BR0015879A - Processo para preparação de tensoativos catiÈnicos - Google Patents
Processo para preparação de tensoativos catiÈnicosInfo
- Publication number
- BR0015879A BR0015879A BR0015879-8A BR0015879A BR0015879A BR 0015879 A BR0015879 A BR 0015879A BR 0015879 A BR0015879 A BR 0015879A BR 0015879 A BR0015879 A BR 0015879A
- Authority
- BR
- Brazil
- Prior art keywords
- acid
- cationic surfactants
- condensation
- amino acids
- preparing cationic
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C231/00—Preparation of carboxylic acid amides
- C07C231/02—Preparation of carboxylic acid amides from carboxylic acids or from esters, anhydrides, or halides thereof by reaction with ammonia or amines
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C277/00—Preparation of guanidine or its derivatives, i.e. compounds containing the group, the singly-bound nitrogen atoms not being part of nitro or nitroso groups
- C07C277/08—Preparation of guanidine or its derivatives, i.e. compounds containing the group, the singly-bound nitrogen atoms not being part of nitro or nitroso groups of substituted guanidines
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Cosmetics (AREA)
- Medicinal Preparation (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
"PROCESSO PARA PREPARAçãO DE TENSOATIVOS CATIÈNICOS". A presente invenção refere-se à preparação de tensoativos catiónicos derivados da condensação de um ácido, preferencialmente um ácido graxo ou um hidroxiácido, com um número de 8-14 átomos de carbono, com aminoácidos esterificados, preferencialmente aminoácidos de grau básico, mais preferencialmente (L)-arginina. O método compreende uma primeira etapa em que é realizada a esterificação do aminoácido com um álcool e, uma segunda etapa, para a realização da condensação com um cloreto de ácido, preferencialmente cloreto de acila de um ácido graxo ou de um hidroxiácido, em que a segunda etapa é realizada em um ambiente aquoso, com um valor de pH entre 6 e 7, preferencialmente entre 6,7 e 6,9.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
PCT/EP2000/005072 WO2001094292A1 (en) | 2000-06-03 | 2000-06-03 | Process for the preparation of cationic surfactants |
Publications (2)
Publication Number | Publication Date |
---|---|
BR0015879A true BR0015879A (pt) | 2003-04-29 |
BR0015879B1 BR0015879B1 (pt) | 2012-02-22 |
Family
ID=8163970
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BRPI0015879-8A BR0015879B1 (pt) | 2000-06-03 | 2000-06-03 | processo para preparação de tensoativos catiÈnicos. |
Country Status (12)
Country | Link |
---|---|
US (1) | US7087769B1 (pt) |
EP (1) | EP1294678B1 (pt) |
AT (1) | ATE319679T1 (pt) |
AU (1) | AU2000255283A1 (pt) |
BR (1) | BR0015879B1 (pt) |
CA (1) | CA2412344C (pt) |
DE (1) | DE60026525T2 (pt) |
DK (1) | DK1294678T3 (pt) |
ES (1) | ES2256017T3 (pt) |
MX (1) | MXPA02011193A (pt) |
PT (1) | PT1294678E (pt) |
WO (1) | WO2001094292A1 (pt) |
Families Citing this family (29)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US8193244B1 (en) | 2008-05-29 | 2012-06-05 | Nevada Naturals, Inc. | Antimicrobial agents |
US8926997B1 (en) | 2003-02-06 | 2015-01-06 | Richard F. Stockel | Polymeric biocidal salts |
US8795638B1 (en) | 2003-08-26 | 2014-08-05 | Nevada Naturals Inc. | Compositions for dental care |
US20100056628A1 (en) * | 2006-09-07 | 2010-03-04 | Stockel Richard F | Preservative compositions |
US10130830B2 (en) | 2005-08-01 | 2018-11-20 | Laboratorios Miret, S.A. | Preservative systems comprising cationic surfactants |
US9555167B2 (en) | 2006-12-11 | 2017-01-31 | 3M Innovative Properties Company | Biocompatible antimicrobial compositions |
BRPI0722020B1 (pt) | 2007-09-13 | 2016-12-13 | Miret Lab | composição sólida compreendendo natamicina e um tensoativo catiônico (lae), dispersão de natamicina e seu método de preparação, solução aquosa e uso |
US9023891B2 (en) | 2008-05-29 | 2015-05-05 | Nevada Naturals, Inc. | Synergistic antimicrobial agents |
US8933122B2 (en) | 2008-07-02 | 2015-01-13 | Laboratorios Miret, S.A. | Use of cationic surfactants as sporicidal agents |
US20100152480A1 (en) * | 2008-12-16 | 2010-06-17 | Ghare Vishwas Sadhu | Process for synthesis of cationic surfactants |
WO2010084052A2 (en) | 2009-01-22 | 2010-07-29 | Laboratorios Miret, S. A. | Use of cationic surfactants as acaricidal agents |
CH701769A1 (de) | 2009-09-08 | 2011-03-15 | Schoeller Textil Ag | Wiederbeladbare Ausrüstungen für Textilien und Formulierungen zur Beladung solcher Ausrüstungen. |
US8278478B2 (en) * | 2009-09-30 | 2012-10-02 | Vishwas Sadhu Ghare | Process for the synthesis of hydrochloride salt of N-fatty acylsubstituted amino acid ethyl esters |
US9284265B1 (en) | 2009-12-02 | 2016-03-15 | Vishwas Sadhu Ghare | Preparation of organic acid salts of cationic surfactants |
US8212061B1 (en) | 2009-12-02 | 2012-07-03 | Vishwas Sadhu Ghare | Preparation of organic acid salts of cationic surfactants |
AU2011232723B2 (en) | 2010-03-23 | 2014-12-18 | Gojo Industries, Inc. | Antimicrobial compositions |
WO2012013577A1 (en) | 2010-07-26 | 2012-02-02 | Laboratorios Miret, S.A. | Composition for coating medical devices containing lae and a polycationic amphoteric polymer |
WO2012052405A2 (en) | 2010-10-21 | 2012-04-26 | Laboratorios Miret, S.A. | Method for the preparation of cationic surfactants |
US8834857B1 (en) | 2011-01-18 | 2014-09-16 | Nevada Naturals Inc. | Deodorizing and skin cleaning |
ITMI20110545A1 (it) | 2011-04-04 | 2012-10-05 | Lundbeck Pharmaceuticals Italy S P A | Metodo per la preparazione di intermedi di processo per la sintesi di argatroban monoidrato |
IN2014MN01480A (pt) | 2011-12-28 | 2015-04-24 | Eburon Organics Internat Ii Llc | |
CN102976978A (zh) * | 2012-12-26 | 2013-03-20 | 天津天成制药有限公司 | L-精氨酸乙酯盐酸盐的制备方法 |
BR112015030324A2 (pt) | 2013-06-06 | 2017-07-25 | 3M Innovative Properties Co | filme, combinação e método |
CN105061266A (zh) * | 2015-07-17 | 2015-11-18 | 武汉志邦化学技术有限公司 | 一种月桂酰精氨酸乙酯盐酸盐的制备方法 |
CN107400069B (zh) * | 2017-08-01 | 2020-02-21 | 浙江大学 | 一种月桂酰精氨酸乙酯盐酸盐的制备方法 |
CN107814754A (zh) * | 2017-11-16 | 2018-03-20 | 中国日用化学工业研究院 | 一种月桂酰精氨酸乙酯盐酸盐的制备方法 |
CN110668977B (zh) * | 2019-10-25 | 2022-03-18 | 浙江圣达生物研究院有限公司 | 一种月桂酰精氨酸乙酯盐酸盐的制备工艺 |
KR102550765B1 (ko) * | 2020-08-18 | 2023-07-03 | 주식회사 우드워드바이오 | 염기성 아미노산 기반 양이온성 계면활성제의 탈염법 및 결정화 정제 방법 |
US20230151302A1 (en) | 2020-12-08 | 2023-05-18 | Laboratorios Miret, S.A. | Cationic surfactants, in particular ethyl lauroyl arginate LAE, for treating or preventing infections and contaminations with Coronavirus |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2531501B2 (ja) * | 1994-06-03 | 1996-09-04 | 味の素株式会社 | N−クロロアセチルグルタミン酸γ−低級アルキルエステルアンモニウム塩 |
ES2092958B1 (es) * | 1995-01-10 | 1997-08-01 | Miret Lab | Procedimiento para la sintesis de tensioactivos cationicos derivados de la condensacion de acidos grasos con aminoacidos de caracter basico esterificados y su aplicacion como agentes antimicrobianos. |
-
2000
- 2000-06-03 ES ES00940305T patent/ES2256017T3/es not_active Expired - Lifetime
- 2000-06-03 DE DE60026525T patent/DE60026525T2/de not_active Expired - Lifetime
- 2000-06-03 BR BRPI0015879-8A patent/BR0015879B1/pt not_active IP Right Cessation
- 2000-06-03 AU AU2000255283A patent/AU2000255283A1/en not_active Abandoned
- 2000-06-03 AT AT00940305T patent/ATE319679T1/de active
- 2000-06-03 DK DK00940305T patent/DK1294678T3/da active
- 2000-06-03 CA CA002412344A patent/CA2412344C/en not_active Expired - Lifetime
- 2000-06-03 WO PCT/EP2000/005072 patent/WO2001094292A1/en active IP Right Grant
- 2000-06-03 MX MXPA02011193A patent/MXPA02011193A/es active IP Right Grant
- 2000-06-03 PT PT00940305T patent/PT1294678E/pt unknown
- 2000-06-03 US US10/467,780 patent/US7087769B1/en not_active Expired - Lifetime
- 2000-06-03 EP EP00940305A patent/EP1294678B1/en not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
DE60026525T2 (de) | 2006-08-10 |
BR0015879B1 (pt) | 2012-02-22 |
US7087769B1 (en) | 2006-08-08 |
EP1294678B1 (en) | 2006-03-08 |
AU2000255283A1 (en) | 2001-12-17 |
DK1294678T3 (da) | 2006-07-10 |
PT1294678E (pt) | 2006-06-30 |
WO2001094292A1 (en) | 2001-12-13 |
DE60026525D1 (de) | 2006-05-04 |
ATE319679T1 (de) | 2006-03-15 |
ES2256017T3 (es) | 2006-07-16 |
CA2412344A1 (en) | 2001-12-13 |
MXPA02011193A (es) | 2003-03-10 |
CA2412344C (en) | 2008-08-19 |
EP1294678A1 (en) | 2003-03-26 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
B07A | Application suspended after technical examination (opinion) [chapter 7.1 patent gazette] | ||
B09B | Patent application refused [chapter 9.2 patent gazette] |
Free format text: INDEFIRO O PEDIDO DE ACORDO COM O(S) ARTIGO(S) 8O E 11 DA LPI. |
|
B12B | Appeal against refusal [chapter 12.2 patent gazette] | ||
B16A | Patent or certificate of addition of invention granted [chapter 16.1 patent gazette] |
Free format text: PRAZO DE VALIDADE: 10 (DEZ) ANOS CONTADOS A PARTIR DE 22/02/2012, OBSERVADAS AS CONDICOES LEGAIS. |
|
B21A | Patent or certificate of addition expired [chapter 21.1 patent gazette] |
Free format text: PATENTE EXTINTA EM 22.02.2022 |