AR241160A2 - Procedimiento para la preparacion de (r)-(-)-2,2'-dimetil-1,3-dioxolano-4-metanol - Google Patents
Procedimiento para la preparacion de (r)-(-)-2,2'-dimetil-1,3-dioxolano-4-metanolInfo
- Publication number
- AR241160A2 AR241160A2 AR29949385A AR29949385A AR241160A2 AR 241160 A2 AR241160 A2 AR 241160A2 AR 29949385 A AR29949385 A AR 29949385A AR 29949385 A AR29949385 A AR 29949385A AR 241160 A2 AR241160 A2 AR 241160A2
- Authority
- AR
- Argentina
- Prior art keywords
- acid
- isopropiliden
- dioxolane
- methanol
- dimethyl
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D317/00—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms
- C07D317/08—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3
- C07D317/72—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 spiro-condensed with carbocyclic rings
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C59/00—Compounds having carboxyl groups bound to acyclic carbon atoms and containing any of the groups OH, O—metal, —CHO, keto, ether, groups, groups, or groups
- C07C59/01—Saturated compounds having only one carboxyl group and containing hydroxy or O-metal groups
- C07C59/10—Polyhydroxy carboxylic acids
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D317/00—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms
- C07D317/08—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3
- C07D317/10—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 not condensed with other rings
- C07D317/14—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 not condensed with other rings with substituted hydrocarbon radicals attached to ring carbon atoms
- C07D317/18—Radicals substituted by singly bound oxygen or sulfur atoms
- C07D317/20—Free hydroxyl or mercaptan
Abstract
UN PROCEDIMIENTO PARA LA PREPARACION DE (R)-(-)-2,2'-DIMETIL-1,3-DIOXOLANO-4-METANOL DE LA FORMULA (I) QUE COMPRENDE PRODUCIR ACIDO 2,3-DIHIDROXIPROPANOICO, HACERLO REACCIONAR CON 2,2-DIMETOXIPROPANO PARA PRODUCIR ISOPROPILIDEN-L-GLICERIDO, O HACER REACCIONAR EL ACIDO 2,3-DIHIDROXIPROPANOICO CON 2,3-DIMETOXIPROPANO EN PRESENCIA DE UN ALCOHOL ALQUILICO PARA PRODUCIR 2,3-ISOPROPILIDEN-L-GLICERICO O EL 2,3-ISOPROPILIDEN-L-GLICERATO DE ALQUILO CON HIDRURO DE ALUMINIO Y LITIO. EL ACIDO 2,3-DIHIDROXIPROPANOICO SE PRODUCE POR REACCION DE L-SERINA CON UN AGENTE NITROSANTE QUE CONSISTE EN UN NITRITO DE UN METAL DEL GRUPO IA DE LA TABLA PERIODICA, EN UNA SOLUCION ACUOSA EN PRESENCIA DE UN ACIDO ELEGIDO ENTRE ACIDO ACETICO, ACIDO FORMICO Y ACIDO PROPANOICO, A APROXIMADAMENTE TEMPERATURA AMBIENTE POR UN PERIODO DE 8 A 20 HORAS.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US06/580,492 US4575558A (en) | 1984-02-15 | 1984-02-15 | Preparation of optically active 1,3-dioxolane-4-methanol compounds |
Publications (2)
Publication Number | Publication Date |
---|---|
AR241160A2 true AR241160A2 (es) | 1991-12-30 |
AR241160A1 AR241160A1 (es) | 1991-12-30 |
Family
ID=24321324
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
AR299493A AR241160A1 (es) | 1984-02-15 | 1985-02-13 | Procedimiento para la preparacion de (r)-(-)-2,2'-dimetil-1,3-dioxolano-4-metanol |
Country Status (10)
Country | Link |
---|---|
US (1) | US4575558A (es) |
EP (1) | EP0173714B1 (es) |
JP (1) | JPH0662492B2 (es) |
AR (1) | AR241160A1 (es) |
AU (1) | AU568429B2 (es) |
CA (1) | CA1218375A (es) |
DE (1) | DE3577433D1 (es) |
IT (1) | IT1182199B (es) |
WO (1) | WO1985003704A1 (es) |
ZA (1) | ZA851056B (es) |
Families Citing this family (16)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
ES2029831T3 (es) * | 1986-03-12 | 1992-10-01 | Euroceltique Sa | Un procedimiento para la preparacion de una composicion contraceptiva para aplicacion a la vagina de un mamifero hembra. |
IL82416A0 (en) * | 1986-05-08 | 1987-11-30 | Gist Brocades Nv | Process for the preparation of r-2,2-r1,r2-1,3-dioxolane-4-methanol |
US4931575A (en) * | 1987-03-13 | 1990-06-05 | The Board Of Governors For Higher Education, State Of Rhode Island And Providence Plantations | Chiral glycerol derivatives |
IT1205834B (it) * | 1987-04-22 | 1989-03-31 | Elbart | Derivati tiodiossolanici ad attivita' mucolitica a procedimento per la loro preparazione |
US5283346A (en) * | 1989-03-23 | 1994-02-01 | Hoffmann-La Roche Inc. | Dioxolanes |
US4956285A (en) * | 1989-06-29 | 1990-09-11 | Gist-Brocades N.V. | Process for the preparation of S-2,2-R1,R2 -1,3 -dioxolane-4-methanols |
NL8902035A (nl) * | 1989-08-09 | 1991-03-01 | Stamicarbon | Enantioselectieve bereiding van s-2r1,2r2-1,3-dioxolaan-4-methanol en derivaten daarvan. |
ATE118755T1 (de) * | 1989-11-01 | 1995-03-15 | Shell Int Research | Verfahren zur trennung von r und s-2, 2-r1,r2-1,3-dioxolan-4-carbonsäure. |
US5391785A (en) * | 1990-01-16 | 1995-02-21 | La Jolla Pharmaceutial Company | Intermediates for providing functional groups on the 5' end of oligonucleotides |
JP2899111B2 (ja) * | 1991-07-15 | 1999-06-02 | ラ ホヤ ファーマシューティカル カンパニー | オリゴヌクレオチドの5’末端へ官能基を提供するための修飾された亜リン酸中間体 |
DE69724442D1 (de) * | 1996-09-10 | 2003-10-02 | Daiso Co Ltd | Verfahren zur herstellung von 1,3-dioxolan-4-methanol-verbindungen |
JP3822644B2 (ja) * | 1996-09-10 | 2006-09-20 | ダイソー株式会社 | 1,3―ジオキソラン―4―メタノール化合物の製造法 |
US6985768B2 (en) * | 2003-02-28 | 2006-01-10 | Medtronic, Inc. | Physiological event detection |
FR2949478B1 (fr) * | 2009-09-03 | 2011-09-02 | Rhodia Poliamida E Especialidades Ltda | Compositions de finissage du cuir comprenant des derives de dioxolane |
US8349777B2 (en) * | 2010-11-22 | 2013-01-08 | Chevron Oronite Company Llc | Lubricating composition containing 1,3-dioxolane-4-methanol compounds as antiwear additives |
KR101128856B1 (ko) * | 2011-03-08 | 2012-03-23 | 주식회사 엘지생활건강 | 물세탁 및 드라이 크리닝용 친환경 용제 및 이를 포함한 세탁용 조성물 |
Family Cites Families (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE503497C (de) * | 1927-10-13 | 1930-08-07 | Henkel & Cie Gmbh | Verfahren zur Herstellung von Kondensationsprodukten aus mehrwertigen Alkoholen und deren Derivaten mit Ketonen |
GB429096A (en) * | 1932-11-16 | 1935-05-16 | Descollonges Freres | Process of manufacture of odorous chemical compounds and products resulting therefrom |
US2752391A (en) * | 1952-12-04 | 1956-06-26 | Rohm & Haas | Preparation of glyceric acid |
US3058981A (en) * | 1958-11-14 | 1962-10-16 | Richardson Merrell Inc | 2-methyl-2-nonyl-4-hydroxymethyl-1, 3-dioxolane and carbamates thereof |
DE2045090A1 (de) * | 1969-10-02 | 1971-06-16 | Perstorp Ab, Perstorp (Schweden) | Substituierte 1,3 Dioxolane |
IT1136945B (it) * | 1981-03-18 | 1986-09-03 | Anic Spa | Processo per la preparazione di l-carnitina |
JPS57158778A (en) * | 1981-03-25 | 1982-09-30 | Suntory Ltd | 2,2,4-trimethyl-5-hydroxymethyl-1,3-dioxolane |
-
1984
- 1984-02-15 US US06/580,492 patent/US4575558A/en not_active Expired - Lifetime
-
1985
- 1985-02-08 CA CA000473922A patent/CA1218375A/en not_active Expired
- 1985-02-11 JP JP60501028A patent/JPH0662492B2/ja not_active Expired - Lifetime
- 1985-02-11 AU AU39963/85A patent/AU568429B2/en not_active Ceased
- 1985-02-11 WO PCT/US1985/000213 patent/WO1985003704A1/en active IP Right Grant
- 1985-02-11 EP EP85901208A patent/EP0173714B1/en not_active Expired - Lifetime
- 1985-02-11 DE DE8585901208T patent/DE3577433D1/de not_active Expired - Lifetime
- 1985-02-12 ZA ZA851056A patent/ZA851056B/xx unknown
- 1985-02-13 AR AR299493A patent/AR241160A1/es active
- 1985-02-14 IT IT47683/85A patent/IT1182199B/it active
Also Published As
Publication number | Publication date |
---|---|
WO1985003704A1 (en) | 1985-08-29 |
IT8547683A1 (it) | 1986-08-14 |
EP0173714A4 (en) | 1986-07-24 |
AR241160A1 (es) | 1991-12-30 |
AU3996385A (en) | 1985-09-10 |
AU568429B2 (en) | 1987-12-24 |
JPH0662492B2 (ja) | 1994-08-17 |
IT1182199B (it) | 1987-09-30 |
IT8547683A0 (it) | 1985-02-14 |
EP0173714B1 (en) | 1990-05-02 |
DE3577433D1 (de) | 1990-06-07 |
EP0173714A1 (en) | 1986-03-12 |
JPS61501206A (ja) | 1986-06-19 |
US4575558A (en) | 1986-03-11 |
CA1218375A (en) | 1987-02-24 |
ZA851056B (en) | 1985-09-25 |
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