ATE285989T1 - Sphäroidische graphitteilchen mit einem niedrigen gehalt an oberflächenverunreinigungen sowie verfahren zu deren herstellung - Google Patents

Sphäroidische graphitteilchen mit einem niedrigen gehalt an oberflächenverunreinigungen sowie verfahren zu deren herstellung

Info

Publication number
ATE285989T1
ATE285989T1 AT01982009T AT01982009T ATE285989T1 AT E285989 T1 ATE285989 T1 AT E285989T1 AT 01982009 T AT01982009 T AT 01982009T AT 01982009 T AT01982009 T AT 01982009T AT E285989 T1 ATE285989 T1 AT E285989T1
Authority
AT
Austria
Prior art keywords
graphite particles
mill
spherioidic
production
function
Prior art date
Application number
AT01982009T
Other languages
English (en)
Inventor
Abdelbast Guerfi
Fernand Brochu
Kimio Kinoshita
Karim Zaghib
Original Assignee
Hydro Quebec
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hydro Quebec filed Critical Hydro Quebec
Application granted granted Critical
Publication of ATE285989T1 publication Critical patent/ATE285989T1/de

Links

Classifications

    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/13Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
    • H01M4/133Electrodes based on carbonaceous material, e.g. graphite-intercalation compounds or CFx
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30Processes for preparing, regenerating, or reactivating
    • B01J20/32Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
    • B01J20/3202Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the carrier, support or substrate used for impregnation or coating
    • B01J20/3204Inorganic carriers, supports or substrates
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30Processes for preparing, regenerating, or reactivating
    • B01J20/32Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
    • B01J20/3231Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the coating or impregnating layer
    • B01J20/3234Inorganic material layers
    • B01J20/3236Inorganic material layers containing metal, other than zeolites, e.g. oxides, hydroxides, sulphides or salts
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30Processes for preparing, regenerating, or reactivating
    • B01J20/32Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
    • B01J20/3291Characterised by the shape of the carrier, the coating or the obtained coated product
    • B01J20/3293Coatings on a core, the core being particle or fiber shaped, e.g. encapsulated particles, coated fibers
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00Carbon; Compounds thereof
    • C01B32/20Graphite
    • C01B32/21After-treatment
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N27/00Investigating or analysing materials by the use of electric, electrochemical, or magnetic means
    • G01N27/26Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating electrochemical variables; by using electrolysis or electrophoresis
    • G01N27/403Cells and electrode assemblies
    • G01N27/406Cells and probes with solid electrolytes
    • G01N27/407Cells and probes with solid electrolytes for investigating or analysing gases
    • G01N27/4075Composition or fabrication of the electrodes and coatings thereon, e.g. catalysts
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00Secondary cells; Manufacture thereof
    • H01M10/05Accumulators with non-aqueous electrolyte
    • H01M10/052Li-accumulators
    • H01M10/0525Rocking-chair batteries, i.e. batteries with lithium insertion or intercalation in both electrodes; Lithium-ion batteries
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/04Processes of manufacture in general
    • H01M4/0402Methods of deposition of the material
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/04Processes of manufacture in general
    • H01M4/0402Methods of deposition of the material
    • H01M4/0404Methods of deposition of the material by coating on electrode collectors
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/04Processes of manufacture in general
    • H01M4/0402Methods of deposition of the material
    • H01M4/0409Methods of deposition of the material by a doctor blade method, slip-casting or roller coating
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/13Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
    • H01M4/139Processes of manufacture
    • H01M4/1393Processes of manufacture of electrodes based on carbonaceous material, e.g. graphite-intercalation compounds or CFx
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/36Selection of substances as active materials, active masses, active liquids
    • H01M4/58Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
    • H01M4/583Carbonaceous material, e.g. graphite-intercalation compounds or CFx
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/36Selection of substances as active materials, active masses, active liquids
    • H01M4/58Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
    • H01M4/583Carbonaceous material, e.g. graphite-intercalation compounds or CFx
    • H01M4/587Carbonaceous material, e.g. graphite-intercalation compounds or CFx for inserting or intercalating light metals
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/62Selection of inactive substances as ingredients for active masses, e.g. binders, fillers
    • H01M4/621Binders
    • H01M4/622Binders being polymers
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/62Selection of inactive substances as ingredients for active masses, e.g. binders, fillers
    • H01M4/621Binders
    • H01M4/622Binders being polymers
    • H01M4/623Binders being polymers fluorinated polymers
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/86Inert electrodes with catalytic activity, e.g. for fuel cells
    • H01M4/96Carbon-based electrodes
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M50/00Constructional details or processes of manufacture of the non-active parts of electrochemical cells other than fuel cells, e.g. hybrid cells
    • H01M50/10Primary casings; Jackets or wrappings
    • H01M50/102Primary casings; Jackets or wrappings characterised by their shape or physical structure
    • H01M50/109Primary casings; Jackets or wrappings characterised by their shape or physical structure of button or coin shape
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M8/00Fuel cells; Manufacture thereof
    • H01M8/02Details
    • H01M8/0202Collectors; Separators, e.g. bipolar separators; Interconnectors
    • H01M8/023Porous and characterised by the material
    • H01M8/0234Carbonaceous material
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/70Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/51Particles with a specific particle size distribution
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/61Micrometer sized, i.e. from 1-100 micrometer
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/11Powder tap density
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/12Surface area
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/80Compositional purity
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00Secondary cells; Manufacture thereof
    • H01M10/05Accumulators with non-aqueous electrolyte
    • H01M10/052Li-accumulators
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M2004/021Physical characteristics, e.g. porosity, surface area
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M2004/026Electrodes composed of, or comprising, active material characterised by the polarity
    • H01M2004/027Negative electrodes
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/86Inert electrodes with catalytic activity, e.g. for fuel cells
    • H01M2004/8678Inert electrodes with catalytic activity, e.g. for fuel cells characterised by the polarity
    • H01M2004/8684Negative electrodes
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10Energy storage using batteries
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/30Hydrogen technology
    • Y02E60/50Fuel cells
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P70/00Climate change mitigation technologies in the production process for final industrial or consumer products
    • Y02P70/50Manufacturing or production processes characterised by the final manufactured product
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00Stock material or miscellaneous articles
    • Y10T428/29Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2913Rod, strand, filament or fiber
    • Y10T428/2918Rod, strand, filament or fiber including free carbon or carbide or therewith [not as steel]
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00Stock material or miscellaneous articles
    • Y10T428/29Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2913Rod, strand, filament or fiber
    • Y10T428/2933Coated or with bond, impregnation or core
    • Y10T428/2964Artificial fiber or filament
    • Y10T428/2967Synthetic resin or polymer
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00Stock material or miscellaneous articles
    • Y10T428/29Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2982Particulate matter [e.g., sphere, flake, etc.]
    • Y10T428/2991Coated

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Materials Engineering (AREA)
  • Health & Medical Sciences (AREA)
  • Immunology (AREA)
  • General Health & Medical Sciences (AREA)
  • Pathology (AREA)
  • General Physics & Mathematics (AREA)
  • Molecular Biology (AREA)
  • Physics & Mathematics (AREA)
  • Biochemistry (AREA)
  • Sustainable Development (AREA)
  • Geology (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Sustainable Energy (AREA)
  • Carbon And Carbon Compounds (AREA)
  • Battery Electrode And Active Subsutance (AREA)
  • Secondary Cells (AREA)
  • Fuel Cell (AREA)
  • Inert Electrodes (AREA)
AT01982009T 2000-10-25 2001-10-24 Sphäroidische graphitteilchen mit einem niedrigen gehalt an oberflächenverunreinigungen sowie verfahren zu deren herstellung ATE285989T1 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CA002324431A CA2324431A1 (fr) 2000-10-25 2000-10-25 Nouveau procede d'obtention de particule du graphite naturel sous forme spherique: modelisation et application
PCT/CA2001/001511 WO2002034670A1 (fr) 2000-10-25 2001-10-24 Particules de graphite ayant la forme d'un patatoïde et un faible taux d'impuretés en surface, procédé pour leur préparation

Publications (1)

Publication Number Publication Date
ATE285989T1 true ATE285989T1 (de) 2005-01-15

Family

ID=4167466

Family Applications (1)

Application Number Title Priority Date Filing Date
AT01982009T ATE285989T1 (de) 2000-10-25 2001-10-24 Sphäroidische graphitteilchen mit einem niedrigen gehalt an oberflächenverunreinigungen sowie verfahren zu deren herstellung

Country Status (8)

Country Link
US (7) US20040053050A1 (de)
EP (1) EP1334065B1 (de)
JP (3) JP4610851B2 (de)
AT (1) ATE285989T1 (de)
AU (1) AU2002213710A1 (de)
CA (2) CA2324431A1 (de)
DE (1) DE60108163T2 (de)
WO (1) WO2002034670A1 (de)

Families Citing this family (28)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA2324431A1 (fr) * 2000-10-25 2002-04-25 Hydro-Quebec Nouveau procede d'obtention de particule du graphite naturel sous forme spherique: modelisation et application
JP2002348110A (ja) 2001-05-28 2002-12-04 Mitsui Mining Co Ltd 黒鉛粒子、及びその製造方法
FR2834818B1 (fr) * 2002-01-14 2006-09-15 Atofina Poudre microcomposite a base de plaquettes de graphite et d'un fluoropolymere et objets fabriques avec cette poudre
CA2374132A1 (fr) * 2002-03-01 2003-09-01 Hydro Quebec Procede de purification en surface d'un graphite contenant des impuretes a l'aide d'une solution aqueuse diluee de nh4f et de h2so4
JPWO2005090262A1 (ja) * 2004-03-19 2008-01-31 日本碍子株式会社 多孔質セラミック構造体の製造方法
CN101184798A (zh) * 2005-05-27 2008-05-21 纳幕尔杜邦公司 具有低热膨胀系数的树脂组合物和由其制备的制品
WO2007021640A2 (en) * 2005-08-11 2007-02-22 United States Of America As Represented By The Administrator Of The National Aeronautics And Space Administration Bimetallic treatment system and its application for removal and remediation of polychlorinated biphenyls (pcbs)
US7842639B2 (en) * 2006-05-19 2010-11-30 The United States Of America As Represented By The Administrator Of The National Aeronautics And Space Administration Mechanical alloying of a hydrogenation catalyst used for the remediation of contaminated compounds
JP5151278B2 (ja) 2007-07-06 2013-02-27 ソニー株式会社 二次電池用負極および二次電池
EP2285407A4 (de) * 2008-05-16 2014-10-01 U S A As Representated By The Administrator Of The Nat Aeronautics And Space Administration Nullwertiges metallisches behandlungssystem und seine anwendung zur entfernung und dekontamination von polychlorierten biphenylen
JP2010073793A (ja) * 2008-09-17 2010-04-02 Japan Gore Tex Inc 電気二重層キャパシタ用電極および電気二重層キャパシタ
JP5386666B2 (ja) * 2008-11-04 2014-01-15 東海カーボン株式会社 リチウム二次電池用負極材、その製造方法およびリチウム二次電池
EP2393753B1 (de) * 2009-02-03 2013-09-25 Timcal S.a. Neues graphitmaterial
US20120258374A1 (en) * 2009-09-10 2012-10-11 The University Western Australia Process for Producing Hydrogen from Hydrocarbons
US9558860B2 (en) * 2010-09-10 2017-01-31 Samsung Electronics Co., Ltd. Graphene-enhanced anode particulates for lithium ion batteries
GB201307898D0 (en) * 2012-06-14 2013-06-12 Hexcel Composites Ltd Improvements in composite materials
WO2014097511A1 (ja) 2012-12-20 2014-06-26 パナソニック株式会社 アルカリ電池
JP2014194852A (ja) * 2013-03-28 2014-10-09 Mt Carbon Co Ltd リチウムイオン二次電池負極用の非晶質炭素材料及び黒鉛質炭素材料、それらを用いたリチウムイオン二次電池並びにリチウムイオン二次電池負極用の炭素材料の製造方法
US9991507B2 (en) * 2013-07-26 2018-06-05 Lg Chem, Ltd. Electrode for secondary battery having improved energy density and lithium secondary battery including the same
US20170047581A1 (en) * 2014-02-11 2017-02-16 Batelle Memorial Institute Additives to enhance electrode wetting and performance and methods of making electrodes comprising the same
JP6226944B2 (ja) * 2015-12-09 2017-11-08 Dowaエレクトロニクス株式会社 銀被覆黒鉛粒子、銀被覆黒鉛混合粉及びその製造方法、並びに導電性ペースト
WO2018186958A1 (en) * 2017-04-03 2018-10-11 The George Washington University Methods and systems for the production of crystalline flake graphite from biomass or other carbonaceous materials
JP7140480B2 (ja) * 2017-09-14 2022-09-21 トヨタ自動車株式会社 リチウムイオン二次電池と該電池の負極用黒鉛材およびその製造方法
CN108751187A (zh) * 2018-04-23 2018-11-06 合肥国轩高科动力能源有限公司 一种酸改性球形天然石墨负极材料的制备方法
US20210316994A1 (en) * 2018-08-31 2021-10-14 Zhanjiang Juxin New Energy Co., Ltd Spherical Graphite for Lithium Battery and Preparation Method thereof
CN109503166B (zh) * 2018-09-29 2021-07-23 广东凯金新能源科技股份有限公司 一种平台型锂离子电池用石墨负极材料及其制法
EP4298056A1 (de) * 2021-02-24 2024-01-03 Focus Graphite Inc. Erweiterte anodenmaterialien mit kugelförmigen additivverstärkten graphitpartikeln und verfahren zur herstellung davon
CN113307309A (zh) * 2021-04-08 2021-08-27 桂林理工大学 一种氟化锂包覆层转化提高锂离子电池三元正极材料循环性能的方法

Family Cites Families (33)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3440181A (en) 1965-03-22 1969-04-22 Dow Chemical Co Metal coated vermicular expanded graphite and polymer composition containing same
US4054687A (en) * 1976-06-01 1977-10-18 United Technologies Corporation Method for making a fuel cell electrode
US4028274A (en) * 1976-06-01 1977-06-07 United Technologies Corporation Support material for a noble metal catalyst and method for making the same
US4240830A (en) * 1978-11-30 1980-12-23 Westinghouse Electric Corp. Method for making sintered metal-coated graphite for high-current collector brushes
US4270348A (en) * 1979-07-23 1981-06-02 General Motors Corporation Materials and method for preventing high temperature seize between metal parts
US4263376A (en) * 1980-02-04 1981-04-21 Institute Of Gas Technology Fuel cell electrode
US4637197A (en) * 1984-10-15 1987-01-20 Epoxy Technology, Inc. Method and compositions for removal of moisture
JPS61219566A (ja) * 1985-03-25 1986-09-29 Toshiba Corp 研磨定盤用材料
US5045349A (en) * 1989-08-16 1991-09-03 The United States Of America As Represented By The Secretary Of The Navy Silver-nickel composite cathodes for alkaline secondary batteries
JPH05213611A (ja) * 1991-08-09 1993-08-24 Asahi Glass Co Ltd 黒鉛質粉体および黒鉛粉体の親水化処理方法
US5686138A (en) * 1991-11-12 1997-11-11 Sanyo Electric Co., Ltd. Lithium secondary battery
US5432029A (en) * 1993-05-14 1995-07-11 Sharp Kabushiki Kaisha Lithium secondary battery
JP2976300B1 (ja) * 1995-11-14 1999-11-10 大阪瓦斯株式会社 リチウム二次電池用負極材料の製造方法
JP3481063B2 (ja) * 1995-12-25 2003-12-22 シャープ株式会社 非水系二次電池
JP3873325B2 (ja) 1996-07-25 2007-01-24 大阪瓦斯株式会社 リチウム二次電池負極用炭素材及びその製造方法
FR2755372B1 (fr) * 1996-11-07 1998-12-24 Elf Aquitaine Dispositif d'ionophorese comportant au moins un ensemble electrode a membrane, pour l'administration transcutanee de principes actifs a un sujet
JP4029947B2 (ja) * 1997-05-30 2008-01-09 三菱化学株式会社 高充填性炭素質粉末の製造方法
JP3916012B2 (ja) * 1997-05-30 2007-05-16 三菱化学株式会社 非水系二次電池用電極
ID21480A (id) 1997-05-30 1999-06-17 Matsushita Electric Ind Co Ltd Sel sekunder elektrolit bukan-air
JP3193342B2 (ja) * 1997-05-30 2001-07-30 松下電器産業株式会社 非水電解質二次電池
JPH1131508A (ja) * 1997-07-09 1999-02-02 Matsushita Electric Ind Co Ltd 非水電解液二次電池
JPH11157816A (ja) 1997-11-21 1999-06-15 Unitika Ltd 金属被覆された球状ガラス状炭素
US6828064B1 (en) * 1998-01-07 2004-12-07 Eveready Battery Company, Inc. Alkaline cell having a cathode incorporating enhanced graphite
JP3787030B2 (ja) * 1998-03-18 2006-06-21 関西熱化学株式会社 鱗片状天然黒鉛改質粒子、その製造法、および二次電池
EP0977292A2 (de) * 1998-07-31 2000-02-02 Mitsui Mining Co., Ltd. Anodenmaterial für Sekundärbatterie, Verfahren zur Herstellung und Lithium-Sekundärbatterie
JP3106129B2 (ja) * 1998-07-31 2000-11-06 三井鉱山株式会社 リチウム二次電池用負極材料、その製造方法、及びリチウム二次電池
JP3620703B2 (ja) * 1998-09-18 2005-02-16 キヤノン株式会社 二次電池用負極電極材、電極構造体、二次電池、及びこれらの製造方法
CA2310374C (en) 1998-09-18 2007-09-04 Canon Kabushiki Kaisha Electrode material for anode of rechargeable lithium battery, electrode structural body using said electrode material, rechargeable lithium battery using said electrode structuralbody, process for producing said electrode structural body, and process for producing said rechargeable lithium battery
JP3685364B2 (ja) * 1999-03-23 2005-08-17 シャープ株式会社 炭素被覆黒鉛粒子の製造方法及び非水系二次電池
US6528033B1 (en) 2000-01-18 2003-03-04 Valence Technology, Inc. Method of making lithium-containing materials
JP2003528019A (ja) * 2000-02-25 2003-09-24 ハイドロ−ケベック 天然グラファイトの表面精製および粉砕および粒度分布に及ぼす不純物の効果
CA2324431A1 (fr) * 2000-10-25 2002-04-25 Hydro-Quebec Nouveau procede d'obtention de particule du graphite naturel sous forme spherique: modelisation et application
KR101047983B1 (ko) 2008-07-31 2011-07-13 한국과학기술연구원 Aa' 적층 흑연 및 그 제조 방법

Also Published As

Publication number Publication date
US20130323600A1 (en) 2013-12-05
JP4610851B2 (ja) 2011-01-12
DE60108163D1 (de) 2005-02-03
US20100092808A1 (en) 2010-04-15
JP2004511422A (ja) 2004-04-15
JP5740079B2 (ja) 2015-06-24
AU2002213710A1 (en) 2002-05-06
US20070071669A1 (en) 2007-03-29
CA2422660A1 (fr) 2002-05-02
CA2422660C (fr) 2011-06-14
US20130011554A1 (en) 2013-01-10
US20040053050A1 (en) 2004-03-18
US20160060119A1 (en) 2016-03-03
JP2009184915A (ja) 2009-08-20
US9444092B2 (en) 2016-09-13
JP2014028753A (ja) 2014-02-13
EP1334065A1 (de) 2003-08-13
US9508983B2 (en) 2016-11-29
US9312537B2 (en) 2016-04-12
US9412999B2 (en) 2016-08-09
EP1334065B1 (de) 2004-12-29
US20160141603A1 (en) 2016-05-19
US9184437B2 (en) 2015-11-10
DE60108163T2 (de) 2005-12-08
CA2324431A1 (fr) 2002-04-25
WO2002034670A1 (fr) 2002-05-02

Similar Documents

Publication Publication Date Title
ATE285989T1 (de) Sphäroidische graphitteilchen mit einem niedrigen gehalt an oberflächenverunreinigungen sowie verfahren zu deren herstellung
ATE478115T1 (de) Wässrige polyolefinharzdispersion, herstellungsverfahren dafür und diese enthaltendes wasserbasis-beschichtungsmaterial
WO2004038504A3 (en) Nanometer-scale engineered structures, methods and apparatus for fabrication thereof, and applications to mask repair, enhancement, and fabrication
TW200700362A (en) Process for producing an organic compound
EP2058278A3 (de) Expandierter Graphit und Verfahren zu seiner Herstellung
EP2284147A3 (de) Verfahren zur Herstellung eines Chlorhydrins
ATE235571T1 (de) Niobpulver und verfahren zu dessen herstellung
EP0982765A3 (de) Verfahren zur Reinigung eines Halbleitersubstrats
SG91943A1 (en) Regular-shaped particles of activated clay, method of producing the same and use thereof
EP1460056A4 (de) Verfahren zur herstellung von kohlensäureester
TW200518246A (en) Substrate and method for manufacturing the same
CA2179162A1 (en) Production of pentafluoroethane
EP1477481A4 (de) Verfahren zur herstellung eines chinazolin-4-onderivats
TW200704594A (en) Acidic zirconia sol and production process thereof
SG151328A1 (en) High solids content dispersions
EP1415968A4 (de) Verfahren zur herstellung einer etherverbindung
MY115656A (en) Method for recovering reusable elements from rare aerth-iron alloy
MY137537A (en) Method for producing organic acid
EP1515195A3 (de) Magnetischer Toner und Herstellungsverfahren
NZ506897A (en) Method for inhibiting the deposition of white pitch in paper production
PL1699537T3 (pl) Sposób wydzielania trioksanu z mieszaniny trioksan/formaldehyd/woda
EP1123735A3 (de) Mikroreaktor für Reaktionsmedien in Form einer Suspension
EP1327626A4 (de) Verfahren zur reinigung von plavastatin
EP1232873A4 (de) Harzzusammensetzung zu einem tintenstrahlaufzeichnungsblatt, das aufzeichnungsblatt, verfahren zur aufzeichnung und verfahren zur herstellung das aufzeichnungsblatt.
EP1426456A3 (de) Verfahren zur Herstellung von Hartmetallwerkzeuge oder Teile auf Wolframkarbidbasis

Legal Events

Date Code Title Description
RER Ceased as to paragraph 5 lit. 3 law introducing patent treaties