ATE16247T1 - Verfahren zum fraktionieren von gemischen durch elutionschromatographie mit einer ueberkritischen fluiden phase und anlage zur durchfuehrung dieses verfahrens. - Google Patents

Verfahren zum fraktionieren von gemischen durch elutionschromatographie mit einer ueberkritischen fluiden phase und anlage zur durchfuehrung dieses verfahrens.

Info

Publication number
ATE16247T1
ATE16247T1 AT83401040T AT83401040T ATE16247T1 AT E16247 T1 ATE16247 T1 AT E16247T1 AT 83401040 T AT83401040 T AT 83401040T AT 83401040 T AT83401040 T AT 83401040T AT E16247 T1 ATE16247 T1 AT E16247T1
Authority
AT
Austria
Prior art keywords
mixtures
fractionation
elution chromatography
carrying
equipment
Prior art date
Application number
AT83401040T
Other languages
English (en)
Inventor
Michel Perrut
Original Assignee
Elf Aquitaine
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Elf Aquitaine filed Critical Elf Aquitaine
Application granted granted Critical
Publication of ATE16247T1 publication Critical patent/ATE16247T1/de

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D15/00Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08Selective adsorption, e.g. chromatography
    • B01D15/26Selective adsorption, e.g. chromatography characterised by the separation mechanism
    • B01D15/40Selective adsorption, e.g. chromatography characterised by the separation mechanism using supercritical fluid as mobile phase or eluent
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00Purification; Separation; Use of additives
    • C07C7/12Purification; Separation; Use of additives by adsorption, i.e. purification or separation of hydrocarbons with the aid of solids, e.g. with ion-exchangers
    • C07C7/13Purification; Separation; Use of additives by adsorption, i.e. purification or separation of hydrocarbons with the aid of solids, e.g. with ion-exchangers by molecular-sieve technique
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/26Conditioning of the fluid carrier; Flow patterns
    • G01N30/28Control of physical parameters of the fluid carrier
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/26Conditioning of the fluid carrier; Flow patterns
    • G01N30/28Control of physical parameters of the fluid carrier
    • G01N30/34Control of physical parameters of the fluid carrier of fluid composition, e.g. gradient
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/62Detectors specially adapted therefor
    • G01N2030/621Detectors specially adapted therefor signal-to-noise ratio
    • G01N2030/623Detectors specially adapted therefor signal-to-noise ratio by modulation of sample feed or detector response
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/26Conditioning of the fluid carrier; Flow patterns
    • G01N30/38Flow patterns
    • G01N30/44Flow patterns using recycling of the fraction to be distributed
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/80Fraction collectors
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/50Improvements relating to the production of bulk chemicals
    • Y02P20/54Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids

Landscapes

  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Immunology (AREA)
  • General Health & Medical Sciences (AREA)
  • Pathology (AREA)
  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Physics & Mathematics (AREA)
  • Water Supply & Treatment (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
AT83401040T 1982-06-03 1983-05-25 Verfahren zum fraktionieren von gemischen durch elutionschromatographie mit einer ueberkritischen fluiden phase und anlage zur durchfuehrung dieses verfahrens. ATE16247T1 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR8209649A FR2527934A1 (fr) 1982-06-03 1982-06-03 Procede de fractionnement de melanges par chromatographie d'elution avec fluide en etat supercritique et installation pour sa mise en oeuvre
EP83401040A EP0099765B1 (de) 1982-06-03 1983-05-25 Verfahren zum Fraktionieren von Gemischen durch Elutionschromatographie mit einer überkritischen fluiden Phase und Anlage zur Durchführung dieses Verfahrens

Publications (1)

Publication Number Publication Date
ATE16247T1 true ATE16247T1 (de) 1985-11-15

Family

ID=9274587

Family Applications (1)

Application Number Title Priority Date Filing Date
AT83401040T ATE16247T1 (de) 1982-06-03 1983-05-25 Verfahren zum fraktionieren von gemischen durch elutionschromatographie mit einer ueberkritischen fluiden phase und anlage zur durchfuehrung dieses verfahrens.

Country Status (7)

Country Link
US (1) US4478720A (de)
EP (1) EP0099765B1 (de)
JP (1) JPS5917157A (de)
AT (1) ATE16247T1 (de)
CA (1) CA1202913A (de)
DE (1) DE3361112D1 (de)
FR (1) FR2527934A1 (de)

Families Citing this family (59)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS60241908A (ja) * 1984-05-15 1985-11-30 Morinaga & Co Ltd 多成分系原料より精製成分を製造する方法
JPH0664032B2 (ja) * 1985-10-12 1994-08-22 出光石油化学株式会社 超臨界流体による混合物からの特定成分の分離方法
JPS62138753A (ja) * 1985-12-12 1987-06-22 Hitachi Ltd 液体クロマトグラフイによる分画・分取方法および装置
JPS62155908A (ja) * 1985-12-28 1987-07-10 Idemitsu Petrochem Co Ltd 超臨界流体による水/アルコ−ル混合物の分離方法
JPS62192028A (ja) * 1986-02-18 1987-08-22 Hitachi Maxell Ltd 磁気記録媒体
US4684465A (en) * 1986-10-10 1987-08-04 Combustion Engineering, Inc. Supercritical fluid chromatograph with pneumatically controlled pump
US4681678A (en) * 1986-10-10 1987-07-21 Combustion Engineering, Inc. Sample dilution system for supercritical fluid chromatography
US4859342A (en) * 1986-10-14 1989-08-22 Suntory Limited Process for industrially separating biopolymers
DE3717456C1 (de) * 1987-05-23 1988-07-21 Eberhard Gerstel Gaschromatograph und Verfahren zur gaschromatographischen Trennung
US4816159A (en) * 1987-08-31 1989-03-28 Aluminum Company Of America Supercritical fluid chromatography packing material
US4880543A (en) * 1987-08-31 1989-11-14 Aluminum Company Of America Supercritical fluid chromatography packing material containing alumina
JPS6483152A (en) * 1987-09-25 1989-03-28 Japan Spectroscopic Co Recycling chromatograph
US5180487A (en) * 1987-09-25 1993-01-19 Nihon Bunko Kogyo Kabushiki Kaisha Pump apparatus for transferring a liquified gas used in a recycle chromatograph
DE3863891D1 (de) * 1987-10-08 1991-08-29 Givaudan & Cie Sa Vorrichtung zum verzweigen von gasstroemen.
US5169522A (en) * 1990-09-25 1992-12-08 Ht Chemicals, Inc. Column slurry packing compressor
US5139681A (en) * 1990-10-09 1992-08-18 The Dow Chemical Company On-line multidimensional chromatographic system with large volume injection handling for supercritical fluid chromatography
JPH06502248A (ja) * 1990-10-09 1994-03-10 ザ ダウ ケミカル カンパニー オンライン超臨界流体抽出多次元クロマトグラフィーシステム
US5234599A (en) * 1990-10-09 1993-08-10 The Dow Chemical Company On-line multidimensional chromatographic system with large volume injection handling for supercritical fluid chromatography
US5372716A (en) * 1991-02-28 1994-12-13 Suprex Corporation Supercritical fluid extraction coupled to analytical chromatography system
CA2111695A1 (en) * 1991-06-26 1993-01-07 Noubar B. Afeyan Method and apparatus for detecting trace contaminants
CA2111084C (fr) * 1992-04-29 2004-07-06 Roger-Marc Nicoud Procede et dispositif de fractionnement d'un melange en lit mobile simule en presence d'un gaz comprime, d'un fluide supercritique ou d'un liquide subcritique
FR2694208B1 (fr) * 1992-07-30 1994-09-23 Separex Sa Procédé et dispositif industriels de fractionnement de mélanges de composants par chromatographie.
FR2690630B1 (fr) * 1992-04-29 1994-07-22 Separex Sa Procede et dispositif de fractionnement de melanges de composants par voie chromatographique a l'aide d'un eluant a pression supercritique.
US5458783A (en) * 1992-08-13 1995-10-17 Suprex Corporation Supercritical fluid extraction coupled to analytical chromatography system
US5346622A (en) * 1993-03-04 1994-09-13 Hewlett-Packard Company Hydrocarbon class separation and quantitation by split column effluent analysis
US5470377A (en) * 1993-03-08 1995-11-28 Whitlock; David R. Separation of solutes in gaseous solvents
ES2097047T3 (es) * 1993-04-29 1997-03-16 Norsk Hydro As Procedimientos para el fraccionamiento cromatografico de acidos grasos y sus derivados.
FI102758B (fi) * 1995-03-03 1999-02-15 Santen Pharmaceutical Co Ltd Menetelmä puhtaan syklosporiinimuodon valmistamiseksi
US5630943A (en) * 1995-11-30 1997-05-20 Merck Patent Gesellschaft Mit Beschrankter Haftung Discontinuous countercurrent chromatographic process and apparatus
US6063284A (en) * 1997-05-15 2000-05-16 Em Industries, Inc. Single column closed-loop recycling with periodic intra-profile injection
US6048369A (en) * 1998-06-03 2000-04-11 North Carolina State University Method of dyeing hydrophobic textile fibers with colorant materials in supercritical fluid carbon dioxide
US6413428B1 (en) * 1999-09-16 2002-07-02 Berger Instruments, Inc. Apparatus and method for preparative supercritical fluid chromatography
US6685828B2 (en) 1999-09-16 2004-02-03 Berger Instruments, Inc. Automated sample collection in supercritical fluid chromatography
US6261326B1 (en) 2000-01-13 2001-07-17 North Carolina State University Method for introducing dyes and other chemicals into a textile treatment system
US6632353B2 (en) 2000-06-26 2003-10-14 Berger Instruments, Inc. Rapid sample collection in supercritical fluid chromatography
US6558540B2 (en) * 2000-06-26 2003-05-06 Berger Instruments, Inc. Exhaust gas collection system for supercritical fluid chromatography
US6676710B2 (en) 2000-10-18 2004-01-13 North Carolina State University Process for treating textile substrates
US6601438B2 (en) 2001-09-28 2003-08-05 Systec, Inc. Apparatus for conducting high-temperature liquid chromotography analysis
US6802967B2 (en) * 2002-03-06 2004-10-12 Shimadzu Corporation Multi-dimension liquid chromatography separation system
JP2003347624A (ja) * 2002-05-27 2003-12-05 Konica Minolta Holdings Inc 有機半導体材料の精製方法、該精製方法を用いて得られた有機半導体材料及びそれを用いた半導体素子
US6908557B2 (en) * 2002-06-25 2005-06-21 Thar Technologies, Inc. Collection system for chromatographic system
SE0202188D0 (sv) 2002-07-11 2002-07-11 Pronova Biocare As A process for decreasing environmental pollutants in an oil or a fat, a volatile fat or oil environmental pollutants decreasing working fluid, a health supplement, and an animal feed product
EP2295529B2 (de) 2002-07-11 2022-05-18 Basf As Verfahren zur Verminderung von Umweltschadstoffen in einem Öl oder einem Fett und Fischfutterprodukt
KR101156146B1 (ko) * 2003-12-09 2012-06-18 재팬 사이언스 앤드 테크놀로지 에이젼시 질소면의 표면상의 구조물 제조를 통한 고효율 3족 질화물계 발광다이오드
JP4319551B2 (ja) * 2004-01-05 2009-08-26 ダイセル化学工業株式会社 超臨界流体クロマトグラフィーによる物質の分離方法及びこれに用いられる気液分離装置
US20060188397A1 (en) * 2005-01-07 2006-08-24 Lalit Chordia Method and apparatus for fraction collection
FR2882528B1 (fr) * 2005-02-25 2007-05-25 Pic Solution Soc Par Actions S Procede mixte de chromatographie en phase supercritique et installation pour sa mise en oeuvre
FR2889665B1 (fr) * 2005-08-12 2007-11-09 Pic Solution Soc Par Actions S Procede et installation pour la regulation du taux de modificateur dans une chromatographie ou extraction supercritique avec recyclage
FR2897277B1 (fr) * 2006-02-10 2008-04-18 Novasep Soc Par Actions Simpli Procede et dispositif de separation.
US20080053908A1 (en) * 2006-09-01 2008-03-06 Lalit Chordia High pressure flash chromatography
KR100925919B1 (ko) * 2008-01-04 2009-11-09 창원대학교 산학협력단 압축공기를 이용한 베어링의 가변예압장치 및 방법
US8215922B2 (en) 2008-06-24 2012-07-10 Aurora Sfc Systems, Inc. Compressible fluid pumping system for dynamically compensating compressible fluids over large pressure ranges
US9163618B2 (en) 2008-06-24 2015-10-20 Agilent Technologies, Inc. Automated conversion between SFC and HPLC
WO2010056313A1 (en) * 2008-11-12 2010-05-20 Thar Instruments, Inc. Collection system for purification flowstreams
US8419936B2 (en) * 2010-03-23 2013-04-16 Agilent Technologies, Inc. Low noise back pressure regulator for supercritical fluid chromatography
CN107107076B (zh) 2015-01-30 2019-11-08 安捷伦科技有限公司 撞击式离心分离器及其制造方法和级分收集系统
US11154795B2 (en) 2016-10-21 2021-10-26 Novasep Equipment Solutions Use of compressed gas for moving eluent applied to chromatography
US20230075933A1 (en) * 2021-09-09 2023-03-09 Dionex Corporation Check standard recycle setup for ion chromatography
CN114272646A (zh) * 2021-12-30 2022-04-05 江苏汉邦科技有限公司 一种高效率超临界设备

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AT260178B (de) * 1965-08-09 1968-02-12 Studiengesellschaft Kohle Mbh Verfahren zur gaschromatographischen Trennung
GB1350580A (en) * 1970-05-28 1974-04-18 British Petroleum Co Gas chromatography
DE2729462A1 (de) * 1977-06-30 1979-01-18 Wolfgang Dr Hartmann Vorrichtung und verfahren zur chromatographischen trennung von substanzen geringen dampfdrucks

Also Published As

Publication number Publication date
EP0099765A1 (de) 1984-02-01
FR2527934B1 (de) 1984-12-07
JPS5917157A (ja) 1984-01-28
DE3361112D1 (en) 1985-12-05
EP0099765B1 (de) 1985-10-30
US4478720A (en) 1984-10-23
JPH0248061B2 (de) 1990-10-23
FR2527934A1 (fr) 1983-12-09
CA1202913A (en) 1986-04-08

Similar Documents

Publication Publication Date Title
ATE16247T1 (de) Verfahren zum fraktionieren von gemischen durch elutionschromatographie mit einer ueberkritischen fluiden phase und anlage zur durchfuehrung dieses verfahrens.
NO954508L (no) Fremgangsmåte ved fraksjonering av sulfittkokevæske
DE69513966D1 (de) Methode zum fraktionieren einer lösung
DK434983A (da) Fremgangsmaade til rensning af brugt motorolie eller syntetisk raaolie
DE3460804D1 (en) Method of carrying out chemical reactions and for the simultaneous fractionation of a mixture into several fractions by a distillation column
ATE30045T1 (de) Verfahren zur herstellung fluessiger kohlenwasserstoffe.
DE69020825D1 (de) Kontinuierliches Verfahren und Vorrichtung für eine chromatographische Trennung einer Mischung von mindestens drei Bestandteilen in drei gereinigte Ausflüsse mittels eines Lösungsmittels bei zwei verschiedenen Temperaturen und/oder Drucken.
ZA828033B (en) Process for the selective hydrogenation of polyunsaturated hydrocarbons in hydrocarbon mixtures
ATE68099T1 (de) Verfahren zur hydrierenden behandlung von mit chlorbiphenylen u. dgl. kontaminierten mineraloelen.
DK0403392T3 (da) Ny fremgangsmåde til fremstilling af xylose
GB2045224B (en) Process for removing oils or petroleum hydrocarbons from the surface of water
ATE2545T1 (de) Verfahren zum spalten von schweren kohlenwasserstoffen.
ATE14301T1 (de) Adsorption- und trennungsverfahren in der fluessigen phase.
ATE24886T1 (de) Verfahren zur entfernung von acetylen aus einem c2-strom.
DK150686D0 (da) Fremgangsmaade til rensning af vaeksthormon-lignende materialer
FR2551452B1 (fr) Procede pour la valorisation de petroles bruts lourds
DE69401102D1 (de) Verfahren zum Trennen der Komponenten einer flüssigen Mischung
YU41255B (en) Process for the elimination of the aromate ricn fraction ffom the mixture of liguid hydrocarbons
DE3864569D1 (de) Absorptionskolonne zum chromatographischen trennen von stoffgemischen.
EP0453569A4 (en) Manufacture of absolute alcohol
HUT40055A (en) Process and equipment for washing of surfaces, heavily polluted by fine soluable mineral materials or petroleum
DE3581574D1 (de) Verfahren und vorrichtung zum trennen von komponenten eines gemisches durch schichtchromatografie.
ATE33673T1 (de) Selbstkuehlendes verfahren zur extraktion von schweren kohlenwasserstofffraktionen.
DE19535426A1 (de) Verfahren zum Gewinnen organischer Substanzen aus einer Mischung
RO81748B1 (ro) PROCEDEU PENTRU îNDEPARTAREA DEPUNERILOR DE POLIMERI îN INSTALATII DE RECTIFICARE

Legal Events

Date Code Title Description
UEP Publication of translation of european patent specification
EELA Cancelled due to lapse of time