ATE304510T1 - Verfahren und vorrichtung zur herstellung von schwerem wasser - Google Patents

Verfahren und vorrichtung zur herstellung von schwerem wasser

Info

Publication number
ATE304510T1
ATE304510T1 AT01273576T AT01273576T ATE304510T1 AT E304510 T1 ATE304510 T1 AT E304510T1 AT 01273576 T AT01273576 T AT 01273576T AT 01273576 T AT01273576 T AT 01273576T AT E304510 T1 ATE304510 T1 AT E304510T1
Authority
AT
Austria
Prior art keywords
heavy water
circe
bhw
producing heavy
stages
Prior art date
Application number
AT01273576T
Other languages
English (en)
Inventor
William R C Graham
Original Assignee
Ca Atomic Energy Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ca Atomic Energy Ltd filed Critical Ca Atomic Energy Ltd
Application granted granted Critical
Publication of ATE304510T1 publication Critical patent/ATE304510T1/de

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B5/00—Water
    • C01B5/02—Heavy water; Preparation by chemical reaction of hydrogen isotopes or their compounds, e.g. 4ND3 + 7O2 ---> 4NO2 + 6D2O, 2D2 + O2 ---> 2D2O
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D59/00—Separation of different isotopes of the same chemical element
    • B01D59/28—Separation by chemical exchange
    • B01D59/32—Separation by chemical exchange by exchange between fluids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D59/00—Separation of different isotopes of the same chemical element
    • B01D59/28—Separation by chemical exchange
    • B01D59/32—Separation by chemical exchange by exchange between fluids
    • B01D59/33—Separation by chemical exchange by exchange between fluids involving dual temperature exchange
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen; Reversible storage of hydrogen
    • C01B3/02—Production of hydrogen; Production of gaseous mixtures containing hydrogen
    • C01B3/32—Production of hydrogen; Production of gaseous mixtures containing hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide or air
    • C01B3/34—Production of hydrogen; Production of gaseous mixtures containing hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide or air by reaction of hydrocarbons with gasifying agents
    • C01B3/38—Production of hydrogen; Production of gaseous mixtures containing hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide or air by reaction of hydrocarbons with gasifying agents using catalysts
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/02—Processes for making hydrogen or synthesis gas
    • C01B2203/0205—Processes for making hydrogen or synthesis gas containing a reforming step
    • C01B2203/0227—Processes for making hydrogen or synthesis gas containing a reforming step containing a catalytic reforming step
    • C01B2203/0233—Processes for making hydrogen or synthesis gas containing a reforming step containing a catalytic reforming step the reforming step being a steam reforming step
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/02—Processes for making hydrogen or synthesis gas
    • C01B2203/0283—Processes for making hydrogen or synthesis gas containing a CO-shift step, i.e. a water gas shift step
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04—Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/042—Purification by adsorption on solids
    • C01B2203/043—Regenerative adsorption process in two or more beds, one for adsorption, the other for regeneration
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04—Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0465—Composition of the impurity
    • C01B2203/047—Composition of the impurity the impurity being carbon monoxide
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04—Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0465—Composition of the impurity
    • C01B2203/0475—Composition of the impurity the impurity being carbon dioxide
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/06—Integration with other chemical processes
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/06—Integration with other chemical processes
    • C01B2203/068—Ammonia synthesis
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/12—Feeding the process for making hydrogen or synthesis gas
    • C01B2203/1205—Composition of the feed
    • C01B2203/1211—Organic compounds or organic mixtures used in the process for making hydrogen or synthesis gas
    • C01B2203/1235—Hydrocarbons
    • C01B2203/1241—Natural gas or methane
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/12—Feeding the process for making hydrogen or synthesis gas
    • C01B2203/1258—Pre-treatment of the feed
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/14—Details of the flowsheet
    • C01B2203/148—Details of the flowsheet involving a recycle stream to the feed of the process for making hydrogen or synthesis gas
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/80—Aspect of integrated processes for the production of hydrogen or synthesis gas not covered by groups C01B2203/02 - C01B2203/1695
    • C01B2203/82—Several process steps of C01B2203/02 - C01B2203/08 integrated into a single apparatus

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Combustion & Propulsion (AREA)
  • Hydrogen, Water And Hydrids (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)
  • Catalysts (AREA)
AT01273576T 2001-01-31 2001-12-18 Verfahren und vorrichtung zur herstellung von schwerem wasser ATE304510T1 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US09/774,046 US6858190B2 (en) 2001-01-31 2001-01-31 Heavy water production process and apparatus
PCT/CA2001/001821 WO2002060814A1 (en) 2001-01-31 2001-12-18 Heavy water production process and apparatus

Publications (1)

Publication Number Publication Date
ATE304510T1 true ATE304510T1 (de) 2005-09-15

Family

ID=25100081

Family Applications (1)

Application Number Title Priority Date Filing Date
AT01273576T ATE304510T1 (de) 2001-01-31 2001-12-18 Verfahren und vorrichtung zur herstellung von schwerem wasser

Country Status (9)

Country Link
US (1) US6858190B2 (de)
EP (1) EP1355850B1 (de)
KR (1) KR100808706B1 (de)
CN (1) CN100381354C (de)
AT (1) ATE304510T1 (de)
CA (1) CA2434271C (de)
DE (1) DE60113457T2 (de)
RO (1) RO121959B1 (de)
WO (1) WO2002060814A1 (de)

Families Citing this family (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102006062740A1 (de) * 2006-01-05 2008-06-26 Bullemer, Bernhard, Prof. Dr. Desinfektionsbedürftiger Gegenstand und Desinfektionsverfahren hierfür, Medikament
CN101264862B (zh) * 2007-03-16 2010-10-13 柯香文 一种制取重水及氘气的生产方法
US20110027166A1 (en) * 2009-07-29 2011-02-03 Stuart Andrew T B Chlorate and chlorine dioxide systems adapted for the production of deuterium enriched water
WO2011152909A2 (en) 2010-03-09 2011-12-08 Kurion, Inc. Isotope-specific separation and vitrification using ion-specific media
US9981868B2 (en) 2010-04-02 2018-05-29 Kurion, Inc. Mobile processing system for hazardous and radioactive isotope removal
US10940437B2 (en) 2010-04-02 2021-03-09 Veolia Nuclear Solutions, Inc. Advanced tritium system and advanced permeation system for separation of tritium from radioactive wastes
WO2011123851A1 (en) * 2010-04-02 2011-10-06 Kurion, Inc. Tritium and permeation system for separation of tritium from radioactive wastes and reactor water
KR101277343B1 (ko) * 2010-09-30 2013-06-20 한국수력원자력 주식회사 양온 교대 액상 촉매 반응탑을 이용한 중수소 감축수의 제조장치 및 방법
WO2013191780A2 (en) 2012-03-26 2013-12-27 Kurion, Inc. Submersible filters for use in separating radioactive isotopes from radioactive waste materials
US9670064B1 (en) 2012-09-27 2017-06-06 Consolidated Nuclear Security, LLC Production of heavy water
CN103849884B (zh) * 2012-11-28 2016-01-13 柯香文 一种用于轻水电解法制取超轻水的设备
EP3160599B1 (de) 2014-06-24 2019-08-07 Kurion, Inc. Mobiles verarbeitungssystem zur entfernung gefährlicher und radioaktiver isotope
CN113800586A (zh) * 2021-09-23 2021-12-17 大连理工大学 一种双向强化生产重氧水与重水的方法
GB202214710D0 (en) 2022-10-06 2022-11-23 Nacamed As New methods for production of deuterium oxide and deuterium gas
KR102846452B1 (ko) * 2023-06-29 2025-08-14 (주)아이티켐 Cece를 이용한 중수의 분리 및 농축 장치
CN119819120B (zh) * 2024-12-24 2025-11-25 中国原子能科学研究院 一种双温水氢交换装置
CN119793338B (zh) * 2024-12-24 2026-01-06 中国原子能科学研究院 一种水氢交换系统

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2098554A (en) * 1936-07-14 1937-11-09 Air O Cel Ind Inc Heat insulating wall
BE542187A (de) * 1954-10-22
NL199776A (de) * 1956-04-30 1900-01-01
US3983226A (en) * 1969-07-30 1976-09-28 Atomic Energy Of Canada Limited Gas stripping and recirculation process in heavy water separation plant
US3807960A (en) * 1969-08-04 1974-04-30 V Thayer Apparatus for enrichment of deuterium between water and hydrogen sulfide by countercurrent mass transfer
US3981976A (en) * 1970-01-28 1976-09-21 Atomic Energy Of Canada Limited Process for hydrogen isotope concentration between liquid water and hydrogen gas
CA907292A (en) * 1970-01-28 1972-08-15 H. Stevens William Process and catalyst for enriching a fluid with hydrogen isotopes
CA1014515A (en) * 1974-05-03 1977-07-26 Her Majesty In Right Of Canada As Represented By Atomic Energy Of Canada Limited Method of producing heavy water involving catalytic-electrolytic exchange processes
CH616602A5 (de) * 1975-09-22 1980-04-15 Sulzer Ag
CA1095848A (en) * 1978-03-30 1981-02-17 Electrolyser Corporation Ltd. (The) Heavy-water extraction from non-electrolytic hydrogen streams
DE3033289A1 (de) * 1980-09-01 1982-03-25 Gebrüder Sulzer AG, 8401 Winterthur Verfahren zur herstellung von mit deuterium angereichertem wasser bei der gewinnung von wasserstoff
DE3033290A1 (de) * 1980-09-01 1982-03-25 Gebrüder Sulzer AG, 8401 Winterthur Verfahren zur herstellung von mit deuterium angereichertem wasser bei der gewinnung von wasserstoff
CN1036744A (zh) * 1989-04-18 1989-11-01 葛晓峰 重水电磁提炼法
US5591319A (en) * 1995-05-10 1997-01-07 Atomic Energy Of Canada Limited/Energie Atomique Du Canada Limitee Electrolytic pre-enrichment method and apparatus for the combined electrolysis and catalytic exchange process

Also Published As

Publication number Publication date
CA2434271C (en) 2009-11-24
RO121959B1 (ro) 2008-09-30
KR20040004517A (ko) 2004-01-13
CN1487903A (zh) 2004-04-07
EP1355850B1 (de) 2005-09-14
US6858190B2 (en) 2005-02-22
CA2434271A1 (en) 2002-08-08
WO2002060814A1 (en) 2002-08-08
CN100381354C (zh) 2008-04-16
US20020141916A1 (en) 2002-10-03
DE60113457D1 (de) 2005-10-20
EP1355850A1 (de) 2003-10-29
KR100808706B1 (ko) 2008-02-29
DE60113457T2 (de) 2006-06-22

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