(O)=C1O RBWSWDPRDBEWCR-RKJRWTFHSA-N 0.000 description 1
- 125000000020 sulfo group Chemical group O=S(=O)([*])O[H] 0.000 description 1
- 239000002562 thickening agent Substances 0.000 description 1
- 229940116269 uric acid Drugs 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B62/00—Reactive dyes, i.e. dyes which form covalent bonds with the substrates or which polymerise with themselves
- C09B62/44—Reactive dyes, i.e. dyes which form covalent bonds with the substrates or which polymerise with themselves with the reactive group not directly attached to a heterocyclic ring
- C09B62/503—Reactive dyes, i.e. dyes which form covalent bonds with the substrates or which polymerise with themselves with the reactive group not directly attached to a heterocyclic ring the reactive group being an esterified or non-esterified hydroxyalkyl sulfonyl or mercaptoalkyl sulfonyl group, a quaternised or non-quaternised aminoalkyl sulfonyl group, a heterylmercapto alkyl sulfonyl group, a vinyl sulfonyl or a substituted vinyl sulfonyl group, or a thiophene-dioxide group
- C09B62/507—Azo dyes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0071—Process features in the making of dyestuff preparations; Dehydrating agents; Dispersing agents; Dustfree compositions
- C09B67/0072—Preparations with anionic dyes or reactive dyes
- C09B67/0073—Preparations of acid or reactive dyes in liquid form
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/02—Material containing basic nitrogen
- D06P3/04—Material containing basic nitrogen containing amide groups
- D06P3/10—Material containing basic nitrogen containing amide groups using reactive dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/58—Material containing hydroxyl groups
- D06P3/60—Natural or regenerated cellulose
- D06P3/66—Natural or regenerated cellulose using reactive dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/82—Textiles which contain different kinds of fibres
- D06P3/8204—Textiles which contain different kinds of fibres fibres of different chemical nature
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Coloring (AREA)
Applications Claiming Priority (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19742417256 DE2417256C3 (de) | 1974-04-09 | Flüssige Farbstoffzubereitungen eines Reaktivfarbstoffes | |
| DE19742417254 DE2417254C3 (de) | 1974-04-09 | Flüssige Farbstoffzubereitungen eines Reaktivfarbstoffes | |
| DE19742417253 DE2417253C2 (de) | 1974-04-09 | Flüssige Farbstoffzubereitungen eines Reaktivfarbstoffes | |
| DE19742454893 DE2454893C3 (de) | 1974-11-20 | 1974-11-20 | Flüssige, wäßrige Färbepräparationen eines Reaktivfarbstoffes und deren Verwendung |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA1070903A true CA1070903A (en) | 1980-02-05 |
Family
ID=27431841
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA224,031A Expired CA1070903A (en) | 1974-04-09 | 1975-04-08 | Liquid preparations of reactive dyestuffs |
Country Status (9)
| Country | Link |
|---|---|
| JP (2) | JPS50136316A (enrdf_load_stackoverflow) |
| AU (1) | AU499813B2 (enrdf_load_stackoverflow) |
| CA (1) | CA1070903A (enrdf_load_stackoverflow) |
| CH (1) | CH580149A5 (enrdf_load_stackoverflow) |
| CS (1) | CS187467B2 (enrdf_load_stackoverflow) |
| FR (1) | FR2267351B1 (enrdf_load_stackoverflow) |
| GB (1) | GB1506206A (enrdf_load_stackoverflow) |
| IN (1) | IN143735B (enrdf_load_stackoverflow) |
| IT (1) | IT1034904B (enrdf_load_stackoverflow) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS58142941A (ja) * | 1982-02-19 | 1983-08-25 | Sumitomo Chem Co Ltd | セルロ−ス繊維用反応染料組成物 |
| DE3424506A1 (de) * | 1984-07-04 | 1986-01-09 | Hoechst Ag, 6230 Frankfurt | Verfahren zur herstellung salzarmer, fluessiger, waessriger zubereitungen von faserreaktiven farbstoffen |
| JPH0745635B2 (ja) * | 1987-03-26 | 1995-05-17 | 住友化学工業株式会社 | 反応染料の液状水性組成物 |
-
1975
- 1975-04-02 IN IN670/CAL/75A patent/IN143735B/en unknown
- 1975-04-07 JP JP50041359A patent/JPS50136316A/ja active Pending
- 1975-04-07 IT IT22079/75A patent/IT1034904B/it active
- 1975-04-08 CH CH446575A patent/CH580149A5/xx not_active IP Right Cessation
- 1975-04-08 CA CA224,031A patent/CA1070903A/en not_active Expired
- 1975-04-08 AU AU79937/75A patent/AU499813B2/en not_active Expired
- 1975-04-09 FR FR7511025A patent/FR2267351B1/fr not_active Expired
- 1975-04-09 CS CS752434A patent/CS187467B2/cs unknown
- 1975-04-09 GB GB14521/75A patent/GB1506206A/en not_active Expired
-
1976
- 1976-03-29 JP JP51033691A patent/JPS51119035A/ja active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| FR2267351A1 (enrdf_load_stackoverflow) | 1975-11-07 |
| IN143735B (enrdf_load_stackoverflow) | 1978-01-21 |
| GB1506206A (en) | 1978-04-05 |
| FR2267351B1 (enrdf_load_stackoverflow) | 1978-11-03 |
| IT1034904B (it) | 1979-10-10 |
| JPS51119035A (en) | 1976-10-19 |
| AU7993775A (en) | 1976-10-14 |
| JPS50136316A (enrdf_load_stackoverflow) | 1975-10-29 |
| CH580149A5 (enrdf_load_stackoverflow) | 1976-09-30 |
| AU499813B2 (en) | 1979-05-03 |
| CS187467B2 (en) | 1979-01-31 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MKEX | Expiry |