AR080922A1 - Proceso para la preparacion de amidas del acido pirazolcarboxilico e intermediarios del mismo - Google Patents
Proceso para la preparacion de amidas del acido pirazolcarboxilico e intermediarios del mismoInfo
- Publication number
- AR080922A1 AR080922A1 ARP110101326A ARP110101326A AR080922A1 AR 080922 A1 AR080922 A1 AR 080922A1 AR P110101326 A ARP110101326 A AR P110101326A AR P110101326 A ARP110101326 A AR P110101326A AR 080922 A1 AR080922 A1 AR 080922A1
- Authority
- AR
- Argentina
- Prior art keywords
- formula
- compound
- reacting
- until
- bromine
- Prior art date
Links
- 239000002253 acid Substances 0.000 title 1
- 150000001875 compounds Chemical class 0.000 abstract 22
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical group [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 abstract 4
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Chemical group BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 abstract 4
- 229910052794 bromium Chemical group 0.000 abstract 4
- 229910052801 chlorine Inorganic materials 0.000 abstract 4
- 239000000460 chlorine Substances 0.000 abstract 4
- 125000001309 chloro group Chemical group Cl* 0.000 abstract 4
- NAWXUBYGYWOOIX-SFHVURJKSA-N (2s)-2-[[4-[2-(2,4-diaminoquinazolin-6-yl)ethyl]benzoyl]amino]-4-methylidenepentanedioic acid Chemical compound C1=CC2=NC(N)=NC(N)=C2C=C1CCC1=CC=C(C(=O)N[C@@H](CC(=C)C(O)=O)C(O)=O)C=C1 NAWXUBYGYWOOIX-SFHVURJKSA-N 0.000 abstract 2
- 239000003054 catalyst Substances 0.000 abstract 2
- ZSWFCLXCOIISFI-UHFFFAOYSA-N cyclopentadiene Chemical compound C1C=CC=C1 ZSWFCLXCOIISFI-UHFFFAOYSA-N 0.000 abstract 2
- 239000012442 inert solvent Substances 0.000 abstract 2
- 239000007800 oxidant agent Substances 0.000 abstract 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 abstract 1
- 239000002841 Lewis acid Substances 0.000 abstract 1
- 239000005922 Phosphane Substances 0.000 abstract 1
- XYFCBTPGUUZFHI-UHFFFAOYSA-N Phosphine Chemical compound P XYFCBTPGUUZFHI-UHFFFAOYSA-N 0.000 abstract 1
- 229910052802 copper Inorganic materials 0.000 abstract 1
- 239000010949 copper Substances 0.000 abstract 1
- 150000004678 hydrides Chemical class 0.000 abstract 1
- 150000007517 lewis acids Chemical class 0.000 abstract 1
- 239000003446 ligand Substances 0.000 abstract 1
- 125000002524 organometallic group Chemical group 0.000 abstract 1
- 230000001590 oxidative effect Effects 0.000 abstract 1
- 229910000064 phosphane Inorganic materials 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
- C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
- C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/23—Preparation of halogenated hydrocarbons by dehalogenation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/26—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton
- C07C17/30—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by a Diels-Alder synthesis
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/04—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups
- C07C209/06—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups by substitution of halogen atoms
- C07C209/10—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups by substitution of halogen atoms with formation of amino groups bound to carbon atoms of six-membered aromatic rings or from amines having nitrogen atoms bound to carbon atoms of six-membered aromatic rings
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C25/00—Compounds containing at least one halogen atom bound to a six-membered aromatic ring
- C07C25/24—Halogenated aromatic hydrocarbons with unsaturated side chains
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/132—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C35/00—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a ring other than a six-membered aromatic ring
- C07C35/48—Halogenated derivatives
- C07C35/52—Alcohols with a condensed ring system
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
- C07C45/29—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation of hydroxy groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
- C07D303/02—Compounds containing oxirane rings
- C07D303/12—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms
- C07D303/16—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms by esterified hydroxyl radicals
- C07D303/17—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms by esterified hydroxyl radicals containing oxirane rings condensed with carbocyclic ring systems having three or more relevant rings
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2603/00—Systems containing at least three condensed rings
- C07C2603/56—Ring systems containing bridged rings
- C07C2603/58—Ring systems containing bridged rings containing three rings
- C07C2603/60—Ring systems containing bridged rings containing three rings containing at least one ring with less than six members
- C07C2603/66—Ring systems containing bridged rings containing three rings containing at least one ring with less than six members containing five-membered rings
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Catalysts (AREA)
- Epoxy Compounds (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP10160438 | 2010-04-20 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| AR080922A1 true AR080922A1 (es) | 2012-05-16 |
Family
ID=44072655
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ARP110101326A AR080922A1 (es) | 2010-04-20 | 2011-04-18 | Proceso para la preparacion de amidas del acido pirazolcarboxilico e intermediarios del mismo |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US8519152B2 (enExample) |
| EP (1) | EP2560959B1 (enExample) |
| JP (1) | JP5684896B2 (enExample) |
| CN (1) | CN102906072B (enExample) |
| AR (1) | AR080922A1 (enExample) |
| BR (1) | BR112012026631B1 (enExample) |
| ES (1) | ES2513540T3 (enExample) |
| IL (1) | IL222398A (enExample) |
| MX (1) | MX2012012005A (enExample) |
| TW (1) | TWI428325B (enExample) |
| UY (1) | UY33340A (enExample) |
| WO (1) | WO2011131545A1 (enExample) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2011131544A1 (en) * | 2010-04-20 | 2011-10-27 | Syngenta Participations Ag | Process for the preparation of pyrazole carboxylic acid amides |
| TWI534126B (zh) * | 2011-01-25 | 2016-05-21 | 先正達合夥公司 | 用於製備吡唑羧酸醯胺之方法 |
| GB201403438D0 (en) | 2014-02-27 | 2014-04-16 | Syngenta Participations Ag | Polymorphs |
| AU2023309261A1 (en) | 2022-07-22 | 2024-12-12 | Syngenta Crop Protection Ag | Solid form of a heterocyclic amide derivative |
| CN116143635B (zh) * | 2022-12-01 | 2025-02-25 | 江苏七洲绿色科技研究院有限公司 | 一种9-二氯亚甲基-5-氨基-苯并降冰片烯的制备方法 |
| WO2025157998A1 (en) | 2024-01-26 | 2025-07-31 | Syngenta Crop Protection Ag | Chemical process |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH075487B2 (ja) | 1985-11-14 | 1995-01-25 | 住友化学工業株式会社 | １―ブロモ―２―クロロ―４―フルオロベンゼンの製造法 |
| US5093347A (en) | 1991-01-28 | 1992-03-03 | Monsanto Company | 3-difluoromethylpyrazolecarboxamide fungicides, compositions and use |
| US7223879B2 (en) | 1998-07-10 | 2007-05-29 | Massachusetts Institute Of Technology | Ligands for metals and improved metal-catalyzed processes based thereon |
| GEP20115161B (en) * | 2005-10-25 | 2011-02-10 | Syngenta Participations Ag | Heterocyclic amide derivatives useful as microbiocides |
| WO2007124907A2 (en) | 2006-04-27 | 2007-11-08 | Syngenta Participations Ag | Heterocyclyl-carboxylic acid (benzonorbornene-5-yl)amide derivatives as fungicides for agrochemical use |
| EP2076123B1 (en) | 2006-10-25 | 2011-06-01 | Syngenta Limited | Process for the production of substituted bromobenzenes |
| EP2370412A1 (en) * | 2008-12-24 | 2011-10-05 | Syngenta Limited | Methods for the preparation of fungicides |
-
2011
- 2011-04-14 MX MX2012012005A patent/MX2012012005A/es active IP Right Grant
- 2011-04-14 ES ES11714550.8T patent/ES2513540T3/es active Active
- 2011-04-14 CN CN201180019785.1A patent/CN102906072B/zh active Active
- 2011-04-14 WO PCT/EP2011/055871 patent/WO2011131545A1/en not_active Ceased
- 2011-04-14 EP EP11714550.8A patent/EP2560959B1/en active Active
- 2011-04-14 US US13/642,406 patent/US8519152B2/en active Active
- 2011-04-14 BR BR112012026631-4A patent/BR112012026631B1/pt active IP Right Grant
- 2011-04-14 JP JP2013505409A patent/JP5684896B2/ja active Active
- 2011-04-15 UY UY0001033340A patent/UY33340A/es active IP Right Grant
- 2011-04-18 AR ARP110101326A patent/AR080922A1/es active IP Right Grant
- 2011-04-19 TW TW100113507A patent/TWI428325B/zh active
-
2012
- 2012-10-11 IL IL222398A patent/IL222398A/en active IP Right Grant
Also Published As
| Publication number | Publication date |
|---|---|
| MX2012012005A (es) | 2012-12-17 |
| IL222398A (en) | 2017-01-31 |
| BR112012026631B1 (pt) | 2017-07-25 |
| EP2560959A1 (en) | 2013-02-27 |
| CN102906072A (zh) | 2013-01-30 |
| UY33340A (es) | 2011-12-01 |
| ES2513540T3 (es) | 2014-10-27 |
| US8519152B2 (en) | 2013-08-27 |
| JP2013525317A (ja) | 2013-06-20 |
| EP2560959B1 (en) | 2014-08-20 |
| CN102906072B (zh) | 2014-07-02 |
| WO2011131545A1 (en) | 2011-10-27 |
| TWI428325B (zh) | 2014-03-01 |
| BR112012026631A2 (pt) | 2015-09-15 |
| JP5684896B2 (ja) | 2015-03-18 |
| US20130035496A1 (en) | 2013-02-07 |
| TW201204704A (en) | 2012-02-01 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG | Grant, registration |