GB981715A - A method for the reduction of haze in beer - Google Patents

A method for the reduction of haze in beer

Info

Publication number
GB981715A
GB981715A GB1052963A GB1052963A GB981715A GB 981715 A GB981715 A GB 981715A GB 1052963 A GB1052963 A GB 1052963A GB 1052963 A GB1052963 A GB 1052963A GB 981715 A GB981715 A GB 981715A
Authority
GB
United Kingdom
Prior art keywords
silica gel
beer
haze
porous
acid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB1052963A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
fur BRAUEREIINDUSTRIE GLARUS A
Original Assignee
fur BRAUEREIINDUSTRIE GLARUS A
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from CH755362A external-priority patent/CH443191A/en
Application filed by fur BRAUEREIINDUSTRIE GLARUS A filed Critical fur BRAUEREIINDUSTRIE GLARUS A
Publication of GB981715A publication Critical patent/GB981715A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12HPASTEURISATION, STERILISATION, PRESERVATION, PURIFICATION, CLARIFICATION OR AGEING OF ALCOHOLIC BEVERAGES; METHODS FOR ALTERING THE ALCOHOL CONTENT OF FERMENTED SOLUTIONS OR ALCOHOLIC BEVERAGES
    • C12H1/00Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • Health & Medical Sciences (AREA)
  • General Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Food Science & Technology (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Distillation Of Fermentation Liquor, Processing Of Alcohols, Vinegar And Beer (AREA)

Abstract

A finely powdered ground silica gel being coarse-porous to medium-porous, having a surface area of 200 to 600 m.2/g., a pore volume of 0.5 to 1.5 ml./g. and a pore diameter of 40 to 180 <\>rA, the silica gel having been ground to such a degree that at least 75% (preferably at least 90%) by weight of the particles of the ground silica gel passing through a sieve of 44 microns mesh size (325 A.S.T.M. standard mesh) is used in the treatment of beer to reduce haze (see Division C6). In order to secure a desired pH, the silica gel may be subjected to treatment with acid, which acid is thereafter washed out with water, and the silica gel is then dried; pH values between 4.0 and 8.0 taken in a 5% suspension in distilled water, are preferred. The silica gel particles are stated to absorb in addition to the haze-forming compounds certain micro-organisms in the beer and the substances upon which the yeast and bacteria in the beer feed, provided the silica gel is used in sufficient amounts (more than approximately 50 g./ml. Specification 938,153 is referred to.ALSO:The reduction of haze in beer is accomplished by admixing with the beer a finely powdered ground silica gel being coarse-porous to medium-porous, having a surface area of 200-600 m.2/g., a pore volume of 0.5-1.5 ml./g. and a pore diameter of 40-180 <\>rA, at least 75% (preferably at least 90%) by weight of the particles of the ground silica gel passing through a sieve of 44 microns mesh size (325 A.S.T.M. standard mesh), and then filtering off the silica gel from the beer. A filter aid may additionally be used. In order to secure a desired pH, the silica gel may be subjected to treatment with acid, which acid is thereafter washed out with water, and the silica gel is then dried; pH values between 4.0 and 8.0 taken in a 5% suspension in distilled water, are preferred. The silica gel particles are stated to absorb in addition to the haze-forming compounds certain micro-organisms in the beer and the substances upon which the yeast and bacteria in the beer feed, provided the silica gel is used in sufficient amounts (more than approximately 50 g./ml.). Under preferred conditions of operation described, beer is brought to the desired final degree of attenuation in the fermentation vessel, volatile substances such as hydrogen sulphide and mercaptans are removed by washing the beer with carbon dioxide, and the non-volatile substances such as tannic compounds disturbing the flavour are removed and haze formation is reduced by treatment with sufficient of the silica gel. The washing with carbon dioxide may be effected either by fermenting under counter-pressure or carbonizing the beer after the main fermentation, and thereafter relieving the pressure. Tannin or enzymes may be added to the beer to precipitate a part of the higher molecular weight protein therein. Specification 938,153 is referred to.ALSO:Beer haze is reduced by admixing with the beer a finely powdered ground silica gel which is coarse-porous to medium-porous, having a surface area of 200-600 m.2/g., a pore volume of 0,5-1,5 ml./g. and a pore diameter of 40-180 , at least 75% (preferably at least 90%) by weight of the particles of the ground silica gel being capable of passing through a sieve of 44 microns mesh size (325 A.S.T.M. standard mesh), and then filtering off the silica gel from the beer. A filter aid may additionally be used. In order to secure a desired pH, the silica gel may be subjected to treatment with acid, which acid is thereafter washed out with water, and the silica gel is then dried; pH values between 4,0 and 8,0, taken in a 5% suspension in distilled water, are preferred. The silica gel particles are stated to absorb in addition to the haze-forming compounds certain micro-organisms in the beer and the substances upon which the yeast and bacteria in the beer feed, provided the silica gel is used in sufficient amounts (more than approximately 50 g./ml.). Under the preferred conditions of operation described, beer is brought to the desired final degree of attenuation in the fermentation vessel, volatile substances such as hydrogen sulphide and mercaptans are removed by washing the beer with carbon dioxide, and the non-volatile substances such as tannic compounds disturbing the flavour are removed, and haze formation is reduced by treatment with sufficient of the silica gel. The washing with carbon dioxide may be effected either by fermenting under counter-pressure or carbonizing the beer after the main fermentation, and thereafter relieving the pressure. Tannin or enzymes may be added to the beer to precipitate a part of the higher-molecular-weight protein therein. Specification 938,153 is referred to.
GB1052963A 1962-04-05 1963-03-18 A method for the reduction of haze in beer Expired GB981715A (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DEA0039883 1962-04-05
CH755362A CH443191A (en) 1961-10-19 1962-06-22 Process to increase the protein stability of beer using wide-pore silica gel as an adsorbent
DEA0041693 1962-11-23

Publications (1)

Publication Number Publication Date
GB981715A true GB981715A (en) 1965-01-27

Family

ID=27175824

Family Applications (1)

Application Number Title Priority Date Filing Date
GB1052963A Expired GB981715A (en) 1962-04-05 1963-03-18 A method for the reduction of haze in beer

Country Status (2)

Country Link
DK (1) DK105752C (en)
GB (1) GB981715A (en)

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4515821A (en) * 1982-09-08 1985-05-07 Internationale Octrooi Maatschappij "Octropa" Calcined silicas and their use in beer clarification
US4636394A (en) * 1984-04-16 1987-01-13 J. E. Siebel Sons' Company, Inc. Method and compositions for chillproofing beverages
JPS62207712A (en) * 1986-03-05 1987-09-12 Fuji Debuison Kagaku Kk Hydrous silica gel for stabilizing beer
EP0287232A1 (en) * 1987-03-30 1988-10-19 Unilever Plc Amorphous silicas
US7229655B2 (en) * 2003-12-30 2007-06-12 Pq Corporation Composition of, and process for using, silica xerogel for beer stabilization
WO2010019312A1 (en) * 2008-08-12 2010-02-18 E. I. Du Pont De Nemours And Company Silica microgels for reducing chill haze
US10633621B2 (en) 2006-08-07 2020-04-28 Grace Gmbh Beer clarification aid based on silica xerogel with high filterability

Cited By (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4515821A (en) * 1982-09-08 1985-05-07 Internationale Octrooi Maatschappij "Octropa" Calcined silicas and their use in beer clarification
US4636394A (en) * 1984-04-16 1987-01-13 J. E. Siebel Sons' Company, Inc. Method and compositions for chillproofing beverages
US4880650A (en) * 1986-03-05 1989-11-14 Fuji-Davison Chemical, Ltd. Method for stabilization treatment of beer with hydrated silica gel
EP0235352A3 (en) * 1986-03-05 1988-06-15 Fuji-Davison Chemical Ltd. Hydrated silica gel for stabilization treatment of beer
JPS62207712A (en) * 1986-03-05 1987-09-12 Fuji Debuison Kagaku Kk Hydrous silica gel for stabilizing beer
JPH0327483B2 (en) * 1986-03-05 1991-04-16 Fuji Deuison Kagaku Kk
EP0287232A1 (en) * 1987-03-30 1988-10-19 Unilever Plc Amorphous silicas
JPS63252915A (en) * 1987-03-30 1988-10-20 ユニリーバ ナームローゼ ベンノートシヤープ Amorphous silica and manufacture
JPH0569045B2 (en) * 1987-03-30 1993-09-30 Unilever Nv
US7229655B2 (en) * 2003-12-30 2007-06-12 Pq Corporation Composition of, and process for using, silica xerogel for beer stabilization
US7538067B2 (en) 2003-12-30 2009-05-26 Pq Corporation Composition of, and process for preparing, silica xerogel for beer stabilization
US10633621B2 (en) 2006-08-07 2020-04-28 Grace Gmbh Beer clarification aid based on silica xerogel with high filterability
WO2010019312A1 (en) * 2008-08-12 2010-02-18 E. I. Du Pont De Nemours And Company Silica microgels for reducing chill haze
CN102119211A (en) * 2008-08-12 2011-07-06 纳幕尔杜邦公司 Silica microgels for reducing chill haze
US8409647B2 (en) 2008-08-12 2013-04-02 E. I. Du Pont De Nemours And Company Silica microgels for reducing chill haze

Also Published As

Publication number Publication date
DK105752C (en) 1966-11-07

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