ATE74583T1 - Verfahren zur herstellung eines tertiaeren alkylethers durch reaktive destillation. - Google Patents
Verfahren zur herstellung eines tertiaeren alkylethers durch reaktive destillation.Info
- Publication number
- ATE74583T1 ATE74583T1 AT89400623T AT89400623T ATE74583T1 AT E74583 T1 ATE74583 T1 AT E74583T1 AT 89400623 T AT89400623 T AT 89400623T AT 89400623 T AT89400623 T AT 89400623T AT E74583 T1 ATE74583 T1 AT E74583T1
- Authority
- AT
- Austria
- Prior art keywords
- zone
- reaction
- distillation
- production
- alkyl ether
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 2
- 150000005215 alkyl ethers Chemical group 0.000 title 1
- 238000004519 manufacturing process Methods 0.000 title 1
- 238000000066 reactive distillation Methods 0.000 title 1
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 abstract 6
- BZLVMXJERCGZMT-UHFFFAOYSA-N Methyl tert-butyl ether Chemical compound COC(C)(C)C BZLVMXJERCGZMT-UHFFFAOYSA-N 0.000 abstract 6
- 238000004821 distillation Methods 0.000 abstract 4
- VQTUBCCKSQIDNK-UHFFFAOYSA-N Isobutene Chemical compound CC(C)=C VQTUBCCKSQIDNK-UHFFFAOYSA-N 0.000 abstract 2
- 229930195733 hydrocarbon Natural products 0.000 abstract 2
- 150000002430 hydrocarbons Chemical class 0.000 abstract 2
- 239000007791 liquid phase Substances 0.000 abstract 2
- 239000000203 mixture Substances 0.000 abstract 2
- 239000012071 phase Substances 0.000 abstract 2
- 230000001174 ascending effect Effects 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 239000007788 liquid Substances 0.000 abstract 1
- 238000002360 preparation method Methods 0.000 abstract 1
- 239000011347 resin Substances 0.000 abstract 1
- 229920005989 resin Polymers 0.000 abstract 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
- B01J8/04—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
- B01J8/0492—Feeding reactive fluids
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C43/00—Ethers; Compounds having groups, groups or groups
- C07C43/02—Ethers
- C07C43/03—Ethers having all ether-oxygen atoms bound to acyclic carbon atoms
- C07C43/04—Saturated ethers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/009—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in combination with chemical reactions
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
- B01D3/16—Fractionating columns in which vapour bubbles through liquid
- B01D3/22—Fractionating columns in which vapour bubbles through liquid with horizontal sieve plates or grids; Construction of sieve plates or grids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
- B01D3/16—Fractionating columns in which vapour bubbles through liquid
- B01D3/24—Fractionating columns in which vapour bubbles through liquid with sloping plates or elements mounted stepwise
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
- B01J8/04—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
- B01J8/0446—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical
- B01J8/0449—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical beds
- B01J8/0453—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical beds the beds being superimposed one above the other
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
- C07C41/01—Preparation of ethers
- C07C41/05—Preparation of ethers by addition of compounds to unsaturated compounds
- C07C41/06—Preparation of ethers by addition of compounds to unsaturated compounds by addition of organic compounds only
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
- C07C41/01—Preparation of ethers
- C07C41/34—Separation; Purification; Stabilisation; Use of additives
- C07C41/40—Separation; Purification; Stabilisation; Use of additives by change of physical state, e.g. by crystallisation
- C07C41/42—Separation; Purification; Stabilisation; Use of additives by change of physical state, e.g. by crystallisation by distillation
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S203/00—Distillation: processes, separatory
- Y10S203/06—Reactor-distillation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Crystallography & Structural Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR8803095A FR2628418B1 (fr) | 1988-03-08 | 1988-03-08 | Procede de preparation d'un ether alkylique tertiaire par distillation reactive |
| US07/171,340 US4847431A (en) | 1988-03-08 | 1988-03-21 | Process for manufacturing a tertiary alkyl ether by reactive distillation |
| EP89400623A EP0332525B1 (de) | 1988-03-08 | 1989-03-06 | Verfahren zur Herstellung eines tertiären Alkylethers durch reaktive Destillation |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE74583T1 true ATE74583T1 (de) | 1992-04-15 |
Family
ID=26226548
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT89400623T ATE74583T1 (de) | 1988-03-08 | 1989-03-06 | Verfahren zur herstellung eines tertiaeren alkylethers durch reaktive destillation. |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US4847431A (de) |
| EP (1) | EP0332525B1 (de) |
| JP (1) | JP2681211B2 (de) |
| KR (1) | KR930000920B1 (de) |
| AT (1) | ATE74583T1 (de) |
| DE (1) | DE68901149D1 (de) |
| ES (1) | ES2032116T3 (de) |
| FR (1) | FR2628418B1 (de) |
Families Citing this family (28)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5120403A (en) * | 1989-03-23 | 1992-06-09 | Chemical Research & Licensing Company | Method for operating a catalytic distillation process |
| US5221441A (en) * | 1989-03-23 | 1993-06-22 | Chemical Research & Licensing Company | Method for operating a catalytic distillation process |
| US4978807A (en) * | 1989-03-23 | 1990-12-18 | Chemical Research & Licensing Company | Method for the preparation of methyl tertiary butyl ether |
| US5262576A (en) * | 1989-03-23 | 1993-11-16 | Chemical Research & Licensing Company | Method for the alkylation of organic aromatic compounds |
| US5073236A (en) * | 1989-11-13 | 1991-12-17 | Gelbein Abraham P | Process and structure for effecting catalytic reactions in distillation structure |
| US5108550A (en) * | 1990-02-06 | 1992-04-28 | Koch Engineering Company, Inc. | Catalyst system for distillation reactor |
| US5948211A (en) * | 1990-02-06 | 1999-09-07 | Koch-Glitsch, Inc. | Distillation column downcomer having liquid permeable wall |
| US5593548A (en) * | 1990-02-06 | 1997-01-14 | Koch Engineering Company, Inc. | Method for concurrent reaction with distillation |
| US5855741A (en) * | 1990-02-06 | 1999-01-05 | Koch Engineering Company, Inc. | Apparatus for concurrent reaction with distillation |
| US5447609A (en) * | 1990-02-06 | 1995-09-05 | Koch Engineering Company, Inc. | Catalytic reaction and mass transfer process |
| US5454913A (en) * | 1990-02-06 | 1995-10-03 | Koch Engineering Company, Inc. | Internals for distillation columns including those for use in catalytic reactions |
| US5057468A (en) * | 1990-05-21 | 1991-10-15 | Chemical Research & Licensing Company | Catalytic distillation structure |
| US5130102A (en) * | 1990-06-11 | 1992-07-14 | Chemical Research & Licensing Company | Catalytic distillation reactor |
| EP0467278B1 (de) * | 1990-07-20 | 1994-09-21 | The Dow Chemical Company | Verfahren zur kontinuierlichen Herstellung von Reaktionsprodukten |
| IT1243773B (it) * | 1990-08-01 | 1994-06-28 | Snam Progetti | Procedimento per la preparazione di eteri alchilici terziari ed apparecchiatura di distillazione reattiva |
| US5262012A (en) * | 1990-09-19 | 1993-11-16 | Chemical Research & Licensing Company | Catalytic distillation system |
| ES2057965T3 (es) * | 1991-03-08 | 1994-10-16 | Inst Francais Du Petrole | Aparato de destilacion-reaccion y su utilizacion. |
| FR2684893A1 (fr) * | 1991-12-16 | 1993-06-18 | Inst Francais Du Petrole | Procede de distillation reactive catalytique et appareillage pour sa mise en óoeuvre. |
| US5338517A (en) * | 1992-05-18 | 1994-08-16 | Chemical Research & Licensing Company | Catalytic distillation column reactor and tray |
| US5601797A (en) * | 1992-08-10 | 1997-02-11 | Glitsch, Inc. | Liquid-phase catalyst-assembly for chemical process tower |
| US5714640A (en) * | 1994-01-21 | 1998-02-03 | Mobil Oil Corporation | Vapor pocket reactor |
| HUT71029A (en) * | 1994-03-04 | 1995-11-28 | Glitsch | Chemical process tower, catalytic unit and method for locating of contact substance |
| US5752538A (en) * | 1995-12-13 | 1998-05-19 | Praxair Technology, Inc. | Liquid distributor for packed columns |
| US5925685A (en) * | 1996-11-18 | 1999-07-20 | Catalytic Distillation Technologies | Method for carrying out heterogeneous catalysis |
| US6565816B1 (en) | 1997-06-25 | 2003-05-20 | Koch-Glitsch, Inc. | Saddle structure for reactive distillation |
| DE19728732A1 (de) * | 1997-07-04 | 1999-01-07 | Basf Ag | Verfahren zur Gewinnung von Isobuten aus solches enthaltenden C¶4¶-Kohlenwasserstoffgemischen |
| DE10102082A1 (de) * | 2000-10-19 | 2002-05-02 | Oxeno Olefinchemie Gmbh | Verfahren zur Herstellung von hochreinem Raffinat II und Methyl-tert.-butylether |
| WO2009011603A1 (en) * | 2007-07-16 | 2009-01-22 | Fde Process Systems Limited | Improvements in a method of distillation and/or a distillation column |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3629478A (en) * | 1969-08-22 | 1971-12-21 | Chevron Res | Separation of linear olefins from tertiary olefins |
| US4232177A (en) * | 1979-02-21 | 1980-11-04 | Chemical Research & Licensing Company | Catalytic distillation process |
| EP0008860B2 (de) * | 1978-07-27 | 1991-12-04 | CHEMICAL RESEARCH & LICENSING COMPANY | Katalysatorsystem |
| IT1137527B (it) * | 1981-04-10 | 1986-09-10 | Anic Spa | Procedimento per la preparazione di eteri alchilici terziari |
| US4439350A (en) * | 1982-06-21 | 1984-03-27 | Chemical Research & Licensing Company | Contact structure for use in catalytic distillation |
| US4471154A (en) * | 1983-06-10 | 1984-09-11 | Chevron Research Company | Staged, fluidized-bed distillation-reactor and a process for using such reactor |
-
1988
- 1988-03-08 FR FR8803095A patent/FR2628418B1/fr not_active Expired - Lifetime
- 1988-03-21 US US07/171,340 patent/US4847431A/en not_active Expired - Lifetime
-
1989
- 1989-03-06 AT AT89400623T patent/ATE74583T1/de not_active IP Right Cessation
- 1989-03-06 EP EP89400623A patent/EP0332525B1/de not_active Expired - Lifetime
- 1989-03-06 ES ES198989400623T patent/ES2032116T3/es not_active Expired - Lifetime
- 1989-03-06 DE DE8989400623T patent/DE68901149D1/de not_active Expired - Lifetime
- 1989-03-08 JP JP1057691A patent/JP2681211B2/ja not_active Expired - Fee Related
- 1989-03-08 KR KR1019890002829A patent/KR930000920B1/ko not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| KR930000920B1 (ko) | 1993-02-11 |
| ES2032116T3 (es) | 1993-01-01 |
| FR2628418B1 (fr) | 1991-01-04 |
| FR2628418A1 (fr) | 1989-09-15 |
| DE68901149D1 (de) | 1992-05-14 |
| EP0332525A1 (de) | 1989-09-13 |
| US4847431A (en) | 1989-07-11 |
| EP0332525B1 (de) | 1992-04-08 |
| JPH01316337A (ja) | 1989-12-21 |
| JP2681211B2 (ja) | 1997-11-26 |
| KR890014424A (ko) | 1989-10-23 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| REN | Ceased due to non-payment of the annual fee |