BR112012029753B8 - método para absorver líquidos hidrofóbicos, e, uso de uma espuma de poliuretano - Google Patents

método para absorver líquidos hidrofóbicos, e, uso de uma espuma de poliuretano Download PDF

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Publication number
BR112012029753B8
BR112012029753B8 BR112012029753A BR112012029753A BR112012029753B8 BR 112012029753 B8 BR112012029753 B8 BR 112012029753B8 BR 112012029753 A BR112012029753 A BR 112012029753A BR 112012029753 A BR112012029753 A BR 112012029753A BR 112012029753 B8 BR112012029753 B8 BR 112012029753B8
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BR
Brazil
Prior art keywords
polyurethane foam
hydrophobic liquids
absorbing hydrophobic
absorbing
oil
Prior art date
Application number
BR112012029753A
Other languages
English (en)
Portuguese (pt)
Other versions
BR112012029753A2 (pt
BR112012029753B1 (pt
Inventor
Cristadoro Anna
Van Der Net Antje
Bruchmann Bernd
Leberfinger Marcus
Mohmeyer Nils
Fritz Ralf
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Se filed Critical Basf Se
Publication of BR112012029753A2 publication Critical patent/BR112012029753A2/pt
Publication of BR112012029753B1 publication Critical patent/BR112012029753B1/pt
Publication of BR112012029753B8 publication Critical patent/BR112012029753B8/pt

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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/42—Polycondensates having carboxylic or carbonic ester groups in the main chain
    • C08G18/4236—Polycondensates having carboxylic or carbonic ester groups in the main chain containing only aliphatic groups
    • C08G18/4238—Polycondensates having carboxylic or carbonic ester groups in the main chain containing only aliphatic groups derived from dicarboxylic acids and dialcohols
    • C08G18/4241—Polycondensates having carboxylic or carbonic ester groups in the main chain containing only aliphatic groups derived from dicarboxylic acids and dialcohols from dicarboxylic acids and dialcohols in combination with polycarboxylic acids and/or polyhydroxy compounds which are at least trifunctional
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/22—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising organic material
    • B01J20/26—Synthetic macromolecular compounds
    • B01J20/264—Synthetic macromolecular compounds derived from different types of monomers, e.g. linear or branched copolymers, block copolymers, graft copolymers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28002—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their physical properties
    • B01J20/28011—Other properties, e.g. density, crush strength
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28014—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
    • B01J20/28042—Shaped bodies; Monolithic structures
    • B01J20/28045—Honeycomb or cellular structures; Solid foams or sponges
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/28—Treatment of water, waste water, or sewage by sorption
    • C02F1/285—Treatment of water, waste water, or sewage by sorption using synthetic organic sorbents
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/68—Treatment of water, waste water, or sewage by addition of specified substances, e.g. trace elements, for ameliorating potable water
    • C02F1/681—Treatment of water, waste water, or sewage by addition of specified substances, e.g. trace elements, for ameliorating potable water by addition of solid materials for removing an oily layer on water
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/4009—Two or more macromolecular compounds not provided for in one single group of groups C08G18/42 - C08G18/64
    • C08G18/4072—Mixtures of compounds of group C08G18/63 with other macromolecular compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/42—Polycondensates having carboxylic or carbonic ester groups in the main chain
    • C08G18/4202—Two or more polyesters of different physical or chemical nature
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/42—Polycondensates having carboxylic or carbonic ester groups in the main chain
    • C08G18/4244—Polycondensates having carboxylic or carbonic ester groups in the main chain containing oxygen in the form of ether groups
    • C08G18/4247—Polycondensates having carboxylic or carbonic ester groups in the main chain containing oxygen in the form of ether groups derived from polyols containing at least one ether group and polycarboxylic acids
    • C08G18/4252—Polycondensates having carboxylic or carbonic ester groups in the main chain containing oxygen in the form of ether groups derived from polyols containing at least one ether group and polycarboxylic acids derived from polyols containing polyether groups and polycarboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/42—Polycondensates having carboxylic or carbonic ester groups in the main chain
    • C08G18/44—Polycarbonates
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/63—Block or graft polymers obtained by polymerising compounds having carbon-to-carbon double bonds on to polymers
    • C08G18/632—Block or graft polymers obtained by polymerising compounds having carbon-to-carbon double bonds on to polymers onto polyethers
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K3/00—Materials not provided for elsewhere
    • C09K3/32—Materials not provided for elsewhere for absorbing liquids to remove pollution, e.g. oil, gasoline, fat
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2101/00—Nature of the contaminant
    • C02F2101/30—Organic compounds
    • C02F2101/32—Hydrocarbons, e.g. oil
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2103/00—Nature of the water, waste water, sewage or sludge to be treated
    • C02F2103/007—Contaminated open waterways, rivers, lakes or ponds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2110/00—Foam properties
    • C08G2110/0008—Foam properties flexible
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2110/00—Foam properties
    • C08G2110/0033—Foam properties having integral skins
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2110/00—Foam properties
    • C08G2110/0041—Foam properties having specified density
    • C08G2110/0058—≥50 and <150kg/m3
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2110/00—Foam properties
    • C08G2110/0041—Foam properties having specified density
    • C08G2110/0066—≥ 150kg/m3
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2110/00—Foam properties
    • C08G2110/0083—Foam properties prepared using water as the sole blowing agent
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A20/00—Water conservation; Efficient water supply; Efficient water use
    • Y02A20/20—Controlling water pollution; Waste water treatment
    • Y02A20/204—Keeping clear the surface of open water from oil spills

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Engineering & Computer Science (AREA)
  • Analytical Chemistry (AREA)
  • Environmental & Geological Engineering (AREA)
  • Hydrology & Water Resources (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Water Supply & Treatment (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Public Health (AREA)
  • Materials Engineering (AREA)
  • Polyurethanes Or Polyureas (AREA)
  • Manufacture Of Porous Articles, And Recovery And Treatment Of Waste Products (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
BR112012029753A 2010-05-27 2011-05-18 método para absorver líquidos hidrofóbicos, e, uso de uma espuma de poliuretano BR112012029753B8 (pt)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP10164188A EP2390275A1 (de) 2010-05-27 2010-05-27 Ölaufnehmende Polyurethanschwämme mit guten mechanischen Eigenschaften
PCT/EP2011/058051 WO2011147724A1 (de) 2010-05-27 2011-05-18 Ölaufnehmende polyurethanschwämme mit guten mechanischen eigenschaften

Publications (3)

Publication Number Publication Date
BR112012029753A2 BR112012029753A2 (pt) 2017-03-07
BR112012029753B1 BR112012029753B1 (pt) 2020-04-22
BR112012029753B8 true BR112012029753B8 (pt) 2020-05-12

Family

ID=42557258

Family Applications (1)

Application Number Title Priority Date Filing Date
BR112012029753A BR112012029753B8 (pt) 2010-05-27 2011-05-18 método para absorver líquidos hidrofóbicos, e, uso de uma espuma de poliuretano

Country Status (10)

Country Link
EP (2) EP2390275A1 (https=)
JP (1) JP6338372B2 (https=)
KR (1) KR101844092B1 (https=)
CN (1) CN102906145B (https=)
AU (1) AU2011257432B2 (https=)
BR (1) BR112012029753B8 (https=)
CA (1) CA2799130C (https=)
MX (1) MX2012013514A (https=)
MY (1) MY160512A (https=)
WO (1) WO2011147724A1 (https=)

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US8987357B2 (en) 2011-05-27 2015-03-24 Basf Se Thermoplastic molding composition
WO2015041158A1 (ja) * 2013-09-20 2015-03-26 三菱瓦斯化学株式会社 油吸着材として使用できるポリカーボネート樹脂
KR101645117B1 (ko) * 2015-01-02 2016-08-12 한국가스공사 경질 우레탄 폼 제조용 조성물 및 이의 제조 방법
ES2861314T3 (es) * 2015-02-26 2021-10-06 Test 1 S R L Elemento absorbente, ensamblaje y procedimiento de fabricación
CN105131233B (zh) * 2015-07-21 2017-10-10 浙江川洋家居股份有限公司 一种聚酯改性海绵及其制备方法
CN106925238B (zh) * 2017-04-10 2019-04-09 福州大学 一种海绵负载型有机溶剂吸收剂及其制备方法
CN108727193B (zh) * 2017-04-24 2021-03-16 中国石油化工股份有限公司 碳酸二苯酯类化合物的制备方法
CN107892759A (zh) * 2017-10-19 2018-04-10 苏州无为环境科技有限公司 一种脂肪酸修饰的超疏水聚氨酯泡沫吸油材料的制备方法
CN108587122A (zh) * 2018-03-23 2018-09-28 长沙小新新能源科技有限公司 一种高吸油高回弹海绵及其制备方法
CN113308899B (zh) * 2021-05-26 2022-05-06 东华大学 一种表面上浆后的碳纤维及其制备方法和应用
KR102841094B1 (ko) * 2022-11-11 2025-07-31 한국과학기술연구원 유흡착재
CN116042129B (zh) * 2022-12-15 2023-12-26 上海兰庆新材料技术股份有限公司 一种丙烯酸酯基uv光固化保护膜及其制备方法
CN118206800B (zh) * 2024-04-17 2024-10-18 扬州三江环安设备有限公司 一种吸油性聚氨酯泡沫材料及其制备方法
KR102776718B1 (ko) 2024-06-27 2025-03-06 문기배 실리카겔을 이용한 친환경적인 스펀지의 제조방법
KR102776714B1 (ko) 2024-06-27 2025-03-06 문기배 친환경적인 스펀지의 제조방법

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US3523093A (en) 1961-11-28 1970-08-04 Paul Stamberger Method of producing polyurethanes by reacting polyisocyanate with a preformed polymer resulting from polymerization of ethylenically unsaturated monomers
US3304273A (en) 1963-02-06 1967-02-14 Stamberger Paul Method of preparing polyurethanes from liquid, stable, reactive, filmforming polymer/polyol mixtures formed by polymerizing an ethylenically unsaturated monomer in a polyol
GB1022434A (en) 1961-11-28 1966-03-16 Union Carbide Corp Improvements in and relating to polymers
DE1152536B (de) 1962-03-30 1963-08-08 Bayer Ag Verfahren zur Herstellung Urethangruppen enthaltender Schaumstoffe
DE1152537B (de) 1962-06-02 1963-08-08 Bayer Ag Verfahren zur Herstellung von homogenen, Urethangruppen aufweisenden Kunststoffen
DE2738268A1 (de) 1977-08-25 1979-03-08 Basf Ag Hydrophobe polyurethanschaumstoffe zur oelabsorption
DE3405875A1 (de) 1984-02-18 1985-08-22 Basf Ag, 6700 Ludwigshafen Verfahren zur herstellung von zelligen oder kompakten polyurethan-polyharnstoff-formkoerpern mit verbesserten entformungseigenschaften sowie innere formtrennmittel fuer das polyisocyanat-polyadditionsverfahren
DE3607447A1 (de) 1986-03-07 1987-09-10 Basf Ag Verfahren zur herstellung von formkoerpern mit einem zelligen kern und einer verdichteten randzone mit verbesserten entformungseigenschaften
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JP4526036B2 (ja) 2006-08-17 2010-08-18 株式会社タイトー カードゲーム装置用のカードテーブル及びそのカードテーブルを具備したカードゲーム装置
EP1911781A1 (en) * 2006-10-12 2008-04-16 Arizona Chemical Company Oil absorbing foam
EP2099841B1 (de) 2006-12-11 2011-02-23 Basf Se Hochelastische polyurethanweichschaumstoffe
JP5649981B2 (ja) 2008-03-14 2015-01-07 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ 粗い気泡のポリウレタンエラストマー

Also Published As

Publication number Publication date
EP2576651A1 (de) 2013-04-10
WO2011147724A1 (de) 2011-12-01
BR112012029753A2 (pt) 2017-03-07
JP2013530270A (ja) 2013-07-25
EP2390275A1 (de) 2011-11-30
KR101844092B1 (ko) 2018-03-30
MX2012013514A (es) 2013-01-24
CA2799130C (en) 2019-10-15
CN102906145A (zh) 2013-01-30
CA2799130A1 (en) 2011-12-01
BR112012029753B1 (pt) 2020-04-22
EP2576651B1 (de) 2014-08-13
CN102906145B (zh) 2015-06-24
KR20130109979A (ko) 2013-10-08
AU2011257432B2 (en) 2015-02-26
AU2011257432A1 (en) 2012-12-13
JP6338372B2 (ja) 2018-06-06
MY160512A (en) 2017-03-15

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