BRPI0618572A2 - composição de silicone intumescido e, processo de produção da mesma - Google Patents
composição de silicone intumescido e, processo de produção da mesma Download PDFInfo
- Publication number
- BRPI0618572A2 BRPI0618572A2 BRPI0618572-0A BRPI0618572A BRPI0618572A2 BR PI0618572 A2 BRPI0618572 A2 BR PI0618572A2 BR PI0618572 A BRPI0618572 A BR PI0618572A BR PI0618572 A2 BRPI0618572 A2 BR PI0618572A2
- Authority
- BR
- Brazil
- Prior art keywords
- trisiloxane
- silicone
- silicone composition
- carbon atoms
- monovalent hydrocarbon
- Prior art date
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- 239000000203 mixture Substances 0.000 title claims abstract description 227
- 229920001296 polysiloxane Polymers 0.000 title claims abstract description 219
- 238000004519 manufacturing process Methods 0.000 title description 2
- -1 alkyl trisiloxane Chemical compound 0.000 claims abstract description 116
- 239000007787 solid Substances 0.000 claims abstract description 66
- 229920005573 silicon-containing polymer Polymers 0.000 claims abstract description 46
- 238000000034 method Methods 0.000 claims abstract description 38
- 230000008569 process Effects 0.000 claims abstract description 33
- 239000012530 fluid Substances 0.000 claims description 93
- 239000007795 chemical reaction product Substances 0.000 claims description 73
- 125000004432 carbon atom Chemical group C* 0.000 claims description 65
- 239000004215 Carbon black (E152) Substances 0.000 claims description 59
- 229930195733 hydrocarbon Natural products 0.000 claims description 59
- 238000009472 formulation Methods 0.000 claims description 38
- 239000000047 product Substances 0.000 claims description 25
- HLPWCQDWRYCGLK-UHFFFAOYSA-N ethyl-methyl-bis(trimethylsilyloxy)silane Chemical compound C[Si](C)(C)O[Si](C)(CC)O[Si](C)(C)C HLPWCQDWRYCGLK-UHFFFAOYSA-N 0.000 claims description 21
- 239000000463 material Substances 0.000 claims description 21
- 239000004721 Polyphenylene oxide Substances 0.000 claims description 20
- 229920000570 polyether Polymers 0.000 claims description 20
- 238000004132 cross linking Methods 0.000 claims description 18
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical group [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 17
- 229910052710 silicon Inorganic materials 0.000 claims description 17
- 238000006243 chemical reaction Methods 0.000 claims description 15
- 239000010703 silicon Substances 0.000 claims description 14
- 230000008961 swelling Effects 0.000 claims description 14
- 125000000217 alkyl group Chemical group 0.000 claims description 13
- 125000004435 hydrogen atom Chemical group [H]* 0.000 claims description 13
- 229930195735 unsaturated hydrocarbon Natural products 0.000 claims description 13
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 11
- LMHYXNDDEXUHJR-UHFFFAOYSA-N octyl(silyloxysilyloxy)silane Chemical compound CCCCCCCC[SiH2]O[SiH2]O[SiH3] LMHYXNDDEXUHJR-UHFFFAOYSA-N 0.000 claims description 11
- 229920000642 polymer Polymers 0.000 claims description 11
- 238000006116 polymerization reaction Methods 0.000 claims description 11
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 10
- 229910052799 carbon Inorganic materials 0.000 claims description 10
- 125000000466 oxiranyl group Chemical group 0.000 claims description 10
- 239000004593 Epoxy Substances 0.000 claims description 9
- 230000001166 anti-perspirative effect Effects 0.000 claims description 9
- 239000003213 antiperspirant Substances 0.000 claims description 9
- 150000001875 compounds Chemical class 0.000 claims description 9
- KPUWHANPEXNPJT-UHFFFAOYSA-N disiloxane Chemical class [SiH3]O[SiH3] KPUWHANPEXNPJT-UHFFFAOYSA-N 0.000 claims description 8
- ZQTYRTSKQFQYPQ-UHFFFAOYSA-N trisiloxane Chemical compound [SiH3]O[SiH2]O[SiH3] ZQTYRTSKQFQYPQ-UHFFFAOYSA-N 0.000 claims description 8
- 229910004298 SiO 2 Inorganic materials 0.000 claims description 7
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical group [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 claims description 7
- 229920001577 copolymer Polymers 0.000 claims description 7
- 239000003205 fragrance Substances 0.000 claims description 7
- 239000004615 ingredient Substances 0.000 claims description 7
- 125000005375 organosiloxane group Chemical group 0.000 claims description 7
- 239000004909 Moisturizer Substances 0.000 claims description 6
- 238000004040 coloring Methods 0.000 claims description 6
- 239000002781 deodorant agent Substances 0.000 claims description 6
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims description 6
- 230000001333 moisturizer Effects 0.000 claims description 6
- 239000003795 chemical substances by application Substances 0.000 claims description 5
- 239000002537 cosmetic Substances 0.000 claims description 5
- 229910052909 inorganic silicate Inorganic materials 0.000 claims description 5
- 239000000377 silicon dioxide Substances 0.000 claims description 5
- 229910020489 SiO3 Inorganic materials 0.000 claims description 4
- 229910052681 coesite Inorganic materials 0.000 claims description 4
- 229910052906 cristobalite Inorganic materials 0.000 claims description 4
- 239000006210 lotion Substances 0.000 claims description 4
- 239000010445 mica Substances 0.000 claims description 4
- 229910052618 mica group Inorganic materials 0.000 claims description 4
- 239000003921 oil Substances 0.000 claims description 4
- 239000000049 pigment Substances 0.000 claims description 4
- 235000012239 silicon dioxide Nutrition 0.000 claims description 4
- 229910052682 stishovite Inorganic materials 0.000 claims description 4
- 229910052905 tridymite Inorganic materials 0.000 claims description 4
- 102000004190 Enzymes Human genes 0.000 claims description 3
- 108090000790 Enzymes Proteins 0.000 claims description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 3
- 230000029936 alkylation Effects 0.000 claims description 3
- 238000005804 alkylation reaction Methods 0.000 claims description 3
- 229940121375 antifungal agent Drugs 0.000 claims description 3
- 239000003429 antifungal agent Substances 0.000 claims description 3
- 239000004599 antimicrobial Substances 0.000 claims description 3
- 230000003115 biocidal effect Effects 0.000 claims description 3
- 239000003139 biocide Substances 0.000 claims description 3
- 239000004927 clay Substances 0.000 claims description 3
- 238000012377 drug delivery Methods 0.000 claims description 3
- 239000003792 electrolyte Substances 0.000 claims description 3
- 239000003974 emollient agent Substances 0.000 claims description 3
- 239000000284 extract Substances 0.000 claims description 3
- 239000000945 filler Substances 0.000 claims description 3
- DKTNAXGQGMVGFM-UHFFFAOYSA-N hexyl(silyloxysilyloxy)silane Chemical compound CCCCCC[SiH2]O[SiH2]O[SiH3] DKTNAXGQGMVGFM-UHFFFAOYSA-N 0.000 claims description 3
- 239000005556 hormone Substances 0.000 claims description 3
- 229940088597 hormone Drugs 0.000 claims description 3
- 239000003906 humectant Substances 0.000 claims description 3
- 229910052739 hydrogen Inorganic materials 0.000 claims description 3
- 239000001257 hydrogen Substances 0.000 claims description 3
- 229920005862 polyol Polymers 0.000 claims description 3
- 150000003077 polyols Chemical class 0.000 claims description 3
- 239000011252 protective cream Substances 0.000 claims description 3
- 150000003839 salts Chemical class 0.000 claims description 3
- 239000000126 substance Substances 0.000 claims description 3
- 239000004094 surface-active agent Substances 0.000 claims description 3
- 239000002562 thickening agent Substances 0.000 claims description 3
- 230000000699 topical effect Effects 0.000 claims description 3
- 239000011782 vitamin Substances 0.000 claims description 3
- 229940088594 vitamin Drugs 0.000 claims description 3
- 229930003231 vitamin Natural products 0.000 claims description 3
- 235000013343 vitamin Nutrition 0.000 claims description 3
- 150000003722 vitamin derivatives Chemical class 0.000 claims description 3
- 239000003963 antioxidant agent Substances 0.000 claims description 2
- 230000003078 antioxidant effect Effects 0.000 claims description 2
- ZQFXRJQZKDYGFV-UHFFFAOYSA-N butan-2-yl(silyloxysilyloxy)silane Chemical compound CC(CC)[SiH2]O[SiH2]O[SiH3] ZQFXRJQZKDYGFV-UHFFFAOYSA-N 0.000 claims description 2
- NKNJFTJIZOSWNM-UHFFFAOYSA-N diethyl-bis(trimethylsilyloxy)silane Chemical compound C[Si](C)(C)O[Si](CC)(CC)O[Si](C)(C)C NKNJFTJIZOSWNM-UHFFFAOYSA-N 0.000 claims description 2
- 238000007865 diluting Methods 0.000 claims description 2
- 150000002430 hydrocarbons Chemical class 0.000 claims description 2
- CXQXSVUQTKDNFP-UHFFFAOYSA-N octamethyltrisiloxane Chemical compound C[Si](C)(C)O[Si](C)(C)O[Si](C)(C)C CXQXSVUQTKDNFP-UHFFFAOYSA-N 0.000 claims description 2
- 239000003755 preservative agent Substances 0.000 claims description 2
- 230000002335 preservative effect Effects 0.000 claims description 2
- 125000000999 tert-butyl group Chemical group [H]C([H])([H])C(*)(C([H])([H])[H])C([H])([H])[H] 0.000 claims description 2
- 239000006096 absorbing agent Substances 0.000 claims 2
- 238000004140 cleaning Methods 0.000 claims 2
- 229920002545 silicone oil Polymers 0.000 claims 2
- 230000003064 anti-oxidating effect Effects 0.000 claims 1
- 239000007800 oxidant agent Substances 0.000 claims 1
- ZBYSWWMOCOYCFE-UHFFFAOYSA-N propan-2-yl(silyloxysilyloxy)silane Chemical compound C(C)(C)[SiH2]O[SiH2]O[SiH3] ZBYSWWMOCOYCFE-UHFFFAOYSA-N 0.000 claims 1
- 230000005855 radiation Effects 0.000 claims 1
- ULZQWVNAVWGFLG-UHFFFAOYSA-N tert-butyl-[dimethylsilyloxy(dimethyl)silyl]oxy-dimethylsilane Chemical compound C[SiH](C)O[Si](C)(C)O[Si](C)(C)C(C)(C)C ULZQWVNAVWGFLG-UHFFFAOYSA-N 0.000 claims 1
- 239000000499 gel Substances 0.000 description 52
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 18
- 239000004205 dimethyl polysiloxane Substances 0.000 description 17
- 235000013870 dimethyl polysiloxane Nutrition 0.000 description 17
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 description 17
- 239000003054 catalyst Substances 0.000 description 16
- 230000000670 limiting effect Effects 0.000 description 14
- 125000000962 organic group Chemical group 0.000 description 14
- 239000004711 α-olefin Substances 0.000 description 13
- XAYDWGMOPRHLEP-UHFFFAOYSA-N 6-ethenyl-7-oxabicyclo[4.1.0]heptane Chemical compound C1CCCC2OC21C=C XAYDWGMOPRHLEP-UHFFFAOYSA-N 0.000 description 9
- 150000004678 hydrides Chemical class 0.000 description 9
- 229910052697 platinum Inorganic materials 0.000 description 9
- XMSXQFUHVRWGNA-UHFFFAOYSA-N Decamethylcyclopentasiloxane Chemical compound C[Si]1(C)O[Si](C)(C)O[Si](C)(C)O[Si](C)(C)O[Si](C)(C)O1 XMSXQFUHVRWGNA-UHFFFAOYSA-N 0.000 description 8
- 239000000843 powder Substances 0.000 description 7
- 150000003254 radicals Chemical class 0.000 description 7
- 230000000475 sunscreen effect Effects 0.000 description 6
- 239000000516 sunscreening agent Substances 0.000 description 6
- 150000001336 alkenes Chemical group 0.000 description 5
- 239000012632 extractable Substances 0.000 description 5
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 description 5
- 239000011541 reaction mixture Substances 0.000 description 5
- 230000001953 sensory effect Effects 0.000 description 5
- 238000001704 evaporation Methods 0.000 description 4
- 230000008020 evaporation Effects 0.000 description 4
- 125000003903 2-propenyl group Chemical group [H]C([*])([H])C([H])=C([H])[H] 0.000 description 3
- 239000006071 cream Substances 0.000 description 3
- 238000000605 extraction Methods 0.000 description 3
- 238000005259 measurement Methods 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- 150000002924 oxiranes Chemical class 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- 229910052990 silicon hydride Inorganic materials 0.000 description 3
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 3
- 229920002554 vinyl polymer Polymers 0.000 description 3
- KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 description 2
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 2
- PDWFFEHBPAYQGO-UHFFFAOYSA-N [dimethyl(trimethylsilyloxy)silyl]oxy-hexyl-dimethylsilane Chemical compound CCCCCC[Si](C)(C)O[Si](C)(C)O[Si](C)(C)C PDWFFEHBPAYQGO-UHFFFAOYSA-N 0.000 description 2
- 238000005054 agglomeration Methods 0.000 description 2
- 230000002776 aggregation Effects 0.000 description 2
- 125000003342 alkenyl group Chemical group 0.000 description 2
- SPDPBNKCNIQAOH-UHFFFAOYSA-N bis[[ethyl(dimethyl)silyl]oxy]-dimethylsilane Chemical compound CC[Si](C)(C)O[Si](C)(C)O[Si](C)(C)CC SPDPBNKCNIQAOH-UHFFFAOYSA-N 0.000 description 2
- 125000002091 cationic group Chemical group 0.000 description 2
- 238000010538 cationic polymerization reaction Methods 0.000 description 2
- 229920006037 cross link polymer Polymers 0.000 description 2
- 125000004122 cyclic group Chemical group 0.000 description 2
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 2
- 125000000524 functional group Chemical group 0.000 description 2
- PNJMJEXVQAFSBS-UHFFFAOYSA-N hexyl-methyl-bis(trimethylsilyloxy)silane Chemical compound CCCCCC[Si](C)(O[Si](C)(C)C)O[Si](C)(C)C PNJMJEXVQAFSBS-UHFFFAOYSA-N 0.000 description 2
- 239000003112 inhibitor Substances 0.000 description 2
- 125000000959 isobutyl group Chemical group [H]C([H])([H])C([H])(C([H])([H])[H])C([H])([H])* 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 description 2
- 239000002453 shampoo Substances 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 230000008719 thickening Effects 0.000 description 2
- SCRSFLUHMDMRFP-UHFFFAOYSA-N trimethyl-(methyl-octyl-trimethylsilyloxysilyl)oxysilane Chemical compound CCCCCCCC[Si](C)(O[Si](C)(C)C)O[Si](C)(C)C SCRSFLUHMDMRFP-UHFFFAOYSA-N 0.000 description 2
- CCEFMUBVSUDRLG-KXUCPTDWSA-N (4R)-limonene 1,2-epoxide Natural products C1[C@H](C(=C)C)CC[C@@]2(C)O[C@H]21 CCEFMUBVSUDRLG-KXUCPTDWSA-N 0.000 description 1
- WEEGYLXZBRQIMU-UHFFFAOYSA-N 1,8-cineole Natural products C1CC2CCC1(C)OC2(C)C WEEGYLXZBRQIMU-UHFFFAOYSA-N 0.000 description 1
- LSWYGACWGAICNM-UHFFFAOYSA-N 2-(prop-2-enoxymethyl)oxirane Chemical compound C=CCOCC1CO1 LSWYGACWGAICNM-UHFFFAOYSA-N 0.000 description 1
- MUUOUUYKIVSIAR-UHFFFAOYSA-N 2-but-3-enyloxirane Chemical compound C=CCCC1CO1 MUUOUUYKIVSIAR-UHFFFAOYSA-N 0.000 description 1
- LEIIXLILAPNBBU-UHFFFAOYSA-N 2-cyclopentyloxane Chemical compound C1CCCC1C1OCCCC1 LEIIXLILAPNBBU-UHFFFAOYSA-N 0.000 description 1
- UKTHULMXFLCNAV-UHFFFAOYSA-N 2-hex-5-enyloxirane Chemical compound C=CCCCCC1CO1 UKTHULMXFLCNAV-UHFFFAOYSA-N 0.000 description 1
- FCZHJHKCOZGQJZ-UHFFFAOYSA-N 2-oct-7-enyloxirane Chemical compound C=CCCCCCCC1CO1 FCZHJHKCOZGQJZ-UHFFFAOYSA-N 0.000 description 1
- SFKLLRAGIKFMKR-UHFFFAOYSA-N 3,3-dimethylbutyl-methyl-bis(trimethylsilyloxy)silane Chemical compound CC(C)(C)CC[Si](C)(O[Si](C)(C)C)O[Si](C)(C)C SFKLLRAGIKFMKR-UHFFFAOYSA-N 0.000 description 1
- SLJFKNONPLNAPF-UHFFFAOYSA-N 3-Vinyl-7-oxabicyclo[4.1.0]heptane Chemical compound C1C(C=C)CCC2OC21 SLJFKNONPLNAPF-UHFFFAOYSA-N 0.000 description 1
- 239000005995 Aluminium silicate Substances 0.000 description 1
- 241000195940 Bryophyta Species 0.000 description 1
- IMXCIRKUELDKDH-UHFFFAOYSA-N CC(C(C(C(C([SiH2]O[SiH2]O[SiH3])(C)C)(C)C)(C)C)(C)C)(CCC)C Chemical compound CC(C(C(C(C([SiH2]O[SiH2]O[SiH3])(C)C)(C)C)(C)C)(C)C)(CCC)C IMXCIRKUELDKDH-UHFFFAOYSA-N 0.000 description 1
- DIBANWVTJWLIBX-UHFFFAOYSA-N CCCC[SiH2]O[SiH2]O[SiH3] Chemical compound CCCC[SiH2]O[SiH2]O[SiH3] DIBANWVTJWLIBX-UHFFFAOYSA-N 0.000 description 1
- SNRUBQQJIBEYMU-UHFFFAOYSA-N Dodecane Natural products CCCCCCCCCCCC SNRUBQQJIBEYMU-UHFFFAOYSA-N 0.000 description 1
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 1
- 239000005977 Ethylene Substances 0.000 description 1
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 1
- CCEFMUBVSUDRLG-XNWIYYODSA-N Limonene-1,2-epoxide Chemical compound C1[C@H](C(=C)C)CCC2(C)OC21 CCEFMUBVSUDRLG-XNWIYYODSA-N 0.000 description 1
- 239000004368 Modified starch Substances 0.000 description 1
- 229920000881 Modified starch Polymers 0.000 description 1
- 239000004677 Nylon Substances 0.000 description 1
- GOOHAUXETOMSMM-UHFFFAOYSA-N Propylene oxide Chemical compound CC1CO1 GOOHAUXETOMSMM-UHFFFAOYSA-N 0.000 description 1
- 102220569696 Pyridoxal-dependent decarboxylase domain-containing protein 1_M11S_mutation Human genes 0.000 description 1
- KJTLSVCANCCWHF-UHFFFAOYSA-N Ruthenium Chemical compound [Ru] KJTLSVCANCCWHF-UHFFFAOYSA-N 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- QCEWLBLANFHURF-UHFFFAOYSA-N [SiH3]O[SiH2]O[SiH2]O[SiH3].[SiH3]O[SiH2]O[SiH2]O[SiH2]O[SiH3] Chemical class [SiH3]O[SiH2]O[SiH2]O[SiH3].[SiH3]O[SiH2]O[SiH2]O[SiH2]O[SiH3] QCEWLBLANFHURF-UHFFFAOYSA-N 0.000 description 1
- HFRICAKEFCIBMJ-UHFFFAOYSA-N [dimethyl(trimethylsilyloxy)silyl]oxy-ethyl-dimethylsilane Chemical compound CC[Si](C)(C)O[Si](C)(C)O[Si](C)(C)C HFRICAKEFCIBMJ-UHFFFAOYSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 238000012644 addition polymerization Methods 0.000 description 1
- 125000002947 alkylene group Chemical group 0.000 description 1
- 125000000304 alkynyl group Chemical group 0.000 description 1
- 235000012211 aluminium silicate Nutrition 0.000 description 1
- 238000010539 anionic addition polymerization reaction Methods 0.000 description 1
- 230000003712 anti-aging effect Effects 0.000 description 1
- 150000005840 aryl radicals Chemical class 0.000 description 1
- 239000000440 bentonite Substances 0.000 description 1
- 229910000278 bentonite Inorganic materials 0.000 description 1
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 description 1
- ZGCLPAXFEARXQK-UHFFFAOYSA-N bis[[butyl(dimethyl)silyl]oxy]-dimethylsilane Chemical compound CCCC[Si](C)(C)O[Si](C)(C)O[Si](C)(C)CCCC ZGCLPAXFEARXQK-UHFFFAOYSA-N 0.000 description 1
- IHIHWDWZXUUGCK-UHFFFAOYSA-N bis[[dimethyl(propyl)silyl]oxy]-dimethylsilane Chemical compound CCC[Si](C)(C)O[Si](C)(C)O[Si](C)(C)CCC IHIHWDWZXUUGCK-UHFFFAOYSA-N 0.000 description 1
- IMLREYFJPXWLCY-UHFFFAOYSA-N bis[[tert-butyl(dimethyl)silyl]oxy]-dimethylsilane Chemical compound CC(C)(C)[Si](C)(C)O[Si](C)(C)O[Si](C)(C)C(C)(C)C IMLREYFJPXWLCY-UHFFFAOYSA-N 0.000 description 1
- 229940073609 bismuth oxychloride Drugs 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- BSAFXXVXXFRPRG-UHFFFAOYSA-N butan-2-yl-methyl-bis(trimethylsilyloxy)silane Chemical compound CCC(C)[Si](C)(O[Si](C)(C)C)O[Si](C)(C)C BSAFXXVXXFRPRG-UHFFFAOYSA-N 0.000 description 1
- VWKJPEJDHKSUJL-UHFFFAOYSA-N butyl-[dimethyl(trimethylsilyloxy)silyl]oxy-dimethylsilane Chemical compound CCCC[Si](C)(C)O[Si](C)(C)O[Si](C)(C)C VWKJPEJDHKSUJL-UHFFFAOYSA-N 0.000 description 1
- QYWFUCXJWVFMFO-UHFFFAOYSA-N butyl-methyl-bis(trimethylsilyloxy)silane Chemical compound CCCC[Si](C)(O[Si](C)(C)C)O[Si](C)(C)C QYWFUCXJWVFMFO-UHFFFAOYSA-N 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 239000002826 coolant Substances 0.000 description 1
- 230000001186 cumulative effect Effects 0.000 description 1
- 125000000113 cyclohexyl group Chemical group [H]C1([H])C([H])([H])C([H])([H])C([H])(*)C([H])([H])C1([H])[H] 0.000 description 1
- 125000000640 cyclooctyl group Chemical group [H]C1([H])C([H])([H])C([H])([H])C([H])([H])C([H])(*)C([H])([H])C([H])([H])C1([H])[H] 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 125000002704 decyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
- PSCLWXNXYREBTJ-UHFFFAOYSA-N di(propan-2-yl)-bis(trimethylsilyloxy)silane Chemical compound C[Si](C)(C)O[Si](C(C)C)(O[Si](C)(C)C)C(C)C PSCLWXNXYREBTJ-UHFFFAOYSA-N 0.000 description 1
- LZKUTZXMOXXZFT-UHFFFAOYSA-N dimethyl-bis(triethylsilyloxy)silane Chemical compound CC[Si](CC)(CC)O[Si](C)(C)O[Si](CC)(CC)CC LZKUTZXMOXXZFT-UHFFFAOYSA-N 0.000 description 1
- LRCFXGAMWKDGLA-UHFFFAOYSA-N dioxosilane;hydrate Chemical compound O.O=[Si]=O LRCFXGAMWKDGLA-UHFFFAOYSA-N 0.000 description 1
- POJVZMLYQHGZBY-UHFFFAOYSA-N dipropyl-bis(trimethylsilyloxy)silane Chemical compound CCC[Si](CCC)(O[Si](C)(C)C)O[Si](C)(C)C POJVZMLYQHGZBY-UHFFFAOYSA-N 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 125000003438 dodecyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- FMUSYAWFJOLIMV-UHFFFAOYSA-N ethyl-bis[[ethyl(dimethyl)silyl]oxy]-methylsilane Chemical compound CC[Si](C)(C)O[Si](C)(CC)O[Si](C)(C)CC FMUSYAWFJOLIMV-UHFFFAOYSA-N 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 229910021485 fumed silica Inorganic materials 0.000 description 1
- 230000037308 hair color Effects 0.000 description 1
- 239000000118 hair dye Substances 0.000 description 1
- 239000008266 hair spray Substances 0.000 description 1
- 230000003741 hair volume Effects 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 125000003187 heptyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- FBBGAOSWVUEIQT-UHFFFAOYSA-N heptyl-methyl-bis(trimethylsilyloxy)silane Chemical compound CCCCCCC[Si](C)(O[Si](C)(C)C)O[Si](C)(C)C FBBGAOSWVUEIQT-UHFFFAOYSA-N 0.000 description 1
- ZKXLCEBTPLJGGJ-UHFFFAOYSA-N hexan-2-yl-methyl-bis(trimethylsilyloxy)silane Chemical compound CCCCC(C)[Si](C)(O[Si](C)(C)C)O[Si](C)(C)C ZKXLCEBTPLJGGJ-UHFFFAOYSA-N 0.000 description 1
- QBPSJZHQKWHDQQ-UHFFFAOYSA-N hexan-3-yl-methyl-bis(trimethylsilyloxy)silane Chemical compound CCCC(CC)[Si](C)(O[Si](C)(C)C)O[Si](C)(C)C QBPSJZHQKWHDQQ-UHFFFAOYSA-N 0.000 description 1
- 125000004051 hexyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
- 238000006459 hydrosilylation reaction Methods 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 239000000077 insect repellent Substances 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 229910052741 iridium Inorganic materials 0.000 description 1
- GKOZUEZYRPOHIO-UHFFFAOYSA-N iridium atom Chemical compound [Ir] GKOZUEZYRPOHIO-UHFFFAOYSA-N 0.000 description 1
- 125000001449 isopropyl group Chemical group [H]C([H])([H])C([H])(*)C([H])([H])[H] 0.000 description 1
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 235000019426 modified starch Nutrition 0.000 description 1
- 238000012544 monitoring process Methods 0.000 description 1
- 235000011929 mousse Nutrition 0.000 description 1
- 125000004108 n-butyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
- SJYNFBVQFBRSIB-UHFFFAOYSA-N norbornadiene Chemical compound C1=CC2C=CC1C2 SJYNFBVQFBRSIB-UHFFFAOYSA-N 0.000 description 1
- 229920001778 nylon Polymers 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- 229910052762 osmium Inorganic materials 0.000 description 1
- SYQBFIAQOQZEGI-UHFFFAOYSA-N osmium atom Chemical compound [Os] SYQBFIAQOQZEGI-UHFFFAOYSA-N 0.000 description 1
- BWOROQSFKKODDR-UHFFFAOYSA-N oxobismuth;hydrochloride Chemical compound Cl.[Bi]=O BWOROQSFKKODDR-UHFFFAOYSA-N 0.000 description 1
- 229910052763 palladium Inorganic materials 0.000 description 1
- 125000001147 pentyl group Chemical group C(CCCC)* 0.000 description 1
- 239000013503 personal care ingredient Substances 0.000 description 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
- 238000012643 polycondensation polymerization Methods 0.000 description 1
- 239000002685 polymerization catalyst Substances 0.000 description 1
- 239000010970 precious metal Substances 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 229910052703 rhodium Inorganic materials 0.000 description 1
- 239000010948 rhodium Substances 0.000 description 1
- MHOVAHRLVXNVSD-UHFFFAOYSA-N rhodium atom Chemical compound [Rh] MHOVAHRLVXNVSD-UHFFFAOYSA-N 0.000 description 1
- 229910052707 ruthenium Inorganic materials 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 125000002914 sec-butyl group Chemical group [H]C([H])([H])C([H])([H])C([H])(*)C([H])([H])[H] 0.000 description 1
- 230000035910 sensory benefits Effects 0.000 description 1
- 229960004029 silicic acid Drugs 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 239000000454 talc Substances 0.000 description 1
- 229910052623 talc Inorganic materials 0.000 description 1
- 235000012222 talc Nutrition 0.000 description 1
- QNHGVVMOYPEFLU-UHFFFAOYSA-N tert-butyl-methyl-bis(trimethylsilyloxy)silane Chemical compound C[Si](C)(C)O[Si](C)(C(C)(C)C)O[Si](C)(C)C QNHGVVMOYPEFLU-UHFFFAOYSA-N 0.000 description 1
- 239000004408 titanium dioxide Substances 0.000 description 1
- 125000003944 tolyl group Chemical group 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 125000000725 trifluoropropyl group Chemical group [H]C([H])(*)C([H])([H])C(F)(F)F 0.000 description 1
- SRPFBWXLOGEXJT-UHFFFAOYSA-N trimethyl-(methyl-pentyl-trimethylsilyloxysilyl)oxysilane Chemical compound CCCCC[Si](C)(O[Si](C)(C)C)O[Si](C)(C)C SRPFBWXLOGEXJT-UHFFFAOYSA-N 0.000 description 1
- PGRZLADNCDNGTC-UHFFFAOYSA-N trimethyl-(methyl-propyl-trimethylsilyloxysilyl)oxysilane Chemical compound CCC[Si](C)(O[Si](C)(C)C)O[Si](C)(C)C PGRZLADNCDNGTC-UHFFFAOYSA-N 0.000 description 1
- IIPLONCQUDDCAY-UHFFFAOYSA-N trimethyl-[methyl-(2-methylbutan-2-yl)-trimethylsilyloxysilyl]oxysilane Chemical compound CCC(C)(C)[Si](C)(O[Si](C)(C)C)O[Si](C)(C)C IIPLONCQUDDCAY-UHFFFAOYSA-N 0.000 description 1
- GQRUIQOFMCJKJP-UHFFFAOYSA-N trimethyl-[methyl-(3-methylbutyl)-trimethylsilyloxysilyl]oxysilane Chemical compound CC(C)CC[Si](C)(O[Si](C)(C)C)O[Si](C)(C)C GQRUIQOFMCJKJP-UHFFFAOYSA-N 0.000 description 1
- JGSGMDRRTNHCKH-UHFFFAOYSA-N trimethyl-[methyl-(3-methylpentyl)-trimethylsilyloxysilyl]oxysilane Chemical compound CCC(C)CC[Si](C)(O[Si](C)(C)C)O[Si](C)(C)C JGSGMDRRTNHCKH-UHFFFAOYSA-N 0.000 description 1
- FMIMVQOAKBPLEJ-UHFFFAOYSA-N trimethyl-[methyl-(4-methylpentyl)-trimethylsilyloxysilyl]oxysilane Chemical compound CC(C)CCC[Si](C)(O[Si](C)(C)C)O[Si](C)(C)C FMIMVQOAKBPLEJ-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/895—Polysiloxanes containing silicon bound to unsaturated aliphatic groups, e.g. vinyl dimethicone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/58—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
- A61K8/585—Organosilicon compounds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L83/00—Compositions of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon only; Compositions of derivatives of such polymers
- C08L83/04—Polysiloxanes
- C08L83/06—Polysiloxanes containing silicon bound to oxygen-containing groups
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Chemical & Material Sciences (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Organic Chemistry (AREA)
- Polymers & Plastics (AREA)
- Medicinal Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Cosmetics (AREA)
- Silicon Polymers (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US11/274,450 US8017687B2 (en) | 2005-11-15 | 2005-11-15 | Swollen silicone composition and process of producing same |
| US11/274.450 | 2005-11-15 | ||
| PCT/US2006/043329 WO2007058825A1 (en) | 2005-11-15 | 2006-11-06 | Swollen silicone composition and process of producing same |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| BRPI0618572A2 true BRPI0618572A2 (pt) | 2011-09-06 |
Family
ID=37898566
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BRPI0618572-0A BRPI0618572A2 (pt) | 2005-11-15 | 2006-11-06 | composição de silicone intumescido e, processo de produção da mesma |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US8017687B2 (enExample) |
| EP (2) | EP2228053A1 (enExample) |
| JP (1) | JP5457034B2 (enExample) |
| KR (1) | KR101396825B1 (enExample) |
| CN (2) | CN101360477A (enExample) |
| AU (1) | AU2006315780A1 (enExample) |
| BR (1) | BRPI0618572A2 (enExample) |
| CA (1) | CA2629100A1 (enExample) |
| RU (1) | RU2008123832A (enExample) |
| WO (1) | WO2007058825A1 (enExample) |
| ZA (2) | ZA200804069B (enExample) |
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|---|---|---|---|---|
| US7863361B2 (en) * | 2005-11-15 | 2011-01-04 | Momentive Performance Materials Inc. | Swollen silicone composition, process of producing same and products thereof |
| US7993732B2 (en) * | 2006-07-28 | 2011-08-09 | Ricoh Company, Ltd. | Heat-sensitive pressure-sensitive adhesive and heat-sensitive adhesive material |
| US20100003201A1 (en) * | 2008-07-07 | 2010-01-07 | Momentive Performance Materials, Inc. | Silicone composition |
| US20100135949A1 (en) * | 2008-12-01 | 2010-06-03 | Becton, Dickinson And Company | Antimicrobial compositions |
| US8821455B2 (en) | 2009-07-09 | 2014-09-02 | Becton, Dickinson And Company | Antimicrobial coating for dermally invasive devices |
| KR20130038847A (ko) | 2010-03-23 | 2013-04-18 | 가부시키가이샤 아사히 러버 | 실리콘 수지제 반사 기재, 그 제조 방법, 및 그 반사 기재에 이용하는 원재료 조성물 |
| KR101966263B1 (ko) | 2011-01-19 | 2019-04-08 | 프레지던트 앤드 펠로우즈 오브 하바드 칼리지 | 고압 안정성, 광학 투과도 및 자가 회복 특징을 갖는 미끄러운 표면 |
| CN103703085B (zh) | 2011-01-19 | 2016-09-28 | 哈佛学院院长等 | 光滑注液多孔表面和其生物学应用 |
| US9352119B2 (en) | 2012-05-15 | 2016-05-31 | Becton, Dickinson And Company | Blood control IV catheter with antimicrobial properties |
| WO2014012080A1 (en) | 2012-07-12 | 2014-01-16 | President And Fellows Of Harvard College | Slippery self-lubricating polymer surfaces |
| US9630224B2 (en) | 2012-07-13 | 2017-04-25 | President And Fellows Of Harvard College | Slippery liquid-infused porous surfaces having improved stability |
| CN104769049A (zh) | 2012-07-13 | 2015-07-08 | 哈佛学院 | 多功能抗性材料 |
| US9579486B2 (en) | 2012-08-22 | 2017-02-28 | Becton, Dickinson And Company | Blood control IV catheter with antimicrobial properties |
| US9750928B2 (en) | 2013-02-13 | 2017-09-05 | Becton, Dickinson And Company | Blood control IV catheter with stationary septum activator |
| US9695323B2 (en) | 2013-02-13 | 2017-07-04 | Becton, Dickinson And Company | UV curable solventless antimicrobial compositions |
| US9327095B2 (en) | 2013-03-11 | 2016-05-03 | Becton, Dickinson And Company | Blood control catheter with antimicrobial needle lube |
| US9750927B2 (en) | 2013-03-11 | 2017-09-05 | Becton, Dickinson And Company | Blood control catheter with antimicrobial needle lube |
| EP2969258A4 (en) | 2013-03-13 | 2016-11-30 | Harvard College | COMPRESSIVE COMPOSITION FOR PREPARING GLOSSY SURFACES WITH LIQUID INFUSION AND METHOD OF USE |
| US10376686B2 (en) | 2014-04-23 | 2019-08-13 | Becton, Dickinson And Company | Antimicrobial caps for medical connectors |
| US9789279B2 (en) | 2014-04-23 | 2017-10-17 | Becton, Dickinson And Company | Antimicrobial obturator for use with vascular access devices |
| US9675793B2 (en) | 2014-04-23 | 2017-06-13 | Becton, Dickinson And Company | Catheter tubing with extraluminal antimicrobial coating |
| US10232088B2 (en) | 2014-07-08 | 2019-03-19 | Becton, Dickinson And Company | Antimicrobial coating forming kink resistant feature on a vascular access device |
| US9839602B2 (en) * | 2014-12-16 | 2017-12-12 | Momentive Performance Materials Inc. | Personal care compositions containing crosslinked silicone polymer networks and their method of preparation |
| US20160296459A1 (en) * | 2015-04-09 | 2016-10-13 | Momentive Performance Materials Inc. | Extended longevity fragrance delivery composition |
| CN108026279B (zh) * | 2015-07-20 | 2022-04-01 | 莫门蒂夫性能材料有限公司 | 不对称取代的聚有机硅氧烷衍生物 |
| US10493244B2 (en) | 2015-10-28 | 2019-12-03 | Becton, Dickinson And Company | Extension tubing strain relief |
| JP6961822B2 (ja) * | 2017-11-20 | 2021-11-05 | ワッカー ケミー アクチエンゲゼルシャフトWacker Chemie AG | 天然油を含有するシリコーンエラストマーゲル |
| WO2020077160A1 (en) | 2018-10-11 | 2020-04-16 | Freeflow Medical Devices Llc | Fluoropolymer based anti-thrombotic coatings |
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-
2005
- 2005-11-15 US US11/274,450 patent/US8017687B2/en active Active
-
2006
- 2006-11-06 CA CA002629100A patent/CA2629100A1/en not_active Abandoned
- 2006-11-06 EP EP10004452A patent/EP2228053A1/en not_active Ceased
- 2006-11-06 JP JP2008540124A patent/JP5457034B2/ja not_active Expired - Fee Related
- 2006-11-06 WO PCT/US2006/043329 patent/WO2007058825A1/en not_active Ceased
- 2006-11-06 EP EP06837054A patent/EP1968533A1/en not_active Withdrawn
- 2006-11-06 KR KR1020087011371A patent/KR101396825B1/ko not_active Expired - Fee Related
- 2006-11-06 CN CNA2006800511477A patent/CN101360477A/zh active Pending
- 2006-11-06 RU RU2008123832/04A patent/RU2008123832A/ru not_active Application Discontinuation
- 2006-11-06 BR BRPI0618572-0A patent/BRPI0618572A2/pt not_active IP Right Cessation
- 2006-11-06 AU AU2006315780A patent/AU2006315780A1/en not_active Abandoned
- 2006-11-06 CN CN200680051139.2A patent/CN101360476B/zh active Active
-
2008
- 2008-05-13 ZA ZA200804069A patent/ZA200804069B/xx unknown
- 2008-05-14 ZA ZA200804141A patent/ZA200804141B/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| WO2007058825A1 (en) | 2007-05-24 |
| ZA200804141B (en) | 2009-02-25 |
| JP5457034B2 (ja) | 2014-04-02 |
| KR20080071986A (ko) | 2008-08-05 |
| RU2008123832A (ru) | 2009-12-27 |
| CN101360477A (zh) | 2009-02-04 |
| EP1968533A1 (en) | 2008-09-17 |
| CA2629100A1 (en) | 2007-05-24 |
| CN101360476B (zh) | 2015-08-05 |
| AU2006315780A1 (en) | 2007-05-24 |
| US20070112112A1 (en) | 2007-05-17 |
| EP2228053A1 (en) | 2010-09-15 |
| KR101396825B1 (ko) | 2014-05-19 |
| JP2009516025A (ja) | 2009-04-16 |
| US8017687B2 (en) | 2011-09-13 |
| ZA200804069B (en) | 2009-08-26 |
| CN101360476A (zh) | 2009-02-04 |
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