BR112015008477B1 - método para a síntese de 5-(clorometil)-2-furaldeído (cmf) de sacarídeos - Google Patents

método para a síntese de 5-(clorometil)-2-furaldeído (cmf) de sacarídeos Download PDF

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Publication number
BR112015008477B1
BR112015008477B1 BR112015008477-0A BR112015008477A BR112015008477B1 BR 112015008477 B1 BR112015008477 B1 BR 112015008477B1 BR 112015008477 A BR112015008477 A BR 112015008477A BR 112015008477 B1 BR112015008477 B1 BR 112015008477B1
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BR
Brazil
Prior art keywords
phase
cmf
organic phase
liquid
organic
Prior art date
Application number
BR112015008477-0A
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English (en)
Portuguese (pt)
Other versions
BR112015008477A2 (pt
Inventor
Aviad Cahana
Edward Nikitin
Jeremy Standiford
Kyle Ellis
Zhang Luzheng
Timothy George
Peter Mikochik
Original Assignee
Xf Technologies Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
Application filed by Xf Technologies Inc filed Critical Xf Technologies Inc
Publication of BR112015008477A2 publication Critical patent/BR112015008477A2/pt
Publication of BR112015008477B1 publication Critical patent/BR112015008477B1/pt

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40—Radicals substituted by oxygen atoms
    • C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
    • C07D307/48—Furfural
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40—Radicals substituted by oxygen atoms
    • C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40—Radicals substituted by oxygen atoms
    • C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
    • C07D307/48—Furfural
    • C07D307/50—Preparation from natural products

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Saccharide Compounds (AREA)
BR112015008477-0A 2012-10-16 2013-09-03 método para a síntese de 5-(clorometil)-2-furaldeído (cmf) de sacarídeos BR112015008477B1 (pt)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
US201261714225P 2012-10-16 2012-10-16
US61/714,225 2012-10-16
US201361818418P 2013-05-01 2013-05-01
US61/818,418 2013-05-01
PCT/US2013/057795 WO2014062303A2 (en) 2012-10-16 2013-09-03 Efficient, high-yield conversion of monosaccharides to 5-(chloromethyl)-2-furaldehyde

Publications (2)

Publication Number Publication Date
BR112015008477A2 BR112015008477A2 (pt) 2017-07-04
BR112015008477B1 true BR112015008477B1 (pt) 2020-12-08

Family

ID=50488863

Family Applications (1)

Application Number Title Priority Date Filing Date
BR112015008477-0A BR112015008477B1 (pt) 2012-10-16 2013-09-03 método para a síntese de 5-(clorometil)-2-furaldeído (cmf) de sacarídeos

Country Status (10)

Country Link
US (1) US9102644B2 (https=)
EP (1) EP2909187A4 (https=)
CN (1) CN105102440A (https=)
BR (1) BR112015008477B1 (https=)
CA (1) CA2888298C (https=)
IN (1) IN2015DN03835A (https=)
MX (1) MX363821B (https=)
PH (1) PH12015500818A1 (https=)
SG (1) SG11201502939WA (https=)
WO (1) WO2014062303A2 (https=)

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
MX346916B (es) 2011-06-09 2017-04-05 Micromidas Inc Utilizacion de reactor de fases multiples para la conversion de biomasa para producir furanos substituidos.
BR112015009121A2 (pt) 2012-10-26 2017-07-04 Micromidas Inc métodos para produzir 5-(halometil)furfural
MY193787A (en) 2013-03-14 2022-10-27 Micromidas Inc Solid forms of 5-(halomethyl) furfural and methods for preparing thereof
KR102247145B1 (ko) 2013-03-14 2021-05-04 마이크로마이다스, 인코포레이티드 5-(할로메틸)푸르푸랄의 정제 방법
ES2932619T3 (es) 2013-09-20 2023-01-23 Origin Mat Operating Inc Métodos para producir 5-(halometil)furfural
EP3498699A1 (en) 2017-12-13 2019-06-19 Basf Se Chromatography method for the purification of furfural derivatives
EP3740662B1 (en) 2018-01-19 2023-08-16 Qmaxx Products Group, Inc. Metal cleaning compositions comprising furoate esters and uses therefor
KR102660275B1 (ko) * 2018-01-31 2024-04-23 퓨라닉스 테크놀러지스 비.브이. 고상 리그노셀룰로오스 물질의 전환 방법
US11332454B2 (en) 2018-01-31 2022-05-17 Furanix Technologies B.V. Process for the conversion of a solid lignocellulosic material
EP3840746A1 (en) 2018-08-23 2021-06-30 Novartis AG New pharmaceutical use for the treatment of heart failure
WO2020039394A1 (en) 2018-08-24 2020-02-27 Novartis Ag New drug combinations
BR112022018316A2 (pt) 2020-04-17 2022-10-25 Dow Global Technologies Llc Formulação agrícola
MX2024010807A (es) * 2022-03-04 2024-09-11 Avantium Knowledge Centre Bv Metodo de extraccion de 5-clorometilfurfural con un disolvente organico de fibras celulosicas y fibras no celulosicas artificiales hidrolizadas en conjunto con acido clorhidrico.

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4154744A (en) * 1976-10-12 1979-05-15 Sumitomo Chemical Company, Limited Process for producing a furan derivative
US4335049A (en) * 1980-07-16 1982-06-15 Sumitomo Chemical Company, Limited Process for producing 5-methylfurfural
DE3842825A1 (de) * 1988-01-08 1989-07-20 Krupp Gmbh Verfahren und vorrichtung zur herstellung von furfural
US7829732B2 (en) * 2008-03-17 2010-11-09 Regents Of The University Of California High-yield conversion of cellulosic biomass into furanic biofuels and value-added products
CA2864086C (en) * 2011-02-28 2018-07-10 Midori Renewables, Inc. Polymeric acid catalysts and uses thereof

Also Published As

Publication number Publication date
US9102644B2 (en) 2015-08-11
EP2909187A4 (en) 2016-05-11
CA2888298A1 (en) 2014-04-24
PH12015500818A1 (en) 2015-06-08
IN2015DN03835A (https=) 2015-10-02
EP2909187A2 (en) 2015-08-26
MX2015004716A (es) 2016-08-17
BR112015008477A2 (pt) 2017-07-04
WO2014062303A3 (en) 2015-07-16
WO2014062303A2 (en) 2014-04-24
MX363821B (es) 2019-04-04
CA2888298C (en) 2022-05-31
SG11201502939WA (en) 2015-05-28
US20140187802A1 (en) 2014-07-03
CN105102440A (zh) 2015-11-25

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Legal Events

Date Code Title Description
B06U Preliminary requirement: requests with searches performed by other patent offices: procedure suspended [chapter 6.21 patent gazette]
B06A Patent application procedure suspended [chapter 6.1 patent gazette]
B09A Decision: intention to grant [chapter 9.1 patent gazette]
B16A Patent or certificate of addition of invention granted [chapter 16.1 patent gazette]

Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 03/09/2013, OBSERVADAS AS CONDICOES LEGAIS.

B25C Requirement related to requested transfer of rights

Owner name: XF TECHNOLOGIES INC. (US)

Free format text: A FIM DE ATENDER A TRANSFERENCIA, REQUERIDA ATRAVES DA PETICAO NO 870240090206 DE 22/10/2024, E NECESSARIO APRESENTAR DOCUMENTO NOTARIZADO E COM APOSTILAMENTO OU LEGALIZACAO CONSULAR. ALEM DISSO, E PRECISO APRESENTAR A GUIA DE CUMPRIMENTO DE EXIGENCIA.

B25A Requested transfer of rights approved

Owner name: XF BIOSOLUTIONS LLC (US)