ATE391131T1 - Verfahren zur herstellung von acylphosphinen - Google Patents
Verfahren zur herstellung von acylphosphinenInfo
- Publication number
- ATE391131T1 ATE391131T1 AT04763601T AT04763601T ATE391131T1 AT E391131 T1 ATE391131 T1 AT E391131T1 AT 04763601 T AT04763601 T AT 04763601T AT 04763601 T AT04763601 T AT 04763601T AT E391131 T1 ATE391131 T1 AT E391131T1
- Authority
- AT
- Austria
- Prior art keywords
- sub
- alkali metal
- phenyl
- formula
- acylphosphines
- Prior art date
Links
- 238000004519 manufacturing process Methods 0.000 title 1
- 229910052783 alkali metal Inorganic materials 0.000 abstract 4
- 150000001340 alkali metals Chemical class 0.000 abstract 4
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 abstract 2
- 239000012190 activator Substances 0.000 abstract 2
- 238000000034 method Methods 0.000 abstract 2
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 abstract 2
- -1 phosphorus halides Chemical class 0.000 abstract 2
- 239000002904 solvent Substances 0.000 abstract 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 150000001338 aliphatic hydrocarbons Chemical class 0.000 abstract 1
- 125000003545 alkoxy group Chemical group 0.000 abstract 1
- 150000004945 aromatic hydrocarbons Chemical class 0.000 abstract 1
- MVPPADPHJFYWMZ-IDEBNGHGSA-N chlorobenzene Chemical group Cl[13C]1=[13CH][13CH]=[13CH][13CH]=[13CH]1 MVPPADPHJFYWMZ-IDEBNGHGSA-N 0.000 abstract 1
- MVPPADPHJFYWMZ-UHFFFAOYSA-N chlorobenzene Substances ClC1=CC=CC=C1 MVPPADPHJFYWMZ-UHFFFAOYSA-N 0.000 abstract 1
- ZUOUZKKEUPVFJK-UHFFFAOYSA-N diphenyl Chemical group C1=CC=CC=C1C1=CC=CC=C1 ZUOUZKKEUPVFJK-UHFFFAOYSA-N 0.000 abstract 1
- 239000006185 dispersion Substances 0.000 abstract 1
- 150000004820 halides Chemical class 0.000 abstract 1
- 229910052736 halogen Inorganic materials 0.000 abstract 1
- 150000002367 halogens Chemical class 0.000 abstract 1
- 239000000543 intermediate Substances 0.000 abstract 1
- 238000002955 isolation Methods 0.000 abstract 1
- 239000002923 metal particle Substances 0.000 abstract 1
- 125000001624 naphthyl group Chemical group 0.000 abstract 1
- 239000002245 particle Substances 0.000 abstract 1
- 229910052698 phosphorus Inorganic materials 0.000 abstract 1
- 239000011574 phosphorus Substances 0.000 abstract 1
- 238000002360 preparation method Methods 0.000 abstract 1
- 229910052708 sodium Inorganic materials 0.000 abstract 1
- 239000011734 sodium Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/50—Organo-phosphines
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/50—Organo-phosphines
- C07F9/5036—Phosphines containing the structure -C(=X)-P or NC-P
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/50—Organo-phosphines
- C07F9/53—Organo-phosphine oxides; Organo-phosphine thioxides
- C07F9/5337—Phosphine oxides or thioxides containing the structure -C(=X)-P(=X) or NC-P(=X) (X = O, S, Se)
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Crystallography & Structural Chemistry (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Saccharide Compounds (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP03016649 | 2003-07-31 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE391131T1 true ATE391131T1 (de) | 2008-04-15 |
Family
ID=34130031
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT04763601T ATE391131T1 (de) | 2003-07-31 | 2004-07-29 | Verfahren zur herstellung von acylphosphinen |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US20060229469A1 (enExample) |
| EP (1) | EP1651655B1 (enExample) |
| JP (1) | JP4461142B2 (enExample) |
| KR (1) | KR20060066077A (enExample) |
| CN (1) | CN100436461C (enExample) |
| AT (1) | ATE391131T1 (enExample) |
| DE (1) | DE602004012865T2 (enExample) |
| TW (1) | TW200523265A (enExample) |
| WO (1) | WO2005014606A1 (enExample) |
Families Citing this family (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| PL1648908T3 (pl) * | 2003-07-18 | 2007-01-31 | Igm Malta Ltd | Sposób wytwarzania acylofosfanów i ich pochodnych |
| JP5243789B2 (ja) | 2004-03-15 | 2013-07-24 | シティ・オブ・ホープ | 二本鎖ｒｎａによる遺伝子発現の特異的阻害のための方法及び組成物 |
| KR101230940B1 (ko) * | 2004-11-23 | 2013-02-08 | 시바 홀딩 인크 | 아실포스판 및 이의 유도체의 제조방법 |
| EP1838721B1 (en) * | 2005-01-17 | 2011-12-21 | Basf Se | Process for preparing acylphosphanes and their oxides and sulphides |
| DE102005005946A1 (de) * | 2005-02-10 | 2006-08-17 | Basf Ag | Verfahren zur Herstellung tertiärer Phosphine |
| CN102241792B (zh) * | 2010-05-10 | 2012-12-12 | 天津市裕北涂料有限公司 | 亲水性高分子聚合物光敏引发剂及其制备方法 |
| CN102471633B (zh) * | 2010-06-30 | 2015-03-18 | 帝斯曼知识产权资产管理有限公司 | D1479稳定的液体双酰基膦光引发剂及其在可辐射固化组合物中的用途 |
| CN102675365A (zh) * | 2012-05-16 | 2012-09-19 | 湖北固润科技股份有限公司 | 一种紫外光引发剂xbpo合成方法 |
| GB201213163D0 (en) | 2012-07-24 | 2012-09-05 | Lambson Ltd | Photopolymerisation processes and novel compounds therefor |
| CN103980310B (zh) * | 2014-05-30 | 2016-01-13 | 天津久日新材料股份有限公司 | 苯基双(2,4,6-三甲基苯甲酰基)氧化膦的制备方法 |
| CN104592298B (zh) * | 2014-12-31 | 2016-07-06 | 湖北固润科技股份有限公司 | 一种酰基膦高效光引发剂及其制备方法 |
| CN105348322B (zh) * | 2015-12-03 | 2017-08-25 | 山东久日化学科技有限公司 | 一种苯基双（2,4,6‑三甲基苯甲酰基）氧化膦的制备方法 |
| CN110183487A (zh) * | 2019-05-30 | 2019-08-30 | 王清才 | 一种苯基双(2,4,6-三甲基苯甲酰基)氧化膦的制备方法 |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2642344A (en) * | 1950-07-15 | 1953-06-16 | Du Pont | Alkali metal dispersions |
| DE2007535C3 (de) * | 1970-02-19 | 1974-12-12 | Basf Ag, 6700 Ludsigshafen | Verfahren zur Herstellung von Triarylphosphinen |
| DE2909994A1 (de) * | 1979-03-14 | 1980-10-02 | Basf Ag | Acylphosphinoxidverbindungen, ihre herstellung und verwendung |
| DE3763681D1 (de) * | 1986-02-11 | 1990-08-23 | Ici Plc | Produktion von phosphiniten und phosphoniten. |
| RU2091385C1 (ru) * | 1991-09-23 | 1997-09-27 | Циба-Гейги АГ | Бисацилфосфиноксиды, состав и способ нанесения покрытий |
| US5276219A (en) * | 1992-11-06 | 1994-01-04 | Fmc Corporation | Preparation of lithium alkoxides |
| US5318228A (en) * | 1992-12-15 | 1994-06-07 | Neos Technology Inc. | Sodium dispersion and organohalide reaction processes |
| GB2280671A (en) * | 1993-08-04 | 1995-02-08 | Ass Octel | Sodium amide complexes |
| US5321148A (en) * | 1993-12-30 | 1994-06-14 | Fmc Corporation | Process for preparing functionalized alkyllithium compounds |
| US5912378A (en) * | 1994-07-25 | 1999-06-15 | Fmc Corporation | Process for preparing trimethylsilyloxy functionalized alkyllithium compounds |
| ATE221893T1 (de) * | 1998-11-30 | 2002-08-15 | Ciba Sc Holding Ag | Verfahren zur herstellung von acylphosphinen und derivaten |
| PL1648908T3 (pl) * | 2003-07-18 | 2007-01-31 | Igm Malta Ltd | Sposób wytwarzania acylofosfanów i ich pochodnych |
-
2004
- 2004-07-13 TW TW093120905A patent/TW200523265A/zh unknown
- 2004-07-29 KR KR1020067002067A patent/KR20060066077A/ko not_active Ceased
- 2004-07-29 WO PCT/EP2004/008497 patent/WO2005014606A1/en not_active Ceased
- 2004-07-29 AT AT04763601T patent/ATE391131T1/de not_active IP Right Cessation
- 2004-07-29 US US10/565,542 patent/US20060229469A1/en not_active Abandoned
- 2004-07-29 DE DE602004012865T patent/DE602004012865T2/de not_active Expired - Lifetime
- 2004-07-29 JP JP2006521522A patent/JP4461142B2/ja not_active Expired - Fee Related
- 2004-07-29 EP EP04763601A patent/EP1651655B1/en not_active Expired - Lifetime
- 2004-07-29 CN CNB2004800220275A patent/CN100436461C/zh not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| DE602004012865D1 (de) | 2008-05-15 |
| EP1651655B1 (en) | 2008-04-02 |
| CN100436461C (zh) | 2008-11-26 |
| JP2007533599A (ja) | 2007-11-22 |
| KR20060066077A (ko) | 2006-06-15 |
| CN1829723A (zh) | 2006-09-06 |
| DE602004012865T2 (de) | 2008-07-31 |
| TW200523265A (en) | 2005-07-16 |
| JP4461142B2 (ja) | 2010-05-12 |
| EP1651655A1 (en) | 2006-05-03 |
| WO2005014606A1 (en) | 2005-02-17 |
| US20060229469A1 (en) | 2006-10-12 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| RER | Ceased as to paragraph 5 lit. 3 law introducing patent treaties |