CA1056645A - Method of obtaining a smoking agent - Google Patents
Method of obtaining a smoking agentInfo
- Publication number
- CA1056645A CA1056645A CA220,598A CA220598A CA1056645A CA 1056645 A CA1056645 A CA 1056645A CA 220598 A CA220598 A CA 220598A CA 1056645 A CA1056645 A CA 1056645A
- Authority
- CA
- Canada
- Prior art keywords
- distillation
- smoke
- fraction
- acid
- tar
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000000034 method Methods 0.000 title claims abstract description 54
- 230000000391 smoking effect Effects 0.000 title claims description 33
- 238000004821 distillation Methods 0.000 claims abstract description 43
- 239000000779 smoke Substances 0.000 claims abstract description 39
- 235000013305 food Nutrition 0.000 claims abstract description 36
- 230000008569 process Effects 0.000 claims abstract description 36
- 239000002253 acid Substances 0.000 claims abstract description 28
- 238000009835 boiling Methods 0.000 claims abstract description 27
- 150000001875 compounds Chemical class 0.000 claims abstract description 21
- 239000000654 additive Substances 0.000 claims abstract description 14
- 230000000996 additive effect Effects 0.000 claims abstract description 13
- 229910052500 inorganic mineral Inorganic materials 0.000 claims abstract description 12
- 239000011707 mineral Substances 0.000 claims abstract description 12
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 11
- 150000005846 sugar alcohols Polymers 0.000 claims abstract description 11
- 239000007864 aqueous solution Substances 0.000 claims abstract description 8
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000004411 aluminium Substances 0.000 claims abstract description 7
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229910052782 aluminium Inorganic materials 0.000 claims abstract description 7
- 239000000463 material Substances 0.000 claims abstract description 7
- 229920005610 lignin Polymers 0.000 claims abstract description 6
- 239000001913 cellulose Substances 0.000 claims abstract description 5
- 229920002678 cellulose Polymers 0.000 claims abstract description 5
- 238000006243 chemical reaction Methods 0.000 claims abstract description 5
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims abstract description 4
- 238000010438 heat treatment Methods 0.000 claims abstract description 3
- 239000003795 chemical substances by application Substances 0.000 claims description 49
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 33
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 18
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims description 14
- 238000000605 extraction Methods 0.000 claims description 14
- 239000000428 dust Substances 0.000 claims description 12
- 230000001747 exhibiting effect Effects 0.000 claims description 11
- 235000010755 mineral Nutrition 0.000 claims description 11
- 235000011007 phosphoric acid Nutrition 0.000 claims description 9
- 239000002994 raw material Substances 0.000 claims description 9
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 7
- -1 aliphatic alcohols Chemical class 0.000 claims description 7
- 229930195733 hydrocarbon Natural products 0.000 claims description 7
- 239000000243 solution Substances 0.000 claims description 7
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims description 6
- 239000012298 atmosphere Substances 0.000 claims description 6
- 150000002989 phenols Chemical class 0.000 claims description 5
- 238000000197 pyrolysis Methods 0.000 claims description 5
- 238000001179 sorption measurement Methods 0.000 claims description 5
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims description 4
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 4
- 239000001569 carbon dioxide Substances 0.000 claims description 4
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 4
- 239000003960 organic solvent Substances 0.000 claims description 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 3
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical class [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 3
- 238000010521 absorption reaction Methods 0.000 claims description 3
- 229910052799 carbon Inorganic materials 0.000 claims description 3
- 150000001735 carboxylic acids Chemical class 0.000 claims description 3
- 150000001983 dialkylethers Chemical class 0.000 claims description 3
- 229910052736 halogen Inorganic materials 0.000 claims description 3
- 238000006386 neutralization reaction Methods 0.000 claims description 3
- 235000017557 sodium bicarbonate Nutrition 0.000 claims description 3
- 229910000030 sodium bicarbonate Inorganic materials 0.000 claims description 3
- 239000002594 sorbent Substances 0.000 claims description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 2
- 150000001338 aliphatic hydrocarbons Chemical class 0.000 claims description 2
- 229910052786 argon Inorganic materials 0.000 claims description 2
- 238000009833 condensation Methods 0.000 claims description 2
- 239000011261 inert gas Substances 0.000 claims description 2
- 229910052757 nitrogen Inorganic materials 0.000 claims description 2
- 239000000741 silica gel Substances 0.000 claims description 2
- 229910002027 silica gel Inorganic materials 0.000 claims description 2
- 235000015112 vegetable and seed oil Nutrition 0.000 claims description 2
- 239000008158 vegetable oil Substances 0.000 claims description 2
- 238000005406 washing Methods 0.000 claims description 2
- 230000005494 condensation Effects 0.000 claims 1
- 229920002545 silicone oil Polymers 0.000 claims 1
- 239000011701 zinc Substances 0.000 abstract description 4
- 229910052725 zinc Inorganic materials 0.000 abstract description 4
- 229920001213 Polysorbate 20 Polymers 0.000 abstract 1
- 239000000256 polyoxyethylene sorbitan monolaurate Substances 0.000 abstract 1
- 239000000047 product Substances 0.000 description 15
- 239000000126 substance Substances 0.000 description 9
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 8
- 239000003921 oil Substances 0.000 description 8
- 235000019198 oils Nutrition 0.000 description 8
- 239000002699 waste material Substances 0.000 description 8
- 230000000711 cancerogenic effect Effects 0.000 description 6
- 231100000315 carcinogenic Toxicity 0.000 description 6
- 239000000203 mixture Substances 0.000 description 6
- 239000012141 concentrate Substances 0.000 description 5
- 235000008504 concentrate Nutrition 0.000 description 5
- 230000003647 oxidation Effects 0.000 description 5
- 238000007254 oxidation reaction Methods 0.000 description 5
- 239000001117 sulphuric acid Substances 0.000 description 5
- 235000011149 sulphuric acid Nutrition 0.000 description 5
- 239000002023 wood Substances 0.000 description 5
- 101000937129 Drosophila melanogaster Cadherin-related tumor suppressor Proteins 0.000 description 4
- 238000001704 evaporation Methods 0.000 description 4
- 230000008020 evaporation Effects 0.000 description 4
- 150000002430 hydrocarbons Chemical class 0.000 description 4
- 239000002904 solvent Substances 0.000 description 4
- 239000003963 antioxidant agent Substances 0.000 description 3
- 230000003078 antioxidant effect Effects 0.000 description 3
- 235000014113 dietary fatty acids Nutrition 0.000 description 3
- 239000000194 fatty acid Substances 0.000 description 3
- 229930195729 fatty acid Natural products 0.000 description 3
- 150000004665 fatty acids Chemical class 0.000 description 3
- 230000001473 noxious effect Effects 0.000 description 3
- 238000000926 separation method Methods 0.000 description 3
- QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 description 2
- 230000000844 anti-bacterial effect Effects 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 230000027455 binding Effects 0.000 description 2
- 238000009739 binding Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000000839 emulsion Substances 0.000 description 2
- 238000000895 extractive distillation Methods 0.000 description 2
- 239000000706 filtrate Substances 0.000 description 2
- 239000011521 glass Substances 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 239000012299 nitrogen atmosphere Substances 0.000 description 2
- 150000007530 organic bases Chemical class 0.000 description 2
- 238000007670 refining Methods 0.000 description 2
- 235000007586 terpenes Nutrition 0.000 description 2
- GHPYJLCQYMAXGG-WCCKRBBISA-N (2R)-2-amino-3-(2-boronoethylsulfanyl)propanoic acid hydrochloride Chemical compound Cl.N[C@@H](CSCCB(O)O)C(O)=O GHPYJLCQYMAXGG-WCCKRBBISA-N 0.000 description 1
- 101100004286 Caenorhabditis elegans best-5 gene Proteins 0.000 description 1
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 1
- 239000005977 Ethylene Substances 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 239000003463 adsorbent Substances 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 229910000323 aluminium silicate Inorganic materials 0.000 description 1
- AVKUERGKIZMTKX-NJBDSQKTSA-N ampicillin Chemical compound C1([C@@H](N)C(=O)N[C@H]2[C@H]3SC([C@@H](N3C2=O)C(O)=O)(C)C)=CC=CC=C1 AVKUERGKIZMTKX-NJBDSQKTSA-N 0.000 description 1
- 230000003064 anti-oxidating effect Effects 0.000 description 1
- 239000012223 aqueous fraction Substances 0.000 description 1
- 150000004945 aromatic hydrocarbons Chemical class 0.000 description 1
- 230000003385 bacteriostatic effect Effects 0.000 description 1
- 239000000969 carrier Substances 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 238000011437 continuous method Methods 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 230000032798 delamination Effects 0.000 description 1
- 230000001066 destructive effect Effects 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 1
- 230000005686 electrostatic field Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 239000000727 fraction Substances 0.000 description 1
- 238000004508 fractional distillation Methods 0.000 description 1
- 238000005194 fractionation Methods 0.000 description 1
- 239000011121 hardwood Substances 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 229910052753 mercury Inorganic materials 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 235000005985 organic acids Nutrition 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- 238000005554 pickling Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 238000009738 saturating Methods 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 238000009936 smoking Methods 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 150000003505 terpenes Chemical class 0.000 description 1
- 235000019871 vegetable fat Nutrition 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/20—Synthetic spices, flavouring agents or condiments
- A23L27/27—Smoke flavours
Landscapes
- Polymers & Plastics (AREA)
- Nutrition Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Health & Medical Sciences (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Compounds Of Unknown Constitution (AREA)
- Seasonings (AREA)
- General Preparation And Processing Of Foods (AREA)
- Meat, Egg Or Seafood Products (AREA)
- Indole Compounds (AREA)
- Medicines Containing Plant Substances (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PL1974169004A PL96145B3 (pl) | 1974-02-22 | 1974-02-22 | Sposob wytwarzania srodka aromatyzujacego i/lub antyseptycznego i/lub przeciwdzialajacego utlenianiu |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA1056645A true CA1056645A (en) | 1979-06-19 |
Family
ID=19966186
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA220,598A Expired CA1056645A (en) | 1974-02-22 | 1975-02-21 | Method of obtaining a smoking agent |
Country Status (15)
| Country | Link |
|---|---|
| JP (1) | JPS517159A (en, 2012) |
| AR (1) | AR209293A1 (en, 2012) |
| CA (1) | CA1056645A (en, 2012) |
| CH (1) | CH614845A5 (en, 2012) |
| DE (1) | DE2507385C3 (en, 2012) |
| DK (1) | DK68575A (en, 2012) |
| FI (1) | FI57689C (en, 2012) |
| FR (1) | FR2262100B1 (en, 2012) |
| GB (1) | GB1504406A (en, 2012) |
| IE (1) | IE40680B1 (en, 2012) |
| NL (1) | NL7502109A (en, 2012) |
| NO (1) | NO140365C (en, 2012) |
| PL (1) | PL96145B3 (en, 2012) |
| SE (1) | SE405929B (en, 2012) |
| SU (1) | SU575008A3 (en, 2012) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111165869A (zh) * | 2020-01-17 | 2020-05-19 | 湖南中烟工业有限责任公司 | 一种经低危害增烟处理的卷烟 |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4154866A (en) * | 1976-08-24 | 1979-05-15 | Stange Co. | Method of producing from wood tar a liquid smoke product for use in food processing, and product of said method |
| US4594251A (en) * | 1983-04-08 | 1986-06-10 | Union Carbide Corporation | Preparation of tar-depleted liquid smoke treated casings |
| WO2005117612A1 (en) * | 2004-06-04 | 2005-12-15 | Kim Plaschke | Preparation of smoke extract |
-
1974
- 1974-02-22 PL PL1974169004A patent/PL96145B3/xx unknown
-
1975
- 1975-02-17 FI FI750433A patent/FI57689C/fi not_active IP Right Cessation
- 1975-02-18 NO NO750544A patent/NO140365C/no unknown
- 1975-02-20 DE DE2507385A patent/DE2507385C3/de not_active Expired
- 1975-02-20 SE SE7501926A patent/SE405929B/xx unknown
- 1975-02-21 GB GB7434/75A patent/GB1504406A/en not_active Expired
- 1975-02-21 NL NL7502109A patent/NL7502109A/xx not_active Application Discontinuation
- 1975-02-21 JP JP50021789A patent/JPS517159A/ja active Pending
- 1975-02-21 DK DK68575*#A patent/DK68575A/da not_active Application Discontinuation
- 1975-02-21 IE IE361/75A patent/IE40680B1/xx unknown
- 1975-02-21 CA CA220,598A patent/CA1056645A/en not_active Expired
- 1975-02-21 SU SU7502110025A patent/SU575008A3/ru active
- 1975-02-21 CH CH217075A patent/CH614845A5/xx not_active IP Right Cessation
- 1975-02-24 AR AR257729A patent/AR209293A1/es active
- 1975-02-24 FR FR7505669A patent/FR2262100B1/fr not_active Expired
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111165869A (zh) * | 2020-01-17 | 2020-05-19 | 湖南中烟工业有限责任公司 | 一种经低危害增烟处理的卷烟 |
Also Published As
| Publication number | Publication date |
|---|---|
| SE405929B (sv) | 1979-01-15 |
| FI750433A7 (en, 2012) | 1975-08-23 |
| SE7501926L (en, 2012) | 1975-08-25 |
| AU7848275A (en) | 1976-08-26 |
| IE40680B1 (en) | 1979-08-01 |
| JPS517159A (en) | 1976-01-21 |
| NO750544L (en, 2012) | 1975-08-25 |
| DE2507385B2 (de) | 1979-10-25 |
| FR2262100A1 (en, 2012) | 1975-09-19 |
| NO140365B (no) | 1979-05-14 |
| NL7502109A (nl) | 1975-08-26 |
| FI57689C (fi) | 1980-10-10 |
| FI57689B (fi) | 1980-06-30 |
| CH614845A5 (en) | 1979-12-28 |
| DE2507385A1 (de) | 1975-08-28 |
| AR209293A1 (es) | 1977-04-15 |
| NO140365C (no) | 1979-08-22 |
| GB1504406A (en) | 1978-03-22 |
| FR2262100B1 (en, 2012) | 1978-10-27 |
| DE2507385C3 (de) | 1980-07-03 |
| DK68575A (en, 2012) | 1975-10-27 |
| IE40680L (en) | 1975-08-22 |
| PL96145B3 (pl) | 1977-12-31 |
| SU575008A3 (ru) | 1977-09-30 |
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