BE1024606B1 - Verbeterde soldeer en werkwijze voor het produceren van lood met hoge zuiverheid - Google Patents
Verbeterde soldeer en werkwijze voor het produceren van lood met hoge zuiverheid Download PDFInfo
- Publication number
- BE1024606B1 BE1024606B1 BE2017/5681A BE201705681A BE1024606B1 BE 1024606 B1 BE1024606 B1 BE 1024606B1 BE 2017/5681 A BE2017/5681 A BE 2017/5681A BE 201705681 A BE201705681 A BE 201705681A BE 1024606 B1 BE1024606 B1 BE 1024606B1
- Authority
- BE
- Belgium
- Prior art keywords
- metal
- lead
- ppm
- metal mixture
- present
- Prior art date
Links
- 238000004519 manufacturing process Methods 0.000 title description 16
- 229910052751 metal Inorganic materials 0.000 claims abstract description 304
- 239000002184 metal Substances 0.000 claims abstract description 303
- 239000000203 mixture Substances 0.000 claims abstract description 199
- 238000000034 method Methods 0.000 claims abstract description 165
- 239000010949 copper Substances 0.000 claims abstract description 138
- 229910052802 copper Inorganic materials 0.000 claims abstract description 111
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims abstract description 104
- 229910052718 tin Inorganic materials 0.000 claims abstract description 97
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 claims abstract description 96
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims abstract description 84
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims abstract description 62
- 229910052787 antimony Inorganic materials 0.000 claims abstract description 42
- WATWJIUSRGPENY-UHFFFAOYSA-N antimony atom Chemical compound [Sb] WATWJIUSRGPENY-UHFFFAOYSA-N 0.000 claims abstract description 41
- 229910052782 aluminium Inorganic materials 0.000 claims abstract description 36
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims abstract description 35
- 229910052759 nickel Inorganic materials 0.000 claims abstract description 34
- 239000011651 chromium Substances 0.000 claims abstract description 25
- 239000010936 titanium Substances 0.000 claims abstract description 25
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 claims abstract description 14
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims abstract description 14
- 229910052804 chromium Inorganic materials 0.000 claims abstract description 14
- 229910052719 titanium Inorganic materials 0.000 claims abstract description 14
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 claims abstract description 14
- 229910052721 tungsten Inorganic materials 0.000 claims abstract description 14
- 239000010937 tungsten Substances 0.000 claims abstract description 14
- 238000001704 evaporation Methods 0.000 claims abstract description 12
- LEONUFNNVUYDNQ-UHFFFAOYSA-N vanadium atom Chemical compound [V] LEONUFNNVUYDNQ-UHFFFAOYSA-N 0.000 claims abstract description 12
- 230000008020 evaporation Effects 0.000 claims abstract description 10
- 239000011133 lead Substances 0.000 claims description 162
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims description 97
- 229910052717 sulfur Inorganic materials 0.000 claims description 79
- 239000011593 sulfur Substances 0.000 claims description 77
- 238000004821 distillation Methods 0.000 claims description 64
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 60
- 239000000047 product Substances 0.000 claims description 55
- 239000007788 liquid Substances 0.000 claims description 43
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 claims description 25
- 150000001875 compounds Chemical class 0.000 claims description 24
- 239000011572 manganese Substances 0.000 claims description 24
- 229910052709 silver Inorganic materials 0.000 claims description 24
- 239000004332 silver Substances 0.000 claims description 24
- 150000001342 alkaline earth metals Chemical class 0.000 claims description 19
- 239000007787 solid Substances 0.000 claims description 19
- 229910052783 alkali metal Inorganic materials 0.000 claims description 18
- 150000001340 alkali metals Chemical class 0.000 claims description 18
- 229910052784 alkaline earth metal Inorganic materials 0.000 claims description 18
- 238000002844 melting Methods 0.000 claims description 17
- 230000008018 melting Effects 0.000 claims description 17
- 239000006228 supernatant Substances 0.000 claims description 17
- 229910052785 arsenic Inorganic materials 0.000 claims description 13
- RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic atom Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 claims description 13
- JBQYATWDVHIOAR-UHFFFAOYSA-N tellanylidenegermanium Chemical compound [Te]=[Ge] JBQYATWDVHIOAR-UHFFFAOYSA-N 0.000 claims description 13
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 claims description 12
- 229910052748 manganese Inorganic materials 0.000 claims description 12
- 229910052738 indium Inorganic materials 0.000 claims description 11
- APFVFJFRJDLVQX-UHFFFAOYSA-N indium atom Chemical compound [In] APFVFJFRJDLVQX-UHFFFAOYSA-N 0.000 claims description 11
- 229910052797 bismuth Inorganic materials 0.000 claims description 10
- 230000005484 gravity Effects 0.000 claims description 10
- JCXGWMGPZLAOME-UHFFFAOYSA-N bismuth atom Chemical compound [Bi] JCXGWMGPZLAOME-UHFFFAOYSA-N 0.000 claims description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 claims description 8
- 238000004590 computer program Methods 0.000 claims description 7
- 229910052710 silicon Inorganic materials 0.000 claims description 6
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 5
- 229910052760 oxygen Inorganic materials 0.000 claims description 5
- 239000001301 oxygen Substances 0.000 claims description 5
- 239000010703 silicon Substances 0.000 claims description 5
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 3
- 238000002203 pretreatment Methods 0.000 claims description 3
- 230000001419 dependent effect Effects 0.000 claims 1
- 238000005292 vacuum distillation Methods 0.000 abstract description 78
- 239000011701 zinc Substances 0.000 abstract description 36
- 229910052725 zinc Inorganic materials 0.000 abstract description 29
- 229910052742 iron Inorganic materials 0.000 abstract description 25
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 abstract description 24
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 abstract description 3
- 229910052720 vanadium Inorganic materials 0.000 abstract description 3
- 229910000679 solder Inorganic materials 0.000 description 87
- 150000002739 metals Chemical class 0.000 description 73
- 230000008569 process Effects 0.000 description 64
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- 238000011144 upstream manufacturing Methods 0.000 description 37
- 239000012071 phase Substances 0.000 description 36
- 230000008901 benefit Effects 0.000 description 34
- 239000006227 byproduct Substances 0.000 description 34
- 239000000126 substance Substances 0.000 description 32
- 239000002994 raw material Substances 0.000 description 30
- 238000011084 recovery Methods 0.000 description 30
- 229910001338 liquidmetal Inorganic materials 0.000 description 28
- 238000001816 cooling Methods 0.000 description 23
- -1 ferrous metals Chemical class 0.000 description 23
- 239000000463 material Substances 0.000 description 21
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 20
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 20
- 230000015572 biosynthetic process Effects 0.000 description 17
- 238000004140 cleaning Methods 0.000 description 15
- 230000002829 reductive effect Effects 0.000 description 15
- 239000002893 slag Substances 0.000 description 14
- 229910052739 hydrogen Inorganic materials 0.000 description 13
- 239000001257 hydrogen Substances 0.000 description 13
- 239000010970 precious metal Substances 0.000 description 13
- 238000000926 separation method Methods 0.000 description 13
- 238000009853 pyrometallurgy Methods 0.000 description 11
- OMZSGWSJDCOLKM-UHFFFAOYSA-N copper(II) sulfide Chemical compound [S-2].[Cu+2] OMZSGWSJDCOLKM-UHFFFAOYSA-N 0.000 description 10
- 238000001514 detection method Methods 0.000 description 9
- 238000006722 reduction reaction Methods 0.000 description 8
- 238000007670 refining Methods 0.000 description 8
- 239000004576 sand Substances 0.000 description 8
- 239000011734 sodium Substances 0.000 description 8
- 238000006243 chemical reaction Methods 0.000 description 7
- 230000000694 effects Effects 0.000 description 7
- 230000002452 interceptive effect Effects 0.000 description 7
- 230000009467 reduction Effects 0.000 description 7
- 206010011906 Death Diseases 0.000 description 6
- 238000001311 chemical methods and process Methods 0.000 description 6
- 239000000428 dust Substances 0.000 description 6
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- 239000008187 granular material Substances 0.000 description 6
- 238000010438 heat treatment Methods 0.000 description 6
- 238000004064 recycling Methods 0.000 description 6
- 239000000377 silicon dioxide Substances 0.000 description 6
- 235000012239 silicon dioxide Nutrition 0.000 description 6
- 239000000243 solution Substances 0.000 description 6
- 238000004458 analytical method Methods 0.000 description 5
- 238000004880 explosion Methods 0.000 description 5
- 239000012535 impurity Substances 0.000 description 5
- 239000007791 liquid phase Substances 0.000 description 5
- 238000012545 processing Methods 0.000 description 5
- 239000000523 sample Substances 0.000 description 5
- 238000005476 soldering Methods 0.000 description 5
- 229910045601 alloy Inorganic materials 0.000 description 4
- 239000000956 alloy Substances 0.000 description 4
- 230000009286 beneficial effect Effects 0.000 description 4
- 238000005219 brazing Methods 0.000 description 4
- 238000011143 downstream manufacturing Methods 0.000 description 4
- 230000000670 limiting effect Effects 0.000 description 4
- 230000003647 oxidation Effects 0.000 description 4
- 238000007254 oxidation reaction Methods 0.000 description 4
- 238000002360 preparation method Methods 0.000 description 4
- GEHJYWRUCIMESM-UHFFFAOYSA-L sodium sulfite Chemical compound [Na+].[Na+].[O-]S([O-])=O GEHJYWRUCIMESM-UHFFFAOYSA-L 0.000 description 4
- CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical compound [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 description 3
- KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 description 3
- 229910000074 antimony hydride Inorganic materials 0.000 description 3
- RBFQJDQYXXHULB-UHFFFAOYSA-N arsane Chemical compound [AsH3] RBFQJDQYXXHULB-UHFFFAOYSA-N 0.000 description 3
- 229910052729 chemical element Inorganic materials 0.000 description 3
- 238000001944 continuous distillation Methods 0.000 description 3
- 230000006378 damage Effects 0.000 description 3
- 239000010931 gold Substances 0.000 description 3
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 3
- 238000000746 purification Methods 0.000 description 3
- 239000007858 starting material Substances 0.000 description 3
- OUULRIDHGPHMNQ-UHFFFAOYSA-N stibane Chemical compound [SbH3] OUULRIDHGPHMNQ-UHFFFAOYSA-N 0.000 description 3
- 239000002699 waste material Substances 0.000 description 3
- ODINCKMPIJJUCX-UHFFFAOYSA-N Calcium oxide Chemical compound [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 description 2
- 229910052774 Proactinium Inorganic materials 0.000 description 2
- 238000003723 Smelting Methods 0.000 description 2
- 230000002411 adverse Effects 0.000 description 2
- 238000001636 atomic emission spectroscopy Methods 0.000 description 2
- 239000002585 base Substances 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 230000015556 catabolic process Effects 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 239000007795 chemical reaction product Substances 0.000 description 2
- 239000000356 contaminant Substances 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 230000003247 decreasing effect Effects 0.000 description 2
- 230000002939 deleterious effect Effects 0.000 description 2
- 230000001627 detrimental effect Effects 0.000 description 2
- 239000003779 heat-resistant material Substances 0.000 description 2
- 230000006872 improvement Effects 0.000 description 2
- 229910052745 lead Inorganic materials 0.000 description 2
- WABPQHHGFIMREM-UHFFFAOYSA-N lead(0) Chemical compound [Pb] WABPQHHGFIMREM-UHFFFAOYSA-N 0.000 description 2
- 238000012423 maintenance Methods 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 150000002736 metal compounds Chemical class 0.000 description 2
- 229910044991 metal oxide Inorganic materials 0.000 description 2
- 150000004706 metal oxides Chemical class 0.000 description 2
- 238000012544 monitoring process Methods 0.000 description 2
- 238000005191 phase separation Methods 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- NIFIFKQPDTWWGU-UHFFFAOYSA-N pyrite Chemical compound [Fe+2].[S-][S-] NIFIFKQPDTWWGU-UHFFFAOYSA-N 0.000 description 2
- 229910052683 pyrite Inorganic materials 0.000 description 2
- 239000011028 pyrite Substances 0.000 description 2
- 239000010948 rhodium Substances 0.000 description 2
- 239000011669 selenium Substances 0.000 description 2
- 150000003376 silicon Chemical class 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 235000010265 sodium sulphite Nutrition 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 239000002341 toxic gas Substances 0.000 description 2
- 230000007704 transition Effects 0.000 description 2
- GPPXJZIENCGNKB-UHFFFAOYSA-N vanadium Chemical compound [V]#[V] GPPXJZIENCGNKB-UHFFFAOYSA-N 0.000 description 2
- 239000012808 vapor phase Substances 0.000 description 2
- 238000004876 x-ray fluorescence Methods 0.000 description 2
- 229910018072 Al 2 O 3 Inorganic materials 0.000 description 1
- 238000012935 Averaging Methods 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 229910017482 Cu 6 Sn 5 Inorganic materials 0.000 description 1
- GYHNNYVSQQEPJS-UHFFFAOYSA-N Gallium Chemical compound [Ga] GYHNNYVSQQEPJS-UHFFFAOYSA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 1
- KJTLSVCANCCWHF-UHFFFAOYSA-N Ruthenium Chemical compound [Ru] KJTLSVCANCCWHF-UHFFFAOYSA-N 0.000 description 1
- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 description 1
- 229910004298 SiO 2 Inorganic materials 0.000 description 1
- KEAYESYHFKHZAL-UHFFFAOYSA-N Sodium Chemical compound [Na] KEAYESYHFKHZAL-UHFFFAOYSA-N 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 229910000746 Structural steel Inorganic materials 0.000 description 1
- UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 description 1
- 229910001361 White metal Inorganic materials 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 238000004220 aggregation Methods 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 229910000070 arsenic hydride Inorganic materials 0.000 description 1
- 238000013475 authorization Methods 0.000 description 1
- 235000013361 beverage Nutrition 0.000 description 1
- 238000009529 body temperature measurement Methods 0.000 description 1
- 229910052793 cadmium Inorganic materials 0.000 description 1
- BDOSMKKIYDKNTQ-UHFFFAOYSA-N cadmium atom Chemical compound [Cd] BDOSMKKIYDKNTQ-UHFFFAOYSA-N 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 description 1
- 239000003638 chemical reducing agent Substances 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 229910017052 cobalt Inorganic materials 0.000 description 1
- 239000010941 cobalt Substances 0.000 description 1
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 239000002826 coolant Substances 0.000 description 1
- BWFPGXWASODCHM-UHFFFAOYSA-N copper monosulfide Chemical class [Cu]=S BWFPGXWASODCHM-UHFFFAOYSA-N 0.000 description 1
- QUQFTIVBFKLPCL-UHFFFAOYSA-L copper;2-amino-3-[(2-amino-2-carboxylatoethyl)disulfanyl]propanoate Chemical compound [Cu+2].[O-]C(=O)C(N)CSSCC(N)C([O-])=O QUQFTIVBFKLPCL-UHFFFAOYSA-L 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000009795 derivation Methods 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 230000003467 diminishing effect Effects 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 230000004907 flux Effects 0.000 description 1
- 229910052733 gallium Inorganic materials 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 238000007429 general method Methods 0.000 description 1
- 229910052732 germanium Inorganic materials 0.000 description 1
- GNPVGFCGXDBREM-UHFFFAOYSA-N germanium atom Chemical compound [Ge] GNPVGFCGXDBREM-UHFFFAOYSA-N 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 229910052741 iridium Inorganic materials 0.000 description 1
- GKOZUEZYRPOHIO-UHFFFAOYSA-N iridium atom Chemical compound [Ir] GKOZUEZYRPOHIO-UHFFFAOYSA-N 0.000 description 1
- 239000012263 liquid product Substances 0.000 description 1
- 230000007257 malfunction Effects 0.000 description 1
- 238000007726 management method Methods 0.000 description 1
- 229910000510 noble metal Inorganic materials 0.000 description 1
- 229910052762 osmium Inorganic materials 0.000 description 1
- SYQBFIAQOQZEGI-UHFFFAOYSA-N osmium atom Chemical compound [Os] SYQBFIAQOQZEGI-UHFFFAOYSA-N 0.000 description 1
- 229910052763 palladium Inorganic materials 0.000 description 1
- 235000011837 pasties Nutrition 0.000 description 1
- 229910052697 platinum Inorganic materials 0.000 description 1
- 238000009428 plumbing Methods 0.000 description 1
- 239000011819 refractory material Substances 0.000 description 1
- 229910052703 rhodium Inorganic materials 0.000 description 1
- MHOVAHRLVXNVSD-UHFFFAOYSA-N rhodium atom Chemical compound [Rh] MHOVAHRLVXNVSD-UHFFFAOYSA-N 0.000 description 1
- 229910052707 ruthenium Inorganic materials 0.000 description 1
- 230000002000 scavenging effect Effects 0.000 description 1
- 238000006748 scratching Methods 0.000 description 1
- 230000002393 scratching effect Effects 0.000 description 1
- 229910052711 selenium Inorganic materials 0.000 description 1
- 238000000368 spark atomic emission spectrometry Methods 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 150000004763 sulfides Chemical class 0.000 description 1
- XTQHKBHJIVJGKJ-UHFFFAOYSA-N sulfur monoxide Chemical class S=O XTQHKBHJIVJGKJ-UHFFFAOYSA-N 0.000 description 1
- 229910052815 sulfur oxide Inorganic materials 0.000 description 1
- 230000029305 taxis Effects 0.000 description 1
- 229910052714 tellurium Inorganic materials 0.000 description 1
- PORWMNRCUJJQNO-UHFFFAOYSA-N tellurium atom Chemical compound [Te] PORWMNRCUJJQNO-UHFFFAOYSA-N 0.000 description 1
- 229910052716 thallium Inorganic materials 0.000 description 1
- BKVIYDNLLOSFOA-UHFFFAOYSA-N thallium Chemical compound [Tl] BKVIYDNLLOSFOA-UHFFFAOYSA-N 0.000 description 1
- 125000000101 thioether group Chemical group 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 230000001960 triggered effect Effects 0.000 description 1
- 239000002912 waste gas Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 239000010969 white metal Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B7/00—Working up raw materials other than ores, e.g. scrap, to produce non-ferrous metals and compounds thereof; Methods of a general interest or applied to the winning of more than two metals
- C22B7/04—Working-up slag
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K35/00—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting
- B23K35/22—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting characterised by the composition or nature of the material
- B23K35/24—Selection of soldering or welding materials proper
- B23K35/26—Selection of soldering or welding materials proper with the principal constituent melting at less than 400 degrees C
- B23K35/268—Pb as the principal constituent
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/10—Vacuum distillation
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B13/00—Obtaining lead
- C22B13/06—Refining
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B25/00—Obtaining tin
- C22B25/06—Obtaining tin from scrap, especially tin scrap
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B9/00—General processes of refining or remelting of metals; Apparatus for electroslag or arc remelting of metals
- C22B9/10—General processes of refining or remelting of metals; Apparatus for electroslag or arc remelting of metals with refining or fluxing agents; Use of materials therefor, e.g. slagging or scorifying agents
- C22B9/106—General processes of refining or remelting of metals; Apparatus for electroslag or arc remelting of metals with refining or fluxing agents; Use of materials therefor, e.g. slagging or scorifying agents the refining being obtained by intimately mixing the molten metal with a molten salt or slag
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C11/00—Alloys based on lead
- C22C11/06—Alloys based on lead with tin as the next major constituent
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C11/00—Alloys based on lead
- C22C11/08—Alloys based on lead with antimony or bismuth as the next major constituent
- C22C11/10—Alloys based on lead with antimony or bismuth as the next major constituent with tin
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Organic Chemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Manufacturing & Machinery (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Conductive Materials (AREA)
- Arc Welding In General (AREA)
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| EP16190907.2 | 2016-09-27 | ||
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| US12202076B2 (en) | 2017-04-10 | 2025-01-21 | Metallo Belgium | Process for the production of crude solder |
| BE1025775B1 (nl) | 2017-12-14 | 2019-07-11 | Metallo Belgium | Verbeterde soldeerproductiewerkwijze |
| BE1025771B1 (nl) | 2017-12-14 | 2019-07-08 | Metallo Belgium | Verbeterde koperproductiewerkwijze |
| BE1025769B1 (nl) | 2017-12-14 | 2019-07-08 | Metallo Belgium | Verbeterde pyrometallurgische werkwijze |
| BE1025772B1 (nl) | 2017-12-14 | 2019-07-08 | Metallo Belgium | Verbetering in koper-/tin-/loodproductie |
| BE1025770B1 (nl) | 2017-12-14 | 2019-07-08 | Metallo Belgium | Verbeterde pyroraffinagewerkwijze |
| WO2020157168A1 (en) | 2019-01-30 | 2020-08-06 | Metallo Belgium | Improved co-production of lead and tin products |
| CN113316654B (zh) * | 2019-01-30 | 2023-08-04 | 梅塔洛比利时公司 | 改进的锡生产，包括含锡、铅、银和锑的组合物 |
| PE20212093A1 (es) | 2019-01-30 | 2021-11-04 | Metallo Belgium | Procedimiento mejorado para producir plomo de alta pureza |
| CN110919233B (zh) * | 2019-11-15 | 2021-06-04 | 东莞市输变电工程公司 | 一种焊剂及其制备方法与引燃剂 |
| CN114651076B (zh) | 2019-11-22 | 2024-11-01 | 奥鲁毕斯贝尔塞公司 | 从二次原材料中回收铜的方法 |
| CN111607708B (zh) * | 2020-07-14 | 2022-02-11 | 湖南金马冶金技术开发有限公司 | 一种高砷合金连续真空蒸馏脱砷工艺及系统 |
| CN113528846A (zh) * | 2021-06-18 | 2021-10-22 | 广西壮族自治区环境保护科学研究院 | 一种含砷废渣资源化利用的处理方法 |
| CN115852167B (zh) * | 2022-11-14 | 2025-06-06 | 昆明理工大学 | 一种环保的粗锡火法精炼工艺 |
| CN116100187B (zh) * | 2022-12-16 | 2024-07-23 | 无锡市斯威克科技有限公司 | 低熔点三元合金焊料、超低温焊带及其制备方法与应用 |
| WO2025041020A1 (en) * | 2023-08-21 | 2025-02-27 | Attero Recycling Pvt. Ltd. | A method for recovering metal values from solder dross |
Family Cites Families (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3188199A (en) | 1962-06-25 | 1965-06-08 | Du Pont | Process for recovering lead from by-product lead materials |
| AT251301B (de) | 1962-09-27 | 1966-12-27 | Nat Smelting Co Ltd | Verfahren zur Raffination von unreinem Zink |
| JPS5476461A (en) * | 1977-11-30 | 1979-06-19 | Nippon Almit Kk | Solder alloy for bonding capacitor end |
| US4153451A (en) | 1978-05-01 | 1979-05-08 | Ethyl Corporation | Lead recovery and waste disposal process |
| JPS5518505A (en) * | 1978-07-21 | 1980-02-08 | Senjiyu Kinzoku Kogyo Kk | Soldering alloy for attaching silver electrode leading wire |
| US4487638A (en) * | 1982-11-24 | 1984-12-11 | Burroughs Corporation | Semiconductor die-attach technique and composition therefor |
| CN1012046B (zh) * | 1987-01-07 | 1991-03-20 | 天台县焊接材料厂 | 一种稀土锡铅焊料 |
| CN1104950A (zh) * | 1993-10-04 | 1995-07-12 | 成都市焊料厂 | 一种低锡高效焊料 |
| JPH07299584A (ja) * | 1994-05-02 | 1995-11-14 | Nippon Bell Parts Kk | 超塑性はんだ合金 |
| JP3045453B2 (ja) * | 1994-06-13 | 2000-05-29 | 日本アルミット株式会社 | 高強度半田合金 |
| RU2114200C1 (ru) | 1996-12-03 | 1998-06-27 | Институт металлургии Уральского отделения РАН | Способ переработки отходов свинца, содержащих сурьму, олово и медь |
| JP2002153990A (ja) * | 2000-11-21 | 2002-05-28 | Senju Metal Ind Co Ltd | はんだボール用合金 |
| CN100566904C (zh) | 2005-07-21 | 2009-12-09 | 沈阳黎明航空发动机(集团)有限责任公司 | 一种涂层用靶极材料的内外套钎焊工艺方法 |
| CN101570826A (zh) | 2009-06-08 | 2009-11-04 | 昆明鼎邦科技有限公司 | 一种多级真空蒸馏分离铅锡合金的方法 |
| CN101696475B (zh) * | 2009-10-29 | 2012-08-01 | 昆明理工大学 | 一种分离铅锡锑三元合金的方法 |
| CN102352443B (zh) | 2011-10-31 | 2013-06-05 | 太仓市南仓金属材料有限公司 | 用锡熔炼烟尘生产七水硫酸锌及粗锡和粗铅的方法 |
| CN102534249B (zh) | 2012-02-22 | 2013-03-06 | 郴州丰越环保科技股份有限公司 | 从高银粗锡精炼锡的方法 |
| RU2496894C1 (ru) | 2012-06-14 | 2013-10-27 | Ирина Анатольевна Бобкова | Способ рафинирования меди |
| CN104141152A (zh) | 2014-07-28 | 2014-11-12 | 蒙自矿冶有限责任公司 | 一种粗铅中回收锡的方法 |
| CN104593614A (zh) | 2014-12-30 | 2015-05-06 | 郴州丰越环保科技有限公司 | 高效分离含锑高的铅锡锑三元合金铅、锡、锑的方法 |
| CN104651626A (zh) | 2015-02-05 | 2015-05-27 | 昆明鼎邦科技有限公司 | 一种锡铅锑砷合金真空蒸馏分离锡的方法 |
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- 2017-09-26 PH PH1/2019/500606A patent/PH12019500606B1/en unknown
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| CN109923225A (zh) | 2019-06-21 |
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| CN109923225B (zh) | 2021-08-10 |
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| US11992903B2 (en) | 2024-05-28 |
| MX2019003330A (es) | 2019-09-27 |
| BE1024606A1 (nl) | 2018-04-19 |
| BR112019005833B1 (pt) | 2022-06-07 |
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