AU2022432151A1 - Process and system for lithium production - Google Patents
Process and system for lithium production Download PDFInfo
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- AU2022432151A1 AU2022432151A1 AU2022432151A AU2022432151A AU2022432151A1 AU 2022432151 A1 AU2022432151 A1 AU 2022432151A1 AU 2022432151 A AU2022432151 A AU 2022432151A AU 2022432151 A AU2022432151 A AU 2022432151A AU 2022432151 A1 AU2022432151 A1 AU 2022432151A1
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- Australia
- Prior art keywords
- lithium
- solution
- lithium nitrate
- nitrate
- nitric acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Links
- 238000000034 method Methods 0.000 title claims abstract description 230
- 230000008569 process Effects 0.000 title claims abstract description 176
- 229910052744 lithium Inorganic materials 0.000 title claims abstract description 162
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 title claims abstract description 154
- 238000004519 manufacturing process Methods 0.000 title claims description 58
- IIPYXGDZVMZOAP-UHFFFAOYSA-N lithium nitrate Chemical compound [Li+].[O-][N+]([O-])=O IIPYXGDZVMZOAP-UHFFFAOYSA-N 0.000 claims abstract description 496
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims abstract description 136
- 229910017604 nitric acid Inorganic materials 0.000 claims abstract description 136
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 121
- FUJCRWPEOMXPAD-UHFFFAOYSA-N lithium oxide Chemical compound [Li+].[Li+].[O-2] FUJCRWPEOMXPAD-UHFFFAOYSA-N 0.000 claims abstract description 120
- 229910001947 lithium oxide Inorganic materials 0.000 claims abstract description 120
- 239000013078 crystal Substances 0.000 claims abstract description 81
- 239000002002 slurry Substances 0.000 claims abstract description 73
- 239000007788 liquid Substances 0.000 claims abstract description 54
- 238000007669 thermal treatment Methods 0.000 claims abstract description 40
- 229910052914 metal silicate Inorganic materials 0.000 claims abstract description 21
- WMFOQBRAJBCJND-UHFFFAOYSA-M Lithium hydroxide Chemical compound [Li+].[OH-] WMFOQBRAJBCJND-UHFFFAOYSA-M 0.000 claims description 156
- 239000000243 solution Substances 0.000 claims description 140
- 239000000047 product Substances 0.000 claims description 87
- XGZVUEUWXADBQD-UHFFFAOYSA-L lithium carbonate Chemical compound [Li+].[Li+].[O-]C([O-])=O XGZVUEUWXADBQD-UHFFFAOYSA-L 0.000 claims description 85
- 229910052808 lithium carbonate Inorganic materials 0.000 claims description 82
- 238000000354 decomposition reaction Methods 0.000 claims description 50
- PQVSTLUFSYVLTO-UHFFFAOYSA-N ethyl n-ethoxycarbonylcarbamate Chemical compound CCOC(=O)NC(=O)OCC PQVSTLUFSYVLTO-UHFFFAOYSA-N 0.000 claims description 48
- GLXDVVHUTZTUQK-UHFFFAOYSA-M lithium hydroxide monohydrate Substances [Li+].O.[OH-] GLXDVVHUTZTUQK-UHFFFAOYSA-M 0.000 claims description 48
- 229940040692 lithium hydroxide monohydrate Drugs 0.000 claims description 48
- 238000001556 precipitation Methods 0.000 claims description 43
- 229910052642 spodumene Inorganic materials 0.000 claims description 39
- CNLWCVNCHLKFHK-UHFFFAOYSA-N aluminum;lithium;dioxido(oxo)silane Chemical group [Li+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O CNLWCVNCHLKFHK-UHFFFAOYSA-N 0.000 claims description 38
- 238000002844 melting Methods 0.000 claims description 31
- 230000008018 melting Effects 0.000 claims description 31
- 239000007787 solid Substances 0.000 claims description 27
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 claims description 25
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 24
- 238000010438 heat treatment Methods 0.000 claims description 24
- 238000006243 chemical reaction Methods 0.000 claims description 22
- 238000000926 separation method Methods 0.000 claims description 22
- 239000002244 precipitate Substances 0.000 claims description 19
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 18
- 238000002425 crystallisation Methods 0.000 claims description 18
- 238000012545 processing Methods 0.000 claims description 18
- -1 carbonate compound Chemical class 0.000 claims description 17
- 239000000356 contaminant Substances 0.000 claims description 17
- 239000007789 gas Substances 0.000 claims description 17
- 229910052604 silicate mineral Inorganic materials 0.000 claims description 13
- 239000000203 mixture Substances 0.000 claims description 11
- 239000012047 saturated solution Substances 0.000 claims description 11
- 238000001704 evaporation Methods 0.000 claims description 10
- 230000008020 evaporation Effects 0.000 claims description 10
- 229910052701 rubidium Inorganic materials 0.000 claims description 10
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 10
- 229910052500 inorganic mineral Inorganic materials 0.000 claims description 9
- 238000002386 leaching Methods 0.000 claims description 9
- 239000011707 mineral Substances 0.000 claims description 9
- 229910052757 nitrogen Inorganic materials 0.000 claims description 9
- 230000006698 induction Effects 0.000 claims description 8
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 claims description 7
- 238000009835 boiling Methods 0.000 claims description 7
- 239000008346 aqueous phase Substances 0.000 claims description 6
- 238000005188 flotation Methods 0.000 claims description 6
- 229910000027 potassium carbonate Inorganic materials 0.000 claims description 6
- 239000003513 alkali Substances 0.000 claims description 4
- 229910052822 amblygonite Inorganic materials 0.000 claims description 4
- 238000005119 centrifugation Methods 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 4
- 230000008929 regeneration Effects 0.000 claims description 3
- 238000011069 regeneration method Methods 0.000 claims description 3
- HEHRHMRHPUNLIR-UHFFFAOYSA-N aluminum;hydroxy-[hydroxy(oxo)silyl]oxy-oxosilane;lithium Chemical compound [Li].[Al].O[Si](=O)O[Si](O)=O.O[Si](=O)O[Si](O)=O HEHRHMRHPUNLIR-UHFFFAOYSA-N 0.000 claims description 2
- 229910000174 eucryptite Inorganic materials 0.000 claims description 2
- 229910052629 lepidolite Inorganic materials 0.000 claims description 2
- 229910052618 mica group Inorganic materials 0.000 claims description 2
- 229910052670 petalite Inorganic materials 0.000 claims description 2
- 230000001419 dependent effect Effects 0.000 claims 3
- 229910017121 AlSiO Inorganic materials 0.000 claims 1
- 230000029087 digestion Effects 0.000 description 29
- 150000002823 nitrates Chemical class 0.000 description 27
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 25
- 229910052708 sodium Inorganic materials 0.000 description 25
- 239000011734 sodium Substances 0.000 description 21
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 20
- 229910052700 potassium Inorganic materials 0.000 description 20
- 239000011591 potassium Substances 0.000 description 20
- CPLXHLVBOLITMK-UHFFFAOYSA-N Magnesium oxide Chemical compound [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 19
- 238000000605 extraction Methods 0.000 description 17
- 238000000746 purification Methods 0.000 description 17
- 239000012141 concentrate Substances 0.000 description 15
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 14
- 239000004411 aluminium Substances 0.000 description 14
- 229910052782 aluminium Inorganic materials 0.000 description 14
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 14
- 239000012065 filter cake Substances 0.000 description 14
- 229910002089 NOx Inorganic materials 0.000 description 13
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 13
- 229910052760 oxygen Inorganic materials 0.000 description 13
- 239000001301 oxygen Substances 0.000 description 13
- 238000010586 diagram Methods 0.000 description 10
- 239000000395 magnesium oxide Substances 0.000 description 10
- 235000012245 magnesium oxide Nutrition 0.000 description 10
- 238000003860 storage Methods 0.000 description 10
- 229910052783 alkali metal Inorganic materials 0.000 description 9
- 239000000706 filtrate Substances 0.000 description 9
- JCXJVPUVTGWSNB-UHFFFAOYSA-N nitrogen dioxide Inorganic materials O=[N]=O JCXJVPUVTGWSNB-UHFFFAOYSA-N 0.000 description 9
- 229910052792 caesium Inorganic materials 0.000 description 8
- TVFDJXOCXUVLDH-UHFFFAOYSA-N caesium atom Chemical compound [Cs] TVFDJXOCXUVLDH-UHFFFAOYSA-N 0.000 description 8
- 230000008025 crystallization Effects 0.000 description 8
- 238000001914 filtration Methods 0.000 description 8
- 229910052751 metal Inorganic materials 0.000 description 8
- 239000002184 metal Substances 0.000 description 8
- 235000010755 mineral Nutrition 0.000 description 8
- 239000012071 phase Substances 0.000 description 8
- 238000005498 polishing Methods 0.000 description 8
- IGLNJRXAVVLDKE-UHFFFAOYSA-N rubidium atom Chemical compound [Rb] IGLNJRXAVVLDKE-UHFFFAOYSA-N 0.000 description 8
- 235000017550 sodium carbonate Nutrition 0.000 description 8
- 238000005406 washing Methods 0.000 description 8
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 7
- 239000002253 acid Substances 0.000 description 7
- 230000008901 benefit Effects 0.000 description 7
- 229910052791 calcium Inorganic materials 0.000 description 7
- 239000011575 calcium Substances 0.000 description 7
- 239000012467 final product Substances 0.000 description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 7
- 239000012535 impurity Substances 0.000 description 7
- 229910052742 iron Inorganic materials 0.000 description 7
- 235000015320 potassium carbonate Nutrition 0.000 description 7
- FGIUAXJPYTZDNR-UHFFFAOYSA-N potassium nitrate Chemical class [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 description 7
- 238000011084 recovery Methods 0.000 description 7
- 150000003839 salts Chemical class 0.000 description 7
- 150000001340 alkali metals Chemical class 0.000 description 6
- 239000006227 byproduct Substances 0.000 description 6
- 150000002739 metals Chemical class 0.000 description 6
- 235000011181 potassium carbonates Nutrition 0.000 description 6
- 235000010344 sodium nitrate Nutrition 0.000 description 6
- 239000000126 substance Substances 0.000 description 6
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 5
- 239000004743 Polypropylene Substances 0.000 description 5
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 5
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 5
- 238000010276 construction Methods 0.000 description 5
- VCJMYUPGQJHHFU-UHFFFAOYSA-N iron(3+);trinitrate Chemical compound [Fe+3].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O VCJMYUPGQJHHFU-UHFFFAOYSA-N 0.000 description 5
- 239000007791 liquid phase Substances 0.000 description 5
- 229910052749 magnesium Inorganic materials 0.000 description 5
- 239000011777 magnesium Substances 0.000 description 5
- 229910001862 magnesium hydroxide Inorganic materials 0.000 description 5
- 229940072033 potash Drugs 0.000 description 5
- 235000010333 potassium nitrate Nutrition 0.000 description 5
- VWDWKYIASSYTQR-UHFFFAOYSA-N sodium nitrate Chemical class [Na+].[O-][N+]([O-])=O VWDWKYIASSYTQR-UHFFFAOYSA-N 0.000 description 5
- 239000010936 titanium Substances 0.000 description 5
- 229910052719 titanium Inorganic materials 0.000 description 5
- 238000011144 upstream manufacturing Methods 0.000 description 5
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 4
- 229910002651 NO3 Inorganic materials 0.000 description 4
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 4
- 229910001963 alkali metal nitrate Inorganic materials 0.000 description 4
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 description 4
- 229910021502 aluminium hydroxide Inorganic materials 0.000 description 4
- JLDSOYXADOWAKB-UHFFFAOYSA-N aluminium nitrate Chemical compound [Al+3].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O JLDSOYXADOWAKB-UHFFFAOYSA-N 0.000 description 4
- 239000002585 base Substances 0.000 description 4
- 238000001816 cooling Methods 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 230000005611 electricity Effects 0.000 description 4
- 238000006460 hydrolysis reaction Methods 0.000 description 4
- PAZHGORSDKKUPI-UHFFFAOYSA-N lithium metasilicate Chemical compound [Li+].[Li+].[O-][Si]([O-])=O PAZHGORSDKKUPI-UHFFFAOYSA-N 0.000 description 4
- 229910052912 lithium silicate Inorganic materials 0.000 description 4
- 238000011020 pilot scale process Methods 0.000 description 4
- 235000011182 sodium carbonates Nutrition 0.000 description 4
- 238000012546 transfer Methods 0.000 description 4
- VTLYFUHAOXGGBS-UHFFFAOYSA-N Fe3+ Chemical compound [Fe+3] VTLYFUHAOXGGBS-UHFFFAOYSA-N 0.000 description 3
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 description 3
- 238000007605 air drying Methods 0.000 description 3
- 239000007864 aqueous solution Substances 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 239000003153 chemical reaction reagent Substances 0.000 description 3
- 230000007423 decrease Effects 0.000 description 3
- 238000013461 design Methods 0.000 description 3
- 238000006073 displacement reaction Methods 0.000 description 3
- 239000013067 intermediate product Substances 0.000 description 3
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 3
- VTHJTEIRLNZDEV-UHFFFAOYSA-L magnesium dihydroxide Chemical compound [OH-].[OH-].[Mg+2] VTHJTEIRLNZDEV-UHFFFAOYSA-L 0.000 description 3
- 239000000347 magnesium hydroxide Substances 0.000 description 3
- 235000012254 magnesium hydroxide Nutrition 0.000 description 3
- 238000006386 neutralization reaction Methods 0.000 description 3
- 229920001155 polypropylene Polymers 0.000 description 3
- 230000001376 precipitating effect Effects 0.000 description 3
- 239000013535 sea water Substances 0.000 description 3
- 229910001220 stainless steel Inorganic materials 0.000 description 3
- 239000010414 supernatant solution Substances 0.000 description 3
- 239000002699 waste material Substances 0.000 description 3
- 229910021532 Calcite Inorganic materials 0.000 description 2
- 241000549556 Nanos Species 0.000 description 2
- MWUXSHHQAYIFBG-UHFFFAOYSA-N Nitric oxide Chemical compound O=[N] MWUXSHHQAYIFBG-UHFFFAOYSA-N 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 2
- 238000013459 approach Methods 0.000 description 2
- 239000010953 base metal Substances 0.000 description 2
- 229910000019 calcium carbonate Inorganic materials 0.000 description 2
- ZCCIPPOKBCJFDN-UHFFFAOYSA-N calcium nitrate Chemical compound [Ca+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O ZCCIPPOKBCJFDN-UHFFFAOYSA-N 0.000 description 2
- 239000000498 cooling water Substances 0.000 description 2
- XUCJHNOBJLKZNU-UHFFFAOYSA-M dilithium;hydroxide Chemical compound [Li+].[Li+].[OH-] XUCJHNOBJLKZNU-UHFFFAOYSA-M 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 230000006870 function Effects 0.000 description 2
- 239000000499 gel Substances 0.000 description 2
- 229920001903 high density polyethylene Polymers 0.000 description 2
- 239000004700 high-density polyethylene Substances 0.000 description 2
- 230000007062 hydrolysis Effects 0.000 description 2
- 238000012423 maintenance Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 238000012544 monitoring process Methods 0.000 description 2
- 230000002093 peripheral effect Effects 0.000 description 2
- 230000002572 peristaltic effect Effects 0.000 description 2
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 2
- 230000035484 reaction time Effects 0.000 description 2
- 238000007670 refining Methods 0.000 description 2
- 230000001172 regenerating effect Effects 0.000 description 2
- 239000011435 rock Substances 0.000 description 2
- 229920006395 saturated elastomer Polymers 0.000 description 2
- 239000000377 silicon dioxide Substances 0.000 description 2
- 238000004513 sizing Methods 0.000 description 2
- 239000004317 sodium nitrate Substances 0.000 description 2
- 238000010561 standard procedure Methods 0.000 description 2
- 239000010878 waste rock Substances 0.000 description 2
- 239000010964 304L stainless steel Substances 0.000 description 1
- MGWGWNFMUOTEHG-UHFFFAOYSA-N 4-(3,5-dimethylphenyl)-1,3-thiazol-2-amine Chemical compound CC1=CC(C)=CC(C=2N=C(N)SC=2)=C1 MGWGWNFMUOTEHG-UHFFFAOYSA-N 0.000 description 1
- 229910018626 Al(OH) Inorganic materials 0.000 description 1
- 229910017113 AlSi2 Inorganic materials 0.000 description 1
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
- MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 description 1
- HBBGRARXTFLTSG-UHFFFAOYSA-N Lithium ion Chemical compound [Li+] HBBGRARXTFLTSG-UHFFFAOYSA-N 0.000 description 1
- KKCBUQHMOMHUOY-UHFFFAOYSA-N Na2O Inorganic materials [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 description 1
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 238000005273 aeration Methods 0.000 description 1
- 238000005275 alloying Methods 0.000 description 1
- 230000003466 anti-cipated effect Effects 0.000 description 1
- PPTSBERGOGHCHC-UHFFFAOYSA-N boron lithium Chemical compound [Li].[B] PPTSBERGOGHCHC-UHFFFAOYSA-N 0.000 description 1
- 238000001354 calcination Methods 0.000 description 1
- 150000004649 carbonic acid derivatives Chemical class 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 150000001768 cations Chemical class 0.000 description 1
- 239000004568 cement Substances 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000000975 co-precipitation Methods 0.000 description 1
- 229910052681 coesite Inorganic materials 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 229910052906 cristobalite Inorganic materials 0.000 description 1
- 239000012043 crude product Substances 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 230000003111 delayed effect Effects 0.000 description 1
- 238000007865 diluting Methods 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 229910001882 dioxygen Inorganic materials 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 239000008157 edible vegetable oil Substances 0.000 description 1
- 238000004146 energy storage Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 230000005496 eutectics Effects 0.000 description 1
- 229960004887 ferric hydroxide Drugs 0.000 description 1
- 239000003337 fertilizer Substances 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 238000011010 flushing procedure Methods 0.000 description 1
- 238000009291 froth flotation Methods 0.000 description 1
- 230000004927 fusion Effects 0.000 description 1
- 229910001679 gibbsite Inorganic materials 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 239000010931 gold Substances 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 231100001261 hazardous Toxicity 0.000 description 1
- 239000000383 hazardous chemical Substances 0.000 description 1
- 238000005338 heat storage Methods 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- IEECXTSVVFWGSE-UHFFFAOYSA-M iron(3+);oxygen(2-);hydroxide Chemical compound [OH-].[O-2].[Fe+3] IEECXTSVVFWGSE-UHFFFAOYSA-M 0.000 description 1
- FLTRNWIFKITPIO-UHFFFAOYSA-N iron;trihydrate Chemical compound O.O.O.[Fe] FLTRNWIFKITPIO-UHFFFAOYSA-N 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- 150000002641 lithium Chemical class 0.000 description 1
- YQNQTEBHHUSESQ-UHFFFAOYSA-N lithium aluminate Chemical compound [Li+].[O-][Al]=O YQNQTEBHHUSESQ-UHFFFAOYSA-N 0.000 description 1
- 229910001416 lithium ion Inorganic materials 0.000 description 1
- 229910001760 lithium mineral Inorganic materials 0.000 description 1
- WHXSMMKQMYFTQS-BKFZFHPZSA-N lithium-12 Chemical compound [12Li] WHXSMMKQMYFTQS-BKFZFHPZSA-N 0.000 description 1
- YIXJRHPUWRPCBB-UHFFFAOYSA-N magnesium nitrate Inorganic materials [Mg+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O YIXJRHPUWRPCBB-UHFFFAOYSA-N 0.000 description 1
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000003472 neutralizing effect Effects 0.000 description 1
- 238000010979 pH adjustment Methods 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 1
- 229940085991 phosphate ion Drugs 0.000 description 1
- 229910052697 platinum Inorganic materials 0.000 description 1
- 239000004323 potassium nitrate Substances 0.000 description 1
- 159000000001 potassium salts Chemical class 0.000 description 1
- 239000010970 precious metal Substances 0.000 description 1
- 239000002243 precursor Substances 0.000 description 1
- 238000004801 process automation Methods 0.000 description 1
- 238000004886 process control Methods 0.000 description 1
- 238000011112 process operation Methods 0.000 description 1
- 230000007425 progressive decline Effects 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 238000005086 pumping Methods 0.000 description 1
- 238000010926 purge Methods 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 230000002441 reversible effect Effects 0.000 description 1
- 238000010517 secondary reaction Methods 0.000 description 1
- 235000012239 silicon dioxide Nutrition 0.000 description 1
- 229910052938 sodium sulfate Inorganic materials 0.000 description 1
- 235000011152 sodium sulphate Nutrition 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 229910052682 stishovite Inorganic materials 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 238000009283 thermal hydrolysis Methods 0.000 description 1
- 239000002341 toxic gas Substances 0.000 description 1
- 229910052723 transition metal Inorganic materials 0.000 description 1
- 150000003624 transition metals Chemical class 0.000 description 1
- 229910052905 tridymite Inorganic materials 0.000 description 1
- 238000010977 unit operation Methods 0.000 description 1
- 239000003039 volatile agent Substances 0.000 description 1
- 239000002918 waste heat Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D15/00—Lithium compounds
- C01D15/02—Oxides; Hydroxides
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/20—Nitrogen oxides; Oxyacids of nitrogen; Salts thereof
- C01B21/38—Nitric acid
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D15/00—Lithium compounds
- C01D15/08—Carbonates; Bicarbonates
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D15/00—Lithium compounds
- C01D15/10—Nitrates
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F7/00—Compounds of aluminium
- C01F7/02—Aluminium oxide; Aluminium hydroxide; Aluminates
- C01F7/20—Preparation of aluminium oxide or hydroxide from aluminous ores using acids or salts
- C01F7/24—Preparation of aluminium oxide or hydroxide from aluminous ores using acids or salts with nitric acid or nitrogen oxides
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B1/00—Preliminary treatment of ores or scrap
- C22B1/02—Roasting processes
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B21/00—Obtaining aluminium
- C22B21/0015—Obtaining aluminium by wet processes
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B21/00—Obtaining aluminium
- C22B21/04—Obtaining aluminium with alkali metals earth alkali metals included
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B26/00—Obtaining alkali, alkaline earth metals or magnesium
- C22B26/10—Obtaining alkali metals
- C22B26/12—Obtaining lithium
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/04—Extraction of metal compounds from ores or concentrates by wet processes by leaching
- C22B3/06—Extraction of metal compounds from ores or concentrates by wet processes by leaching in inorganic acid solutions, e.g. with acids generated in situ; in inorganic salt solutions other than ammonium salt solutions
- C22B3/065—Nitric acids or salts thereof
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
- C22B3/22—Treatment or purification of solutions, e.g. obtained by leaching by physical processes, e.g. by filtration, by magnetic means, or by thermal decomposition
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
- C22B3/44—Treatment or purification of solutions, e.g. obtained by leaching by chemical processes
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B7/00—Working up raw materials other than ores, e.g. scrap, to produce non-ferrous metals and compounds thereof; Methods of a general interest or applied to the winning of more than two metals
- C22B7/006—Wet processes
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Mechanical Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Geology (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Metallurgy (AREA)
- Environmental & Geological Engineering (AREA)
- Inorganic Chemistry (AREA)
- Geochemistry & Mineralogy (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Silicates, Zeolites, And Molecular Sieves (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| AU2024205225A AU2024205225B2 (en) | 2022-01-17 | 2024-07-30 | Process and system for lithium production |
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| AU2022900080A AU2022900080A0 (en) | 2022-01-17 | Process and system for lithium production | |
| AU2022900080 | 2022-01-17 | ||
| PCT/AU2022/051538 WO2023133608A1 (en) | 2022-01-17 | 2022-12-19 | Process and system for lithium production |
Related Child Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AU2024205225A Division AU2024205225B2 (en) | 2022-01-17 | 2024-07-30 | Process and system for lithium production |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| AU2022432151A1 true AU2022432151A1 (en) | 2024-08-08 |
Family
ID=87278503
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AU2022432151A Pending AU2022432151A1 (en) | 2022-01-17 | 2022-12-19 | Process and system for lithium production |
| AU2024205225A Active AU2024205225B2 (en) | 2022-01-17 | 2024-07-30 | Process and system for lithium production |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AU2024205225A Active AU2024205225B2 (en) | 2022-01-17 | 2024-07-30 | Process and system for lithium production |
Country Status (10)
| Country | Link |
|---|---|
| US (5) | US20250091889A1 (https=) |
| EP (1) | EP4466225A4 (https=) |
| JP (1) | JP2025503715A (https=) |
| KR (1) | KR20240159568A (https=) |
| CN (2) | CN118871390A (https=) |
| AU (2) | AU2022432151A1 (https=) |
| CA (1) | CA3248339A1 (https=) |
| CL (1) | CL2024002095A1 (https=) |
| MX (1) | MX2024008794A (https=) |
| WO (1) | WO2023133608A1 (https=) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US12091727B2 (en) | 2022-09-30 | 2024-09-17 | James G. Blencoe | Process for extracting lithium, aluminum, and silicon materials from a hard rock source |
| AU2024230147A1 (en) * | 2023-02-27 | 2025-09-18 | ICSIP Pty Ltd | Lithium recovery from sedimentary silicates |
| US20250372745A1 (en) * | 2024-05-28 | 2025-12-04 | Ace Green Recycling Inc. | Recovery of nitric acid from nox gasses |
| WO2026006872A1 (en) * | 2024-07-05 | 2026-01-08 | Altilium Licensing Ltd | Nitric acid recovery and recycling process |
Family Cites Families (45)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1531336A (en) | 1924-04-10 | 1925-03-31 | Norsk Hydro Elektrisk | Process for the treatment of leucite |
| US1863986A (en) | 1928-04-18 | 1932-06-21 | Jourdan Felix | Process for the treatment of leucitic rocks with nitrous vapors in a continuous cycle |
| US1976564A (en) | 1932-03-18 | 1934-10-09 | Jourdan Felix | Process for the treatment of silicates with acids in order to obtain their soluble salts |
| GB402977A (en) | 1932-03-18 | 1933-12-14 | Felix Jourdan | Improvements in process for the treatment of silicates with acids in order to obtaintheir soluble salts |
| US2024026A (en) | 1933-11-17 | 1935-12-10 | Warner Chemical Company | Recovering lithium compounds |
| US2021988A (en) | 1934-01-20 | 1935-11-26 | Grasselli Chemical Co | Production of lithium compounds |
| BE560581A (https=) * | 1956-09-07 | 1900-01-01 | ||
| US3965239A (en) | 1973-11-16 | 1976-06-22 | International Ore Technology, Inc. | Recovery of nitric acid soluble transition metals from sulfur and iron containing ores of the same |
| JPH024442A (ja) | 1988-06-21 | 1990-01-09 | Agency Of Ind Science & Technol | 高性能リチウム吸着剤およびその製造方法 |
| US5350717A (en) | 1993-06-04 | 1994-09-27 | Corning Incorporated | Method for treating beta-spodumene ceramics |
| JP3589542B2 (ja) | 1996-03-26 | 2004-11-17 | シャープ株式会社 | 正極活物質の製造方法及び非水系二次電池 |
| US6555078B1 (en) * | 1996-09-26 | 2003-04-29 | Fmc Corporation | Method of preparing lithium salts |
| JP3676926B2 (ja) | 1997-06-04 | 2005-07-27 | 株式会社日鉱マテリアルズ | 電池正極廃材からコバルト、ニッケルもしくはマンガンおよびリチウムを回収および再生する方法ならびに電池正極材原料 |
| CN1117164C (zh) | 1999-12-10 | 2003-08-06 | 中国科学院青海盐湖研究所 | 金属锂的热还原制备及提纯工艺和设备 |
| US6543444B1 (en) | 2000-04-10 | 2003-04-08 | John E. Lewis | System and method for air time remaining calculations in a self-contained breathing apparatus |
| US7104124B2 (en) | 2001-05-04 | 2006-09-12 | Stabile James R | Method for indicating duration of gas supply remaining and providing result to user thereof |
| FR2868160B1 (fr) | 2004-03-24 | 2007-09-28 | Taema Sa | Systeme de traitement des donnees de pression dans un reservoir |
| JP4760353B2 (ja) | 2005-12-14 | 2011-08-31 | トヨタ自動車株式会社 | 液体水素タンク残量検知システム |
| US20070193379A1 (en) | 2006-02-21 | 2007-08-23 | Mccluskey William P | Electronic Scale for Measuring Gas in Pressurized Cylinders Over a Wide Range of Capacities |
| JP5473523B2 (ja) * | 2009-10-08 | 2014-04-16 | Ｄｏｗａエコシステム株式会社 | スズ含有廃棄物の精製方法及びガラスの澄泡剤 |
| FR2952432B1 (fr) | 2009-11-10 | 2012-06-01 | Air Liquide | Procede et dispositif de suivi du contenu d'un reservoir mobile de fluide |
| CN102892708B (zh) | 2010-01-07 | 2015-04-22 | 银河锂业国际有限公司 | 用于制造碳酸锂的方法 |
| FI122831B (fi) | 2010-05-25 | 2012-07-31 | Outotec Oyj | Menetelmä spodumeenin käsittelemiseksi |
| JP2014508863A (ja) | 2011-03-18 | 2014-04-10 | オーバイト アルミナ インコーポレイテッド | アルミニウム含有材料から希土類元素を回収する方法 |
| WO2013097186A1 (en) * | 2011-12-30 | 2013-07-04 | Robert Bosch Gmbh | Lithium-metal oxide nanofarticles, preparation method and use thereof |
| EA201491632A1 (ru) | 2012-03-19 | 2015-03-31 | Оутотек (Финлэнд) Ой | Способ извлечения карбоната лития |
| CN102765734A (zh) | 2012-07-13 | 2012-11-07 | 江西赣锋锂业股份有限公司 | 一种从锂辉石提取锂制备锂盐的方法 |
| AU2013201833B2 (en) | 2012-08-13 | 2014-07-17 | Reed Advanced Materials Pty Ltd | Processing of Lithium Containing Ore |
| CA3275949A1 (en) | 2014-02-24 | 2025-10-31 | Nemaska Lithium Inc. | Methods for treating lithium-containing materials |
| AR095821A1 (es) | 2014-04-09 | 2015-11-11 | Consejo Nac De Investig Científicas Y Técnicas (Conicet) | Procedimiento de obtención de compuestos de litio |
| CN105039699B (zh) | 2015-06-03 | 2018-01-02 | 江西合纵锂业科技有限公司 | 锂云母固氟重构提取碱金属渣处理与资源化利用方法 |
| CN106906359B (zh) * | 2015-12-22 | 2018-12-11 | 理查德.亨威克 | 从硅酸盐矿物收取锂 |
| CN108277367B (zh) | 2017-01-06 | 2020-09-18 | 中国科学院过程工程研究所 | 一种从含锂矿石中提锂的方法 |
| CN107473242B (zh) | 2017-09-19 | 2019-03-05 | 江西赣锋锂业股份有限公司 | 一种利用碳酸锂制备高纯氧化锂的方法 |
| US10648090B2 (en) * | 2018-02-17 | 2020-05-12 | Lilac Solutions, Inc. | Integrated system for lithium extraction and conversion |
| CN113365947A (zh) | 2018-11-29 | 2021-09-07 | 伊希普私人有限公司 | 锂化学品和金属锂的制备 |
| CN110042262A (zh) | 2019-05-27 | 2019-07-23 | 中国地质科学院矿产综合利用研究所 | 一种选择性浸出低品位沉积型锂矿的方法 |
| CA3160982A1 (en) | 2019-11-15 | 2021-05-20 | Metso Outotec Finland Oy | Arrangement and method for recovering lithium hydroxide |
| AU2021222020A1 (en) | 2020-02-20 | 2022-09-15 | North Carolina State University | Process for extraction of lithium |
| CA3199218A1 (en) | 2020-11-20 | 2022-05-27 | David Henry SNYDACKER | Lithium production with volatile acid |
| CN113651342A (zh) | 2021-09-06 | 2021-11-16 | 四川顺应动力电池材料有限公司 | 一种采用硝酸常压法处理锂云母生产锂产品的方法 |
| CN113772696A (zh) | 2021-09-09 | 2021-12-10 | 四川顺应动力电池材料有限公司 | 一种采用硝酸加压法处理锂云母生产多种锂产品的方法 |
| CN114105171B (zh) | 2021-11-04 | 2023-10-31 | 四川顺应锂材料科技有限公司 | 一种锂云母资源化综合利用的方法及制备的氢氧化锂 |
| CN113998714A (zh) | 2021-11-24 | 2022-02-01 | 四川顺应动力电池材料有限公司 | 一种生产电池级氢氧化锂的方法 |
| CN114318008B (zh) | 2021-12-27 | 2022-09-23 | 四川顺应锂材料科技有限公司 | 一种硝酸二次逆向浸出锂辉石提锂的方法 |
-
2022
- 2022-12-19 CA CA3248339A patent/CA3248339A1/en active Pending
- 2022-12-19 MX MX2024008794A patent/MX2024008794A/es unknown
- 2022-12-19 CN CN202280093238.6A patent/CN118871390A/zh active Pending
- 2022-12-19 US US18/729,344 patent/US20250091889A1/en active Pending
- 2022-12-19 WO PCT/AU2022/051538 patent/WO2023133608A1/en not_active Ceased
- 2022-12-19 JP JP2024542084A patent/JP2025503715A/ja active Pending
- 2022-12-19 EP EP22919308.1A patent/EP4466225A4/en active Pending
- 2022-12-19 AU AU2022432151A patent/AU2022432151A1/en active Pending
- 2022-12-19 CN CN202411429177.3A patent/CN119528181A/zh active Pending
- 2022-12-19 KR KR1020247027505A patent/KR20240159568A/ko active Pending
-
2024
- 2024-07-10 CL CL2024002095A patent/CL2024002095A1/es unknown
- 2024-07-29 US US18/787,464 patent/US12479738B2/en active Active
- 2024-07-30 AU AU2024205225A patent/AU2024205225B2/en active Active
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2025
- 2025-09-22 US US19/336,109 patent/US20260022023A1/en active Pending
- 2025-09-22 US US19/336,101 patent/US20260015247A1/en active Pending
- 2025-09-22 US US19/336,126 patent/US20260070800A1/en active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| US20250091889A1 (en) | 2025-03-20 |
| CN119528181A (zh) | 2025-02-28 |
| US12479738B2 (en) | 2025-11-25 |
| US20260022023A1 (en) | 2026-01-22 |
| CN118871390A (zh) | 2024-10-29 |
| AU2024205225B2 (en) | 2025-09-04 |
| KR20240159568A (ko) | 2024-11-05 |
| MX2024008794A (es) | 2024-08-15 |
| CL2024002095A1 (es) | 2024-10-25 |
| EP4466225A1 (en) | 2024-11-27 |
| US20240409425A1 (en) | 2024-12-12 |
| JP2025503715A (ja) | 2025-02-04 |
| US20260070800A1 (en) | 2026-03-12 |
| AU2024205225A1 (en) | 2024-08-15 |
| US20260015247A1 (en) | 2026-01-15 |
| WO2023133608A1 (en) | 2023-07-20 |
| CA3248339A1 (en) | 2023-07-20 |
| EP4466225A4 (en) | 2026-01-28 |
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