BRPI0715390B1 - auxiliar de clarificação de cerveja com base em sílica xerogel com alta capacidade de filtragem - Google Patents

auxiliar de clarificação de cerveja com base em sílica xerogel com alta capacidade de filtragem Download PDF

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Publication number
BRPI0715390B1
BRPI0715390B1 BRPI0715390A BRPI0715390A BRPI0715390B1 BR PI0715390 B1 BRPI0715390 B1 BR PI0715390B1 BR PI0715390 A BRPI0715390 A BR PI0715390A BR PI0715390 A BRPI0715390 A BR PI0715390A BR PI0715390 B1 BRPI0715390 B1 BR PI0715390B1
Authority
BR
Brazil
Prior art keywords
composition
xerogel
weight
fines
less
Prior art date
Application number
BRPI0715390A
Other languages
English (en)
Portuguese (pt)
Inventor
Andreas Seewald
Dominik Sedlmayer
Georg Lüers
Massoud Jalalpoor
Original Assignee
Grace Gmbh & Co Kg
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Grace Gmbh & Co Kg filed Critical Grace Gmbh & Co Kg
Publication of BRPI0715390A2 publication Critical patent/BRPI0715390A2/pt
Publication of BRPI0715390B1 publication Critical patent/BRPI0715390B1/pt

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Classifications

    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12HPASTEURISATION, STERILISATION, PRESERVATION, PURIFICATION, CLARIFICATION OR AGEING OF ALCOHOLIC BEVERAGES; METHODS FOR ALTERING THE ALCOHOL CONTENT OF FERMENTED SOLUTIONS OR ALCOHOLIC BEVERAGES
    • C12H1/00Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages
    • C12H1/02Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages combined with removal of precipitate or added materials, e.g. adsorption material
    • C12H1/04Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages combined with removal of precipitate or added materials, e.g. adsorption material with the aid of ion-exchange material or inert clarification material, e.g. adsorption material
    • C12H1/0408Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages combined with removal of precipitate or added materials, e.g. adsorption material with the aid of ion-exchange material or inert clarification material, e.g. adsorption material with the aid of inorganic added material
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/10Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
    • B01J20/103Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate comprising silica
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28002Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their physical properties
    • B01J20/28004Sorbent size or size distribution, e.g. particle size
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28014Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
    • B01J20/28016Particle form
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28014Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
    • B01J20/28047Gels
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28054Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J20/28057Surface area, e.g. B.E.T specific surface area
    • B01J20/28061Surface area, e.g. B.E.T specific surface area being in the range 100-500 m2/g
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28054Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J20/28069Pore volume, e.g. total pore volume, mesopore volume, micropore volume
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12HPASTEURISATION, STERILISATION, PRESERVATION, PURIFICATION, CLARIFICATION OR AGEING OF ALCOHOLIC BEVERAGES; METHODS FOR ALTERING THE ALCOHOL CONTENT OF FERMENTED SOLUTIONS OR ALCOHOLIC BEVERAGES
    • C12H1/00Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages
    • C12H1/02Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages combined with removal of precipitate or added materials, e.g. adsorption material
    • C12H1/06Precipitation by physical means, e.g. by irradiation, vibrations
    • C12H1/063Separation by filtration

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • Zoology (AREA)
  • General Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Food Science & Technology (AREA)
  • Inorganic Chemistry (AREA)
  • Biochemistry (AREA)
  • Toxicology (AREA)
  • Dispersion Chemistry (AREA)
  • Silicon Compounds (AREA)
  • Distillation Of Fermentation Liquor, Processing Of Alcohols, Vinegar And Beer (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Silicon Polymers (AREA)
BRPI0715390A 2006-08-07 2007-07-27 auxiliar de clarificação de cerveja com base em sílica xerogel com alta capacidade de filtragem BRPI0715390B1 (pt)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US83609106P 2006-08-07 2006-08-07
US60/836.091 2006-08-07
PCT/EP2007/006687 WO2008017393A1 (en) 2006-08-07 2007-07-27 Beer clarification aid based on silica xerogel with high filterability

Publications (2)

Publication Number Publication Date
BRPI0715390A2 BRPI0715390A2 (pt) 2013-06-25
BRPI0715390B1 true BRPI0715390B1 (pt) 2016-03-22

Family

ID=38508779

Family Applications (1)

Application Number Title Priority Date Filing Date
BRPI0715390A BRPI0715390B1 (pt) 2006-08-07 2007-07-27 auxiliar de clarificação de cerveja com base em sílica xerogel com alta capacidade de filtragem

Country Status (19)

Country Link
US (1) US10633621B2 (enExample)
EP (1) EP2049645B1 (enExample)
JP (1) JP2010500010A (enExample)
CN (2) CN101541942A (enExample)
AR (1) AR062237A1 (enExample)
AU (1) AU2007283125A1 (enExample)
BR (1) BRPI0715390B1 (enExample)
CL (1) CL2007002291A1 (enExample)
DK (1) DK2049645T3 (enExample)
ES (1) ES2573227T3 (enExample)
HK (1) HK1222671A1 (enExample)
HU (1) HUE029242T2 (enExample)
MX (1) MX2009001405A (enExample)
PL (1) PL2049645T3 (enExample)
PT (1) PT2049645T (enExample)
RU (1) RU2009108297A (enExample)
SI (1) SI2049645T1 (enExample)
TW (1) TW200817504A (enExample)
WO (1) WO2008017393A1 (enExample)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5443058B2 (ja) * 2008-06-11 2014-03-19 富士シリシア化学株式会社 ビール安定化処理用シリカゲル、およびビール安定化処理方法
US8409647B2 (en) * 2008-08-12 2013-04-02 E. I. Du Pont De Nemours And Company Silica microgels for reducing chill haze
DE102008060446A1 (de) * 2008-12-04 2010-06-10 Krones Ag Verfahren zum Ermitteln der Filtrierbarkeit von Bier
CA3138781A1 (en) * 2018-08-01 2020-02-06 Yanee WUTTHINITIKORNKIT Process of improving the flavour and aroma of liquor
JP2020110090A (ja) * 2019-01-11 2020-07-27 アサヒビール株式会社 発酵麦芽飲料の製造方法及び発酵液の濾過方法
CN112047352B (zh) * 2019-07-08 2021-11-30 福建远翔新材料股份有限公司 一种高吸附效率啤酒防混浊剂用二氧化硅的生产方法
GB202305914D0 (en) * 2023-04-21 2023-06-07 Pq Silicas Uk Ltd Clarifying agents

Family Cites Families (26)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CH407925A (de) 1960-10-29 1966-02-28 Brauereiindustrie Ag F Verfahren zur Erhöhung der Eiweissstabilität von Bier
GB981715A (en) 1962-04-05 1965-01-27 Fur Brauereiindustrie Glarus A A method for the reduction of haze in beer
US3163538A (en) 1962-04-05 1964-12-29 Fur Brauereiindustrie Ag Method for increasing the albumen stability of beer
GB1215928A (en) 1967-04-28 1970-12-16 Unilever Ltd A process for reducing haze in beer
US4053565A (en) * 1968-08-06 1977-10-11 National Petro Chemicals Corporation Silica xerogels
GB1279250A (en) 1968-10-28 1972-06-28 Unilever Ltd Improvements in or relating to a method for the reduction of haze in beer
PH18548A (en) * 1982-09-08 1985-08-09 Unilever Nv Calcined silicas and their use in beer clarification
US4636394A (en) * 1984-04-16 1987-01-13 J. E. Siebel Sons' Company, Inc. Method and compositions for chillproofing beverages
SU1212942A1 (ru) 1984-06-11 1986-02-23 Институт общей и неорганической химии АН АрмССР Способ получени силикагел
GB8431290D0 (en) * 1984-12-12 1985-01-23 Whitbread & Co Plc Coagulable material removal from extracts of malted barley
GB8707526D0 (en) * 1987-03-30 1987-05-07 Unilever Plc Amorphous silicas
US5232724A (en) * 1988-12-22 1993-08-03 Unilever Patent Holdings B.V. Method for stabilizing alcoholic beverages using an aqueous suspension containing amorphous silica
JPH0597421A (ja) * 1991-10-02 1993-04-20 Asahi Glass Co Ltd ビール安定化処理用シリカゲルの製造方法
JP3220198B2 (ja) 1991-12-19 2001-10-22 麒麟麦酒株式会社 濾過助剤
AU690657B2 (en) * 1994-05-18 1998-04-30 Mizusawa Industrial Chemicals, Ltd. Stabilizing agent for beer
JP3316325B2 (ja) 1994-12-20 2002-08-19 富士シリシア化学株式会社 ビール安定化処理用シリカゲル及びその製造方法並びにビールの安定化処理方法
JP3460357B2 (ja) 1995-01-19 2003-10-27 塩野義製薬株式会社 ビールの安定化処理用二酸化ケイ素及びその製造方法
DE19516253A1 (de) * 1995-04-26 1996-10-31 Grace Gmbh Mattierungsmittel auf Basis von aggregiertem Siliciumdioxid mit verbesserter Effizienz
JP3719686B2 (ja) * 1995-07-13 2005-11-24 東ソー・シリカ株式会社 濾過剤用シリカゲル
ES2255267T3 (es) 1998-05-15 2006-06-16 Isp Investments Inc. Composicion de premezcla para la clarificacion de cerveza.
RU2160777C1 (ru) 2000-02-16 2000-12-20 Открытое акционерное общество "Воскресенские минеральные удобрения" Способ осветления пива
US6464770B1 (en) * 2000-08-08 2002-10-15 Advanced Minerals Corporation Perlite products with controlled particle size distribution
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US7229655B2 (en) 2003-12-30 2007-06-12 Pq Corporation Composition of, and process for using, silica xerogel for beer stabilization
RU2264445C1 (ru) 2004-04-16 2005-11-20 Данелян Гагик Михайлович Способ производства пива специального

Also Published As

Publication number Publication date
BRPI0715390A2 (pt) 2013-06-25
CN105400676A (zh) 2016-03-16
DK2049645T3 (en) 2016-06-06
EP2049645B1 (en) 2016-04-06
CN101541942A (zh) 2009-09-23
PL2049645T3 (pl) 2016-09-30
CL2007002291A1 (es) 2008-05-02
EP2049645A1 (en) 2009-04-22
WO2008017393A1 (en) 2008-02-14
US20100112132A1 (en) 2010-05-06
RU2009108297A (ru) 2010-09-20
AR062237A1 (es) 2008-10-22
HK1222671A1 (zh) 2017-07-07
HUE029242T2 (en) 2017-02-28
TW200817504A (en) 2008-04-16
AU2007283125A1 (en) 2008-02-14
SI2049645T1 (sl) 2016-08-31
PT2049645T (pt) 2016-07-14
MX2009001405A (es) 2009-03-13
ES2573227T3 (es) 2016-06-06
JP2010500010A (ja) 2010-01-07
US10633621B2 (en) 2020-04-28

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Legal Events

Date Code Title Description
B07A Application suspended after technical examination (opinion) [chapter 7.1 patent gazette]
B09A Decision: intention to grant [chapter 9.1 patent gazette]
B16A Patent or certificate of addition of invention granted [chapter 16.1 patent gazette]

Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 27/07/2007, OBSERVADAS AS CONDICOES LEGAIS.

B25D Requested change of name of applicant approved