AR100178A1 - Método para preparar un material adsorbente en ausencia de un aglutinante, que comprende una etapa de procesamiento hidrotérmico y un método para extraer litio de soluciones salinas que utiliza dicho material - Google Patents

Método para preparar un material adsorbente en ausencia de un aglutinante, que comprende una etapa de procesamiento hidrotérmico y un método para extraer litio de soluciones salinas que utiliza dicho material

Info

Publication number
AR100178A1
AR100178A1 ARP150101237A ARP150101237A AR100178A1 AR 100178 A1 AR100178 A1 AR 100178A1 AR P150101237 A ARP150101237 A AR P150101237A AR P150101237 A ARP150101237 A AR P150101237A AR 100178 A1 AR100178 A1 AR 100178A1
Authority
AR
Argentina
Prior art keywords
stage
binder
absence
preparing
salin
Prior art date
Application number
ARP150101237A
Other languages
English (en)
Inventor
Charles Joseph Ren Soulairol Romain
Andr Pierre Burdet Fabien
Boualleg Malika
Original Assignee
Eramet
Ifp Energies Now
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Eramet, Ifp Energies Now filed Critical Eramet
Publication of AR100178A1 publication Critical patent/AR100178A1/es

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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/04—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of alkali metals, alkaline earth metals or magnesium
    • B01J20/046—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of alkali metals, alkaline earth metals or magnesium containing halogens, e.g. halides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/04—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of alkali metals, alkaline earth metals or magnesium
    • B01J20/041—Oxides or hydroxides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/06—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising oxides or hydroxides of metals not provided for in group B01J20/04
    • B01J20/08—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising oxides or hydroxides of metals not provided for in group B01J20/04 comprising aluminium oxide or hydroxide; comprising bauxite
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/3007—Moulding, shaping or extruding
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/3078—Thermal treatment, e.g. calcining or pyrolizing
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/3085—Chemical treatments not covered by groups B01J20/3007 - B01J20/3078
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J39/00—Cation exchange; Use of material as cation exchangers; Treatment of material for improving the cation exchange properties
    • B01J39/08—Use of material as cation exchangers; Treatment of material for improving the cation exchange properties
    • B01J39/10—Oxides or hydroxides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J41/00—Anion exchange; Use of material as anion exchangers; Treatment of material for improving the anion exchange properties
    • B01J41/08—Use of material as anion exchangers; Treatment of material for improving the anion exchange properties
    • B01J41/10—Inorganic material
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D15/00—Lithium compounds
    • C01D15/04—Halides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F7/00—Compounds of aluminium
    • C01F7/02—Aluminium oxide; Aluminium hydroxide; Aluminates
    • C01F7/021—After-treatment of oxides or hydroxides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F7/00—Compounds of aluminium
    • C01F7/78—Compounds containing aluminium and two or more other elements, with the exception of oxygen and hydrogen
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/12—Surface area

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Analytical Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Manufacture And Refinement Of Metals (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)

Abstract

La presente se refiere a un método para preparar un material cristalino sólido de fórmula LiCl.2Al(OH)₃,nH₂O, donde n oscila entre 0,01 y 10, donde dicho método comprende al menos las siguientes etapas: a) una etapa de mezclado, en un medio acuoso, de al menos una fuente de alúmina y al menos una fuente de litio para obtener una suspensión, b) una etapa de filtrado para la suspensión obtenida en la etapa a) a fin de obtener una pasta, c) una etapa de secado para la pasta obtenida al final de la etapa b), d) una etapa de conformado de dicha pasta secada inmediatamente después de la etapa de secado c) para obtener un material sólido conformado, donde dicha etapa de conformado d) se lleva a cabo en ausencia de un aglutinante, y e) secado del material sólido conformado obtenido, f) una etapa de procesamiento hidrotérmico para obtener el material cristalino sólido conformado de fórmula LiCl.2Al(OH)₃,nH₂O. La presente también se refiere a un material obtenido a través de este método y a un método para extraer litio de soluciones salinas utilizando el material preparado de esta manera.
ARP150101237A 2014-04-25 2015-04-24 Método para preparar un material adsorbente en ausencia de un aglutinante, que comprende una etapa de procesamiento hidrotérmico y un método para extraer litio de soluciones salinas que utiliza dicho material AR100178A1 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR1453779A FR3020284A1 (fr) 2014-04-25 2014-04-25 Procede de preparation d'un materiau absorbant en l'absence de liant comprenant une etape de traitement hydrothermal et pocede d'extraction de lithium a partir de solutions salines utilisant ledit materiau

Publications (1)

Publication Number Publication Date
AR100178A1 true AR100178A1 (es) 2016-09-14

Family

ID=51063671

Family Applications (1)

Application Number Title Priority Date Filing Date
ARP150101237A AR100178A1 (es) 2014-04-25 2015-04-24 Método para preparar un material adsorbente en ausencia de un aglutinante, que comprende una etapa de procesamiento hidrotérmico y un método para extraer litio de soluciones salinas que utiliza dicho material

Country Status (7)

Country Link
US (1) US20170043317A1 (es)
EP (1) EP3134202A1 (es)
CN (1) CN106457203A (es)
AR (1) AR100178A1 (es)
CL (1) CL2016002663A1 (es)
FR (1) FR3020284A1 (es)
WO (1) WO2015162272A1 (es)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR3044001B1 (fr) 2015-11-24 2017-12-29 Eramet Procede de preparation d'un materiau adsorbant comprenant une etape de malaxage basique et procede d'extraction de lithium a partir de solutions salines utilisant ledit materiau
FR3044002B1 (fr) * 2015-11-24 2017-12-29 Eramet Procede de preparation d'un materiau adsorbant par malaxage basique d'une poudre sechee en etuve ou four ou par atomisation et procede d'extraction de lithium
FR3051787B1 (fr) * 2016-05-25 2022-07-08 Eramet Procede de preparation d'un materiau adsorbant et procede d'extraction de lithium utilisant ledit materiau
CN109200987B (zh) * 2017-06-30 2020-09-15 比亚迪股份有限公司 锂吸附剂及其制备方法
CN108083301A (zh) * 2017-11-10 2018-05-29 江苏旌凯中科超导高技术有限公司 利用磁性粉体铝系锂吸附剂从卤水中提取锂的方法
CN111527046A (zh) 2017-12-22 2020-08-11 株式会社Posco 磷酸锂的制备方法、氢氧化锂的制备方法及碳酸锂的制备方法
CN108187608A (zh) * 2018-02-03 2018-06-22 天津市职业大学 一种结晶性铝盐锂离子吸附剂颗粒及其制备方法
JP7119415B2 (ja) * 2018-02-21 2022-08-17 東京電力ホールディングス株式会社 吸着材の耐脆化性評価方法、及びその方法に用いる粉体捕捉器
KR101944519B1 (ko) * 2018-08-29 2019-02-01 한국지질자원연구원 리튬 용액으로부터 고효율 리튬 회수 방법
CN108993376B (zh) * 2018-09-17 2021-03-26 华东理工大学 一种铝盐锂吸附剂及其制备方法与应用
WO2020219625A1 (en) 2019-04-25 2020-10-29 Saint-Gobain Ceramics & Plastics, Inc. Adsorbent particles and methods of forming thereof
CN111249979B (zh) * 2020-01-20 2020-12-08 西南石油大学 耐高温高压可搅拌中间容器装置和多孔介质驱替实验系统
CN113387710A (zh) * 2021-07-12 2021-09-14 长飞光纤光缆股份有限公司 一种无粘结剂的粉体造粒压片方法
CN116813325B (zh) * 2023-04-01 2024-05-28 东莞市科蓬达电子科技有限公司 一种热敏陶瓷的生产工艺

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US4348297A (en) * 1979-11-19 1982-09-07 The Dow Chemical Company Crystalline lithium aluminates
EP0103034A1 (en) * 1982-09-09 1984-03-21 The Dow Chemical Company Crystalline lithium aluminates and a process for the preparation thereof
WO1994019280A1 (en) * 1993-02-16 1994-09-01 Nauchno-Proizvodstvennoe Aktsionernoe Obschestvo 'ekostar' Process for obtaining lithium chloride from solutions and a device for carrying out the same
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US8637428B1 (en) * 2009-12-18 2014-01-28 Simbol Inc. Lithium extraction composition and method of preparation thereof
CN101829538B (zh) * 2010-05-19 2013-06-26 浙江海虹控股集团有限公司 一种高性能锂吸附剂的制备方法
US8309043B2 (en) * 2010-12-06 2012-11-13 Fmc Corporation Recovery of Li values from sodium saturate brine
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Also Published As

Publication number Publication date
FR3020284A1 (fr) 2015-10-30
CN106457203A (zh) 2017-02-22
EP3134202A1 (fr) 2017-03-01
CL2016002663A1 (es) 2017-01-06
WO2015162272A1 (fr) 2015-10-29
US20170043317A1 (en) 2017-02-16

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