BRPI0707705B1 - Composições de resina de polipropileno clarificada e de masterbatch - Google Patents
Composições de resina de polipropileno clarificada e de masterbatch Download PDFInfo
- Publication number
- BRPI0707705B1 BRPI0707705B1 BRPI0707705-0A BRPI0707705A BRPI0707705B1 BR PI0707705 B1 BRPI0707705 B1 BR PI0707705B1 BR PI0707705 A BRPI0707705 A BR PI0707705A BR PI0707705 B1 BRPI0707705 B1 BR PI0707705B1
- Authority
- BR
- Brazil
- Prior art keywords
- coloring agent
- agent
- composition
- clarifying
- ppm
- Prior art date
Links
- 239000000203 mixture Substances 0.000 title claims abstract description 110
- -1 POLYPROPYLENE Polymers 0.000 title claims abstract description 41
- 239000004743 Polypropylene Substances 0.000 title claims abstract description 37
- 229920001155 polypropylene Polymers 0.000 title claims abstract description 35
- 239000004594 Masterbatch (MB) Substances 0.000 title claims description 33
- 239000003086 colorant Substances 0.000 claims abstract description 144
- 239000008395 clarifying agent Substances 0.000 claims abstract description 53
- 239000000654 additive Substances 0.000 claims abstract description 47
- 239000000049 pigment Substances 0.000 claims abstract description 27
- 229920001169 thermoplastic Polymers 0.000 claims abstract description 23
- 239000004416 thermosoftening plastic Substances 0.000 claims abstract description 23
- 229920000098 polyolefin Polymers 0.000 claims abstract description 10
- 230000000996 additive effect Effects 0.000 claims description 39
- 229920000642 polymer Polymers 0.000 claims description 32
- 239000011342 resin composition Substances 0.000 claims description 19
- 238000002156 mixing Methods 0.000 claims description 16
- 239000002243 precursor Substances 0.000 claims description 16
- 238000004519 manufacturing process Methods 0.000 claims description 14
- 230000003287 optical effect Effects 0.000 claims description 7
- 239000002253 acid Substances 0.000 claims description 6
- 239000003963 antioxidant agent Substances 0.000 claims description 6
- 239000004611 light stabiliser Substances 0.000 claims description 6
- 239000006096 absorbing agent Substances 0.000 claims description 5
- 239000011230 binding agent Substances 0.000 claims description 4
- 229940087101 dibenzylidene sorbitol Drugs 0.000 claims 1
- 239000000779 smoke Substances 0.000 claims 1
- 239000006229 carbon black Substances 0.000 abstract description 22
- 230000000007 visual effect Effects 0.000 abstract description 10
- 230000008901 benefit Effects 0.000 abstract description 9
- 238000011068 loading method Methods 0.000 abstract description 3
- 238000000034 method Methods 0.000 description 44
- 229920003023 plastic Polymers 0.000 description 31
- 239000004033 plastic Substances 0.000 description 29
- 229920005989 resin Polymers 0.000 description 29
- 239000011347 resin Substances 0.000 description 29
- 239000003795 chemical substances by application Substances 0.000 description 17
- 239000006185 dispersion Substances 0.000 description 16
- 230000000052 comparative effect Effects 0.000 description 15
- 239000000975 dye Substances 0.000 description 14
- 238000004806 packaging method and process Methods 0.000 description 12
- 238000001746 injection moulding Methods 0.000 description 11
- 239000000047 product Substances 0.000 description 11
- 150000001875 compounds Chemical class 0.000 description 10
- YWEWWNPYDDHZDI-JJKKTNRVSA-N (1r)-1-[(4r,4ar,8as)-2,6-bis(3,4-dimethylphenyl)-4,4a,8,8a-tetrahydro-[1,3]dioxino[5,4-d][1,3]dioxin-4-yl]ethane-1,2-diol Chemical compound C1=C(C)C(C)=CC=C1C1O[C@H]2[C@@H]([C@H](O)CO)OC(C=3C=C(C)C(C)=CC=3)O[C@H]2CO1 YWEWWNPYDDHZDI-JJKKTNRVSA-N 0.000 description 8
- 239000008187 granular material Substances 0.000 description 8
- 238000012360 testing method Methods 0.000 description 8
- 238000004040 coloring Methods 0.000 description 7
- 239000013078 crystal Substances 0.000 description 7
- 230000000694 effects Effects 0.000 description 7
- 238000002844 melting Methods 0.000 description 7
- 230000008018 melting Effects 0.000 description 7
- 239000000843 powder Substances 0.000 description 7
- JKIJEFPNVSHHEI-UHFFFAOYSA-N Phenol, 2,4-bis(1,1-dimethylethyl)-, phosphite (3:1) Chemical compound CC(C)(C)C1=CC(C(C)(C)C)=CC=C1OP(OC=1C(=CC(=CC=1)C(C)(C)C)C(C)(C)C)OC1=CC=C(C(C)(C)C)C=C1C(C)(C)C JKIJEFPNVSHHEI-UHFFFAOYSA-N 0.000 description 6
- BGYHLZZASRKEJE-UHFFFAOYSA-N [3-[3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoyloxy]-2,2-bis[3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoyloxymethyl]propyl] 3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoate Chemical compound CC(C)(C)C1=C(O)C(C(C)(C)C)=CC(CCC(=O)OCC(COC(=O)CCC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)(COC(=O)CCC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)COC(=O)CCC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)=C1 BGYHLZZASRKEJE-UHFFFAOYSA-N 0.000 description 6
- 238000010348 incorporation Methods 0.000 description 6
- 238000002347 injection Methods 0.000 description 6
- 239000007924 injection Substances 0.000 description 6
- 238000010103 injection stretch blow moulding Methods 0.000 description 6
- 238000005259 measurement Methods 0.000 description 6
- 239000002245 particle Substances 0.000 description 6
- 229920005604 random copolymer Polymers 0.000 description 6
- 238000003860 storage Methods 0.000 description 6
- 239000000126 substance Substances 0.000 description 6
- 241000557626 Corvus corax Species 0.000 description 5
- 238000010101 extrusion blow moulding Methods 0.000 description 5
- 230000006911 nucleation Effects 0.000 description 5
- 238000010899 nucleation Methods 0.000 description 5
- 238000010186 staining Methods 0.000 description 5
- 238000003856 thermoforming Methods 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 4
- 230000015572 biosynthetic process Effects 0.000 description 4
- 238000002485 combustion reaction Methods 0.000 description 4
- 229920001577 copolymer Polymers 0.000 description 4
- 238000002425 crystallisation Methods 0.000 description 4
- 230000008025 crystallization Effects 0.000 description 4
- 238000009472 formulation Methods 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 229910052799 carbon Inorganic materials 0.000 description 3
- 238000005352 clarification Methods 0.000 description 3
- 238000001816 cooling Methods 0.000 description 3
- 239000000155 melt Substances 0.000 description 3
- 238000002360 preparation method Methods 0.000 description 3
- 230000003313 weakening effect Effects 0.000 description 3
- FMZUHGYZWYNSOA-VVBFYGJXSA-N (1r)-1-[(4r,4ar,8as)-2,6-diphenyl-4,4a,8,8a-tetrahydro-[1,3]dioxino[5,4-d][1,3]dioxin-4-yl]ethane-1,2-diol Chemical class C([C@@H]1OC(O[C@@H]([C@@H]1O1)[C@H](O)CO)C=2C=CC=CC=2)OC1C1=CC=CC=C1 FMZUHGYZWYNSOA-VVBFYGJXSA-N 0.000 description 2
- 101100352919 Caenorhabditis elegans ppm-2 gene Proteins 0.000 description 2
- 241000316887 Saissetia oleae Species 0.000 description 2
- CJZGTCYPCWQAJB-UHFFFAOYSA-L calcium stearate Chemical compound [Ca+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O CJZGTCYPCWQAJB-UHFFFAOYSA-L 0.000 description 2
- 235000013539 calcium stearate Nutrition 0.000 description 2
- 239000008116 calcium stearate Substances 0.000 description 2
- 210000004027 cell Anatomy 0.000 description 2
- 239000000805 composite resin Substances 0.000 description 2
- 230000003750 conditioning effect Effects 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- 230000004927 fusion Effects 0.000 description 2
- 239000000976 ink Substances 0.000 description 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
- 238000000465 moulding Methods 0.000 description 2
- 230000000704 physical effect Effects 0.000 description 2
- 239000004597 plastic additive Substances 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 239000004071 soot Substances 0.000 description 2
- 241000894007 species Species 0.000 description 2
- 238000010561 standard procedure Methods 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- OHVLMTFVQDZYHP-UHFFFAOYSA-N 1-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)-2-[4-[2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidin-5-yl]piperazin-1-yl]ethanone Chemical compound N1N=NC=2CN(CCC=21)C(CN1CCN(CC1)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)=O OHVLMTFVQDZYHP-UHFFFAOYSA-N 0.000 description 1
- 241000871495 Heeria argentea Species 0.000 description 1
- AFCARXCZXQIEQB-UHFFFAOYSA-N N-[3-oxo-3-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(CCNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 AFCARXCZXQIEQB-UHFFFAOYSA-N 0.000 description 1
- 239000004677 Nylon Substances 0.000 description 1
- 229910019142 PO4 Inorganic materials 0.000 description 1
- 239000004952 Polyamide Substances 0.000 description 1
- 239000004698 Polyethylene Substances 0.000 description 1
- 239000013036 UV Light Stabilizer Substances 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 238000000071 blow moulding Methods 0.000 description 1
- 239000003610 charcoal Substances 0.000 description 1
- 229920006026 co-polymeric resin Polymers 0.000 description 1
- 239000000571 coke Substances 0.000 description 1
- 230000000112 colonic effect Effects 0.000 description 1
- 239000013065 commercial product Substances 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 229910003460 diamond Inorganic materials 0.000 description 1
- 239000010432 diamond Substances 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 229920001971 elastomer Polymers 0.000 description 1
- 239000000284 extract Substances 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000010419 fine particle Substances 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000007970 homogeneous dispersion Substances 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000006115 industrial coating Substances 0.000 description 1
- 239000001023 inorganic pigment Substances 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 239000003345 natural gas Substances 0.000 description 1
- 229920001778 nylon Polymers 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 1
- 239000010452 phosphate Substances 0.000 description 1
- 239000002985 plastic film Substances 0.000 description 1
- 229920002647 polyamide Polymers 0.000 description 1
- 229920001748 polybutylene Polymers 0.000 description 1
- 229920000728 polyester Polymers 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 229920000139 polyethylene terephthalate Polymers 0.000 description 1
- 239000005020 polyethylene terephthalate Substances 0.000 description 1
- 229920005606 polypropylene copolymer Polymers 0.000 description 1
- 229920005630 polypropylene random copolymer Polymers 0.000 description 1
- 229920002635 polyurethane Polymers 0.000 description 1
- 239000004814 polyurethane Substances 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 239000010453 quartz Substances 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 239000005060 rubber Substances 0.000 description 1
- 239000002453 shampoo Substances 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- 239000012798 spherical particle Substances 0.000 description 1
- 238000005979 thermal decomposition reaction Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/04—Oxygen-containing compounds
- C08K5/15—Heterocyclic compounds having oxygen in the ring
- C08K5/156—Heterocyclic compounds having oxygen in the ring having two oxygen atoms in the ring
- C08K5/1575—Six-membered rings
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Pigments, Carbon Blacks, Or Wood Stains (AREA)
- Manufacture Of Macromolecular Shaped Articles (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US11/349,021 US8232335B2 (en) | 2006-02-07 | 2006-02-07 | Compositions and methods for making clarified aesthetically enhanced articles |
| US11/349,021 | 2006-02-07 | ||
| PCT/US2007/003182 WO2007092462A2 (en) | 2006-02-07 | 2007-02-05 | Compositions and method for making clarified articles |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| BRPI0707705A2 BRPI0707705A2 (pt) | 2011-05-10 |
| BRPI0707705B1 true BRPI0707705B1 (pt) | 2018-05-29 |
Family
ID=38117067
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BRPI0707705-0A BRPI0707705B1 (pt) | 2006-02-07 | 2007-02-05 | Composições de resina de polipropileno clarificada e de masterbatch |
Country Status (7)
| Country | Link |
|---|---|
| US (2) | US8232335B2 (enExample) |
| EP (1) | EP1989252B1 (enExample) |
| JP (1) | JP5086277B2 (enExample) |
| CN (2) | CN101421342A (enExample) |
| AT (1) | ATE509063T1 (enExample) |
| BR (1) | BRPI0707705B1 (enExample) |
| WO (1) | WO2007092462A2 (enExample) |
Families Citing this family (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8232335B2 (en) | 2006-02-07 | 2012-07-31 | Milliken & Company | Compositions and methods for making clarified aesthetically enhanced articles |
| PL2510047T3 (pl) * | 2009-12-07 | 2015-04-30 | Basf Se | Przezroczyste wyroby z polipropylenu o polepszonych właściwościach optycznych i/lub zwiększonej temperaturze krystalizacji |
| CN102958618A (zh) * | 2010-07-02 | 2013-03-06 | 荷兰联合利华有限公司 | 包装的织物清洁组合物 |
| US20120190780A1 (en) * | 2011-01-25 | 2012-07-26 | Danielson Todd D | Additive compositions and thermoplastic polymer compositions comprising the same |
| IN2014MN02452A (enExample) * | 2012-05-11 | 2015-07-10 | Adeka Corp | |
| JP5992364B2 (ja) | 2013-05-31 | 2016-09-14 | 株式会社Adeka | 透明化剤組成物の製造方法及びそれを含有してなるポリオレフィン系樹脂組成物の製造方法 |
| JP2015230610A (ja) * | 2014-06-05 | 2015-12-21 | 大日本印刷株式会社 | カバーガラスおよびカバーガラス保護部材 |
| EP3312102A4 (en) * | 2015-06-17 | 2018-12-05 | Toyo Seikan Co., Ltd. | Direct blow-molded container having excellent surface gloss |
| GB2568050A (en) * | 2017-11-01 | 2019-05-08 | Caesarstone Ltd | Compositions comprising an acrylic polymer and processes of preparing the same |
| CN109082114A (zh) * | 2018-07-23 | 2018-12-25 | 芜湖金光汽车配件有限责任公司 | 一种汽车尼龙塑料件加工工艺 |
| SG11202102319WA (en) * | 2018-11-15 | 2021-04-29 | Abu Dhabi Polymers Co Ltd Borouge | Polymer composition for blow molding applications |
| EP3891195A1 (en) | 2018-12-04 | 2021-10-13 | Basell Poliolefine Italia S.r.l. | Zn catalyst components and process for their preparation |
| WO2020114837A1 (en) | 2018-12-04 | 2020-06-11 | Basell Poliolefine Italia S.R.L. | Process for the preparation of a colored polypropylene |
| US11834558B2 (en) * | 2018-12-21 | 2023-12-05 | Milliken & Company | Additive compositions and thermoplastic polymer compositions comprising the same |
| EP3953398A1 (en) | 2019-04-11 | 2022-02-16 | Basell Poliolefine Italia S.r.l. | Process for the preparation of polypropylene |
| CN111825882B (zh) * | 2019-04-15 | 2022-04-05 | 呈和科技股份有限公司 | 一种包含无机颜料和有机颜料的透明成核剂及其制品 |
| EP4222183A1 (en) | 2020-09-30 | 2023-08-09 | Borealis AG | Process for recycling propylene-ethylene copolymers |
| CN113213757B (zh) * | 2021-05-20 | 2022-07-19 | 莆田市日晶玻璃制品有限公司 | 一种天蓝色玻璃瓶的制造方法 |
| EP4155328A1 (en) | 2021-09-23 | 2023-03-29 | Borealis AG | Propylene-butene random copolymer composition with low extractable content |
Family Cites Families (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5262471A (en) | 1988-11-21 | 1993-11-16 | Fuji Photo Film Co., Ltd. | Method of preparing packaging material for photographic photosensitive material and masterbatch therefor |
| JPH06220270A (ja) * | 1993-01-27 | 1994-08-09 | Mitsubishi Petrochem Co Ltd | 耐傷性プロピレン系樹脂組成物 |
| JP3478604B2 (ja) | 1994-09-08 | 2003-12-15 | 新日本理化株式会社 | 着色ポリオレフィン系樹脂組成物 |
| US5961914A (en) * | 1996-05-03 | 1999-10-05 | Milliken & Company | Method of thermoforming polyolefin resin |
| JPH1017848A (ja) | 1996-07-03 | 1998-01-20 | Ii C Kagaku Kk | ポリオレフイン系樹脂に対する透明化剤、その製造方法及び透明性が改良されたポリオレフイン系樹脂組成物 |
| JPH11349740A (ja) | 1998-06-11 | 1999-12-21 | Asahi Denka Kogyo Kk | 射出成形用着色合成樹脂組成物 |
| JP4201431B2 (ja) | 1999-04-19 | 2008-12-24 | 株式会社Ａｄｅｋａ | 着色合成樹脂組成物 |
| US7303795B2 (en) | 2003-03-13 | 2007-12-04 | Invista North America S.A. R.L. | Molding of polypropylene with enhanced reheat characteristics |
| US20040219319A1 (en) | 2003-04-30 | 2004-11-04 | Brooks Gary T. | High clarity formed articles of polypropylene |
| JP2004346122A (ja) * | 2003-05-20 | 2004-12-09 | Idemitsu Petrochem Co Ltd | 一軸延伸バンド用ポリプロピレン系樹脂組成物及びそれを用いた梱包用バンド |
| US7291669B2 (en) * | 2004-03-16 | 2007-11-06 | Ciba Specialty Chemicals Corporation | Stabilized polyolefin compositions |
| FR2869563B1 (fr) | 2004-04-30 | 2007-09-07 | Sidel Sas | Preforme en polypropylene pour la fabrication de bouteilles ou analogues par soufflage ou etirage-soufflage et procede de soufflage ou d'etirage-soufflage de cette preforme |
| CA2586628C (en) * | 2004-12-17 | 2010-05-11 | Exxonmobil Chemical Patents Inc. | Films from polymer blends |
| US20090258560A1 (en) | 2005-09-30 | 2009-10-15 | Per Magnus Kristiansen | Microporous Films |
| US8232335B2 (en) | 2006-02-07 | 2012-07-31 | Milliken & Company | Compositions and methods for making clarified aesthetically enhanced articles |
| ES2379607T3 (es) | 2006-07-17 | 2012-04-27 | Avery Dennison Corporation | Película polímera multicapa asimétrica y etiqueta de la misma |
| JP5388263B2 (ja) | 2007-09-04 | 2014-01-15 | 株式会社Ａｄｅｋａ | ポリオレフィン樹脂用造核剤マスターバッチ |
-
2006
- 2006-02-07 US US11/349,021 patent/US8232335B2/en active Active
-
2007
- 2007-02-05 CN CNA2007800126332A patent/CN101421342A/zh active Pending
- 2007-02-05 EP EP07763167A patent/EP1989252B1/en active Active
- 2007-02-05 BR BRPI0707705-0A patent/BRPI0707705B1/pt active IP Right Grant
- 2007-02-05 JP JP2008554306A patent/JP5086277B2/ja active Active
- 2007-02-05 CN CN201510216753.0A patent/CN104892977A/zh active Pending
- 2007-02-05 WO PCT/US2007/003182 patent/WO2007092462A2/en not_active Ceased
- 2007-02-05 AT AT07763167T patent/ATE509063T1/de active
-
2012
- 2012-06-26 US US13/533,377 patent/US8653165B2/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| JP2009526123A (ja) | 2009-07-16 |
| US8232335B2 (en) | 2012-07-31 |
| EP1989252A2 (en) | 2008-11-12 |
| ATE509063T1 (de) | 2011-05-15 |
| CN104892977A (zh) | 2015-09-09 |
| US8653165B2 (en) | 2014-02-18 |
| US20070185247A1 (en) | 2007-08-09 |
| US20120316272A1 (en) | 2012-12-13 |
| CN101421342A (zh) | 2009-04-29 |
| BRPI0707705A2 (pt) | 2011-05-10 |
| WO2007092462A2 (en) | 2007-08-16 |
| JP5086277B2 (ja) | 2012-11-28 |
| WO2007092462A3 (en) | 2007-12-06 |
| EP1989252B1 (en) | 2011-05-11 |
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