BR0111347B1 - processo de purificaÇço de lactamas e instalaÇço para a realizaÇço de um processo de purificaÇço de lactamas. - Google Patents

processo de purificaÇço de lactamas e instalaÇço para a realizaÇço de um processo de purificaÇço de lactamas.

Info

Publication number
BR0111347B1
BR0111347B1 BRPI0111347-0A BR0111347A BR0111347B1 BR 0111347 B1 BR0111347 B1 BR 0111347B1 BR 0111347 A BR0111347 A BR 0111347A BR 0111347 B1 BR0111347 B1 BR 0111347B1
Authority
BR
Brazil
Prior art keywords
purification process
lactam
lactam purification
installation
carrying
Prior art date
Application number
BRPI0111347-0A
Other languages
English (en)
Other versions
BR0111347A (pt
Inventor
Daniel Amoros
Phillipe Leconte
Pierre Coqueret
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed filed Critical
Publication of BR0111347A publication Critical patent/BR0111347A/pt
Publication of BR0111347B1 publication Critical patent/BR0111347B1/pt

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
    • C07D201/16—Separation or purification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
    • C07D201/02—Preparation of lactams
    • C07D201/08—Preparation of lactams from carboxylic acids or derivatives thereof, e.g. hydroxy carboxylic acids, lactones or nitriles
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S203/00—Distillation: processes, separatory
    • Y10S203/90—Particular type of heating

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Other In-Based Heterocyclic Compounds (AREA)
  • Indole Compounds (AREA)
BRPI0111347-0A 2000-05-26 2001-05-28 processo de purificaÇço de lactamas e instalaÇço para a realizaÇço de um processo de purificaÇço de lactamas. BR0111347B1 (pt)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR0006784A FR2809395B1 (fr) 2000-05-26 2000-05-26 Procede de purification de lactames
PCT/FR2001/001644 WO2001090065A1 (fr) 2000-05-26 2001-05-28 Procede de purification de lactames

Publications (2)

Publication Number Publication Date
BR0111347A BR0111347A (pt) 2003-04-29
BR0111347B1 true BR0111347B1 (pt) 2013-02-19

Family

ID=8850676

Family Applications (1)

Application Number Title Priority Date Filing Date
BRPI0111347-0A BR0111347B1 (pt) 2000-05-26 2001-05-28 processo de purificaÇço de lactamas e instalaÇço para a realizaÇço de um processo de purificaÇço de lactamas.

Country Status (19)

Country Link
US (2) US7384518B2 (pt)
EP (2) EP1903032B1 (pt)
JP (1) JP4234928B2 (pt)
KR (1) KR100546988B1 (pt)
CN (1) CN100372835C (pt)
AR (1) AR028636A1 (pt)
AT (1) ATE516267T1 (pt)
AU (1) AU2001274137A1 (pt)
BR (1) BR0111347B1 (pt)
CA (1) CA2409984A1 (pt)
FR (1) FR2809395B1 (pt)
HU (1) HUP0302039A2 (pt)
MX (1) MXPA02011471A (pt)
PL (1) PL359094A1 (pt)
RU (1) RU2230059C1 (pt)
SK (1) SK16592002A3 (pt)
TW (1) TWI286543B (pt)
UA (1) UA75358C2 (pt)
WO (1) WO2001090065A1 (pt)

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP3667140B2 (ja) * 1999-03-04 2005-07-06 パイオニア株式会社 ディスクチェンジャ装置
KR20040031007A (ko) † 2001-08-27 2004-04-09 디에스엠 아이피 어셋츠 비.브이. 감압하 알칼리 카프로락탐 생성물의 증류 방법
DE10253094A1 (de) * 2002-11-13 2004-05-27 Basf Ag Verfahren zur Reinigung von Caprolactam
RU2458052C1 (ru) * 2011-04-15 2012-08-10 Открытое акционерное общество "КуйбышевАзот" Способ управления процессом дистилляции капролактама
EP2602276B1 (de) * 2011-12-08 2015-07-29 PE Polymer Engineering Plant Construction GmbH Verfahren und Vorrichtung zur Aufbereitung von hoch wasserhaltigem Recyclingcaprolactam bei der kontinuierlichen Herstellung von Polyamid 6
KR101573569B1 (ko) * 2012-12-27 2015-12-01 롯데케미칼 주식회사 분리막 세정 시스템 및 이를 이용한 분리막 세정 방법
DE102013107238A1 (de) * 2013-07-09 2015-01-15 L'Air Liquide, Société Anonyme pour l'Etude et l'Exploitation des Procédés Georges Claude Verfahren zur Rückgewinnung von Epsilon-Caprolactam aus Extraktwasser
KR102551766B1 (ko) * 2017-12-28 2023-07-06 한화솔루션 주식회사 라우로락탐의 정제 방법 및 이의 정제 장치
CN111747878A (zh) * 2020-07-14 2020-10-09 中国石油化工股份有限公司 一种己内酰胺减压蒸馏新方法
CN111848515A (zh) * 2020-07-14 2020-10-30 中国石油化工股份有限公司 一种己内酰胺产品的新型精馏方法
CN114478343A (zh) * 2022-02-24 2022-05-13 江苏扬农化工集团有限公司 己内酰胺的精制提纯方法

Family Cites Families (38)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE226561C (pt)
DE226560C (pt)
DE152914C (pt)
DE267729C (pt)
DE226562C (pt)
US2208598A (en) 1938-09-24 1940-07-23 Du Pont Aliphatic amino-nitriles and process of producing them
US2357484A (en) 1941-09-12 1944-09-05 Du Pont Process for producing compounds containing an n-substituted amide group
US2762835A (en) 1953-03-12 1956-09-11 Celanese Corp Preparation of amino nitriles
JPS4821958B1 (pt) 1969-01-28 1973-07-02
US3931308A (en) * 1973-06-07 1976-01-06 Allied Chemical Corporation Process for conversion of lysine dihydrochloride to lysine monohydrochloride
DE2920436A1 (de) * 1979-05-19 1980-12-04 Bayer Ag Verfahren zur herstellung von epsilon -caprolacton
DE2926279A1 (de) * 1979-06-29 1981-01-08 Basf Ag Verfahren zur reinigung von caprolactam
IT8020902A0 (it) * 1980-03-25 1980-03-25 Snia Viscosa Procedimento ed apparecchiatura per la separazione continua per via termica di miscele liquide dicomposti termolabili.
DD152914A1 (de) * 1980-09-05 1981-12-16 Wolfgang Gruendel Verfahren zum destillativen reinigen von caprolactam
NL8102280A (nl) * 1981-05-09 1982-12-01 Stamicarbon Werkwijze voor het zuiveren van epsilon-caprolactam.
US4720328A (en) * 1981-06-26 1988-01-19 Akzona Incorporated Method for removing impurities from caprolactam
US4767503A (en) * 1983-08-29 1988-08-30 Allied Corporation Removal of light impurities from caprolactam by distillation with water
US4601859A (en) 1984-05-04 1986-07-22 Allied Corporation Selective hydrogenation of aliphatic dinitriles to omega-aminonitriles in ammonia with supported, finely dispersed rhodium-containing catalyst
DD226560A1 (de) * 1984-09-07 1985-08-28 Leuna Werke Veb Verfahren zum reinigen von caprolactam
DD226561A1 (de) * 1984-09-07 1985-08-28 Leuna Werke Veb Verfahren zur reinigung von caprolactam
DD226562A1 (de) * 1984-09-07 1985-08-28 Leuna Werke Veb Verfahren zur destillativen und rektifikativen reinigung von caprolactam
DE3729853A1 (de) * 1987-09-05 1989-03-23 Basf Ag Verfahren zur aufarbeitung von destillationsrueckstaenden, die bei der reinigung von caprolactam anfallen
DE3735054A1 (de) 1987-10-16 1989-04-27 Basf Ag Verfahren zur gewinnung von caprolactam aus leichtsiedern oder schwersiedern der caprolactamdestillation oder gemischen derselben
DD267729A1 (de) * 1987-12-03 1989-05-10 Leuna Werke Veb Verfahren zur aufarbeitung von reaktionsgemischen aus der synthese von n-methyl-epsilon-caprolactam
GB9012453D0 (en) * 1990-06-05 1990-07-25 Ucb Sa Process for the manufacture of n-phenylmaleimide
US5241066A (en) * 1992-06-25 1993-08-31 Basf Corporation Method of recovering caprolactam from mixed waste
DE4235466A1 (de) 1992-10-21 1994-04-28 Bayer Ag Verfahren zur Herstellung von (cyclo)aliphatischen Aminonitrilen
US5458740A (en) * 1994-03-04 1995-10-17 Basf Corporation Process for the purification of crude caprolactam
DE4407222A1 (de) * 1994-03-04 1995-09-07 Basf Ag Verfahren zur Rückgewinnung von Caprolactam aus Oliogo- und/oder Polymeren des Caprolactams
DE4443125A1 (de) * 1994-12-03 1996-06-05 Basf Ag Verfahren zur Herstellung von Caprolactam
FR2728259B1 (fr) 1994-12-14 1997-03-14 Rhone Poulenc Chimie Procede d'hemihydrogenation de dinitriles en aminonitriles
DE19500041A1 (de) 1995-01-03 1996-07-04 Basf Ag Verfahren zur kontinuierlichen Reinigung von aus 6-Aminocapronitril hergestelltem Roh-Caprolactam
DE19548289A1 (de) * 1995-12-22 1997-06-26 Basf Ag Verfahren zur gleichzeitigen Herstellung von Caprolactam und Hexamethylendiamin
FR2751962B1 (fr) * 1996-08-02 1998-09-11 Rhone Poulenc Fibres Procede de purification de lactames
US5990306A (en) * 1997-09-03 1999-11-23 Alliedsignal Inc. Process for the purification of caprolactam obtained from the depolymerization of polyamide-containing carpet
CN1210851A (zh) * 1997-09-08 1999-03-17 中国科学院成都有机化学研究所 一种提纯乙酸乙酯的方法
FR2781796B1 (fr) * 1998-07-28 2000-09-22 Rhone Poulenc Fibres Procede de deshydratation de lactame
DE10029187A1 (de) * 2000-06-19 2001-12-20 Basf Ag Verfahren zur Abtrennung von 6-Aminocapronitril aus Gemischen, die 6-Aminocapronitril, Adipodinitril und Hexamethylendiamin enthalten

Also Published As

Publication number Publication date
US20040014965A1 (en) 2004-01-22
ATE516267T1 (de) 2011-07-15
UA75358C2 (en) 2006-04-17
EP1903032A1 (fr) 2008-03-26
JP2003534321A (ja) 2003-11-18
US7384518B2 (en) 2008-06-10
HUP0302039A2 (hu) 2003-09-29
US20080230368A1 (en) 2008-09-25
EP1903032B1 (fr) 2013-08-14
US8231765B2 (en) 2012-07-31
EP1289948A1 (fr) 2003-03-12
CA2409984A1 (fr) 2001-11-29
SK16592002A3 (sk) 2003-07-01
JP4234928B2 (ja) 2009-03-04
CN1437582A (zh) 2003-08-20
KR100546988B1 (ko) 2006-01-26
WO2001090065A1 (fr) 2001-11-29
BR0111347A (pt) 2003-04-29
TWI286543B (en) 2007-09-11
FR2809395A1 (fr) 2001-11-30
PL359094A1 (en) 2004-08-23
AU2001274137A1 (en) 2001-12-03
MXPA02011471A (es) 2004-01-26
FR2809395B1 (fr) 2002-07-19
AR028636A1 (es) 2003-05-21
KR20030013430A (ko) 2003-02-14
EP1289948B1 (fr) 2011-07-13
CN100372835C (zh) 2008-03-05
RU2230059C1 (ru) 2004-06-10

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Legal Events

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B07A Application suspended after technical examination (opinion) [chapter 7.1 patent gazette]
B15V Prolongation of time limit allowed

Free format text: RECONHECIDO O OBSTACULO ADMINISTRATIVO E DEVOLVIDO O PRAZO DE 25 DIAS PARA MANIFESTACAO A CIENCIA DE PARECER, NOS TERMOS DO ARTIGO 221 PARAGRAFO 2O DA LPI E DA RESOLUCAO 116/04.

B06A Patent application procedure suspended [chapter 6.1 patent gazette]
B15V Prolongation of time limit allowed

Free format text: ATENDENDO O SOLICITADO NA PETICAO NO 018110041832 DE 27/10/2011 / DESP RECONHECEMOS A JUSTA CAUSA, CONCEDENDO O PRAZO DE 67 (SESSENTA E SETE) DIAS CONTADOS A PARTIR DA DATA DE PUBLICACAO NA RPI.

B09A Decision: intention to grant [chapter 9.1 patent gazette]
B16A Patent or certificate of addition of invention granted [chapter 16.1 patent gazette]

Free format text: PRAZO DE VALIDADE: 10 (DEZ) ANOS CONTADOS A PARTIR DE 19/02/2013, OBSERVADAS AS CONDICOES LEGAIS.

B21F Lapse acc. art. 78, item iv - on non-payment of the annual fees in time
B24J Lapse because of non-payment of annual fees (definitively: art 78 iv lpi, resolution 113/2013 art. 12)

Free format text: EM VIRTUDE DA EXTINCAO PUBLICADA NA RPI 2465 DE 03-04-2018 E CONSIDERANDO AUSENCIA DE MANIFESTACAO DENTRO DOS PRAZOS LEGAIS, INFORMO QUE CABE SER MANTIDA A EXTINCAO DA PATENTE E SEUS CERTIFICADOS, CONFORME O DISPOSTO NO ARTIGO 12, DA RESOLUCAO 113/2013.