CA1042179A - Production of zirconium carbonate - Google Patents
Production of zirconium carbonateInfo
- Publication number
- CA1042179A CA1042179A CA222,315A CA222315A CA1042179A CA 1042179 A CA1042179 A CA 1042179A CA 222315 A CA222315 A CA 222315A CA 1042179 A CA1042179 A CA 1042179A
- Authority
- CA
- Canada
- Prior art keywords
- carbonate
- zirconium
- solution
- basic
- salt
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- XJUNLJFOHNHSAR-UHFFFAOYSA-J zirconium(4+);dicarbonate Chemical compound [Zr+4].[O-]C([O-])=O.[O-]C([O-])=O XJUNLJFOHNHSAR-UHFFFAOYSA-J 0.000 title claims abstract description 41
- 238000004519 manufacturing process Methods 0.000 title abstract description 10
- 239000000243 solution Substances 0.000 claims abstract description 50
- 238000000034 method Methods 0.000 claims abstract description 29
- 230000008569 process Effects 0.000 claims abstract description 24
- 150000003754 zirconium Chemical class 0.000 claims abstract description 18
- 238000006243 chemical reaction Methods 0.000 claims abstract description 16
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims abstract description 15
- 239000007864 aqueous solution Substances 0.000 claims abstract description 11
- 239000001099 ammonium carbonate Substances 0.000 claims abstract description 10
- ZXAUZSQITFJWPS-UHFFFAOYSA-J zirconium(4+);disulfate Chemical compound [Zr+4].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O ZXAUZSQITFJWPS-UHFFFAOYSA-J 0.000 claims abstract description 8
- ATRRKUHOCOJYRX-UHFFFAOYSA-N Ammonium bicarbonate Chemical compound [NH4+].OC([O-])=O ATRRKUHOCOJYRX-UHFFFAOYSA-N 0.000 claims abstract description 7
- 235000012501 ammonium carbonate Nutrition 0.000 claims abstract description 7
- 229910052783 alkali metal Inorganic materials 0.000 claims abstract description 6
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 claims description 34
- 239000002244 precipitate Substances 0.000 claims description 13
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical group [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 12
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 6
- RDFNWUYMULDLCS-UHFFFAOYSA-L hydron;oxozirconium(2+);disulfate Chemical compound [H+].[H+].[Zr+2]=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O RDFNWUYMULDLCS-UHFFFAOYSA-L 0.000 claims description 5
- 238000003756 stirring Methods 0.000 claims description 5
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims description 4
- 239000012467 final product Substances 0.000 claims description 4
- 229910000288 alkali metal carbonate Inorganic materials 0.000 claims description 3
- 150000008041 alkali metal carbonates Chemical class 0.000 claims description 3
- 238000005406 washing Methods 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 2
- 239000011541 reaction mixture Substances 0.000 claims 5
- -1 alkali metal bicarbonate Chemical class 0.000 claims 2
- 239000012266 salt solution Substances 0.000 claims 2
- 229910021653 sulphate ion Inorganic materials 0.000 claims 2
- 238000001556 precipitation Methods 0.000 claims 1
- DUNKXUFBGCUVQW-UHFFFAOYSA-J zirconium tetrachloride Chemical group Cl[Zr](Cl)(Cl)Cl DUNKXUFBGCUVQW-UHFFFAOYSA-J 0.000 claims 1
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 abstract description 16
- 229910052726 zirconium Inorganic materials 0.000 abstract description 11
- BVKZGUZCCUSVTD-UHFFFAOYSA-M Bicarbonate Chemical compound OC([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-M 0.000 abstract description 7
- 239000002253 acid Substances 0.000 abstract description 6
- 230000015572 biosynthetic process Effects 0.000 abstract description 5
- 150000001340 alkali metals Chemical class 0.000 abstract description 4
- 150000007524 organic acids Chemical class 0.000 abstract description 4
- 235000012538 ammonium bicarbonate Nutrition 0.000 abstract description 3
- 239000000126 substance Substances 0.000 abstract description 3
- 235000005985 organic acids Nutrition 0.000 abstract description 2
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 17
- 239000000047 product Substances 0.000 description 12
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 10
- 239000003153 chemical reaction reagent Substances 0.000 description 10
- 239000000543 intermediate Substances 0.000 description 10
- 229910002092 carbon dioxide Inorganic materials 0.000 description 6
- 239000000463 material Substances 0.000 description 6
- IPCAPQRVQMIMAN-UHFFFAOYSA-L zirconyl chloride Chemical compound Cl[Zr](Cl)=O IPCAPQRVQMIMAN-UHFFFAOYSA-L 0.000 description 5
- 238000005755 formation reaction Methods 0.000 description 4
- 239000012535 impurity Substances 0.000 description 4
- 229940001593 sodium carbonate Drugs 0.000 description 4
- 235000017550 sodium carbonate Nutrition 0.000 description 4
- 230000001052 transient effect Effects 0.000 description 4
- 238000000354 decomposition reaction Methods 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- QRTRRDMHGTZPBF-UHFFFAOYSA-L oxygen(2-);zirconium(4+);sulfate Chemical compound [O-2].[Zr+4].[O-]S([O-])(=O)=O QRTRRDMHGTZPBF-UHFFFAOYSA-L 0.000 description 3
- 229910052708 sodium Inorganic materials 0.000 description 3
- 239000011734 sodium Substances 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 238000007605 air drying Methods 0.000 description 2
- 239000001569 carbon dioxide Substances 0.000 description 2
- 150000002500 ions Chemical class 0.000 description 2
- 229940023462 paste product Drugs 0.000 description 2
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 2
- 239000000376 reactant Substances 0.000 description 2
- 230000009257 reactivity Effects 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 238000001354 calcination Methods 0.000 description 1
- 150000004649 carbonic acid derivatives Chemical class 0.000 description 1
- 238000000975 co-precipitation Methods 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 230000002844 continuous effect Effects 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 238000006073 displacement reaction Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000012527 feed solution Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 1
- 238000011065 in-situ storage Methods 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012544 monitoring process Methods 0.000 description 1
- 125000004430 oxygen atom Chemical group O* 0.000 description 1
- 229910000027 potassium carbonate Inorganic materials 0.000 description 1
- 230000001376 precipitating effect Effects 0.000 description 1
- 239000004576 sand Substances 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 229910052938 sodium sulfate Inorganic materials 0.000 description 1
- 235000011152 sodium sulphate Nutrition 0.000 description 1
- 239000011877 solvent mixture Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 229910052845 zircon Inorganic materials 0.000 description 1
- GFQYVLUOOAAOGM-UHFFFAOYSA-N zirconium(iv) silicate Chemical group [Zr+4].[O-][Si]([O-])([O-])[O-] GFQYVLUOOAAOGM-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G25/00—Compounds of zirconium
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB11840/74A GB1495267A (en) | 1974-03-18 | 1974-03-18 | Process for the production of basic zirconium carbonate |
Publications (1)
Publication Number | Publication Date |
---|---|
CA1042179A true CA1042179A (en) | 1978-11-14 |
Family
ID=9993663
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CA222,315A Expired CA1042179A (en) | 1974-03-18 | 1975-03-17 | Production of zirconium carbonate |
Country Status (6)
Country | Link |
---|---|
JP (1) | JPS50127897A (enrdf_load_stackoverflow) |
CA (1) | CA1042179A (enrdf_load_stackoverflow) |
DE (1) | DE2510743A1 (enrdf_load_stackoverflow) |
FR (1) | FR2264780B1 (enrdf_load_stackoverflow) |
GB (1) | GB1495267A (enrdf_load_stackoverflow) |
ZA (1) | ZA751656B (enrdf_load_stackoverflow) |
Families Citing this family (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4256718A (en) * | 1978-03-20 | 1981-03-17 | Organon Teknika Corporation | Sodium zirconium carbonate compound and the method of its preparation |
JPS54155199A (en) * | 1978-03-20 | 1979-12-06 | Organon Teknika Bv | Sodium zirconium carbonate compound and its manufacture |
US4360507A (en) * | 1979-01-24 | 1982-11-23 | Organon Teknika Corporation | Sodium zirconium carbonate compound and the method of its preparation |
DE3143921C2 (de) * | 1981-11-05 | 1984-06-28 | Dynamit Nobel Ag, 5210 Troisdorf | Verfahren zur Herstellung von basischem Zirkoniumkarbonat |
NZ215774A (en) * | 1985-05-02 | 1988-08-30 | Ici Australia Ltd | Purification of zirconium compounds |
KR880701275A (ko) * | 1986-06-17 | 1988-07-26 | 알프레드 펄내트 | 가수분해된 지르코늄 함유물질과 산화지르코늄 및 그들의 제조방법 |
US6627164B1 (en) * | 2000-11-28 | 2003-09-30 | Renal Solutions, Inc. | Sodium zirconium carbonate and zirconium basic carbonate and methods of making the same |
CN115340126B (zh) * | 2022-09-15 | 2024-04-12 | 包头稀土研究院 | 稀土锆酸盐颗粒及其制备方法 |
-
1974
- 1974-03-18 GB GB11840/74A patent/GB1495267A/en not_active Expired
-
1975
- 1975-03-12 DE DE19752510743 patent/DE2510743A1/de not_active Withdrawn
- 1975-03-17 FR FR7508229A patent/FR2264780B1/fr not_active Expired
- 1975-03-17 CA CA222,315A patent/CA1042179A/en not_active Expired
- 1975-03-18 ZA ZA00751656A patent/ZA751656B/xx unknown
- 1975-03-18 JP JP50031916A patent/JPS50127897A/ja active Pending
Also Published As
Publication number | Publication date |
---|---|
FR2264780B1 (enrdf_load_stackoverflow) | 1981-01-16 |
GB1495267A (en) | 1977-12-14 |
ZA751656B (en) | 1976-03-31 |
DE2510743A1 (de) | 1975-09-25 |
JPS50127897A (enrdf_load_stackoverflow) | 1975-10-08 |
FR2264780A1 (enrdf_load_stackoverflow) | 1975-10-17 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
US11710857B2 (en) | Recycling of cobalt and nickel from lithium-ion batteries | |
CN107058731B (zh) | 一种以铂钯精矿为原料生产铂钯产品的工艺 | |
CN113184928B (zh) | 硫酸镍溶液的制备方法 | |
CA1042179A (en) | Production of zirconium carbonate | |
CN106068242A (zh) | 活化u3o8以使其转化为水合uo4的方法 | |
US4336236A (en) | Double precipitation reaction for the formation of high purity basic lead carbonate and high purity normal lead carbonate | |
US4119696A (en) | Production of titanium metal values | |
CN108842073A (zh) | 一种碱法处理锌镉渣的方法 | |
CN108128804B (zh) | 纯度高活性好储存稳定的工业碳酸锆及其制备方法 | |
CN109868366A (zh) | 一种滤液循环的湿法回收废铅膏制备高纯红丹的方法 | |
CN106282607B (zh) | 一种利用v5+萃取富集含钒溶液的方法 | |
CN1075171A (zh) | 氢氧化铈的生产方法 | |
US3510259A (en) | Simultaneous leaching of zinc and manganese ores | |
US2144299A (en) | Method of making zinc carbonate and zinc oxide | |
CN107324375A (zh) | 一种碱式氯化锌的制备方法 | |
GB1531561A (en) | Iron oxide pigment and process for preparing such a pigment | |
CN1028769C (zh) | 一种氧化铈的生产方法 | |
US3148051A (en) | Process for the production of metallic copper powder and ammonium sulfate from copper sulfate solutions | |
US3132920A (en) | Process for recovery of vanadium values from aqueous liquors | |
JPS60137823A (ja) | 硫化物の少ない沈降性硫酸バリウムの製造方法 | |
US3106451A (en) | Method of producing manganese sulfate | |
GB2185248A (en) | Recovery of titanium dioxide from ilmenite-type ores | |
US2940823A (en) | Production of potassium manganates | |
JPH0118017B2 (enrdf_load_stackoverflow) | ||
Warren et al. | The recovery of molybdenum from leach solutions by reduction |