ATE16247T1 - Verfahren zum fraktionieren von gemischen durch elutionschromatographie mit einer ueberkritischen fluiden phase und anlage zur durchfuehrung dieses verfahrens. - Google Patents
Verfahren zum fraktionieren von gemischen durch elutionschromatographie mit einer ueberkritischen fluiden phase und anlage zur durchfuehrung dieses verfahrens.Info
- Publication number
- ATE16247T1 ATE16247T1 AT83401040T AT83401040T ATE16247T1 AT E16247 T1 ATE16247 T1 AT E16247T1 AT 83401040 T AT83401040 T AT 83401040T AT 83401040 T AT83401040 T AT 83401040T AT E16247 T1 ATE16247 T1 AT E16247T1
- Authority
- AT
- Austria
- Prior art keywords
- mixtures
- fractionation
- elution chromatography
- carrying
- equipment
- Prior art date
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
- B01D15/08—Selective adsorption, e.g. chromatography
- B01D15/26—Selective adsorption, e.g. chromatography characterised by the separation mechanism
- B01D15/40—Selective adsorption, e.g. chromatography characterised by the separation mechanism using supercritical fluid as mobile phase or eluent
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C7/00—Purification; Separation; Use of additives
- C07C7/12—Purification; Separation; Use of additives by adsorption, i.e. purification or separation of hydrocarbons with the aid of solids, e.g. with ion-exchangers
- C07C7/13—Purification; Separation; Use of additives by adsorption, i.e. purification or separation of hydrocarbons with the aid of solids, e.g. with ion-exchangers by molecular-sieve technique
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/26—Conditioning of the fluid carrier; Flow patterns
- G01N30/28—Control of physical parameters of the fluid carrier
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/26—Conditioning of the fluid carrier; Flow patterns
- G01N30/28—Control of physical parameters of the fluid carrier
- G01N30/34—Control of physical parameters of the fluid carrier of fluid composition, e.g. gradient
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/62—Detectors specially adapted therefor
- G01N2030/621—Detectors specially adapted therefor signal-to-noise ratio
- G01N2030/623—Detectors specially adapted therefor signal-to-noise ratio by modulation of sample feed or detector response
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/26—Conditioning of the fluid carrier; Flow patterns
- G01N30/38—Flow patterns
- G01N30/44—Flow patterns using recycling of the fraction to be distributed
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/80—Fraction collectors
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/54—Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids
Landscapes
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Organic Chemistry (AREA)
- Immunology (AREA)
- General Health & Medical Sciences (AREA)
- Pathology (AREA)
- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Physics & Mathematics (AREA)
- Water Supply & Treatment (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Treatment Of Liquids With Adsorbents In General (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR8209649A FR2527934A1 (fr) | 1982-06-03 | 1982-06-03 | Procede de fractionnement de melanges par chromatographie d'elution avec fluide en etat supercritique et installation pour sa mise en oeuvre |
EP83401040A EP0099765B1 (de) | 1982-06-03 | 1983-05-25 | Verfahren zum Fraktionieren von Gemischen durch Elutionschromatographie mit einer überkritischen fluiden Phase und Anlage zur Durchführung dieses Verfahrens |
Publications (1)
Publication Number | Publication Date |
---|---|
ATE16247T1 true ATE16247T1 (de) | 1985-11-15 |
Family
ID=9274587
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
AT83401040T ATE16247T1 (de) | 1982-06-03 | 1983-05-25 | Verfahren zum fraktionieren von gemischen durch elutionschromatographie mit einer ueberkritischen fluiden phase und anlage zur durchfuehrung dieses verfahrens. |
Country Status (7)
Country | Link |
---|---|
US (1) | US4478720A (de) |
EP (1) | EP0099765B1 (de) |
JP (1) | JPS5917157A (de) |
AT (1) | ATE16247T1 (de) |
CA (1) | CA1202913A (de) |
DE (1) | DE3361112D1 (de) |
FR (1) | FR2527934A1 (de) |
Families Citing this family (59)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS60241908A (ja) * | 1984-05-15 | 1985-11-30 | Morinaga & Co Ltd | 多成分系原料より精製成分を製造する方法 |
JPH0664032B2 (ja) * | 1985-10-12 | 1994-08-22 | 出光石油化学株式会社 | 超臨界流体による混合物からの特定成分の分離方法 |
JPS62138753A (ja) * | 1985-12-12 | 1987-06-22 | Hitachi Ltd | 液体クロマトグラフイによる分画・分取方法および装置 |
JPS62155908A (ja) * | 1985-12-28 | 1987-07-10 | Idemitsu Petrochem Co Ltd | 超臨界流体による水/アルコ−ル混合物の分離方法 |
JPS62192028A (ja) * | 1986-02-18 | 1987-08-22 | Hitachi Maxell Ltd | 磁気記録媒体 |
US4684465A (en) * | 1986-10-10 | 1987-08-04 | Combustion Engineering, Inc. | Supercritical fluid chromatograph with pneumatically controlled pump |
US4681678A (en) * | 1986-10-10 | 1987-07-21 | Combustion Engineering, Inc. | Sample dilution system for supercritical fluid chromatography |
US4859342A (en) * | 1986-10-14 | 1989-08-22 | Suntory Limited | Process for industrially separating biopolymers |
DE3717456C1 (de) * | 1987-05-23 | 1988-07-21 | Eberhard Gerstel | Gaschromatograph und Verfahren zur gaschromatographischen Trennung |
US4816159A (en) * | 1987-08-31 | 1989-03-28 | Aluminum Company Of America | Supercritical fluid chromatography packing material |
US4880543A (en) * | 1987-08-31 | 1989-11-14 | Aluminum Company Of America | Supercritical fluid chromatography packing material containing alumina |
JPS6483152A (en) * | 1987-09-25 | 1989-03-28 | Japan Spectroscopic Co | Recycling chromatograph |
US5180487A (en) * | 1987-09-25 | 1993-01-19 | Nihon Bunko Kogyo Kabushiki Kaisha | Pump apparatus for transferring a liquified gas used in a recycle chromatograph |
DE3863891D1 (de) * | 1987-10-08 | 1991-08-29 | Givaudan & Cie Sa | Vorrichtung zum verzweigen von gasstroemen. |
US5169522A (en) * | 1990-09-25 | 1992-12-08 | Ht Chemicals, Inc. | Column slurry packing compressor |
US5139681A (en) * | 1990-10-09 | 1992-08-18 | The Dow Chemical Company | On-line multidimensional chromatographic system with large volume injection handling for supercritical fluid chromatography |
JPH06502248A (ja) * | 1990-10-09 | 1994-03-10 | ザ ダウ ケミカル カンパニー | オンライン超臨界流体抽出多次元クロマトグラフィーシステム |
US5234599A (en) * | 1990-10-09 | 1993-08-10 | The Dow Chemical Company | On-line multidimensional chromatographic system with large volume injection handling for supercritical fluid chromatography |
US5372716A (en) * | 1991-02-28 | 1994-12-13 | Suprex Corporation | Supercritical fluid extraction coupled to analytical chromatography system |
CA2111695A1 (en) * | 1991-06-26 | 1993-01-07 | Noubar B. Afeyan | Method and apparatus for detecting trace contaminants |
CA2111084C (fr) * | 1992-04-29 | 2004-07-06 | Roger-Marc Nicoud | Procede et dispositif de fractionnement d'un melange en lit mobile simule en presence d'un gaz comprime, d'un fluide supercritique ou d'un liquide subcritique |
FR2694208B1 (fr) * | 1992-07-30 | 1994-09-23 | Separex Sa | Procédé et dispositif industriels de fractionnement de mélanges de composants par chromatographie. |
FR2690630B1 (fr) * | 1992-04-29 | 1994-07-22 | Separex Sa | Procede et dispositif de fractionnement de melanges de composants par voie chromatographique a l'aide d'un eluant a pression supercritique. |
US5458783A (en) * | 1992-08-13 | 1995-10-17 | Suprex Corporation | Supercritical fluid extraction coupled to analytical chromatography system |
US5346622A (en) * | 1993-03-04 | 1994-09-13 | Hewlett-Packard Company | Hydrocarbon class separation and quantitation by split column effluent analysis |
US5470377A (en) * | 1993-03-08 | 1995-11-28 | Whitlock; David R. | Separation of solutes in gaseous solvents |
ES2097047T3 (es) * | 1993-04-29 | 1997-03-16 | Norsk Hydro As | Procedimientos para el fraccionamiento cromatografico de acidos grasos y sus derivados. |
FI102758B (fi) * | 1995-03-03 | 1999-02-15 | Santen Pharmaceutical Co Ltd | Menetelmä puhtaan syklosporiinimuodon valmistamiseksi |
US5630943A (en) * | 1995-11-30 | 1997-05-20 | Merck Patent Gesellschaft Mit Beschrankter Haftung | Discontinuous countercurrent chromatographic process and apparatus |
US6063284A (en) * | 1997-05-15 | 2000-05-16 | Em Industries, Inc. | Single column closed-loop recycling with periodic intra-profile injection |
US6048369A (en) * | 1998-06-03 | 2000-04-11 | North Carolina State University | Method of dyeing hydrophobic textile fibers with colorant materials in supercritical fluid carbon dioxide |
US6413428B1 (en) * | 1999-09-16 | 2002-07-02 | Berger Instruments, Inc. | Apparatus and method for preparative supercritical fluid chromatography |
US6685828B2 (en) | 1999-09-16 | 2004-02-03 | Berger Instruments, Inc. | Automated sample collection in supercritical fluid chromatography |
US6261326B1 (en) | 2000-01-13 | 2001-07-17 | North Carolina State University | Method for introducing dyes and other chemicals into a textile treatment system |
US6632353B2 (en) | 2000-06-26 | 2003-10-14 | Berger Instruments, Inc. | Rapid sample collection in supercritical fluid chromatography |
US6558540B2 (en) * | 2000-06-26 | 2003-05-06 | Berger Instruments, Inc. | Exhaust gas collection system for supercritical fluid chromatography |
US6676710B2 (en) | 2000-10-18 | 2004-01-13 | North Carolina State University | Process for treating textile substrates |
US6601438B2 (en) | 2001-09-28 | 2003-08-05 | Systec, Inc. | Apparatus for conducting high-temperature liquid chromotography analysis |
US6802967B2 (en) * | 2002-03-06 | 2004-10-12 | Shimadzu Corporation | Multi-dimension liquid chromatography separation system |
JP2003347624A (ja) * | 2002-05-27 | 2003-12-05 | Konica Minolta Holdings Inc | 有機半導体材料の精製方法、該精製方法を用いて得られた有機半導体材料及びそれを用いた半導体素子 |
US6908557B2 (en) * | 2002-06-25 | 2005-06-21 | Thar Technologies, Inc. | Collection system for chromatographic system |
SE0202188D0 (sv) | 2002-07-11 | 2002-07-11 | Pronova Biocare As | A process for decreasing environmental pollutants in an oil or a fat, a volatile fat or oil environmental pollutants decreasing working fluid, a health supplement, and an animal feed product |
EP2295529B2 (de) | 2002-07-11 | 2022-05-18 | Basf As | Verfahren zur Verminderung von Umweltschadstoffen in einem Öl oder einem Fett und Fischfutterprodukt |
KR101156146B1 (ko) * | 2003-12-09 | 2012-06-18 | 재팬 사이언스 앤드 테크놀로지 에이젼시 | 질소면의 표면상의 구조물 제조를 통한 고효율 3족 질화물계 발광다이오드 |
JP4319551B2 (ja) * | 2004-01-05 | 2009-08-26 | ダイセル化学工業株式会社 | 超臨界流体クロマトグラフィーによる物質の分離方法及びこれに用いられる気液分離装置 |
US20060188397A1 (en) * | 2005-01-07 | 2006-08-24 | Lalit Chordia | Method and apparatus for fraction collection |
FR2882528B1 (fr) * | 2005-02-25 | 2007-05-25 | Pic Solution Soc Par Actions S | Procede mixte de chromatographie en phase supercritique et installation pour sa mise en oeuvre |
FR2889665B1 (fr) * | 2005-08-12 | 2007-11-09 | Pic Solution Soc Par Actions S | Procede et installation pour la regulation du taux de modificateur dans une chromatographie ou extraction supercritique avec recyclage |
FR2897277B1 (fr) * | 2006-02-10 | 2008-04-18 | Novasep Soc Par Actions Simpli | Procede et dispositif de separation. |
US20080053908A1 (en) * | 2006-09-01 | 2008-03-06 | Lalit Chordia | High pressure flash chromatography |
KR100925919B1 (ko) * | 2008-01-04 | 2009-11-09 | 창원대학교 산학협력단 | 압축공기를 이용한 베어링의 가변예압장치 및 방법 |
US8215922B2 (en) | 2008-06-24 | 2012-07-10 | Aurora Sfc Systems, Inc. | Compressible fluid pumping system for dynamically compensating compressible fluids over large pressure ranges |
US9163618B2 (en) | 2008-06-24 | 2015-10-20 | Agilent Technologies, Inc. | Automated conversion between SFC and HPLC |
WO2010056313A1 (en) * | 2008-11-12 | 2010-05-20 | Thar Instruments, Inc. | Collection system for purification flowstreams |
US8419936B2 (en) * | 2010-03-23 | 2013-04-16 | Agilent Technologies, Inc. | Low noise back pressure regulator for supercritical fluid chromatography |
CN107107076B (zh) | 2015-01-30 | 2019-11-08 | 安捷伦科技有限公司 | 撞击式离心分离器及其制造方法和级分收集系统 |
US11154795B2 (en) | 2016-10-21 | 2021-10-26 | Novasep Equipment Solutions | Use of compressed gas for moving eluent applied to chromatography |
US20230075933A1 (en) * | 2021-09-09 | 2023-03-09 | Dionex Corporation | Check standard recycle setup for ion chromatography |
CN114272646A (zh) * | 2021-12-30 | 2022-04-05 | 江苏汉邦科技有限公司 | 一种高效率超临界设备 |
Family Cites Families (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
AT260178B (de) * | 1965-08-09 | 1968-02-12 | Studiengesellschaft Kohle Mbh | Verfahren zur gaschromatographischen Trennung |
GB1350580A (en) * | 1970-05-28 | 1974-04-18 | British Petroleum Co | Gas chromatography |
DE2729462A1 (de) * | 1977-06-30 | 1979-01-18 | Wolfgang Dr Hartmann | Vorrichtung und verfahren zur chromatographischen trennung von substanzen geringen dampfdrucks |
-
1982
- 1982-06-03 FR FR8209649A patent/FR2527934A1/fr active Granted
-
1983
- 1983-05-25 AT AT83401040T patent/ATE16247T1/de not_active IP Right Cessation
- 1983-05-25 EP EP83401040A patent/EP0099765B1/de not_active Expired
- 1983-05-25 DE DE8383401040T patent/DE3361112D1/de not_active Expired
- 1983-05-31 US US06/499,597 patent/US4478720A/en not_active Expired - Lifetime
- 1983-06-02 JP JP58097053A patent/JPS5917157A/ja active Granted
- 1983-06-02 CA CA000429558A patent/CA1202913A/en not_active Expired
Also Published As
Publication number | Publication date |
---|---|
EP0099765A1 (de) | 1984-02-01 |
FR2527934B1 (de) | 1984-12-07 |
JPS5917157A (ja) | 1984-01-28 |
DE3361112D1 (en) | 1985-12-05 |
EP0099765B1 (de) | 1985-10-30 |
US4478720A (en) | 1984-10-23 |
JPH0248061B2 (de) | 1990-10-23 |
FR2527934A1 (fr) | 1983-12-09 |
CA1202913A (en) | 1986-04-08 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
UEP | Publication of translation of european patent specification | ||
EELA | Cancelled due to lapse of time |