WO2024127845A1 - Firing jig comprising setter and bottom plate - Google Patents

Firing jig comprising setter and bottom plate Download PDF

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Publication number
WO2024127845A1
WO2024127845A1 PCT/JP2023/039647 JP2023039647W WO2024127845A1 WO 2024127845 A1 WO2024127845 A1 WO 2024127845A1 JP 2023039647 W JP2023039647 W JP 2023039647W WO 2024127845 A1 WO2024127845 A1 WO 2024127845A1
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WIPO (PCT)
Prior art keywords
setter
base plate
portions
cross
longitudinal direction
Prior art date
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PCT/JP2023/039647
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French (fr)
Japanese (ja)
Inventor
峻 有馬
Original Assignee
三井金属鉱業株式会社
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Publication date
Application filed by 三井金属鉱業株式会社 filed Critical 三井金属鉱業株式会社
Priority to JP2024525079A priority Critical patent/JP7531075B1/en
Publication of WO2024127845A1 publication Critical patent/WO2024127845A1/en

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    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/64Burning or sintering processes
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27DDETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
    • F27D3/00Charging; Discharging; Manipulation of charge
    • F27D3/12Travelling or movable supports or containers for the charge

Definitions

  • the present invention relates to a baking jig consisting of a setter and a base plate. More specifically, the present invention relates to a baking jig consisting of a setter and a base plate on which the setter is placed, which can effectively prevent the setter from sliding.
  • firing is carried out in a multi-tiered configuration in which multiple setters are stacked at specified intervals using a firing jig in which a setter is placed on a member known as a firing base or firing rack.
  • Conventional ceramic setters include, for example, a setter for hot forming processing made of ceramics whose main component is aluminum nitride and consisting of a porous plate with many holes penetrating from the front to the back, and a ceramic firing kiln tool plate in which at least the front and back sides on which the fired object is placed are given an uneven shape and openings are formed.
  • a ceramic lattice body has been disclosed that has a plurality of first ceramic striated portions and a plurality of second ceramic striated portions that intersect with the first ceramic striated portions, and the first and second striated portions have a specific contact form (see Patent Document 1 for an example).
  • a firing jig called a base plate or the like
  • a firing jig has been disclosed that is characterized by having a frame body having a hollow part in the center and a plurality of bridge parts that span the hollow part of the frame body and cross each other at the hollow part, and the frame body and the bridge parts are integrally molded. It has been reported that this firing jig improves the productivity of manufacturing ceramic products by firing.
  • Patent Document 2 discloses a firing rack configured to place a flat setter on which the object to be fired is loaded, the firing rack comprising a frame having an opening on the surface of which the flat setter is placed, a column extending between the frames passing through the center of the frame, a plurality of surrounding parts surrounded by the frame and the column, and a plurality of sub-columns extending from the center of the surrounding parts toward the frame or the column. It has been reported that this firing rack can reduce unevenness in the in-plane temperature distribution of the loaded flat setter.
  • such ceramic setters and base plates are often stacked in multiple tiers during firing, with a setter placed on each base plate and an object to be fired placed on each setter.
  • A is a setter
  • B is the base plates stacked in multiple tiers
  • C is the object to be fired
  • a setter is placed on each base plate and an object to be fired is placed on top of it, and thus M, a multi-tiered firing jig, is subjected to the firing process.
  • M a multi-tiered firing jig
  • the problem that this invention aims to solve is to provide a firing jig consisting of a combination of a ceramic setter and a base plate, which has good handling properties so that the setter does not slide easily on the base plate due to slight tilt or vibration (horizontal or vertical movement) during stacking operations or when transporting in a multi-layered state.
  • a firing jig consisting of a setter and a base plate on which the setter is placed
  • one or more linear convex portions are provided on a portion of the surface of the setter adjacent to the base plate
  • one or more groove portions are provided on a portion of the surface of the base plate adjacent to the setter, so that when the setter is placed on the base plate, at least one of the convex portions on the setter is accommodated in at least one of the groove portions on the base plate, and that by designing the ratio of the area within the outline of the surface of the setter adjacent to the base plate to the sum of the projected areas of the convex portions of the setter accommodated in the groove portions of the base plate to be within a predetermined range, the convex portions are accommodated and engaged in the groove portions to a greater extent, thereby effectively restricting the movement of the setter on the base plate and making it possible to sufficiently prevent the setter from sliding on the base plate, and ultimately significantly improving the handleability of the firing
  • a firing jig consisting of a setter and a base plate on which the setter is placed
  • the setter includes one or more linear protrusions having a substantially uniform cross section in the longitudinal direction on a portion of a surface S adjacent to the base plate
  • the base plate includes one or more grooves having a substantially uniform cross section in the longitudinal direction on a portion of a surface P adjacent to the setter, the protrusions and the grooves are formed so that at least one of the protrusions of the setter is received in at least one of the grooves of the base plate when the setter is placed on the base plate, here,
  • the area within the contour of the proximity surface S of the setter (excluding the area of the region that protrudes from the contour of the sole plate when the proximity surface S is viewed vertically when the setter is placed on the sole plate) is b, When the setter is placed on the base plate, the total projected area of the convex portion accommodated in the groove portion (wherein the projected
  • the convex portion of the setter being "housed” in the groove portion of the base plate refers to a state in which, when the proximity surface P of the base plate relative to the setter is viewed horizontally in a cross section perpendicular to the longitudinal direction of the groove portion, at least a portion of the convex portion of the setter is positioned below the uppermost surface of the groove portion (an imaginary surface corresponding to the proximity surface P).
  • a firing jig consisting of a setter and a base plate on which it is placed can be adjusted so that the ratio of the area within the contour of the adjacent surface of the setter relative to the base plate and the sum of the projected areas of the convex portions of the setter housed in the grooves of the base plate is within a specified range, allowing the convex portions to be housed and engaged in the grooves to a greater extent, thereby effectively restricting the movement of the setter on the base plate and making it possible to sufficiently prevent the setter from sliding on the base plate, thus providing the advantage of greatly improving the handleability of the firing jig for ceramic products.
  • FIG. 1 is a diagram illustrating a known layered configuration in which ceramic setters and base plates (firing racks) are stacked in multiple stages.
  • FIG. 2 is a diagram showing a combination of a setter and a base plate of a firing jig according to one embodiment of the present invention.
  • Figure 3 is a diagram illustrating the relationship between the contour area b of the proximity surface S of the setter relative to the base plate and the total projected area a of the convex parts accommodated in the groove portion of the base plate when the setter is placed on the base plate in a combination of a setter and base plate of a firing jig according to one embodiment of the present invention.
  • FIG. 1 is a diagram illustrating a known layered configuration in which ceramic setters and base plates (firing racks) are stacked in multiple stages.
  • FIG. 2 is a diagram showing a combination of a setter and a base plate of a firing jig according to one embodiment of the present invention.
  • Figure 3 is
  • FIG. 4 is a diagram illustrating the relationship between the maximum width Wc of the convex portion of the setter and the maximum width Wp of the groove portion of the base plate in a combination of a setter and base plate of a firing jig according to one embodiment of the present invention.
  • FIG. 5 is a diagram illustrating the relationship between the average depth Dg ⁇ av of the grooves of the base plate and the vertical minimum distance Ig between the grooves in a combination of a setter and base plate of a firing jig according to one embodiment of the present invention.
  • FIG. 5 is a diagram illustrating the relationship between the average depth Dg ⁇ av of the grooves of the base plate and the vertical minimum distance Ig between the grooves in a combination of a setter and base plate of a firing jig according to one embodiment of the present invention.
  • FIG. 6 is a diagram illustrating the relationship (aspect ratio) between the maximum width Wc of the convex portion of the setter and the length Lc between both ends in the longitudinal direction in a combination of a setter and a base plate of a firing jig according to one embodiment of the present invention.
  • FIG. 7 is a diagram illustrating the relationship between the maximum height Hc of the convex portion of the setter and the depth Dg of the groove portion of the base plate in which the convex portion is accommodated, in a combination of a setter and base plate of a firing jig according to one embodiment of the present invention.
  • FIG. 7 is a diagram illustrating the relationship between the maximum height Hc of the convex portion of the setter and the depth Dg of the groove portion of the base plate in which the convex portion is accommodated, in a combination of a setter and base plate of a firing jig according to one embodiment of the present invention.
  • FIG. 8 is a diagram illustrating the relationship between the maximum height Hc of the convex portion of the setter and the maximum width Wc of the convex portion in a combination of the setter and the base plate of the firing jig according to one embodiment of the present invention.
  • FIG. 9 is a diagram illustrating a mesh-shaped portion of a setter in a baking jig according to an embodiment of the present invention.
  • FIG. 10 is a diagram illustrating an outline of the relationship between a base plate provided with a V-shaped groove and a setter provided with a protrusion in the embodiment.
  • the setter constituting the firing jig of the present invention includes, on a portion of the adjacent surface S to the base plate which also constitutes the firing jig, one or more linear convex portions with a generally uniform cross section in the longitudinal direction.
  • the base plate constituting the firing jig of the present invention includes, on a portion of the adjacent surface P to the setter which also constitutes the firing jig, one or more groove portions with a generally uniform cross section in the longitudinal direction.
  • the convex portions and the groove portions must be formed so that at least one of the convex portions of the setter is accommodated in at least one of the groove portions of the base plate.
  • FIG. 2 An embodiment of a combination of a setter and a base plate of a baking jig according to the present invention is shown in Fig. 2. Neither the setter nor the base plate of the baking jig according to the present invention is limited to the form shown in Fig. 2, which is merely an example.
  • 1 indicates a firing jig (combination)
  • 2 indicates a setter (a setter of a mesh-like ceramic sheet as an example)
  • 2S indicates the surface of the setter 2 adjacent to the base plate (the back side of the paper in this figure)
  • 3 indicates the base plate
  • 3P indicates the surface of the base plate 3 adjacent to the setter
  • 4 indicates a base portion of the base plate
  • 5 indicates a peripheral wall portion (rib: provided optionally)
  • 6 indicates a groove portion of the base plate corresponding to at least a part of a protrusion portion (not shown as it is on the back side of the paper) provided on the surface 2S of the setter adjacent to the base plate
  • HL indicates an opening (provided optionally).
  • the setter 2 which is one of the components of the firing jig 1 in this example, is a mesh ceramic sheet setter formed entirely of a mesh-like portion consisting of a first striated portion layer made up of first striated portions extending in one direction at approximately constant intervals, and a second striated portion layer made up of second striated portions extending in one direction at approximately constant intervals and approximately perpendicular to the first striated portion.
  • the base plate 3, which is the other component of the firing jig 1, has a base portion 4 which is a substantially rectangular plate-like body, and a peripheral wall portion 5 (rib) formed upright around the entire periphery.
  • the base portion 4 of the base plate 3 may have legs for stacking at each of the four corners of the substantially rectangular shape, or may be configured so that such legs can be attached.
  • the peripheral wall portion 5 is illustrated as forming the entire periphery, but it may also be a part of the periphery.
  • the setter-facing surface 3P of the sole plate 3 forms a plane that can accommodate the entire contour (periphery) of the setter 2's proximity surface 2S, and the peripheral wall 5 is formed so that when the setter 2 is placed on the proximity surface 3P of the sole plate 3, the entire peripheral portion of the setter 2 has a predetermined distance to the peripheral wall.
  • the contact surface of the second striated portion layer with the first striated portion layer forms the proximity surface 2S (back side of the paper) of the setter, and the first striated portion constituting the first striated portion layer forms the convex portion of the setter.
  • the setter 2's proximity surface 3P of the sole plate 3 is provided with multiple groove portions 6, and the positions of these groove portions 6 correspond to the positions of at least some of the multiple convex portions (first striated portions) of the setter, and the convex portions can be accommodated in the groove portions 6 at those locations.
  • the convex parts and the groove parts are formed so that at least one of the convex parts of the setter 2 is accommodated in at least one of the groove parts of the base plate 3, thereby providing the ability to prevent and suppress sliding.
  • the firing jig 1 is stacked in multiple layers, ventilation is ensured between the multiple legs, between the peripheral wall parts 5 if they are formed in part of the periphery, and also in the openings HL if they are formed in part of the base plate, allowing for an efficient firing process.
  • FIG. 3 illustrates a cross section perpendicular to the longitudinal direction of a plurality of protrusions of a setter when the setter is placed on a base plate in a combination of the setter and base plate of a firing jig according to one embodiment of the present invention.
  • 7 indicates the main body (base) of the setter
  • 7S indicates the surface of the setter adjacent to the base plate
  • 8 indicates a plurality of linear convex portions formed on part of the adjacent surface 7S and having a substantially uniform and substantially circular cross-section in the longitudinal direction
  • 9 indicates the main body (base) of the base plate
  • 9P indicates the surface of the base plate adjacent to the setter
  • 10 indicates a plurality of groove portions formed on part of the adjacent surface 9P and having a substantially uniform and substantially circular cross-section in the longitudinal direction.
  • the number of convex portions and groove portions may be one or more, and the number is not particularly limited.
  • the number of convex portions is preferably two or more, and more preferably three or more, five or more, ten or more, twenty or more, or thirty or more.
  • the number of groove portions is preferably two or more, and more preferably three or more, five or more, ten or more, twenty or more, or thirty or more.
  • the number of convex portions and groove portions may each be 100 or less from the viewpoint of manufacturing efficiency.
  • the cross-sectional shape of the convex portion is illustrated as being approximately circular, but is not limited thereto.
  • the cross-sectional shape of the convex portion may be, for example, approximately semicircular, approximately triangular, approximately rectangular, or approximately trapezoidal. From the viewpoint of facilitating the formation of the convex portion, it is preferable that the cross-sectional shape of the convex portion is approximately circular.
  • the setter is a mesh-like ceramic sheet
  • the cross-sectional shape of the convex portion is approximately circular.
  • the cross-sectional shape of the groove portion is exemplified as approximately semicircular in FIG. 3, but is not limited thereto.
  • the cross-sectional shape of the groove portion may be, for example, approximately V-shaped (approximately triangular), approximately rectangular, or approximately trapezoidal. Regardless of these cross-sectional shapes of the convex portion and the groove portion, the desired effect can be achieved as long as the requirements described in this specification are satisfied. From the viewpoint of manufacturing efficiency, the cross-sectional shape of the convex portion may be approximately circular (especially when a mesh-like ceramic sheet is used), and the cross-sectional shape of the groove portion may be approximately V-shaped.
  • two convex portions 8 are formed approximately parallel to each other, and two groove portions 10 are formed approximately parallel to each other, and when the setter 7 is placed on the base plate 9, both of the two convex portions 8 are accommodated in each of the two groove portions 10 arranged in the corresponding positions.
  • two or more convex portions of the setter and groove portions of the base plate are formed approximately parallel to each other, and when the setter is placed on the base plate, the majority of the convex portions, preferably 70% or more of the convex portions, and more preferably substantially all of the convex portions are accommodated in the groove portions of the base plate.
  • This configuration more effectively prevents the setter from sliding on the base plate, and thus significantly improves the handleability of the setter as a firing jig for ceramic products.
  • FIG. 3 an example is shown in which two convex portions 8 are formed approximately parallel to each other and two groove portions 10 are formed approximately parallel to each other, but in another embodiment, when the setter has three or more convex portions, these convex portions may be formed approximately equally spaced apart, and/or when the base plate has three or more groove portions, these groove portions may be formed approximately equally spaced apart.
  • This configuration further increases the probability that the convex portions of the setter will be successfully accommodated in the groove portions of the base plate, thereby further improving the anti-sliding properties of the setter on the base plate.
  • the symbol b indicates the area within the contour of the proximity surface 7S of the setter 7 relative to the base plate 9 (excluding the area of the region that extends beyond the contour of the base plate 9 when the proximity surface 7S is viewed vertically when the setter 7 is placed on the base plate 9).
  • the symbol a1 indicates the projected area of the convex portion 8 accommodated in the groove portion 10 on the left side of the figure when the setter 7 is placed on the base plate 9 (the maximum cross-sectional area of the convex portion in a plane parallel to the proximity surface 7S of the setter 7).
  • the symbol a2 similarly indicates the projected area of the convex portion 8 accommodated in the groove portion 10 on the right side of the figure when the setter 7 is placed on the base plate 9 (the maximum cross-sectional area of the convex portion in a plane parallel to the proximity surface 7S of the setter 7).
  • the symbol a is the sum of the projected areas a1 and a2 of the convex portions 8.
  • FIG. 3 only two protrusions 8 and two grooves 10 are shown as an example for ease of illustration, but if there are three or more protrusions 8 housed in the grooves 10, the sum ( ⁇ ax) of their projected areas ax is a.
  • the relationship between the total projected area a of the convex portion 8 and the contour inner area b of the adjacent surface 7S of the setter 7 satisfies the following formula A.
  • formula A 0.5 ⁇ (a / b) * 100 ⁇ 90
  • the firing jig of the present invention which satisfies the relationship of formula A, the convex part of the setter is firmly and stably accommodated and engaged in the groove part of the base plate, which effectively limits the movement of the setter on the base plate, sufficiently prevents the setter from sliding on the base plate, and ensures ease of designing the layout of the convex part.
  • 1 ⁇ (a/b)*100 ⁇ 90 it is even more preferable that 5 ⁇ (a/b)*100 ⁇ 90, it is even more preferable that 10 ⁇ (a/b)*100 ⁇ 90, it is even more preferable that 20 ⁇ (a/b)*100 ⁇ 90, it is even more preferable that 30 ⁇ (a/b)*100 ⁇ 90, it is even more preferable that 40 ⁇ (a/b)*100 ⁇ 90, it is even more preferable that 50 ⁇ (a/b)*100 ⁇ 90, it is even more preferable that 60 ⁇ (a/b)*100 ⁇ 90, and it is most preferable that 70 ⁇ (a/b)*100 ⁇ 90.
  • FIG. 4 illustrates the relationship between the maximum width Wc of the convex portion of the setter and the maximum width Wp of the groove portion of the base plate when the setter is placed on the base plate for a combination of a setter and base plate of a firing jig according to one embodiment of the present invention.
  • Wc indicates the maximum width of a cross section perpendicular to the longitudinal direction of the convex portion 8 of the setter 7, in a direction parallel to the adjacent surface 7S of the setter 7 relative to the base plate 9.
  • Wp indicates the maximum width of a cross section perpendicular to the longitudinal direction of the groove portion 10 in which the convex portion 8 is housed, in a direction parallel to the adjacent surface 9P of the base plate 9 relative to the setter 7, when the setter 7 is placed on the base plate 9.
  • the cross-sectional shape of the convex portion is exemplified as being substantially circular
  • the cross-sectional shape of the groove portion is exemplified as being substantially semicircular, but as explained with reference to FIG. 3, they are not limited to these shapes.
  • the ratio Wc/Wp of the maximum width Wc in a direction parallel to the adjacent surface 7S of a cross section perpendicular to the longitudinal direction of at least one of the convex portions 8 of the setter 7 and the maximum width Wp in a direction parallel to the adjacent surface 9P of a cross section perpendicular to the longitudinal direction of the groove portion 10 in which the convex portion 8 is accommodated when the setter 7 is placed on the base plate 9 is 2 or less (greater than 0).
  • the convex portion of the setter is accommodated and engaged deep toward the bottom of the groove portion of the base plate, thereby effectively restricting the movement of the setter on the base plate and sufficiently preventing the setter from sliding on the base plate.
  • these effects can greatly improve the handleability of the firing jig for ceramic products.
  • Wc/Wp is preferably (greater than 0) 1.8 or less, more preferably 1.6 or less, even more preferably 1.4 or less, even more preferably 1.2 or less, even more preferably 1.0 or less, and most preferably 0.9 or less.
  • Wc/Wp is preferably 0.2 or more and 1.8 or less, more preferably 0.2 or more and 1.6 or less, even more preferably 0.2 or more and 1.4 or less, even more preferably 0.2 or more and 1.2 or less, even more preferably 0.2 or more and 1.0 or less, and most preferably 0.2 or more and 0.9 or less.
  • Wc/Wp is preferably 0.4 or more and 1.8 or less, more preferably 0.4 or more and 1.6 or less, even more preferably 0.4 or more and 1.4 or less, even more preferably 0.4 or more and 1.2 or less, even more preferably 0.4 or more and 1.0 or less, and most preferably 0.4 or more and 0.9 or less.
  • Figure 5 illustrates the relationship between the average depth Dg ⁇ av of the groove portions of the base plate and the shortest vertical distance Ig between the groove portions when the setter is placed on the base plate for a combination of a setter and base plate of a firing jig according to one embodiment of the present invention.
  • 5 shows an example in which two protrusions 8 are formed substantially parallel to each other, and two grooves 10 are formed substantially parallel to each other, each accommodating the two protrusions 8.
  • three or more protrusions 8 may be formed substantially parallel to each other and at substantially equal intervals, and three or more grooves 10 are formed substantially parallel to each other and at substantially equal intervals, each accommodating the three or more protrusions 8.
  • FIG. 1 illustrates the relationship between the average depth Dg ⁇ av of the groove portions of the base plate and the shortest vertical distance Ig between the groove portions when the setter is placed on the base plate for a combination of a setter and base plate of a firing jig according to one embodiment of the present invention.
  • Dg ⁇ av indicates the average depth of the groove portion 10 of the sole plate 9 (the average value of each groove portion 10 in terms of the length from the adjacent surface 9P of the sole plate 9 relative to the setter 7 to the lowest position in the vertical direction of the cross section perpendicular to the longitudinal direction of the groove portion 10).
  • the average value here refers to the average value of all the groove portions 10 provided on the sole plate 9 when the number of groove portions 10 provided on the sole plate 9 is up to 10, and refers to the average value of any 10 of the groove portions 10 provided on the sole plate 9 when the number of groove portions 10 provided on the sole plate 9 is 11 or more. Also, in FIG.
  • Ig indicates the vertical shortest distance between the groove portions 10 of the sole plate 9 (the average value of multiple vertical shortest distances when three or more groove portions are formed).
  • the average value here refers to the average value of all the vertical shortest distances between the groove portions 10 when the number of the vertical shortest distances between the groove portions 10 is up to 9 (the number of groove portions 10 is up to 10), and refers to the average value of any 9 of the vertical shortest distances when the number of the vertical shortest distances between the groove portions 10 is 10 or more (the number of groove portions 10 is 11 or more).
  • the cross-sectional shape of the convex portion is illustrated as being substantially circular, and the cross-sectional shape of the groove portion is illustrated as being substantially semicircular, but as explained with reference to FIGS. 3 and 4, these shapes are not limited to these.
  • the ratio Ig/Dg ⁇ av of the vertical shortest distance Ig between the groove portions 10 (if three or more groove portions 10 are formed, this refers to the average value of the multiple vertical shortest distances) to the average depth Dg ⁇ av of the groove portions 10 of the base plate 9 (which refers to the average value of each groove portion 10 in terms of the length from the adjacent surface 9P of the cross section perpendicular to the longitudinal direction of the groove portion 10 to the lowest vertical position) is 0.05 or more and 600 or less.
  • the firing jig of one embodiment of the present invention in which the ratio Ig/Dg.av is 0.05 or more and 600 or less, the convex part of the setter is deeply and stably received and engaged with the groove part of the base plate with dense engagement points, thereby effectively restricting the movement of the setter on the base plate and sufficiently preventing the setter from sliding on the base plate. Furthermore, with these effects, the handling property of the firing jig for ceramic products can be significantly improved.
  • Ig/Dg ⁇ av is preferably 0.05 or more and 500 or less, more preferably 0.05 or more and 400 or less, even more preferably 0.05 or more and 300 or less, even more preferably 0.05 or more and 200 or less, even more preferably 0.05 or more and 100 or less, even more preferably 0.05 or more and 50 or less, even more preferably 0.05 or more and 10 or less, even more preferably 0.05 or more and 5 or less, and most preferably 0.05 or more and 2 or less.
  • Ig/Dg ⁇ av is preferably 0.1 or more and 500 or less, more preferably 0.1 or more and 400 or less, even more preferably 0.1 or more and 300 or less, even more preferably 0.1 or more and 200 or less, even more preferably 0.1 or more and 100 or less, even more preferably 0.1 or more and 50 or less, still more preferably 0.1 or more and 10 or less, even more preferably 0.1 or more and 5 or less, and most preferably 0.1 or more and 2 or less.
  • FIG. 6 illustrates an example of the relationship (aspect ratio) between the maximum width Wc of the convex portion of the setter and the length Lc between both ends in the longitudinal direction for a combination of a setter and a base plate of a firing jig according to one embodiment of the present invention.
  • Fig. 6 is a schematic diagram of one of the protruding parts 8 (linear parts in the case of a mesh-like ceramic sheet) provided on the adjacent surface 7S of the setter 7 relative to the base plate 9, viewed perpendicularly to the adjacent surface 7S.
  • the protruding parts 8 linear parts in the case of a mesh-like ceramic sheet
  • Wc indicates the maximum width of the cross section perpendicular to the longitudinal direction of the protruding part 8 of the setter 7, in the direction parallel to the adjacent surface 7S of the setter 7 relative to the base plate 9. Furthermore, Lc indicates the length between both ends of the protruding part 8 in the longitudinal direction.
  • the aspect ratio Lc/Wc of the length Lc between both ends in the longitudinal direction to the maximum width Wc in a direction parallel to the adjacent surface 7S of the cross section perpendicular to the longitudinal direction is 10 or more.
  • the convex portion of the setter is stably accommodated and engaged with the groove portion of the base plate in a manner that has continuous engagement points over a longer distance, thereby effectively restricting the movement of the setter on the base plate and sufficiently preventing the setter from sliding on the base plate.
  • these effects can be accompanied by a significant improvement in the handleability of the firing jig for ceramic products.
  • Lc/Wc is preferably 11 or greater, more preferably 12 or greater, even more preferably 13 or greater, even more preferably 20 or greater, even more preferably 30 or greater, even more preferably 50 or greater, even more preferably 70 or greater, and most preferably 100 or greater.
  • Figure 7 illustrates the relationship between the maximum height Hc of the convex portion of the setter when the setter is placed on the base plate and the depth Dg of the groove portion of the base plate in which this convex portion is accommodated, for a combination of a setter and a base plate of a firing jig according to one embodiment of the present invention.
  • Hc indicates the maximum height of a cross section perpendicular to the longitudinal direction of the protruding portion 8 of the setter 7, in a direction perpendicular to the adjacent surface 7S of the setter 7 relative to the base plate 9.
  • Dg indicates the depth from the adjacent surface 9P of the base plate 9 relative to the setter 7 to the lowest position in the vertical direction of a cross section perpendicular to the longitudinal direction of the groove portion 10 in which the protruding portion 8 is accommodated when the setter 7 is placed on the base plate 9.
  • the cross-sectional shape of the convex portion is illustrated as being substantially circular, and the cross-sectional shape of the groove portion is illustrated as being substantially semicircular, but as explained with reference to FIGS. 3 to 5, these shapes are not limited thereto.
  • the ratio Dg/Hc of the depth Dg from the adjacent surface 9P of a cross section perpendicular to the longitudinal direction of the groove portion 10 in which the convex portion 8 is accommodated when the setter 7 is placed on the base plate 9 to the maximum height Hc in a direction perpendicular to the adjacent surface 7S of at least one cross section perpendicular to the longitudinal direction of the convex portion 8 of the setter 7 is 0.1 or more.
  • the convex part of the setter is stably received and engaged deeper toward the bottom of the groove part of the base plate, which increases the resistance of the setter to movement on the base plate, effectively restricting the movement of the setter and sufficiently preventing the setter from sliding on the base plate. Furthermore, these effects can greatly improve the handleability of the firing jig for ceramic products.
  • Dg/Hc is preferably 0.15 or greater, more preferably 0.2 or greater, even more preferably 0.25 or greater, even more preferably 0.3 or greater, even more preferably 0.35 or greater, even more preferably 0.4 or greater, even more preferably 0.45 or greater, even more preferably 0.50 or greater, even more preferably 0.55 or greater, and most preferably 0.60 or greater.
  • FIG. 8 illustrates the relationship between the maximum height Hc of the convex portion of the setter and the maximum width Wc of the convex portion for a combination of a setter and a base plate of a firing jig according to one embodiment of the present invention.
  • Fig. 8 is a schematic diagram of one of the protrusions 8 provided on the adjacent surface 7S of the setter 7 relative to the floor plate 9, viewed perpendicularly to the longitudinal direction of the protrusion 8.
  • Hc is the maximum height of a cross section perpendicular to the longitudinal direction of the protrusion 8 of the setter 7, in a direction perpendicular to the adjacent surface 7S of the setter 7 relative to the floor plate 9.
  • Wc is the maximum width of the cross section perpendicular to the longitudinal direction of the protrusion 8, in a direction parallel to the adjacent surface 7S.
  • the ratio Wc/Hc of the maximum width Wc in a direction parallel to the adjacent surface 7S of a cross section perpendicular to the longitudinal direction of at least one of the convex portions 8 of the setter 7 to the maximum height Hc in a direction perpendicular to the adjacent surface 7S of a cross section perpendicular to the longitudinal direction of this convex portion 8 is 0.3 or more and 4 or less.
  • the convex portion of the setter can easily form a deep and stable state of insertion and engagement with the groove portion of the base plate, regardless of or in accordance with the cross-sectional shape of the groove portion of the base plate, thereby effectively restricting the movement of the setter on the base plate and sufficiently preventing the setter from sliding on the base plate. Furthermore, these effects can greatly improve the handleability of the firing jig for ceramic products.
  • Wc/Hc is preferably 0.4 or greater and 4 or less, more preferably 0.5 or greater and 4 or less, even more preferably 0.6 or greater and 4 or less, even more preferably 0.7 or greater and 4 or less, even more preferably 0.8 or greater and 4 or less, even more preferably 0.9 or greater and 4 or less, and most preferably 1 or greater and 4 or less.
  • Wc/Hc is preferably 0.4 or greater and 3 or less, more preferably 0.5 or greater and 3 or less, even more preferably 0.6 or greater and 3 or less, even more preferably 0.7 or greater and 3 or less, even more preferably 0.8 or greater and 3 or less, even more preferably 0.9 or greater and 3 or less, and most preferably 1 or greater and 3 or less.
  • Wc/Hc is preferably 0.4 or greater and 2 or less, more preferably 0.5 or greater and 2 or less, even more preferably 0.6 or greater and 2 or less, even more preferably 0.7 or greater and 2 or less, even more preferably 0.8 or greater and 2 or less, even more preferably 0.9 or greater and 2 or less, and most preferably 1 or greater and 2 or less.
  • the setter combined with the base plate in the firing jig according to the present invention is a ceramic sheet including at least a mesh-like portion in a part thereof, and the mesh-like portion includes a first striated portion layer including a plurality of first striated portions arranged at a given interval and extending in one direction, and a second striated portion layer including a plurality of second striated portions arranged at a given interval so as to contact and cross each of the first striated portions and extend in one direction, and the first striated portion layer and the second striated portion layer may be integrally formed ceramic sheets.
  • any known setter structure may be adopted for the portion other than the mesh-like portion of the setter.
  • a setter that is a mesh-like ceramic sheet sintered body formed integrally as a whole may be used.
  • the firing jig according to the present invention when the setter (all or part of it) is a setter including a mesh-like ceramic sheet, the contact surface of the second striated portion layer with the first striated portion layer forms the adjacent surface of the setter with respect to the base plate, and the first striated portion constituting the first striated portion layer forms the convex portion of the setter.
  • first striated layer and the second striated layer are "integrally formed" mesh-like sintered bodies means that the striated groups constituting the first striated layer and the striated groups constituting the second striated layer are fired and connected to each other to form an integral structure at their contact points, and are formed so as not to be easily separated.
  • first striated layer and the second striated layer are fired and connected to each other to form an integral structure at their contact points, and are formed so as not to be easily separated, and the first striated layer and the second striated layer, or different parts of each striated layer, may be formed from a single composition.
  • first and second filamentary layers are formed such that the filaments constituting the first and second filamentary layers are sintered and connected to each other at the contact points to form an integral structure, and are not easily separated, and the first and second filamentary layers, or different portions of each filamentary layer, may be formed from a plurality of different compositions.
  • the mesh portion 11 includes a first striated portion layer composed of a plurality of first striated portions 12 arranged at approximately regular intervals and each striated portion is stretched in one direction, and a second striated portion layer composed of a plurality of second striated portions 13 arranged at approximately regular intervals so as to contact and cross each striated portion of the first striated portion 12 and each striated portion is stretched in one direction.
  • the intersection angle between the two striated portions 12 and 13 can be set appropriately, but for example, the intersection angle of the second striated portion 13 with respect to the first striated portion 12 can be set to 90 degrees.
  • intersection angle of the second striated portion 13 with respect to the first striated portion 12 can be changed within a range of 90 degrees ⁇ 10 degrees.
  • the cross-sectional shape of the first striated portion 12 is not particularly limited, but may be approximately circular or approximately elliptical as shown in the figure.
  • the cross-sectional shape of the second striated portion 13 is not particularly limited, but may be a straight line at the top as shown in the figure, and a curve starting from both ends of the straight line at the bottom (i.e., a shape in which a part of a substantially circular or substantially elliptical shape is cut in a straight line), so that the top surface of the entire second striated portion 13 (i.e., the top surface of the second striated portion layer) forms a single flat surface.
  • the cross-sectional shapes of the first striated portion 12 and the second striated portion 13 can be substantially polygonal such as substantially rectangular, or a shape in which a part of the polygonal shape is cut in a straight line, in addition to the substantially circular and substantially elliptical shapes described above.
  • the mesh portion of the setter may further have a plurality of third striated portions made of ceramics extending in one direction in addition to the first striated portion and the second striated portion (the third striated portion layer may be formed by this).
  • the direction in which the third striated portions extend may be the same as the direction in which the first striated portions extend, or may be inclined obliquely (for example, in a direction greater than -45° and smaller than 45°) with respect to the direction in which the first striated portions extend.
  • the cross-sectional shape of the second striated portion may be substantially circular or substantially elliptical, and the cross-sectional shape of the third striated portion may be a straight line at the upper portion and a curved line starting from both ends of the straight line at the lower portion (i.e., a shape in which a part of the substantially circular or substantially elliptical shape is cut in a straight line), so that the upper surface of the entire third striated portion (i.e., the upper surface of the third striated portion layer) may form a single flat surface.
  • a fourth linear portion or any subsequent linear portions can be formed.
  • a setter may be used that is a mesh-shaped ceramic sheet sintered body formed integrally from a single material. Using such a setter greatly increases the strength of the entire ceramic sheet and also leads to efficient manufacturing of the setter.
  • the mesh-shaped portion occupies a portion of the ceramic sheet, the mesh-shaped portion and the portion other than the mesh-shaped portion may be a ceramic sheet sintered body formed integrally.
  • the strength of the entire ceramic sheet is increased by using the same raw material powder for both, and a decrease in the bonding strength due to the thermal history of heating and cooling during sintering (repeated expansion and contraction) can be prevented.
  • the mesh-like portion of the ceramic sheet has a cross section in which the first striated portion and the second striated portion intersect with each other such that the cross section of the first striated portion has a circular or elliptical shape
  • the cross section of the second striated portion has a shape (approximately arch-shaped) consisting of a straight portion and a convex curved portion having both ends of the straight portion as its ends, and further, when viewed in vertical cross section at the intersection, only the apex of the convex curved portion of the second striated portion and the upwardly convex apex of the circle or ellipse of the first striated portion are in contact (a so-called point contact configuration).
  • the mesh-like portion of the ceramic sheet can have a configuration in which the cross section of the first striated portion has a circular or elliptical shape at a portion other than the intersection between the first striated portion and the second striated portion, and the cross section of the second striated portion has a shape (approximately arch-shaped) composed of a straight portion and a convex curved portion with both ends of the straight portion as ends at a portion other than the intersection, and the first striated portion and the second striated portion each form an intersection where they contact over a surface rather than just a single point.
  • This configuration can be called a surface contact structure as opposed to the so-called point contact described above.
  • the mesh-like portion of the ceramic sheet has a cross section of the first striated portion that has a circular or elliptical shape at a portion other than the intersection of the first striated portion and the second striated portion, and a cross section of the second striated portion that has a shape (approximately arch-shaped) composed of a straight portion and a convex curved portion with both ends of the straight portion as ends at a portion other than the intersection, and further, the projected image of the first striated portion in a plan view has a shape that curves and bulges outward in the width direction at the intersection, so that the width of the projected image at the intersection is larger than the width of the projected image at the portion other than the intersection.
  • the cross section of the first striated portion has a circular or elliptical shape at a portion other than the intersection of the first striated portion and the second striated portion
  • the cross section of the second striated portion has a shape (approximately arch shape) consisting of a straight portion and a convex curved portion with both ends of the straight portion as ends at a portion other than the intersection of the first striated portion and the second striated portion
  • the sintered body may have a straight side portion in at least a portion of the outline in a plan view
  • the first striated portion and the second striated portion may each independently intersect with the straight side portion (outer side) at an angle of 10 degrees or more and 170 degrees or less (i.e., within a wide angle range including angles that are not right angles).
  • the mesh portion of the ceramic sheet may be a plate-shaped ceramic structure having, in addition to a plurality of first striated portions and a plurality of second striated portions, a plurality of third striated portions made of ceramic passing on the diagonals of a quadrilateral defined by the intersection of the first striated portions and the second striated portions, and having a plurality of triangular through holes defined by the first striated portions, the second striated portions, and the third striated portions.
  • the portion other than the mesh-like portion is not particularly limited, but examples include a ceramic plate having many fine pores (including a plate having different pore sizes/different pore densities in different areas) and a sheet in which a first striated layer (support layer) and a second striated layer are arranged in a shape other than a mesh (one example is a so-called lattice-shaped sheet).
  • the raw material powder for manufacturing the setter is not particularly limited and may contain various ceramic materials.
  • Ceramic materials used as the ceramic raw material powder include alumina (Al 2 O 3 ), zirconia (ZrO 2 ), magnesium oxide (MgO), mullite (3Al 2 O 3 -2SiO 2 ), silicon carbide (SiC), silicon nitride (Si 3 N 4 ), aluminum nitride (AlN), boron carbide (B 4 C), cordierite (MgO/Al 2 O 3 /SiO 2 ), aluminum titanate (Al 2 TiO 5 ), magnesium titanate (MgTiO 3 ), titanium diboride (TiB 2 ), and the like, or a combination of two or more of them.
  • alumina Al 2 O 3
  • ZrO 2 zirconia
  • MgO magnesium oxide
  • mullite 3Al 2 O 3 -2SiO 2
  • silicon carbide SiC
  • silicon nitride Si 3 N 4
  • AlN aluminum nitride
  • B 4 C boron carbide
  • a sintered body manufactured using raw material powder that is a combination of one or two or more of these ceramic materials will naturally have a composition that can be produced from these materials.
  • the mass ratio of the ceramic raw material powder in the raw material paste may be generally 20 mass % or more and 85 mass % or less, and preferably 30 mass % or more and 75 mass % or less, based on the mass of the entire paste.
  • the setter may be made entirely of a single composition or may be a combination of parts made of different compositions, in one embodiment, a setter may be used that is integrally made entirely of a single type of material.
  • a setter may be used that is integrally made entirely of a single type of material.
  • the first and second striated layers of the mesh-like portion, or different portions of each striated layer may be formed from a single composition.
  • the first and second striated layers of the mesh-like portion, or different portions of each striated layer may be formed from a plurality of different compositions.
  • a setter may be used that is a mesh-like ceramic sheet sintered body integrally formed as a whole from a single type of material. Use of such a setter significantly increases the strength of the entire ceramic sheet and also leads to efficient manufacture of the setter.
  • the average particle size of the ceramic raw material powder used in the raw material paste may usually be in the range of 0.1 to 20 ⁇ m, and preferably in the range of 0.2 to 10 ⁇ m.
  • the average particle size of the ceramic raw material powder here is the volume cumulative median diameter (D50) value measured by the laser diffraction/scattering method.
  • Water is usually used as the medium of the raw material paste for producing a molded body that is a precursor of the first and second striated layers of the mesh-like portion.
  • a medium other than water alcohol, acetone, ethyl acetate, etc. can also be used. Two or more of these media may be mixed.
  • the mass ratio of the medium in the raw material paste may usually be 10% by mass or more and 60% by mass or less, and preferably 15% by mass or more and 55% by mass or less, based on the mass of the entire paste.
  • the raw material paste for producing the molded body that is the precursor of the first and second striated layers of the mesh-like portion may optionally contain an appropriate amount of any known sintering aid.
  • the raw material paste may also contain any known binder.
  • the mass proportion of the binder in the raw material paste may be, for example, 0% by mass or more and 40% by mass or less, and is preferably 1% by mass or more and 40% by mass or less, relative to the total mass of the raw material paste.
  • the viscosity of the raw material paste is high at the temperature when the linear coated body is applied, in order to be able to successfully manufacture the linear coated body.
  • the viscosity of the raw material paste is not particularly limited, but is preferably 1.5 MPa ⁇ s or more and 5.0 MPa ⁇ s or less at the temperature when it is applied (typically room temperature, such as about 25°C).
  • the viscosity of the raw material paste here refers to the measured value 4 minutes after the start of measurement at a rotation speed of 0.3 rpm using a cone-plate type rotational viscometer or rheometer.
  • the raw material paste may contain any known thickener, flocculating agent, thixotropic agent, etc. as a viscosity adjusting agent.
  • the raw material paste may contain, for example, any known plasticizer, lubricant, dispersant, settling inhibitor, pH adjuster, etc.
  • the raw material paste thus obtained is discharged from a discharge device onto a flat substrate to form a first linear coated body having a plurality of stripes arranged at given intervals and each stripe extending in one direction.
  • the first linear coated body corresponds to the second linear portion of the mesh-like portion.
  • various known devices such as a small extruder or a printer can be used. These discharge devices may typically include a dispenser having a nozzle.
  • an operation can be performed to remove the medium contained in the first striated coated body, dry it, and increase the viscosity.
  • the ratio of the medium in the first striated coated body after the medium removal operation may be reduced to preferably 50% by mass or less, more preferably 30% by mass or less.
  • a second filamentary coated body is formed, each filament extending in one direction and arranged at a given interval so as to contact and intersect with each filament of the first filamentary coated body.
  • the second filamentary coated body corresponds to the first filamentary portion of the mesh-like portion.
  • the raw material paste for forming the second filamentary coated body may be the same as or different from the raw material paste for forming the first filamentary coated body, but it is more preferable that they are the same from the viewpoints of efficiency in forming the filamentary coated body and integrity of the structure and physical properties of the ceramic sheet sintered body to be produced.
  • the specific shapes of the first multiple filamentary coated body and the second multiple filamentary coated body formed as a molded body can be constructed to match the desired shapes of the various mesh-like portions described above.
  • the raw material paste may be used to optionally form a third filamentary coating body having multiple stripes that are arranged at given intervals so as to contact each stripe of the second filamentary coating body and intersect with the first and second filamentary coating bodies, each stripe being stretched in one direction.
  • the raw material paste for forming the optional third filamentary coating body may be the same as or different from the raw material paste for forming the first and second filamentary coating bodies, but it is more preferable that they are the same from the viewpoints of efficiency in forming the filamentary coating body and integrity of the structure and physical properties of the mesh-like portion produced.
  • the molded body thus obtained including the multiple first filamentary coated bodies and the multiple second filamentary coated bodies, is peeled off from the substrate (the workbench on which the molded bodies are formed) and placed in a firing jig (firing furnace), where it is fired to obtain the desired mesh-like portion.
  • a firing jig firing furnace
  • the mesh-like portion including the first filamentary layer made up of the multiple first filamentary portions and the second filamentary layer made up of the multiple second filamentary portions is usually constructed as a sintered body, which is an integrated structure that does not involve physical bonding of the individual components by adhesive.
  • the firing process to obtain the mesh-like portion may be carried out in an air atmosphere (atmospheric pressure) as necessary, or may be carried out under pressure with an inert gas such as nitrogen.
  • the firing temperature may be selected appropriately depending on the type of raw powder of the ceramic material. The same applies to the firing time. Non-limiting examples of the firing temperature may be 500°C or more, 800°C or more, or 1000°C or more, and 4000°C or less, 3500°C or less, or 3000°C or less. Non-limiting examples of the firing time may be 30 minutes or more, 1 hour or more, or 2 hours or more, and 24 hours or less, 12 hours or less, or 6 hours or less.
  • the contact surface of the second striated portion layer with the first striated portion layer in the mesh-like portion forms the adjacent surface S with respect to the base plate of the setter, and the first striated portion constituting the first striated portion layer forms the convex portion of the setter, so there is no need to form the convex portion separately.
  • the ceramic sheet (base portion other than the convex portions) and the convex portions provided on the flat surface of the surface may be formed from the same raw material (i.e., raw material containing the same mixture of ceramic raw material powder and additives) or from different raw materials.
  • the ceramic sheet (base portion other than the convex portions) and the convex portions provided on the flat surface of the surface of the ceramic sheet be formed from the same raw material, from the viewpoint of preventing a decrease in bonding strength due to the thermal history of heating and cooling during firing (repeated expansion and contraction) and the resulting peeling of the convex portions from the sheet.
  • a setter ceramic sheet having a convex portion having a substantially uniform cross section in the longitudinal direction formed separately on the flat surface of the front surface can be manufactured by forming an integral molded body using any of the known molding methods such as press molding, slip casting, vibration molding, etc., and then firing the body under conditions similar to those described above for the firing process of the mesh-like portion.
  • a similar method to that used for manufacturing a ceramic sheet including a mesh-like portion can be adopted, in which the raw material paste is discharged from a discharge device onto a flat substrate to form a first filament coating body and then fired.
  • the ceramic sheet (other than the convex portion) and the convex portion provided on the flat surface of the front surface are separately formed and fired, and then the sintered product of the convex portion can be bonded to a predetermined region on the upper surface of the sintered product of the ceramic sheet (other than the convex portion) with any known ceramic adhesive.
  • Non-limiting examples of such ceramic adhesives include adhesive compositions containing polyimide resins, epoxy resins, or polyamideimide resins, and inorganic adhesive compositions mainly composed of fire-resistant ceramics such as alumina and inorganic polymers (for example, "Aron Ceramic” manufactured by Toa Gosei Co., Ltd.).
  • the ceramic sheet of the setter having a convex portion having a substantially uniform cross section in the longitudinal direction formed separately on the flat surface of the front surface can be obtained by forming a molded body of the ceramic sheet (other than the convex portion) or by sintering this molded body to produce a sintered body, and then machining the surface to form the convex portion. Examples of such machining include, but are not limited to, cutting and polishing using cutting tools such as drills and files.
  • the method for manufacturing the base plate constituting the firing jig according to the present invention is not particularly limited, so long as it is possible to manufacture a base plate including a groove portion satisfying the above requirements on a portion of the surface adjacent to the setter.
  • the ceramic raw material powder and additives for producing the base plate can be appropriately selected from the items described above for the setter.
  • the ceramic raw material powder for the base plate can be one or a combination of two or more of alumina (Al 2 O 3 ), zirconia (ZrO 2 ), magnesium oxide (MgO), mullite (3Al 2 O 3 -2SiO 2 ), silicon carbide (SiC), silicon nitride (Si 3 N 4 ), aluminum nitride (AlN), boron carbide (B 4 C), cordierite (MgO/Al 2 O 3 /SiO 2 ), aluminum titanate (Al 2 TiO 5 ), magnesium titanate (MgTiO 3 ), titanium diboride (TiB 2 ), etc.
  • alumina Al 2 O 3
  • ZrO 2 zirconia
  • MgO magnesium oxide
  • mullite 3Al 2 O 3 -2SiO 2
  • silicon carbide SiC
  • silicon nitride Si 3 N 4
  • AlN aluminum nitride
  • B 4 C boron carbide
  • the base plate including the groove portion can be manufactured by forming an integral molded body having grooves with the desired cross-sectional shape and longitudinal length on its surface using any known molding method such as press molding, cast molding, vibration molding, etc., and then firing the body under conditions similar to those described above for the firing process of the mesh-like portion.
  • the floor plate including the grooves can be obtained by forming a molded body of the base plate (one without grooves) or by sintering the molded body of the base plate to produce a sintered body, and then machining the surface to form the grooves. Examples of such machining include, but are not limited to, cutting and polishing using cutting tools such as drills and files.
  • a lattice-shaped precursor consisting of a first linear body (dried product of the second linear coated body) and a second linear body (dried product of the first linear coated body) perpendicularly intersecting each other was obtained.
  • (3) Firing process The dried lattice-shaped precursor was peeled off from the resin substrate and then placed in an air firing furnace. Degreasing and firing were performed in this firing furnace to obtain a mesh-shaped ceramic sheet 1 made of zirconia. The firing temperature was 1450°C, and the firing time was 3 hours.
  • the first linear portion (having a substantially circular cross-sectional shape) and the second linear portion (having a cross-sectional shape in which a portion of the substantially circular shape is cut linearly) were in point contact at their intersections.
  • the maximum width Wc of the first linear portion in the obtained mesh-shaped zirconia sheet 1 (length in a direction perpendicular to the longitudinal direction, which is the design direction in a plan view, i.e., the maximum width Wc of the cross section perpendicular to the longitudinal direction of the first linear portion in a direction parallel to the adjacent surface of the setter's floor plate) was 4.0 mm.
  • the maximum height Hc of the first filamentary portion (the maximum height of the cross section perpendicular to the longitudinal direction of the first filamentary portion in the direction perpendicular to the adjacent surface of the setter to the floor plate) was estimated to be 4.0 mm, the same as Wc.
  • the interval between the first filamentary portions was 0.1 mm. That is, the size (opening size) of the through hole in the mesh-like ceramic sheet 1 was 0.1 mm ⁇ , and the area of the through hole was 0.01 mm2.
  • the angle between each filamentary portion and the side portion in the mesh-like ceramic sheet 1 was 45°, and the intersection angle between the first filamentary portion and the second filamentary portion was 90°.
  • the outer dimensions of the mesh-like ceramic sheet 1 were 300 mm long x 300 mm wide. Therefore, in this example, the volume b within the contour of the adjacent surface of the mesh-like ceramic sheet 1 relative to the base plate (described later) serving as the setter was 90,000 mm2 (the base plate described later was designed so that when the adjacent surface S is viewed vertically when the setter is placed on the base plate, no area protrudes from the contour of the base plate).
  • the aspect ratio Lc/Wc of the length Lc between both ends of the first filamentary portion in the longitudinal direction to the maximum width Wc of the first filamentary portion of the mesh-like ceramic sheet 1 was 75, and the ratio Wc/Hc of the maximum width Wc of the first filamentary portion to the maximum height Hc of the first filamentary portion was estimated to be 1.0.
  • the mesh-like ceramic sheet 1 is designed so that all of the convex portions (first linear portions) can be accommodated in the groove portions of the base plate (described later) when the mesh-like ceramic sheet 1 is placed on the base plate (described later), the total projected area a of the convex portions accommodated in the groove portions was 69,600 mm2 as determined by image analysis using a digital microscope (manufactured by Keyence, product name "VHX-5000").
  • Table 1 shows the length and width external dimensions of this setter and the outline inner area b of the setter determined thereby, as well as the maximum width Wc (and maximum height Hc) of the first filamentary portions, the spacing between the first filamentary portions, and the total projected area a of the convex portions determined by adjusting these.
  • Setters for ceramic sheets 2 to 4 and 6 to 8, and comparative ceramic sheet 9 were manufactured in the same manner as for mesh-like ceramic sheet 1 for setters, except that the length and width external dimensions of the setter and the outline inner area b of the setter determined thereby, as well as the maximum width Wc of the first filamentary portion, the spacing between the first filamentary portions, and the total projected area a of the convex portions determined by adjusting these were changed as shown in Table 1.
  • Table 1 shows the vertical and horizontal external dimensions of these setters and the outline inner area b of the setters determined thereby, as well as the maximum width Wc of the first filamentary portions, the spacing between the first filamentary portions, and the total projected area a of the convex portions determined by adjusting these.
  • two linear coating bodies were formed with the same raw materials at an interval of 148 mm using a dispenser having a circular nozzle with a diameter of 1.0 mm, and then a firing process was carried out under the same conditions as for the ceramic sheet 1, to obtain a setter for ceramic sheet 5.
  • the maximum width Wc of the cross section perpendicular to the longitudinal direction of the convex portion of the setter obtained from this linear coating body in the direction parallel to the adjacent surface of the setter to the sole plate was 1.0 mm.
  • the cross-sectional shape of the convex portion was a shape in which a part of an approximately circular shape was cut linearly by the flat surface of the sheet.
  • the maximum height Hc of the convex portion (the maximum height of the cross section perpendicular to the longitudinal direction of the convex portion in the direction perpendicular to the adjacent surface of the setter to the sole plate) was estimated to be 0.5 mm.
  • the aspect ratio Lc/Wc of the length Lc between both ends of the convex portion in the longitudinal direction to the maximum width Wc of the convex portion of the ceramic sheet 5 was 150, and the ratio Wc/Hc of the maximum width Wc of the convex portion to the maximum height Hc of the convex portion was estimated to be 2.0.
  • Table 1 shows the vertical and horizontal external dimensions of this setter and the outline inner area b of the setter determined thereby, as well as the maximum width Wc of the convex portions, the spacing between the convex portions, and the total projected area a of the convex portions determined by adjusting these.
  • a precursor molded body was obtained using a mixed material containing 65 parts by mass of alumina, 35 parts by mass of silica, and polyvinyl alcohol (PVA) as a binder as the raw material for manufacturing the floor plate 1 , and then the material was fired at 1700° C. for 4 hours to obtain a rectangular floor plate 1.
  • a rectangular peripheral wall portion 3 mm high and 7 mm wide at the top was provided around the entire periphery of the floor plate 1, and the dimensions were measured so that when a mesh-like ceramic sheet 1 measuring 300 mm long and 300 mm wide was placed on the surface of the floor plate 1, the entire sheet would fit therein and a gap of 3 mm would be provided between the edge of the sheet and the rectangular peripheral wall portion around the entire periphery of the floor plate.
  • a V-shaped groove was provided so that all of the protrusions, which are the first linear portions of the ceramic sheet 1, could be accommodated on the entire surface of the floor plate 1 except for the peripheral wall portion.
  • the V-shaped press processing of the floor plate 1 was performed so that the depth Dg (average depth Dg ⁇ av: according to the above definition, in this case the average value of the depth of any 10 pieces) of the floor plate was 1.00 mm, the maximum width Wp of the groove was 4.00 mm (the maximum width of the cross section perpendicular to the longitudinal direction of the groove in the direction parallel to the adjacent surface P of the floor plate relative to the setter), the vertical shortest distance Ig between the grooves was 0.1 mm (in this case the average value of the vertical shortest distance between each groove) and the ratio Ig/Dg ⁇ av was 0.1, as shown in Table 2.
  • 7e is the main body (base) of the setter
  • 7Se is the adjacent surface of the setter to the sole plate
  • 8e is the convex portion of the setter
  • 9e is the main body (base) of the sole plate
  • 9Pe is the adjacent surface of the sole plate to the setter
  • 10e is the V-shaped groove of the sole plate
  • Hce is the maximum height of the convex portion of the setter
  • Dge is the depth of the groove of the sole plate
  • Dg' is the distance from the adjacent surface 9Pe of the sole plate to the setter to the lowest position of the convex portion 8e.
  • the grooves were designed so that the ratio Dge/Hce of the depth Dge of the sole plate to the maximum height Hce of the convex part of the setter is sufficiently large, and the ratio Dg'/Hce of the distance from the proximal surface 9Pe of the sole plate to the setter to the lowest position of the convex part 8e to Hce is in the range of 0.1 or more.
  • Dg' can be calculated by subtracting the vertical distance between the proximal surface 7Se of the setter to the sole plate and the proximal surface 9Pe of the sole plate to the setter (the gap between the main body 7e of the setter and the main body 9e of the sole plate) from the maximum height Hce of the convex part.
  • Plates 2 to 8 and comparative plate 9 were manufactured in the same manner as plate 1, except that the ceramic sheets 2 to 8 and comparative ceramic sheet 9, which are manufacturing setters, were made to fit the entirety of each sheet and had the above-mentioned peripheral wall portion around the entire circumference of the plate, and groove portions of the shape shown in Table 2 (depth Dg (average depth Dg ⁇ av), maximum width Wp, shortest vertical distance Ig, ratio Ig/Dg ⁇ av) were formed by processing using a press mold.
  • the grooves were designed so that the ratio Dg'/Hce was in the range of 0.1 or more, as in plate 1 (see FIG. 10 again).
  • the grooves were designed so that the ratio Dg'/Hce was in the range of 0.05 or more and 0.02 or more, respectively.
  • Examples 1 to 8 and Comparative Example 1 Evaluation of anti-slip properties using a firing jig
  • the ceramic sheets 1 to 8 and comparative ceramic sheet 9 of the setter were placed on the corresponding base plates 1 to 8 and comparative base plate 9, respectively, so that all of the convex parts of the sheets were contained on the entire surface except for the peripheral wall parts of the base plates, thereby forming the firing jigs of Examples 1 to 8 and Comparative Example 1 in which the setter and base plates were combined.
  • the relationship between the convex portion of the setter and the groove portion of the bottom plate is shown in Table 3.
  • the evaluation criteria for the setter's movement start angle when the floor plate was inclined were as follows: AA (best): 60° or more A (good): 40° or more and less than 60° B (acceptable): 20° or more and less than 40° C (unacceptable): Less than 20°
  • the evaluation criteria for the time when the setter started to move when the base plate was vibrated were as follows: AA (best): 50 seconds or more A (good): 30 seconds or more but less than 50 seconds B (passable): 10 seconds or more but less than 30 seconds C (unacceptable): Less than 10 seconds
  • a firing jig consisting of a setter and a base plate on which the setter is placed
  • the setter includes one or more linear protrusions having a substantially uniform cross section in the longitudinal direction on a portion of a surface S adjacent to the base plate
  • the base plate includes one or more grooves having a substantially uniform cross section in the longitudinal direction on a portion of a surface P adjacent to the setter, the protrusions and the grooves are formed so that at least one of the protrusions of the setter is received in at least one of the grooves of the base plate when the setter is placed on the base plate, here,
  • the area within the contour of the proximity surface S of the setter (excluding the area of the region that protrudes from the contour of the sole plate when the proximity surface S is viewed vertically when the setter is placed on the sole plate) is b, When the setter is placed on the base plate, the total projected area of the convex portion accommodated
  • the setter includes a mesh-like ceramic sheet in at least a portion thereof,
  • This mesh-like ceramic sheet includes a first linear portion layer composed of a plurality of first linear portions, each of which is arranged at a given interval and extends in one direction, and a second linear portion layer composed of a plurality of second linear portions, each of which is arranged at a given interval so as to be in contact with and intersect with each of the first linear portions, and is a ceramic sheet sintered body in which the first linear portion layer and the second linear portion layer are integrally formed, A contact surface of the second filamentary portion layer with respect to the first filamentary portion layer forms a proximity surface S of the setter, and a first filamentary portion constituting the first filamentary portion layer forms a convex portion of the setter.
  • the firing jig according to any one of the above items [1] to [8].
  • HL An opening portion of the bottom plate 7: A main body (base) of the setter 7S: surface of the setter adjacent to the sole plate 8: protruding part of the setter 9: main body (base) of the sole plate 9P: surface of the base plate adjacent to the setter 10: grooved portion of the base plate a1: projected area of the convex portion on the left side in FIG. 3 a2: projected area of the convex portion on the right side in FIG.

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Abstract

The present invention addresses the problem of providing a firing jig that can effectively prevent sliding of a setter. This problem is solved by a firing jig comprising a setter and a bottom plate, wherein: the setter includes, on part of a proximity surface S that comes into proximity with the bottom plate, one or more linear protrusions having a substantially uniform cross-section in the lengthwise direction; the bottom plate includes, on part of a proximity surface P that comes into proximity with the setter, one or more linear grooves having a substantially uniform cross-section in the lengthwise direction; the protrusions and linear grooves are formed such that, when the setter is placed on the bottom plate, at least one of the protrusions is accommodated in at least one of the linear grooves; and 0.5≤(a/b)*100≤90 (expression A) is satisfied, where b is the in-perimeter area of the proximity surface S (excluding the area of a region that extends past the perimeter of the bottom plate in a view perpendicular to the proximity surface S when the setter is placed on the bottom plate), and a is the total of the projected area of the protrusions accommodated in the linear grooves during placement (the maximum cross-sectional area of said protrusions in a plane parallel to the proximity surface S of the setter).

Description

セッターと敷板とからなる焼成治具A firing jig consisting of a setter and a base plate
 本発明は、セッターと敷板とからなる焼成治具に関する。本発明は、より具体的には、セッターとこのセッターが戴置される敷板とからなり、セッターの摺動が効果的に防止され得る焼成治具に関する。 The present invention relates to a baking jig consisting of a setter and a base plate. More specifically, the present invention relates to a baking jig consisting of a setter and a base plate on which the setter is placed, which can effectively prevent the setter from sliding.
 セラミックス製の電子部品やガラスを焼成するときには、被焼成物を棚板等とも称されるセラミックスシートのセッター上に載置して焼成を行うことが一般的である。このようなセッターを用いる焼成プロセスでは、多数の被焼成物を同時に焼成する高い生産効率が要求される。そのため、焼成用の敷板または焼成用ラック等と称される部材上にセッターが戴置された焼成治具を用い、複数のセッターを所定間隔で積層させた多段組みの形態で焼成が行われている。 When firing ceramic electronic components or glass, it is common to place the objects to be fired on a ceramic sheet setter, also known as a shelf, and then fire the objects. Firing processes using such setters require high production efficiency to fire a large number of objects to be fired simultaneously. For this reason, firing is carried out in a multi-tiered configuration in which multiple setters are stacked at specified intervals using a firing jig in which a setter is placed on a member known as a firing base or firing rack.
 セラミックス製セッターに関する従来の技術としては、例えば、窒化アルミニウムを主成分とするセラミックスより作られ、且つ表裏を貫通する多数の穴を持つ多孔板からなる加熱成型加工用セッターや、被焼成物を載置する表面側および裏面側に少なくとも凹凸形状が付与されているとともに、開口部が形成されているセラミック焼成用窯道具板などが知られている。また、被焼成物の急速な加熱および冷却を行うときにセッターに割れ等が発生することを防止するための技術として、セラミックス製の複数の第1線条部と、これと交差するセラミックス製の複数の第2線条部とを有するセラミックス格子体であって、第1線条部と第2線条部とが特定の接触形態を有するものが開示されている(一例として特許文献1参照)。 Conventional ceramic setters include, for example, a setter for hot forming processing made of ceramics whose main component is aluminum nitride and consisting of a porous plate with many holes penetrating from the front to the back, and a ceramic firing kiln tool plate in which at least the front and back sides on which the fired object is placed are given an uneven shape and openings are formed. Also, as a technology for preventing cracks from occurring in the setter when the fired object is rapidly heated and cooled, a ceramic lattice body has been disclosed that has a plurality of first ceramic striated portions and a plurality of second ceramic striated portions that intersect with the first ceramic striated portions, and the first and second striated portions have a specific contact form (see Patent Document 1 for an example).
 一方、敷板等と称される焼成治具として、例えば、中央側に中空部を有する枠体と、枠体の中空部に架け渡され、中空部で互いに交差する複数の架橋部とを備え、枠体と架橋部とが一体成型されることを特徴とする焼成治具が開示されている。この焼成治具によれば、セラミックス製品の焼成による製造の生産性が向上することが報告されている。
 また、他の敷板等と称される焼成治具として、特許文献2には、被焼成物が積載される平板状セッターを配置するように構成された焼成用ラックであって、表面に平板状セッターが配置されるとともに開口部を有する枠体と、枠体の中心を通過して枠体間を伸びる柱部と、枠体と柱部によって囲まれた複数の囲繞部と、囲繞部の中心から枠体または柱部に向けて伸びる複数の副柱部とを備える焼成用ラックが開示されている。この焼成用ラックによれば、積載する平板状セッターの面内温度分布のムラを低減し得ることが報告されている。
On the other hand, as a firing jig called a base plate or the like, for example, a firing jig has been disclosed that is characterized by having a frame body having a hollow part in the center and a plurality of bridge parts that span the hollow part of the frame body and cross each other at the hollow part, and the frame body and the bridge parts are integrally molded. It has been reported that this firing jig improves the productivity of manufacturing ceramic products by firing.
As another firing tool called a base plate, Patent Document 2 discloses a firing rack configured to place a flat setter on which the object to be fired is loaded, the firing rack comprising a frame having an opening on the surface of which the flat setter is placed, a column extending between the frames passing through the center of the frame, a plurality of surrounding parts surrounded by the frame and the column, and a plurality of sub-columns extending from the center of the surrounding parts toward the frame or the column. It has been reported that this firing rack can reduce unevenness in the in-plane temperature distribution of the loaded flat setter.
特開2018-193274号公報JP 2018-193274 A 国際公開2021/033375号International Publication No. 2021/033375
 このようなセラミックス製セッターと敷板(焼成用ラック)とは、図1に例示するように、焼成の際に、各々の敷板の上にセッターを載せ、さらに各々のセッターの上に被焼成物が配された状態で多段組みとして積層されることが多い。図1において、Aはセッターであり、Bは多段積みで積層された敷板であり、Cは被焼成物であり、各々の敷板上にセッターが戴置され、その上に被焼成物が配されることによって、多段積みの焼成治具であるMが焼成プロセスに供される。多段積みとして積層されたセラミックス製セッターと敷板との組み合わせを、その多段積みの状態のまま保管し、さらには搬送することを要する場合もある。そのような積層操作の際や、多段積みの状態のまま搬送する際に、僅かな斜度や振動(すなわち水平方向や上下方向の動作)によりセッターが敷板上で摺動すると、その上に配された被焼成物の安定性も維持されず、被焼成物の変形や破損、焼成の不具合、電子部品等の微細な被焼成物のセッターからの落下などにつながる恐れがある。そのため、セラミックス製セッターと敷板との組み合わせの積層操作時や、それらの多段積み状態での搬送時において、セッターが敷板上で容易に摺動しない良好なハンドリング性が求められている。しかし、そのような摺動を十分に防止し得る技術はこれまで開発されていなかった。 As shown in Figure 1, such ceramic setters and base plates (firing racks) are often stacked in multiple tiers during firing, with a setter placed on each base plate and an object to be fired placed on each setter. In Figure 1, A is a setter, B is the base plates stacked in multiple tiers, and C is the object to be fired; a setter is placed on each base plate and an object to be fired is placed on top of it, and thus M, a multi-tiered firing jig, is subjected to the firing process. There are also cases where the combination of ceramic setters and base plates stacked in multiple tiers needs to be stored in that multi-tiered state, and even transported. If the setter slides on the base plate due to slight tilt or vibration (i.e., horizontal or vertical movement) during such stacking operations or when transporting the stacked products, the stability of the fired objects placed on it will not be maintained, which may lead to deformation or damage to the fired objects, firing defects, and the falling of fine fired objects such as electronic components from the setter. Therefore, when stacking the combination of ceramic setters and base plates or transporting them in a multi-layered state, there is a demand for good handling properties that prevent the setter from sliding easily on the base plate. However, no technology capable of sufficiently preventing such sliding has been developed until now.
 従って、本発明が解決しようとする課題は、セラミックス製セッターと敷板との組み合わせからなる焼成治具であって、それらの積層操作時や、多段積み状態での搬送時において、僅かな斜度や振動(水平方向や上下方向の動作)によりセッターが敷板上で容易に摺動しないような良好なハンドリング性を有する焼成治具を提供することである。 The problem that this invention aims to solve is to provide a firing jig consisting of a combination of a ceramic setter and a base plate, which has good handling properties so that the setter does not slide easily on the base plate due to slight tilt or vibration (horizontal or vertical movement) during stacking operations or when transporting in a multi-layered state.
 本発明者らは、鋭意研究した結果、セッターと、このセッターが戴置される敷板とからなる焼成治具において、敷板に対するセッターの近接面の一部に1つまたは複数の線条をなす凸部を設けると共に、セッターに対する敷板の近接面の一部に1つまたは複数の条溝部を設け、セッターを敷板に戴置する際に、セッターに設けられた凸部の少なくとも1つが敷板に設けられた条溝部の少なくとも1つに収容されるようにしたうえで、敷板に対するセッターの近接面の輪郭内の面積と、敷板の条溝部に収容されるセッターの凸部の投影面積の合計との比率が所定の範囲内になるように設計することによって、凸部が条溝部により大きな程度で収容・係合されることになり、それによってセッターの敷板上での移動が効果的に制限され、セッターの敷板上での摺動を十分に防止することが可能になり、ひいてはセラミックス製品の焼成治具としてのハンドリング性が大幅に向上することを見出し、本発明に係る焼成治具を完成させた。 After extensive research, the inventors have discovered that in a firing jig consisting of a setter and a base plate on which the setter is placed, one or more linear convex portions are provided on a portion of the surface of the setter adjacent to the base plate, and one or more groove portions are provided on a portion of the surface of the base plate adjacent to the setter, so that when the setter is placed on the base plate, at least one of the convex portions on the setter is accommodated in at least one of the groove portions on the base plate, and that by designing the ratio of the area within the outline of the surface of the setter adjacent to the base plate to the sum of the projected areas of the convex portions of the setter accommodated in the groove portions of the base plate to be within a predetermined range, the convex portions are accommodated and engaged in the groove portions to a greater extent, thereby effectively restricting the movement of the setter on the base plate and making it possible to sufficiently prevent the setter from sliding on the base plate, and ultimately significantly improving the handleability of the firing jig for ceramic products, and have completed the firing jig of the present invention.
 従って、本発明の典型的な一態様は、以下のとおりである:
 セッターと、このセッターが戴置される敷板とからなる焼成治具であって、
 前記セッターは、前記敷板に対する近接面Sの一部に、長手方向に略均一な断面を備える1つまたは複数の線条をなす凸部を含み、
 前記敷板は、前記セッターに対する近接面Pの一部に、長手方向に略均一な断面を備える1つまたは複数の条溝部を含み、
 前記セッターが前記敷板に戴置されるとき、前記セッターの凸部の少なくとも1つが前記敷板の条溝部の少なくとも1つに収容されるように、前記凸部および前記条溝部が形成されており、
 ここで、
 前記セッターの近接面Sの輪郭内面積(ただし、前記セッターの前記敷板への戴置の際に、前記近接面Sを垂直視するとき、敷板の輪郭からはみ出る領域の面積を除く)をbとし、
 前記セッターが前記敷板に戴置されるときに、前記条溝部に収容される前記凸部の投影面積(ただし、ここでの投影面積は、前記セッターの近接面Sに平行な面における当該凸部の最大断面積を指す)の合計をaとするとき、
 0.5≦(a/b)*100≦90(式A)の関係を満たす、
 焼成治具。
Thus, one exemplary embodiment of the present invention is as follows:
A firing jig consisting of a setter and a base plate on which the setter is placed,
The setter includes one or more linear protrusions having a substantially uniform cross section in the longitudinal direction on a portion of a surface S adjacent to the base plate,
The base plate includes one or more grooves having a substantially uniform cross section in the longitudinal direction on a portion of a surface P adjacent to the setter,
the protrusions and the grooves are formed so that at least one of the protrusions of the setter is received in at least one of the grooves of the base plate when the setter is placed on the base plate,
here,
The area within the contour of the proximity surface S of the setter (excluding the area of the region that protrudes from the contour of the sole plate when the proximity surface S is viewed vertically when the setter is placed on the sole plate) is b,
When the setter is placed on the base plate, the total projected area of the convex portion accommodated in the groove portion (wherein the projected area here refers to the maximum cross-sectional area of the convex portion in a plane parallel to the adjacent surface S of the setter) is a,
The relationship of 0.5≦(a/b)*100≦90 (Formula A) is satisfied.
Firing fixture.
 なお、本願においてセッターの凸部が敷板の条溝部に「収容」されることとは、敷板のセッターに対する近接面Pを条溝部の長手方向に垂直な断面にて水平視するとき、条溝部の最上面(近接面Pに相当する仮想面)より下方にセッターの凸部の少なくとも一部が配置されている状態を指すものとする。 In this application, the convex portion of the setter being "housed" in the groove portion of the base plate refers to a state in which, when the proximity surface P of the base plate relative to the setter is viewed horizontally in a cross section perpendicular to the longitudinal direction of the groove portion, at least a portion of the convex portion of the setter is positioned below the uppermost surface of the groove portion (an imaginary surface corresponding to the proximity surface P).
 本発明に係るセッターとそれが戴置される敷板とからなる焼成治具によれば、敷板に対するセッターの近接面の輪郭内の面積と、敷板の条溝部に収容されるセッターの凸部の投影面積の合計との比率を所定の範囲内になるように調整することによって、凸部が条溝部により大きな程度で収容・係合されることになり、それによってセッターの敷板上での移動が効果的に制限され、セッターの敷板上での摺動を十分に防止することが可能になり、ひいてはセラミックス製品の焼成治具としてのハンドリング性が大幅に向上するという利点が得られる。 In accordance with the present invention, a firing jig consisting of a setter and a base plate on which it is placed can be adjusted so that the ratio of the area within the contour of the adjacent surface of the setter relative to the base plate and the sum of the projected areas of the convex portions of the setter housed in the grooves of the base plate is within a specified range, allowing the convex portions to be housed and engaged in the grooves to a greater extent, thereby effectively restricting the movement of the setter on the base plate and making it possible to sufficiently prevent the setter from sliding on the base plate, thus providing the advantage of greatly improving the handleability of the firing jig for ceramic products.
図1は、セラミックス製セッターと敷板(焼成用ラック)との多段組みによる公知の積層形態を例示する図である。FIG. 1 is a diagram illustrating a known layered configuration in which ceramic setters and base plates (firing racks) are stacked in multiple stages. 図2は、本発明の一実施形態に係る焼成治具のセッターと敷板との組み合わせを示す図である。FIG. 2 is a diagram showing a combination of a setter and a base plate of a firing jig according to one embodiment of the present invention. 図3は、本発明の一実施形態に係る焼成治具のセッターと敷板との組み合わせにおいて、セッターの敷板に対する近接面Sの輪郭内面積b、および、セッターが敷板に戴置されるときに敷板の条溝部に収容される凸部の投影面積の合計aの関係を例説する図である。Figure 3 is a diagram illustrating the relationship between the contour area b of the proximity surface S of the setter relative to the base plate and the total projected area a of the convex parts accommodated in the groove portion of the base plate when the setter is placed on the base plate in a combination of a setter and base plate of a firing jig according to one embodiment of the present invention. 図4は、本発明の一実施形態に係る焼成治具のセッターと敷板との組み合わせにおいて、セッターの凸部の最大幅員Wcと、敷板の条溝部の最大幅員Wpとの関係を例示する図面である。FIG. 4 is a diagram illustrating the relationship between the maximum width Wc of the convex portion of the setter and the maximum width Wp of the groove portion of the base plate in a combination of a setter and base plate of a firing jig according to one embodiment of the present invention. 図5は、本発明の一実施形態に係る焼成治具のセッターと敷板との組み合わせにおいて、敷板の条溝部の平均深さDg・avと、条溝部間の垂直最短距離Igとの関係を例示する図面である。FIG. 5 is a diagram illustrating the relationship between the average depth Dg·av of the grooves of the base plate and the vertical minimum distance Ig between the grooves in a combination of a setter and base plate of a firing jig according to one embodiment of the present invention. 図6は、本発明の一実施形態に係る焼成治具のセッターと敷板との組み合わせにおいて、セッターの凸部の最大幅員Wcと、その長手方向の両端部間の長さLcとの関係(アスペクト比)を例示する図面である。FIG. 6 is a diagram illustrating the relationship (aspect ratio) between the maximum width Wc of the convex portion of the setter and the length Lc between both ends in the longitudinal direction in a combination of a setter and a base plate of a firing jig according to one embodiment of the present invention. 図7は、本発明の一実施形態に係る焼成治具のセッターと敷板との組み合わせにおいて、セッターの凸部の最大高さHcと、この凸部が収容される敷板の条溝部の深さDgとの関係を例示する図面である。FIG. 7 is a diagram illustrating the relationship between the maximum height Hc of the convex portion of the setter and the depth Dg of the groove portion of the base plate in which the convex portion is accommodated, in a combination of a setter and base plate of a firing jig according to one embodiment of the present invention. 図8は、本発明の一実施形態に係る焼成治具のセッターと敷板との組み合わせにおいて、セッターの凸部の最大高さHcと、この凸部の最大幅員Wcとの関係を例示する図面である。FIG. 8 is a diagram illustrating the relationship between the maximum height Hc of the convex portion of the setter and the maximum width Wc of the convex portion in a combination of the setter and the base plate of the firing jig according to one embodiment of the present invention. 図9は、本発明の一実施形態による焼成治具におけるセッターのメッシュ状部位を例示する図である。FIG. 9 is a diagram illustrating a mesh-shaped portion of a setter in a baking jig according to an embodiment of the present invention. 図10は、実施例におけるV字型の条溝部が設けられた敷板と凸部が設けられたセッターとの関係の概略を例示する図面である。FIG. 10 is a diagram illustrating an outline of the relationship between a base plate provided with a V-shaped groove and a setter provided with a protrusion in the embodiment.
 本発明に係る焼成治具を構成するセッターは、同じく焼成治具を構成する敷板に対する近接面Sの一部に、長手方向に略均一な断面を備える1つまたは複数の線条をなす凸部を含む。他方で、本発明に係る焼成治具を構成する敷板は、同じく焼成治具を構成するセッターに対する近接面Pの一部に、長手方向に略均一な断面を備える1つまたは複数の条溝部を含む。この焼成治具において、セッターが敷板に戴置されるとき、セッターの敷板上での摺動を防止するため、セッターの凸部の少なくとも1つが敷板の条溝部の少なくとも1つに収容されるように、凸部および条溝部が形成されている必要がある。 The setter constituting the firing jig of the present invention includes, on a portion of the adjacent surface S to the base plate which also constitutes the firing jig, one or more linear convex portions with a generally uniform cross section in the longitudinal direction. On the other hand, the base plate constituting the firing jig of the present invention includes, on a portion of the adjacent surface P to the setter which also constitutes the firing jig, one or more groove portions with a generally uniform cross section in the longitudinal direction. In this firing jig, when the setter is placed on the base plate, in order to prevent the setter from sliding on the base plate, the convex portions and the groove portions must be formed so that at least one of the convex portions of the setter is accommodated in at least one of the groove portions of the base plate.
 図2に、本発明に係る焼成治具のセッターと敷板との組み合わせの一実施形態を示す。本発明による焼成治具のセッターおよび敷板のいずれも図2の形態に限定されるわけではなく、これは単なる一例である。
 図2において、1は焼成治具(組み合わせ)、2はセッター(例示としてのメッシュ状セラミックスシートのセッター)、2Sはセッター2の敷板に対する近接面(本図では紙面裏側)、3は敷板、3Pは敷板3のセッターに対する近接面、4は敷板の基材部、5は周壁部(リブ:任意選択で設けられる)、6はセッターの敷板に対する近接面2Sに設けられた凸部(紙面裏側のため図示せず)の少なくとも一部に対応する敷板の条溝部、HLは開口部(任意選択で設けられる)を示す。
An embodiment of a combination of a setter and a base plate of a baking jig according to the present invention is shown in Fig. 2. Neither the setter nor the base plate of the baking jig according to the present invention is limited to the form shown in Fig. 2, which is merely an example.
In Figure 2, 1 indicates a firing jig (combination), 2 indicates a setter (a setter of a mesh-like ceramic sheet as an example), 2S indicates the surface of the setter 2 adjacent to the base plate (the back side of the paper in this figure), 3 indicates the base plate, 3P indicates the surface of the base plate 3 adjacent to the setter, 4 indicates a base portion of the base plate, 5 indicates a peripheral wall portion (rib: provided optionally), 6 indicates a groove portion of the base plate corresponding to at least a part of a protrusion portion (not shown as it is on the back side of the paper) provided on the surface 2S of the setter adjacent to the base plate, and HL indicates an opening (provided optionally).
 本例示における焼成治具1の一部材であるセッター2は、略一定間隔で一方向に延伸する第1線条部で構成された第1線条部層、および略一定間隔でこれと略直行して一方向に延伸する第2線条部で構成された第2線条部層からなるメッシュ状部位で全体的に形成されている、メッシュ状セラミックスシートのセッターである。焼成治具1の他方の部材である敷板3は、略矩形の板状体である基材部4と、その周囲全体に直立して形成された周壁部5(リブ)とを備えている。また図示していないが、敷板3の基材部4は、略矩形の四隅の各々に多段積み用の脚部を有していてよいし、そのような脚部を装着可能なように構成されていてもよい。周壁部5は、周囲全体を形成する構成として例示されているが、周囲の一部であってもよい。敷板3のセッターに対する近接面3Pは、セッター2の敷板に対する近接面2Sの輪郭(周縁)の全体が収容され得る平面をなすと同時に、周壁部5は、セッター2が敷板3の近接面3Pに戴置される際にセッター2の周縁部の全体が周壁部まで所定の間隔を有するように形成されている。本図で例示されているようにセッター2がメッシュ状セラミックスシートのセッターである場合、第2線条部層の第1線条部層に対する接面がセッターの近接面2S(紙面裏側)をなし、第1線条部層を構成する第1線条部がセッターの凸部をなす。この場合、セッター2の敷板に対する近接面2Sに形成された凸部は複数存在する。敷板3のセッターに対する近接面3Pには複数の条溝部6が設けられており、これらの条溝部6の位置はセッターの複数の凸部(第1線条部)の少なくとも一部の位置に対応しており、当該箇所において凸部が条溝部6に収容され得る。このように、セッター2が敷板3に戴置されるとき、セッター2の凸部の少なくとも1つが敷板3の条溝部の少なくとも1つに収容されるように凸部および条溝部が形成されることによって、摺動に対する防止・抑制性能が付与される。また、このような焼成治具1の多段積みでは、複数の脚部の間において、また周壁部5が周囲の一部に形成されている場合はそれらの間において、またさらには開口部HLが敷板の一部に形成されている場合はそこにおいて、通気性が確保され、効率的な焼成プロセスが実施され得る。 The setter 2, which is one of the components of the firing jig 1 in this example, is a mesh ceramic sheet setter formed entirely of a mesh-like portion consisting of a first striated portion layer made up of first striated portions extending in one direction at approximately constant intervals, and a second striated portion layer made up of second striated portions extending in one direction at approximately constant intervals and approximately perpendicular to the first striated portion. The base plate 3, which is the other component of the firing jig 1, has a base portion 4 which is a substantially rectangular plate-like body, and a peripheral wall portion 5 (rib) formed upright around the entire periphery. Although not shown, the base portion 4 of the base plate 3 may have legs for stacking at each of the four corners of the substantially rectangular shape, or may be configured so that such legs can be attached. The peripheral wall portion 5 is illustrated as forming the entire periphery, but it may also be a part of the periphery. The setter-facing surface 3P of the sole plate 3 forms a plane that can accommodate the entire contour (periphery) of the setter 2's proximity surface 2S, and the peripheral wall 5 is formed so that when the setter 2 is placed on the proximity surface 3P of the sole plate 3, the entire peripheral portion of the setter 2 has a predetermined distance to the peripheral wall. When the setter 2 is a mesh-shaped ceramic sheet setter as illustrated in this figure, the contact surface of the second striated portion layer with the first striated portion layer forms the proximity surface 2S (back side of the paper) of the setter, and the first striated portion constituting the first striated portion layer forms the convex portion of the setter. In this case, there are multiple convex portions formed on the setter 2's proximity surface 2S. The setter 2's proximity surface 3P of the sole plate 3 is provided with multiple groove portions 6, and the positions of these groove portions 6 correspond to the positions of at least some of the multiple convex portions (first striated portions) of the setter, and the convex portions can be accommodated in the groove portions 6 at those locations. In this way, when the setter 2 is placed on the base plate 3, the convex parts and the groove parts are formed so that at least one of the convex parts of the setter 2 is accommodated in at least one of the groove parts of the base plate 3, thereby providing the ability to prevent and suppress sliding. In addition, when the firing jig 1 is stacked in multiple layers, ventilation is ensured between the multiple legs, between the peripheral wall parts 5 if they are formed in part of the periphery, and also in the openings HL if they are formed in part of the base plate, allowing for an efficient firing process.
 図3は、本発明の一実施形態に係る焼成治具のセッターと敷板との組み合わせにつき、セッターを敷板に戴置した際のセッターの複数の凸部の長手方向に垂直な断面を例示している。
 図3において、7はセッターの本体(基部)、7Sはセッターの敷板に対する近接面、8は近接面7Sの一部に形成された長手方向に略均一かつ略円形の断面を備える複数の線条をなす凸部、9は敷板の本体(基部)、9Pは敷板のセッターに対する近接面、10は近接面9Pの一部に形成された長手方向に略均一かつ略円形の断面を備える複数の条溝部を示している。
FIG. 3 illustrates a cross section perpendicular to the longitudinal direction of a plurality of protrusions of a setter when the setter is placed on a base plate in a combination of the setter and base plate of a firing jig according to one embodiment of the present invention.
In Figure 3, 7 indicates the main body (base) of the setter, 7S indicates the surface of the setter adjacent to the base plate, 8 indicates a plurality of linear convex portions formed on part of the adjacent surface 7S and having a substantially uniform and substantially circular cross-section in the longitudinal direction, 9 indicates the main body (base) of the base plate, 9P indicates the surface of the base plate adjacent to the setter, and 10 indicates a plurality of groove portions formed on part of the adjacent surface 9P and having a substantially uniform and substantially circular cross-section in the longitudinal direction.
 図3において、図解の容易のため、凸部8および条溝部10がそれぞれ2つ形成されている場合(セッターと敷板との組み合わせからなる焼成治具の一部のみの概略)が示されている。しかし、凸部および条溝部の個数は、それぞれ1つ以上であればよく、その個数は特に限定されない。凸部の個数は、好ましくは2個以上であり、さらに好ましくは3個以上、5個以上、10個以上、20個以上、または30個以上であってよい。また同様に、条溝部の個数は、好ましくは2個以上であり、さらに好ましくは3個以上、5個以上、10個以上、20個以上、または30個以上であってよい。凸部および条溝部の個数は、それぞれ、製造効率の観点から100個以下であってよい。図3において凸部の断面形状は略円形として例示されているが、これに限定されない。凸部の断面形状は、例えば、略半円形、略三角形、略矩形、略台形であってもよい。凸部の形成を容易にする観点から、凸部の断面形状は略円形であることが好ましい。セッターがメッシュ状セラミックスシートである場合、凸部の断面形状は略円形である。また、図3において条溝部の断面形状は略半円形として例示されているが、これに限定されない。条溝部の断面形状は、例えば、略V字形(略三角形)、略矩形、略台形であってもよい。凸部および条溝部のこれらの断面形状にかかわらず、本明細書にて説明される要件を満たす限りは所望の効果が奏され得る。製造効率の観点からは、凸部の断面形状は略円形(特にメッシュ状セラミックスシートを使用する場合)であってよく、条溝部の断面形状は略V字形であってよい。 In FIG. 3, for ease of illustration, the case where two convex portions 8 and two groove portions 10 are formed (outline of only a part of the firing jig consisting of a combination of a setter and a base plate) is shown. However, the number of convex portions and groove portions may be one or more, and the number is not particularly limited. The number of convex portions is preferably two or more, and more preferably three or more, five or more, ten or more, twenty or more, or thirty or more. Similarly, the number of groove portions is preferably two or more, and more preferably three or more, five or more, ten or more, twenty or more, or thirty or more. The number of convex portions and groove portions may each be 100 or less from the viewpoint of manufacturing efficiency. In FIG. 3, the cross-sectional shape of the convex portion is illustrated as being approximately circular, but is not limited thereto. The cross-sectional shape of the convex portion may be, for example, approximately semicircular, approximately triangular, approximately rectangular, or approximately trapezoidal. From the viewpoint of facilitating the formation of the convex portion, it is preferable that the cross-sectional shape of the convex portion is approximately circular. When the setter is a mesh-like ceramic sheet, the cross-sectional shape of the convex portion is approximately circular. In addition, the cross-sectional shape of the groove portion is exemplified as approximately semicircular in FIG. 3, but is not limited thereto. The cross-sectional shape of the groove portion may be, for example, approximately V-shaped (approximately triangular), approximately rectangular, or approximately trapezoidal. Regardless of these cross-sectional shapes of the convex portion and the groove portion, the desired effect can be achieved as long as the requirements described in this specification are satisfied. From the viewpoint of manufacturing efficiency, the cross-sectional shape of the convex portion may be approximately circular (especially when a mesh-like ceramic sheet is used), and the cross-sectional shape of the groove portion may be approximately V-shaped.
 図3においては、2つの凸部8が略平行に形成されており、かつ2つの条溝部10が略平行に形成されており、セッター7が敷板9に戴置された際に、2つの凸部8の両方がそれらに対応する位置に配された2つの条溝部10の各々に収容された状態となっている。このように、セッターの凸部および敷板の条溝部がそれぞれ略平行に2つまたは3つ以上形成されており、セッターの敷板への戴置の際、凸部の過半数、好ましくは凸部の70%以上、さらに好ましくは凸部の実質的に全てが敷板の条溝部に収容されるように構成されている。このような構成によって、セッターの敷板上での摺動をより効果的に防止し、ひいてはセラミックス製品の焼成治具としてのハンドリング性をさらに大幅に向上させることができる。 In FIG. 3, two convex portions 8 are formed approximately parallel to each other, and two groove portions 10 are formed approximately parallel to each other, and when the setter 7 is placed on the base plate 9, both of the two convex portions 8 are accommodated in each of the two groove portions 10 arranged in the corresponding positions. In this way, two or more convex portions of the setter and groove portions of the base plate are formed approximately parallel to each other, and when the setter is placed on the base plate, the majority of the convex portions, preferably 70% or more of the convex portions, and more preferably substantially all of the convex portions are accommodated in the groove portions of the base plate. This configuration more effectively prevents the setter from sliding on the base plate, and thus significantly improves the handleability of the setter as a firing jig for ceramic products.
 図3においては、2つの凸部8が略平行に形成され、かつ2つの条溝部10が略平行に形成された例が示されているが、他の一実施形態において、セッターの凸部が3つ以上の場合にはこれらの凸部が略等間隔に形成され、および/または、敷板の条溝部が3つ以上の場合にはこれらの条溝部が略等間隔に形成されるように構成してよい。このような構成によって、セッターの凸部が敷板の条溝部に好首尾に収容される確率がさらに上がり、それによりセッターの敷板上での摺動防止性をより一層高めることができる。 In FIG. 3, an example is shown in which two convex portions 8 are formed approximately parallel to each other and two groove portions 10 are formed approximately parallel to each other, but in another embodiment, when the setter has three or more convex portions, these convex portions may be formed approximately equally spaced apart, and/or when the base plate has three or more groove portions, these groove portions may be formed approximately equally spaced apart. This configuration further increases the probability that the convex portions of the setter will be successfully accommodated in the groove portions of the base plate, thereby further improving the anti-sliding properties of the setter on the base plate.
 図3において、符号bは、セッター7の敷板9に対する近接面7Sの輪郭内の面積(ただし、セッター7の敷板9への戴置の際に、近接面7Sを垂直視するとき、敷板9の輪郭からはみ出る領域の面積を除くものとする)を示す。また、図3において、符号a1は、セッター7が敷板9に戴置されるときに、図中、左側の条溝部10に収容される凸部8の投影面積(セッター7の近接面7Sに平行な面における当該凸部の最大断面積)を示す。符号a2は、同様にセッター7が敷板9に戴置されるときに、図中、右側の条溝部10に収容される凸部8の投影面積(セッター7の近接面7Sに平行な面における当該凸部の最大断面積)を示す。このとき符号aは、凸部8の投影面積a1およびa2の合計である。図3では、図解の容易のための例示として凸部8および条溝部10がそれぞれ2つのみ描かれているが、条溝部10に収容される凸部8が3つ以上存在する場合は、それらの投影面積axの合計(Σax)がaとなる。 In Figure 3, the symbol b indicates the area within the contour of the proximity surface 7S of the setter 7 relative to the base plate 9 (excluding the area of the region that extends beyond the contour of the base plate 9 when the proximity surface 7S is viewed vertically when the setter 7 is placed on the base plate 9). Also in Figure 3, the symbol a1 indicates the projected area of the convex portion 8 accommodated in the groove portion 10 on the left side of the figure when the setter 7 is placed on the base plate 9 (the maximum cross-sectional area of the convex portion in a plane parallel to the proximity surface 7S of the setter 7). The symbol a2 similarly indicates the projected area of the convex portion 8 accommodated in the groove portion 10 on the right side of the figure when the setter 7 is placed on the base plate 9 (the maximum cross-sectional area of the convex portion in a plane parallel to the proximity surface 7S of the setter 7). In this case, the symbol a is the sum of the projected areas a1 and a2 of the convex portions 8. In FIG. 3, only two protrusions 8 and two grooves 10 are shown as an example for ease of illustration, but if there are three or more protrusions 8 housed in the grooves 10, the sum (Σax) of their projected areas ax is a.
 ここで、凸部8の投影面積の合計aとセッター7の近接面7Sの輪郭内面積bとは以下の式Aの関係が満たされる。
 0.5≦(a/b)*100≦90(式A)
 この式Aの関係が満たされる本発明の焼成治具によれば、セッターの凸部が敷板の条溝部にしっかりと安定して収容・係合され、それによってセッターの敷板上での移動が効果的に制限され、セッターの敷板上での摺動を十分に防止することができると共に、凸部の配置設計の容易性も担保され得る。また、これらの効果に伴ってセラミックス製品の焼成治具としてのハンドリング性を大幅に向上させることができる。
Here, the relationship between the total projected area a of the convex portion 8 and the contour inner area b of the adjacent surface 7S of the setter 7 satisfies the following formula A.
0.5≦(a / b) * 100≦90 (Formula A)
According to the firing jig of the present invention, which satisfies the relationship of formula A, the convex part of the setter is firmly and stably accommodated and engaged in the groove part of the base plate, which effectively limits the movement of the setter on the base plate, sufficiently prevents the setter from sliding on the base plate, and ensures ease of designing the layout of the convex part. These effects also greatly improve the handleability of the firing jig for ceramic products.
 式Aの関係が満たされる範囲内の一実施形態において、上記観点から、1≦(a/b)*100≦90であることが好ましく、5≦(a/b)*100≦90であることがさらに好ましく、10≦(a/b)*100≦90であることがさらにより好ましく、20≦(a/b)*100≦90であることが一層好ましく、30≦(a/b)*100≦90であることがより一層好ましく、40≦(a/b)*100≦90であることがさらにより一層好ましく、50≦(a/b)*100≦90であることがなお一層好ましく、60≦(a/b)*100≦90であることがさらにより一層好ましく、70≦(a/b)*100≦90であることが最も好ましい。
 式Aの関係が満たされる範囲内の別の実施形態において、上記観点から、1≦(a/b)*100≦85であることが好ましく、5≦(a/b)*100≦85であることがさらに好ましく、10≦(a/b)*100≦85であることがさらにより好ましく、20≦(a/b)*100≦85であることが一層好ましく、30≦(a/b)*100≦85であることがより一層好ましく、40≦(a/b)*100≦85であることがさらにより一層好ましく、50≦(a/b)*100≦85であることがなお一層好ましく、60≦(a/b)*100≦85であることがさらにより一層好ましく、70≦(a/b)*100≦85であることが最も好ましい。
 式Aの関係が満たされる範囲内のさらに別の実施形態において、上記観点から、1≦(a/b)*100≦80であることが好ましく、5≦(a/b)*100≦80であることがさらに好ましく、10≦(a/b)*100≦80であることがさらにより好ましく、20≦(a/b)*100≦80であることが一層好ましく、30≦(a/b)*100≦80であることがより一層好ましく、40≦(a/b)*100≦80であることがさらにより一層好ましく、50≦(a/b)*100≦80であることがなお一層好ましく、60≦(a/b)*100≦80であることがさらにより一層好ましく、70≦(a/b)*100≦80であることが最も好ましい。
In one embodiment within the range in which the relationship of formula A is satisfied, from the above viewpoint, it is preferable that 1≦(a/b)*100≦90, it is even more preferable that 5≦(a/b)*100≦90, it is even more preferable that 10≦(a/b)*100≦90, it is even more preferable that 20≦(a/b)*100≦90, it is even more preferable that 30≦(a/b)*100≦90, it is even more preferable that 40≦(a/b)*100≦90, it is even more preferable that 50≦(a/b)*100≦90, it is even more preferable that 60≦(a/b)*100≦90, and it is most preferable that 70≦(a/b)*100≦90.
In another embodiment within the range in which the relationship of formula A is satisfied, from the above viewpoint, it is preferable that 1≦(a/b)*100≦85, it is even more preferable that 5≦(a/b)*100≦85, it is even more preferable that 10≦(a/b)*100≦85, it is even more preferable that 20≦(a/b)*100≦85, it is even more preferable that 30≦(a/b)*100≦85, it is even more preferable that 40≦(a/b)*100≦85, it is even more preferable that 50≦(a/b)*100≦85, it is even more preferable that 60≦(a/b)*100≦85, and it is most preferable that 70≦(a/b)*100≦85.
In yet another embodiment within the range in which the relationship of formula A is satisfied, from the above viewpoint, it is preferable that 1≦(a/b)*100≦80, it is even more preferable that 5≦(a/b)*100≦80, it is even more preferable that 10≦(a/b)*100≦80, it is even more preferable that 20≦(a/b)*100≦80, it is even more preferable that 30≦(a/b)*100≦80, it is even more preferable that 40≦(a/b)*100≦80, it is even more preferable that 50≦(a/b)*100≦80, it is even more preferable that 60≦(a/b)*100≦80, and it is most preferable that 70≦(a/b)*100≦80.
 図4は、本発明の一実施形態に係る焼成治具のセッターと敷板との組み合わせにつき、セッターを敷板に戴置した際の、セッターの凸部の最大幅員Wcと敷板の条溝部の最大幅員Wpとの関係を例示している。
 図4において、Wcは、セッター7の凸部8の長手方向に垂直な断面の、セッター7の敷板9に対する近接面7Sに平行な方向の最大幅員を示す。また、Wpは、セッター7の敷板9への戴置の際、この凸部8が収容される条溝部10の長手方向に垂直な断面の、敷板9のセッター7に対する近接面9Pに平行な方向の最大幅員を示す。
 図4において、凸部の断面形状は略円形として例示され、条溝部の断面形状は略半円形として例示されているが、図3について説明したのと同様にこれらの形状に限定されるわけではない。
FIG. 4 illustrates the relationship between the maximum width Wc of the convex portion of the setter and the maximum width Wp of the groove portion of the base plate when the setter is placed on the base plate for a combination of a setter and base plate of a firing jig according to one embodiment of the present invention.
4, Wc indicates the maximum width of a cross section perpendicular to the longitudinal direction of the convex portion 8 of the setter 7, in a direction parallel to the adjacent surface 7S of the setter 7 relative to the base plate 9. Also, Wp indicates the maximum width of a cross section perpendicular to the longitudinal direction of the groove portion 10 in which the convex portion 8 is housed, in a direction parallel to the adjacent surface 9P of the base plate 9 relative to the setter 7, when the setter 7 is placed on the base plate 9.
In FIG. 4, the cross-sectional shape of the convex portion is exemplified as being substantially circular, and the cross-sectional shape of the groove portion is exemplified as being substantially semicircular, but as explained with reference to FIG. 3, they are not limited to these shapes.
 ここで、セッター7の凸部8の少なくとも1つの長手方向に垂直な断面の近接面7Sに平行な方向の最大幅員Wcと、セッター7の敷板9への戴置の際、この凸部8が収容される条溝部10の長手方向に垂直な断面の近接面9Pに平行な方向の最大幅員Wpとの割合Wc/Wpは、(0超であって)2以下であることが好ましい。
 この割合Wc/Wpが2以下である本発明の一実施形態に係る焼成治具によれば、セッターの凸部が敷板の条溝部の底部に向かって深く収容・係合され、それによってセッターの敷板上での移動が効果的に制限され、セッターの敷板上での摺動を十分に防止することができる。また、これらの効果に伴ってセラミックス製品の焼成治具としてのハンドリング性を大幅に向上させることができる。
Here, it is preferable that the ratio Wc/Wp of the maximum width Wc in a direction parallel to the adjacent surface 7S of a cross section perpendicular to the longitudinal direction of at least one of the convex portions 8 of the setter 7 and the maximum width Wp in a direction parallel to the adjacent surface 9P of a cross section perpendicular to the longitudinal direction of the groove portion 10 in which the convex portion 8 is accommodated when the setter 7 is placed on the base plate 9 is 2 or less (greater than 0).
In the firing jig according to one embodiment of the present invention, in which the ratio Wc/Wp is 2 or less, the convex portion of the setter is accommodated and engaged deep toward the bottom of the groove portion of the base plate, thereby effectively restricting the movement of the setter on the base plate and sufficiently preventing the setter from sliding on the base plate. In addition, these effects can greatly improve the handleability of the firing jig for ceramic products.
 割合Wc/Wpが(0超であって)2以下である関係が満たされる範囲内の一実施形態において、上記観点から、Wc/Wpは、(0超であって)1.8以下であることが好ましく、1.6以下であることがさらに好ましく、1.4以下であることがさらにより好ましく、1.2以下であることが一層好ましく、1.0以下であることがより一層好ましく、0.9以下であることが最も好ましい。
 割合Wc/Wpが(0超であって)2以下である関係が満たされる範囲内の別の実施形態において、上記観点から、Wc/Wpは、0.2以上1.8以下であることが好ましく、0.2以上1.6以下であることがさらに好ましく、0.2以上1.4以下であることがさらにより好ましく、0.2以上1.2以下であることが一層好ましく、0.2以上1.0以下であることがより一層好ましく、0.2以上0.9以下であることが最も好ましい。
 割合Wc/Wpが(0超であって)2以下である関係が満たされる範囲内のさらに別の実施形態において、上記観点から、Wc/Wpは、0.4以上1.8以下であることが好ましく、0.4以上1.6以下であることがさらに好ましく、0.4以上1.4以下であることがさらにより好ましく、0.4以上1.2以下であることが一層好ましく、0.4以上1.0以下であることがより一層好ましく、0.4以上0.9以下であることが最も好ましい。
In one embodiment within the range in which the relationship that the ratio Wc/Wp is (greater than 0) 2 or less is satisfied, from the above viewpoint, Wc/Wp is preferably (greater than 0) 1.8 or less, more preferably 1.6 or less, even more preferably 1.4 or less, even more preferably 1.2 or less, even more preferably 1.0 or less, and most preferably 0.9 or less.
In another embodiment within the range in which the relationship that the ratio Wc/Wp is (greater than 0) 2 or less is satisfied, from the above viewpoint, Wc/Wp is preferably 0.2 or more and 1.8 or less, more preferably 0.2 or more and 1.6 or less, even more preferably 0.2 or more and 1.4 or less, even more preferably 0.2 or more and 1.2 or less, even more preferably 0.2 or more and 1.0 or less, and most preferably 0.2 or more and 0.9 or less.
In yet another embodiment within the range in which the relationship that the ratio Wc/Wp is (greater than 0) and 2 or less is satisfied, from the above viewpoint, Wc/Wp is preferably 0.4 or more and 1.8 or less, more preferably 0.4 or more and 1.6 or less, even more preferably 0.4 or more and 1.4 or less, even more preferably 0.4 or more and 1.2 or less, even more preferably 0.4 or more and 1.0 or less, and most preferably 0.4 or more and 0.9 or less.
 図5は、本発明の一実施形態に係る焼成治具のセッターと敷板との組み合わせにつき、セッターを敷板に戴置した際の、敷板の条溝部の平均深さDg・avと、条溝部間の垂直最短距離Igとの関係を例示している。
 図5においては、2つの凸部8が略平行に形成され、かつ2つの凸部8がそれぞれ収容される2つの条溝部10が略平行に形成された例が示されている。他の実施形態においては、これに加えて、3つ以上の凸部8が略平行かつ略等間隔に形成され、かつ3つ以上の凸部8がそれぞれ収容される3つ以上の条溝部10が略平行かつ略等間隔に形成されるように構成してよい。
 図5において、Dg・avは、敷板9の条溝部10の平均深さ(条溝部10の長手方向に垂直な断面の、敷板9のセッター7に対する近接面9Pから垂直方向の最低位置までの長さについて各条溝部10の平均値)を示す。ここでの平均値は、敷板9に設けられた条溝部10の数が10個までの場合はそれら全ての平均値を指し、敷板9に設けられた条溝部10の数が11個以上の場合はそれらのうちの任意の10個の平均値を指す。また、図5において、Igは、敷板9の条溝部10間の垂直最短距離(条溝部が3つ以上形成されている場合は、複数の垂直最短距離の平均値)を示す。ここでの平均値は、条溝部10間の垂直最短距離の数が9個まで(条溝部10の数が10個まで)の場合はそれら全ての平均値を指し、条溝部10間の垂直最短距離の数が10個以上(条溝部10の数が11個以上)の場合はそれらのうちの任意の9個の平均値を指す。
 図5において、凸部の断面形状は略円形として例示され、条溝部の断面形状は略半円形として例示されているが、図3および図4について説明したのと同様にこれらの形状に限定されるわけではない。
Figure 5 illustrates the relationship between the average depth Dg·av of the groove portions of the base plate and the shortest vertical distance Ig between the groove portions when the setter is placed on the base plate for a combination of a setter and base plate of a firing jig according to one embodiment of the present invention.
5 shows an example in which two protrusions 8 are formed substantially parallel to each other, and two grooves 10 are formed substantially parallel to each other, each accommodating the two protrusions 8. In other embodiments, in addition to this, three or more protrusions 8 may be formed substantially parallel to each other and at substantially equal intervals, and three or more grooves 10 are formed substantially parallel to each other and at substantially equal intervals, each accommodating the three or more protrusions 8.
In FIG. 5, Dg·av indicates the average depth of the groove portion 10 of the sole plate 9 (the average value of each groove portion 10 in terms of the length from the adjacent surface 9P of the sole plate 9 relative to the setter 7 to the lowest position in the vertical direction of the cross section perpendicular to the longitudinal direction of the groove portion 10). The average value here refers to the average value of all the groove portions 10 provided on the sole plate 9 when the number of groove portions 10 provided on the sole plate 9 is up to 10, and refers to the average value of any 10 of the groove portions 10 provided on the sole plate 9 when the number of groove portions 10 provided on the sole plate 9 is 11 or more. Also, in FIG. 5, Ig indicates the vertical shortest distance between the groove portions 10 of the sole plate 9 (the average value of multiple vertical shortest distances when three or more groove portions are formed). The average value here refers to the average value of all the vertical shortest distances between the groove portions 10 when the number of the vertical shortest distances between the groove portions 10 is up to 9 (the number of groove portions 10 is up to 10), and refers to the average value of any 9 of the vertical shortest distances when the number of the vertical shortest distances between the groove portions 10 is 10 or more (the number of groove portions 10 is 11 or more).
In FIG. 5, the cross-sectional shape of the convex portion is illustrated as being substantially circular, and the cross-sectional shape of the groove portion is illustrated as being substantially semicircular, but as explained with reference to FIGS. 3 and 4, these shapes are not limited to these.
 ここで、敷板9の条溝部10の平均深さ(条溝部10の長手方向に垂直な断面の近接面9Pから垂直方向の最低位置までの長さについて各条溝部10の平均値を指す)Dg・avに対する、条溝部10間の垂直最短距離(条溝部10が3つ以上形成されている場合は、複数の垂直最短距離の平均値を指す)Igの比率Ig/Dg・avは、0.05以上600以下であることが好ましい。
 この比率Ig/Dg・avが0.05以上600以下である本発明の一実施形態に係る焼成治具によれば、セッターの凸部が敷板の条溝部に対して、密な係合箇所を有する形で深く安定して収容・係合され、それによってセッターの敷板上での移動が効果的に制限され、セッターの敷板上での摺動を十分に防止することができる。また、これらの効果に伴ってセラミックス製品の焼成治具としてのハンドリング性を大幅に向上させることができる。
Here, it is preferable that the ratio Ig/Dg・av of the vertical shortest distance Ig between the groove portions 10 (if three or more groove portions 10 are formed, this refers to the average value of the multiple vertical shortest distances) to the average depth Dg・av of the groove portions 10 of the base plate 9 (which refers to the average value of each groove portion 10 in terms of the length from the adjacent surface 9P of the cross section perpendicular to the longitudinal direction of the groove portion 10 to the lowest vertical position) is 0.05 or more and 600 or less.
According to the firing jig of one embodiment of the present invention, in which the ratio Ig/Dg.av is 0.05 or more and 600 or less, the convex part of the setter is deeply and stably received and engaged with the groove part of the base plate with dense engagement points, thereby effectively restricting the movement of the setter on the base plate and sufficiently preventing the setter from sliding on the base plate. Furthermore, with these effects, the handling property of the firing jig for ceramic products can be significantly improved.
 比率Ig/Dg・avが0.05以上600以下である関係が満たされる範囲内の一実施形態において、上記観点から、Ig/Dg・avは、0.05以上500以下であることが好ましく、0.05以上400以下であることがより好ましく、0.05以上300以下であることがさらに好ましく、0.05以上200以下であることがさらにより好ましく、0.05以上100以下であることが一層好ましく、0.05以上50以下であることがより一層好ましく、0.05以上10以下であることがなおより一層好ましく、0.05以上5以下であることがさらにより一層好ましく、0.05以上2以下であることが最も好ましい。
 比率Ig/Dg・avが0.05以上600以下である関係が満たされる範囲内の別の実施形態において、上記観点から、Ig/Dg・avは、0.1以上500以下であることが好ましく、0.1以上400以下であることがより好ましく、0.1以上300以下であることがさらに好ましく、0.1以上200以下であることがさらにより好ましく、0.1以上100以下であることが一層好ましく、0.1以上50以下であることがより一層好ましく、0.1以上10以下であることがなおより一層好ましく、0.1以上5以下であることがさらにより一層好ましく、0.1以上2以下であることが最も好ましい。
In one embodiment within the range in which the relationship that the ratio Ig/Dg·av is 0.05 or more and 600 or less is satisfied, from the above viewpoint, Ig/Dg·av is preferably 0.05 or more and 500 or less, more preferably 0.05 or more and 400 or less, even more preferably 0.05 or more and 300 or less, even more preferably 0.05 or more and 200 or less, even more preferably 0.05 or more and 100 or less, even more preferably 0.05 or more and 50 or less, even more preferably 0.05 or more and 10 or less, even more preferably 0.05 or more and 5 or less, and most preferably 0.05 or more and 2 or less.
In another embodiment within the range in which the relationship that the ratio Ig/Dg·av is 0.05 or more and 600 or less is satisfied, from the above viewpoint, Ig/Dg·av is preferably 0.1 or more and 500 or less, more preferably 0.1 or more and 400 or less, even more preferably 0.1 or more and 300 or less, even more preferably 0.1 or more and 200 or less, even more preferably 0.1 or more and 100 or less, even more preferably 0.1 or more and 50 or less, still more preferably 0.1 or more and 10 or less, even more preferably 0.1 or more and 5 or less, and most preferably 0.1 or more and 2 or less.
 図6は、本発明の一実施形態に係る焼成治具のセッターと敷板との組み合わせにつき、セッターの凸部の最大幅員Wcと、その長手方向の両端部間の長さLcとの関係(アスペクト比)を例示している。
 図6は、セッター7の敷板9に対する近接面7S上に1つまたは複数個設けられた凸部8(メッシュ状セラミックシートの場合の線条部)のうちの1つを抽出し、近接面7Sに対して垂直視した概略図である。図6において、Wcは、セッター7の凸部8の長手方向に垂直な断面の、セッター7の敷板9に対する近接面7Sに平行な方向の最大幅員を示す。また、Lcは、その凸部8の長手方向の両端部間の長さを示す。
FIG. 6 illustrates an example of the relationship (aspect ratio) between the maximum width Wc of the convex portion of the setter and the length Lc between both ends in the longitudinal direction for a combination of a setter and a base plate of a firing jig according to one embodiment of the present invention.
Fig. 6 is a schematic diagram of one of the protruding parts 8 (linear parts in the case of a mesh-like ceramic sheet) provided on the adjacent surface 7S of the setter 7 relative to the base plate 9, viewed perpendicularly to the adjacent surface 7S. In Fig. 6, Wc indicates the maximum width of the cross section perpendicular to the longitudinal direction of the protruding part 8 of the setter 7, in the direction parallel to the adjacent surface 7S of the setter 7 relative to the base plate 9. Furthermore, Lc indicates the length between both ends of the protruding part 8 in the longitudinal direction.
 ここで、セッター7の凸部8の少なくとも1つについて、その長手方向に垂直な断面の近接面7Sに平行な方向の最大幅員Wcに対する、その長手方向の両端部間の長さLcのアスペクト比Lc/Wcは、10以上であることが好ましい。
 このアスペクト比Lc/Wcが10以上である本発明の一実施形態に係る焼成治具によれば、セッターの凸部が敷板の条溝部に対して、より長い距離の連続的な係合箇所を有する形で安定して収容・係合され、それによってセッターの敷板上での移動が効果的に制限され、セッターの敷板上での摺動を十分に防止することができる。また、これらの効果に伴ってセラミックス製品の焼成治具としてのハンドリング性を大幅に向上させることができる。
Here, for at least one of the convex portions 8 of the setter 7, it is preferable that the aspect ratio Lc/Wc of the length Lc between both ends in the longitudinal direction to the maximum width Wc in a direction parallel to the adjacent surface 7S of the cross section perpendicular to the longitudinal direction is 10 or more.
According to the firing jig of one embodiment of the present invention, in which the aspect ratio Lc/Wc is 10 or more, the convex portion of the setter is stably accommodated and engaged with the groove portion of the base plate in a manner that has continuous engagement points over a longer distance, thereby effectively restricting the movement of the setter on the base plate and sufficiently preventing the setter from sliding on the base plate. Furthermore, these effects can be accompanied by a significant improvement in the handleability of the firing jig for ceramic products.
 アスペクト比Lc/Wcが10以上である関係が満たされる範囲内の一実施形態において、上記観点から、Lc/Wcは、11以上であることが好ましく、12以上であることがより好ましく、13以上であることがさらに好ましく、20以上であることがさらにより好ましく、30以上であることがなおより好ましく、50以上であることが一層好ましく、70以上であることがより一層好ましく、100以上であることが最も好ましい。 In one embodiment within the range in which the aspect ratio Lc/Wc is 10 or greater, from the above viewpoints, Lc/Wc is preferably 11 or greater, more preferably 12 or greater, even more preferably 13 or greater, even more preferably 20 or greater, even more preferably 30 or greater, even more preferably 50 or greater, even more preferably 70 or greater, and most preferably 100 or greater.
 図7は、本発明の一実施形態に係る焼成治具のセッターと敷板との組み合わせにつき、セッターを敷板に戴置した際の、セッターの凸部の最大高さHcと、この凸部が収容される敷板の条溝部の深さDgとの関係を例示している。
 図7において、Hcは、セッター7の凸部8の長手方向に垂直な断面の、セッター7の敷板9に対する近接面7Sに垂直な方向の最大高さを示す。また、Dgは、セッター7の敷板9への戴置の際、この凸部8が収容される条溝部10の長手方向に垂直な断面の、敷板9のセッター7に対する近接面9Pから垂直方向の最低位置までの深さを示す。
 図7において、凸部の断面形状は略円形として例示され、条溝部の断面形状は略半円形として例示されているが、図3~5について説明したのと同様にこれらの形状に限定されるわけではない。
Figure 7 illustrates the relationship between the maximum height Hc of the convex portion of the setter when the setter is placed on the base plate and the depth Dg of the groove portion of the base plate in which this convex portion is accommodated, for a combination of a setter and a base plate of a firing jig according to one embodiment of the present invention.
7, Hc indicates the maximum height of a cross section perpendicular to the longitudinal direction of the protruding portion 8 of the setter 7, in a direction perpendicular to the adjacent surface 7S of the setter 7 relative to the base plate 9. Also, Dg indicates the depth from the adjacent surface 9P of the base plate 9 relative to the setter 7 to the lowest position in the vertical direction of a cross section perpendicular to the longitudinal direction of the groove portion 10 in which the protruding portion 8 is accommodated when the setter 7 is placed on the base plate 9.
In FIG. 7, the cross-sectional shape of the convex portion is illustrated as being substantially circular, and the cross-sectional shape of the groove portion is illustrated as being substantially semicircular, but as explained with reference to FIGS. 3 to 5, these shapes are not limited thereto.
 ここで、セッター7の凸部8の少なくとも1つの長手方向に垂直な断面の近接面7Sに垂直な方向の最大高さHcに対する、セッター7の敷板9への戴置の際、この凸部8が収容される条溝部10の長手方向に垂直な断面の近接面9Pから垂直方向の最低位置までの深さDgの比率Dg/Hcは、0.1以上であることが好ましい。
 この比率Dg/Hcが0.1以上である本発明の一実施形態に係る焼成治具によれば、セッターの凸部が敷板の条溝部の底部に向かってより深く安定して収容・係合され、それによってセッターの敷板上での運動・移動に対する抵抗性がより大きくなって、セッターの移動が効果的に制限され、セッターの敷板上での摺動を十分に防止することができる。また、これらの効果に伴ってセラミックス製品の焼成治具としてのハンドリング性を大幅に向上させることができる。
Here, it is preferable that the ratio Dg/Hc of the depth Dg from the adjacent surface 9P of a cross section perpendicular to the longitudinal direction of the groove portion 10 in which the convex portion 8 is accommodated when the setter 7 is placed on the base plate 9 to the maximum height Hc in a direction perpendicular to the adjacent surface 7S of at least one cross section perpendicular to the longitudinal direction of the convex portion 8 of the setter 7 is 0.1 or more.
According to the firing jig of the present invention, in which the ratio Dg/Hc is 0.1 or more, the convex part of the setter is stably received and engaged deeper toward the bottom of the groove part of the base plate, which increases the resistance of the setter to movement on the base plate, effectively restricting the movement of the setter and sufficiently preventing the setter from sliding on the base plate. Furthermore, these effects can greatly improve the handleability of the firing jig for ceramic products.
 比率Dg/Hcが0.1以上である関係が満たされる範囲内の一実施形態において、上記観点から、Dg/Hcは、0.15以上であることが好ましく、0.2以上であることがより好ましく、0.25以上であることがさらに好ましく、0.3以上であることがさらにより好ましく、0.35以上であることがなおより好ましく、0.4以上であることが一層好ましく、0.45以上であることがより一層好ましく、0.50以上であることがさらにより一層好ましく、0.55以上であることがなおより一層好ましく、0.60以上であることが最も好ましい。 In one embodiment within the range in which the relationship that the ratio Dg/Hc is 0.1 or greater is satisfied, from the above viewpoint, Dg/Hc is preferably 0.15 or greater, more preferably 0.2 or greater, even more preferably 0.25 or greater, even more preferably 0.3 or greater, even more preferably 0.35 or greater, even more preferably 0.4 or greater, even more preferably 0.45 or greater, even more preferably 0.50 or greater, even more preferably 0.55 or greater, and most preferably 0.60 or greater.
 図8は、本発明の一実施形態に係る焼成治具のセッターと敷板との組み合わせにつき、セッターの凸部の最大高さHcと、この凸部の最大幅員Wcとの関係を例示している。
 図8は、セッター7の敷板9に対する近接面7S上に1つまたは複数個設けられた凸部8のうちの1つを抽出し、凸部8の長手方向に対して垂直視した概略図である。図8において、Hcは、セッター7の凸部8の長手方向に垂直な断面の、セッター7の敷板9に対する近接面7Sに垂直な方向の最大高さである。また、Wcは、この凸部8の長手方向に垂直な断面の近接面7Sに平行な方向の最大幅員を示す。
FIG. 8 illustrates the relationship between the maximum height Hc of the convex portion of the setter and the maximum width Wc of the convex portion for a combination of a setter and a base plate of a firing jig according to one embodiment of the present invention.
Fig. 8 is a schematic diagram of one of the protrusions 8 provided on the adjacent surface 7S of the setter 7 relative to the floor plate 9, viewed perpendicularly to the longitudinal direction of the protrusion 8. In Fig. 8, Hc is the maximum height of a cross section perpendicular to the longitudinal direction of the protrusion 8 of the setter 7, in a direction perpendicular to the adjacent surface 7S of the setter 7 relative to the floor plate 9. Also, Wc is the maximum width of the cross section perpendicular to the longitudinal direction of the protrusion 8, in a direction parallel to the adjacent surface 7S.
 ここで、セッター7の凸部8の少なくとも1つの長手方向に垂直な断面の近接面7Sに垂直な方向の最大高さHcに対する、この凸部8の長手方向に垂直な断面の近接面7Sに平行な方向の最大幅員Wcの比率Wc/Hcは0.3以上4以下であることが好ましい。
 この比率Wc/Hcが0.3以上4以下である本発明の一実施形態に係る焼成治具によれば、敷板の条溝部の断面形状にかかわらず、またはその断面形状により良く対応して、セッターの凸部が敷板の条溝部に対して深く安定した収容・係合状態を形成し易くなり、それによってセッターの敷板上での移動が効果的に制限され、セッターの敷板上での摺動を十分に防止することができる。また、これらの効果に伴ってセラミックス製品の焼成治具としてのハンドリング性を大幅に向上させることができる。
Here, it is preferable that the ratio Wc/Hc of the maximum width Wc in a direction parallel to the adjacent surface 7S of a cross section perpendicular to the longitudinal direction of at least one of the convex portions 8 of the setter 7 to the maximum height Hc in a direction perpendicular to the adjacent surface 7S of a cross section perpendicular to the longitudinal direction of this convex portion 8 is 0.3 or more and 4 or less.
According to the firing jig of one embodiment of the present invention, in which the ratio Wc/Hc is 0.3 to 4, the convex portion of the setter can easily form a deep and stable state of insertion and engagement with the groove portion of the base plate, regardless of or in accordance with the cross-sectional shape of the groove portion of the base plate, thereby effectively restricting the movement of the setter on the base plate and sufficiently preventing the setter from sliding on the base plate. Furthermore, these effects can greatly improve the handleability of the firing jig for ceramic products.
 比率Wc/Hcが0.3以上4以下である関係が満たされる範囲内の一実施形態において、上記観点から、Wc/Hcは、0.4以上4以下であることが好ましく、0.5以上4以下であることがより好ましく、0.6以上4以下であることがさらにより好ましく、0.7以上4以下であることが一層好ましく、0.8以上4以下であることがより一層好ましく、0.9以上4以下であることがさらにより一層好ましく、1以上4以下であることが最も好ましい。
 比率Wc/Hcが0.3以上4以下である関係が満たされる範囲内の別の実施形態において、上記観点から、Wc/Hcは、0.4以上3以下であることが好ましく、0.5以上3以下であることがより好ましく、0.6以上3以下であることがさらにより好ましく、0.7以上3以下であることが一層好ましく、0.8以上3以下であることがより一層好ましく、0.9以上3以下であることがさらにより一層好ましく、1以上3以下であることが最も好ましい。
 比率Wc/Hcが0.3以上4以下である関係が満たされる範囲内のさらなる別の実施形態において、上記観点から、Wc/Hcは、0.4以上2以下であることが好ましく、0.5以上2以下であることがより好ましく、0.6以上2以下であることがさらにより好ましく、0.7以上2以下であることが一層好ましく、0.8以上2以下であることがより一層好ましく、0.9以上2以下であることがさらにより一層好ましく、1以上2以下であることが最も好ましい。
In one embodiment within the range in which the relationship of the ratio Wc/Hc being 0.3 or greater and 4 or less is satisfied, from the above viewpoints, Wc/Hc is preferably 0.4 or greater and 4 or less, more preferably 0.5 or greater and 4 or less, even more preferably 0.6 or greater and 4 or less, even more preferably 0.7 or greater and 4 or less, even more preferably 0.8 or greater and 4 or less, even more preferably 0.9 or greater and 4 or less, and most preferably 1 or greater and 4 or less.
In another embodiment within the range in which the relationship of the ratio Wc/Hc being 0.3 or greater and 4 or less is satisfied, from the above viewpoint, Wc/Hc is preferably 0.4 or greater and 3 or less, more preferably 0.5 or greater and 3 or less, even more preferably 0.6 or greater and 3 or less, even more preferably 0.7 or greater and 3 or less, even more preferably 0.8 or greater and 3 or less, even more preferably 0.9 or greater and 3 or less, and most preferably 1 or greater and 3 or less.
In yet another embodiment within the range in which the relationship of the ratio Wc/Hc being 0.3 or greater and 4 or less is satisfied, from the above viewpoint, Wc/Hc is preferably 0.4 or greater and 2 or less, more preferably 0.5 or greater and 2 or less, even more preferably 0.6 or greater and 2 or less, even more preferably 0.7 or greater and 2 or less, even more preferably 0.8 or greater and 2 or less, even more preferably 0.9 or greater and 2 or less, and most preferably 1 or greater and 2 or less.
 好ましい一実施形態において、本発明に係る焼成治具において敷板と組み合わせられるセッターは、少なくとも一部にメッシュ状部位を含むセラミックスシートであり、このメッシュ状部位は、所与の間隔で配置された各条が一方向に延伸された複数条の第1線条部で構成される第1線条部層、および、第1線条部の各条の上に接してこれと交差するように所与の間隔で配置された、各条が一方向に延伸された複数条の第2線条部で構成される第2線条部層を含み、第1線条部層と第2線条部層とが一体的に形成された部位であるセラミックスシートであってよい。セッターがメッシュ状部位を一部に含む場合、セッターのメッシュ状部位以外の部位は、いかなる公知のセッターの構造が採用されてもよい。一実施形態において、全体が一体的に形成されたメッシュ状のセラミックスシート焼結体であるセッターを用いてもよい。
 本発明に係る焼成治具の一実施形態において、セッター(の全部または一部)がメッシュ状セラミックスシートを含むセッターである場合、第2線条部層の第1線条部層に対する接面がセッターの敷板に対する近接面をなし、第1線条部層を構成する第1線条部がセッターの凸部をなす。
In a preferred embodiment, the setter combined with the base plate in the firing jig according to the present invention is a ceramic sheet including at least a mesh-like portion in a part thereof, and the mesh-like portion includes a first striated portion layer including a plurality of first striated portions arranged at a given interval and extending in one direction, and a second striated portion layer including a plurality of second striated portions arranged at a given interval so as to contact and cross each of the first striated portions and extend in one direction, and the first striated portion layer and the second striated portion layer may be integrally formed ceramic sheets. When the setter includes a mesh-like portion in a part thereof, any known setter structure may be adopted for the portion other than the mesh-like portion of the setter. In one embodiment, a setter that is a mesh-like ceramic sheet sintered body formed integrally as a whole may be used.
In one embodiment of the firing jig according to the present invention, when the setter (all or part of it) is a setter including a mesh-like ceramic sheet, the contact surface of the second striated portion layer with the first striated portion layer forms the adjacent surface of the setter with respect to the base plate, and the first striated portion constituting the first striated portion layer forms the convex portion of the setter.
 ここで、第1線条部層と第2線条部層とが「一体的に形成された」メッシュ状の焼結体であることは、第1線条部層を構成する線条群と第2線条部層を構成する線条群とが、それらの接触箇所にて一体的な構造を成すように焼成・連結されて、容易に分離できないように形成されていることを意味する。一実施形態において、第1線条部層と第2線条部層とは、第1線条部層を構成する線条群と第2線条部層を構成する線条群とが、それらの接触箇所にて一体的な構造を成すように焼成・連結されて、容易に分離できないように形成されており、かつ、第1線条部層と第2線条部層とが、あるいは各線条部層の異なる部分同士が単一の組成から形成されていてよい。他の一実施形態において、第1線条部層と第2線条部層とは、第1線条部層を構成する線条群と第2線条部層を構成する線条群とが、それらの接触箇所にて一体的な構造を成すように焼成・連結されて、容易に分離できないように形成されており、かつ、第1線条部層と第2線条部層とが、あるいは各線条部層の異なる部分同士が異なる複数の組成から形成されていてよい。 Here, the fact that the first striated layer and the second striated layer are "integrally formed" mesh-like sintered bodies means that the striated groups constituting the first striated layer and the striated groups constituting the second striated layer are fired and connected to each other to form an integral structure at their contact points, and are formed so as not to be easily separated. In one embodiment, the first striated layer and the second striated layer are fired and connected to each other to form an integral structure at their contact points, and are formed so as not to be easily separated, and the first striated layer and the second striated layer, or different parts of each striated layer, may be formed from a single composition. In another embodiment, the first and second filamentary layers are formed such that the filaments constituting the first and second filamentary layers are sintered and connected to each other at the contact points to form an integral structure, and are not easily separated, and the first and second filamentary layers, or different portions of each filamentary layer, may be formed from a plurality of different compositions.
 図9に、セッターのメッシュ状部位の一実施形態が例示されている。図9において、メッシュ状部位11は、略一定の間隔で配置された各条が一方向に延伸された複数条の第1線条部12で構成される第1線条部層、およびこの第1線条部12の各条の上に接してこれを交差するように略一定の間隔で配置された、各条が一方向に延伸された複数条の第2線条部13で構成される第2線条部層を含む。両線条部12、13の交差角度は適宜設定され得るが、例えば第1線条部12に対して第2線条部13の交差角度を90度とすることができる。あるいは、第1線条部12に対する第2線条部13の交差角度を90度±10度の範囲で変更させることもできる。第1線条部12の断面形状は、特に限定されないが、図示されているように略円形または略楕円形であってよい。また、第2線条部13の断面形状は、特に限定されないが、図示されているように上部にて直線をなし、下部にてこの直線の両端部を起点とする曲線(すなわち、略円形または略楕円形の一部が直線状に切断された形状)をなして、第2線条部13全体の上面(すなわち第2線条部層の上面)が1つの平坦面を形成していてよい。第1線条部12および第2線条部13の断面形状は、上述された略円形、略楕円形以外に、略矩形等の略多角形、あるいはこの一部が直線状に切断された形状を採り得る。 9 illustrates an embodiment of the mesh portion of the setter. In FIG. 9, the mesh portion 11 includes a first striated portion layer composed of a plurality of first striated portions 12 arranged at approximately regular intervals and each striated portion is stretched in one direction, and a second striated portion layer composed of a plurality of second striated portions 13 arranged at approximately regular intervals so as to contact and cross each striated portion of the first striated portion 12 and each striated portion is stretched in one direction. The intersection angle between the two striated portions 12 and 13 can be set appropriately, but for example, the intersection angle of the second striated portion 13 with respect to the first striated portion 12 can be set to 90 degrees. Alternatively, the intersection angle of the second striated portion 13 with respect to the first striated portion 12 can be changed within a range of 90 degrees ± 10 degrees. The cross-sectional shape of the first striated portion 12 is not particularly limited, but may be approximately circular or approximately elliptical as shown in the figure. The cross-sectional shape of the second striated portion 13 is not particularly limited, but may be a straight line at the top as shown in the figure, and a curve starting from both ends of the straight line at the bottom (i.e., a shape in which a part of a substantially circular or substantially elliptical shape is cut in a straight line), so that the top surface of the entire second striated portion 13 (i.e., the top surface of the second striated portion layer) forms a single flat surface. The cross-sectional shapes of the first striated portion 12 and the second striated portion 13 can be substantially polygonal such as substantially rectangular, or a shape in which a part of the polygonal shape is cut in a straight line, in addition to the substantially circular and substantially elliptical shapes described above.
 別の実施形態において、セッターのメッシュ状部位は、第1線条部および第2線条部を有することに加えて、一方向に向けて延びるセラミックス製の複数の第3線条部を更に有してよい(これによって第3線条部層が構成されていてよい)。このとき、本実施形態においては第3線条部が延びる方向は、第1線条部が延びる方向と同方向であってもよく、第1線条部が延びる方向に対して、斜め方向(例えば-45°よりも大きく且つ45°よりも小さい方向)に傾斜していてもよい。そして、このように第3の線条部が形成される場合、第2線条部の断面形状は略円形または略楕円形であってよく、第3線条部の断面形状は、上部にて直線をなし、下部にてこの直線の両端部を起点とする曲線(すなわち、略円形または略楕円形の一部が直線状に切断された形状)をなして、第3線条部全体の上面(すなわち第3線条部層の上面)が1つの平坦面を形成していてよい。
 これと同様にして、更に第4線条部、あるいは更にそれ以降の線条部を形成することもできる。
In another embodiment, the mesh portion of the setter may further have a plurality of third striated portions made of ceramics extending in one direction in addition to the first striated portion and the second striated portion (the third striated portion layer may be formed by this). In this embodiment, the direction in which the third striated portions extend may be the same as the direction in which the first striated portions extend, or may be inclined obliquely (for example, in a direction greater than -45° and smaller than 45°) with respect to the direction in which the first striated portions extend. When the third striated portions are formed in this manner, the cross-sectional shape of the second striated portion may be substantially circular or substantially elliptical, and the cross-sectional shape of the third striated portion may be a straight line at the upper portion and a curved line starting from both ends of the straight line at the lower portion (i.e., a shape in which a part of the substantially circular or substantially elliptical shape is cut in a straight line), so that the upper surface of the entire third striated portion (i.e., the upper surface of the third striated portion layer) may form a single flat surface.
In the same manner, a fourth linear portion or any subsequent linear portions can be formed.
 好ましい一実施形態において、全体が単一種の材料で一体的に形成されたメッシュ状のセラミックスシート焼結体であるセッターを用いてよい。このようなセッターを用いることにより、セラミックスシート全体の強度が非常に高くなり、またセッターの効率的な製造にもつながる。また、好ましい一実施形態において、メッシュ状部位がセラミックスシートの一部を占める場合、メッシュ状部位とメッシュ状部位以外の部位とは一体的に形成されたセラミックスシート燒結体であってよい。メッシュ状部位とメッシュ状部位以外の部位とが一体的に形成された燒結体を構成する場合、両者の原料粉を同じにすることにより、セラミックスシート全体の強度が高められると共に、焼成時の加熱・冷却の熱履歴(膨張・収縮の繰り返し)による接合強度の低下が防止され得る。 In a preferred embodiment, a setter may be used that is a mesh-shaped ceramic sheet sintered body formed integrally from a single material. Using such a setter greatly increases the strength of the entire ceramic sheet and also leads to efficient manufacturing of the setter. In a preferred embodiment, when the mesh-shaped portion occupies a portion of the ceramic sheet, the mesh-shaped portion and the portion other than the mesh-shaped portion may be a ceramic sheet sintered body formed integrally. When a sintered body is formed in which the mesh-shaped portion and the portion other than the mesh-shaped portion are formed integrally, the strength of the entire ceramic sheet is increased by using the same raw material powder for both, and a decrease in the bonding strength due to the thermal history of heating and cooling during sintering (repeated expansion and contraction) can be prevented.
 セラミックスシートのメッシュ状部位は、一実施形態において、第1線条部と第2線条部とのいずれの交差部にても、第1線条部の断面が円形または楕円形の形状を有しており、第2線条部の断面が直線部と該直線部の両端部を端部とする凸形の曲線部とから構成される形状(略弓形状)を有しており、しかも、交差部の縦断面視で、第2線条部における凸形の曲線部の頂部と第1線条部における円形または楕円形における上向きに凸の頂部のみが接触している構成(いわゆる点接触の構成)を有することができる。 In one embodiment, the mesh-like portion of the ceramic sheet has a cross section in which the first striated portion and the second striated portion intersect with each other such that the cross section of the first striated portion has a circular or elliptical shape, and the cross section of the second striated portion has a shape (approximately arch-shaped) consisting of a straight portion and a convex curved portion having both ends of the straight portion as its ends, and further, when viewed in vertical cross section at the intersection, only the apex of the convex curved portion of the second striated portion and the upwardly convex apex of the circle or ellipse of the first striated portion are in contact (a so-called point contact configuration).
 またセラミックスシートのメッシュ状部位は、他の一実施形態において、第1線条部の断面が、第1線条部と第2線条部との交差部以外の部位にて、円形または楕円形の形状を有しており、第2線条部の断面が、交差部以外の部位にて、直線部と、該直線部の両端部を端部とする凸形の曲線部とから構成される形状(略弓形状)を有しており、かつ第1線条部と第2線条部とが、それぞれ一点のみではなく、面で接触した交差部を成している構成を備えることができる。この構成は、上記のいわゆる点接触に対して面接触の構造と称され得る。 In another embodiment, the mesh-like portion of the ceramic sheet can have a configuration in which the cross section of the first striated portion has a circular or elliptical shape at a portion other than the intersection between the first striated portion and the second striated portion, and the cross section of the second striated portion has a shape (approximately arch-shaped) composed of a straight portion and a convex curved portion with both ends of the straight portion as ends at a portion other than the intersection, and the first striated portion and the second striated portion each form an intersection where they contact over a surface rather than just a single point. This configuration can be called a surface contact structure as opposed to the so-called point contact described above.
 このような面接触による上記構造例の下位概念に相当する一実施形態において、セラミックスシートのメッシュ状部位は、第1線条部の断面が、第1線条部と第2線条部との交差部以外の部位にて、円形または楕円形の形状を有しており、第2線条部の断面が、交差部以外の部位にて、直線部と、該直線部の両端部を端部とする凸形の曲線部とから構成される形状(略弓形状)を有しており、しかも、第1線条部の平面視での投影像が、交差部にて、幅方向外方に向けて湾曲膨出した形状になっており、それによって交差部における投影像の幅が交差部以外の部位における投影像の幅よりも大きくなっている構成を有することができる。 In one embodiment that corresponds to a sub-concept of the above structural example based on such surface contact, the mesh-like portion of the ceramic sheet has a cross section of the first striated portion that has a circular or elliptical shape at a portion other than the intersection of the first striated portion and the second striated portion, and a cross section of the second striated portion that has a shape (approximately arch-shaped) composed of a straight portion and a convex curved portion with both ends of the straight portion as ends at a portion other than the intersection, and further, the projected image of the first striated portion in a plan view has a shape that curves and bulges outward in the width direction at the intersection, so that the width of the projected image at the intersection is larger than the width of the projected image at the portion other than the intersection.
 またセラミックスシートのメッシュ状部位は、更なる他の一実施形態において、第1線条部の断面が、第1線条部と第2線条部との交点以外の部位において、円形または楕円形の形状を有しており、第2線条部の断面が、第1線条部と第2線条部との交点以外の部位において、直線部と該直線部の両端部を端部とする凸形の曲線部とから構成される形状(略弓形状)を有しており、この焼結体は平面視での輪郭の少なくとも一部に直線辺部を有しており、第1線条部および第2線条部とこの直線辺部(外辺)とがそれぞれ独立に10度以上170以下の角度で(すなわち非直角である角度を含む幅広い角度範囲にて)交わっている構造を備えていてよい。 In yet another embodiment of the mesh-like portion of the ceramic sheet, the cross section of the first striated portion has a circular or elliptical shape at a portion other than the intersection of the first striated portion and the second striated portion, and the cross section of the second striated portion has a shape (approximately arch shape) consisting of a straight portion and a convex curved portion with both ends of the straight portion as ends at a portion other than the intersection of the first striated portion and the second striated portion, and the sintered body may have a straight side portion in at least a portion of the outline in a plan view, and the first striated portion and the second striated portion may each independently intersect with the straight side portion (outer side) at an angle of 10 degrees or more and 170 degrees or less (i.e., within a wide angle range including angles that are not right angles).
 またセラミックスシートのメッシュ状部位は、更なる他の一実施形態において、複数の第1線条部および複数の第2線条部に加えて、第1線条部と第2線条部とが交差することで画成される四辺形の対角線上を通るセラミックス製の複数の第3の線条部とを有し、第1線条部、第2線条部および第3の線条部によって画成される複数の三角形の貫通孔が形成されている板状のセラミックス構造体であってよい。 In yet another embodiment, the mesh portion of the ceramic sheet may be a plate-shaped ceramic structure having, in addition to a plurality of first striated portions and a plurality of second striated portions, a plurality of third striated portions made of ceramic passing on the diagonals of a quadrilateral defined by the intersection of the first striated portions and the second striated portions, and having a plurality of triangular through holes defined by the first striated portions, the second striated portions, and the third striated portions.
 メッシュ状部位がセラミックスシートの一部を占める場合のメッシュ状部位以外の部位は、特に限定されないが、例えば、微細な気孔を多数設けたセラミックス板状体(板状体の異なる領域で異なる気孔径/異なる気孔密度を有するものを含む)や、メッシュ以外の形状で第1線条部層(支持体層)および第2線条部層が配置されたシート(一例としてはいわゆる簀子状のシート)等が挙げられる。 When the mesh-like portion occupies a portion of the ceramic sheet, the portion other than the mesh-like portion is not particularly limited, but examples include a ceramic plate having many fine pores (including a plate having different pore sizes/different pore densities in different areas) and a sheet in which a first striated layer (support layer) and a second striated layer are arranged in a shape other than a mesh (one example is a so-called lattice-shaped sheet).
セッターおよび敷板の製造方法
 以降にて、セッターおよび敷板の製造方法を説明するが、これらは非限定的な一例として理解されるべきである。
A method for manufacturing the setter and sole plate will be described below, but these should be understood as non-limiting examples.
 本発明に係る焼成治具を構成するセッターの製造方法は、敷板に対する近接面の一部に上記要件を満たす凸部を含むセッターを製造することが可能である限りは特に限定されない。
 セッターを製造するための原料粉は、特に限定されず、種々のセラミックス素材を含んでいてよい。セラミックス原料粉として用いられるセラミックス素材の例としては、アルミナ(Al)、ジルコニア(ZrO)、酸化マグネシウム(MgO)、ムライト(3Al-2SiO)、炭化ケイ素(SiC)、窒化ケイ素(Si)、窒化アルミニウム(AlN)、炭化ホウ素(BC)、コージェライト(MgO/Al/SiO)、チタン酸アルミニウム(AlTiO)、チタン酸マグネシウム(MgTiO)、二硼化チタン(TiB)などの1種または2種以上の組み合わせが挙げられる。また、これらのセラミックス素材の1種または2種以上の組み合わせである原料粉を用いて製造された焼結体も自ずと、これらの素材から生じ得る組成を有することになる。原料ペースト中のセラミックス原料粉の質量割合は、ペースト全体の質量に対して、通常20質量%以上85質量%以下であってよく、30質量%以上75質量%以下であることが好ましい。
There is no particular limitation on the method for producing the setter constituting the firing jig according to the present invention, so long as it is possible to produce a setter including a protrusion satisfying the above requirements on a part of the surface adjacent to the base plate.
The raw material powder for manufacturing the setter is not particularly limited and may contain various ceramic materials. Examples of ceramic materials used as the ceramic raw material powder include alumina (Al 2 O 3 ), zirconia (ZrO 2 ), magnesium oxide (MgO), mullite (3Al 2 O 3 -2SiO 2 ), silicon carbide (SiC), silicon nitride (Si 3 N 4 ), aluminum nitride (AlN), boron carbide (B 4 C), cordierite (MgO/Al 2 O 3 /SiO 2 ), aluminum titanate (Al 2 TiO 5 ), magnesium titanate (MgTiO 3 ), titanium diboride (TiB 2 ), and the like, or a combination of two or more of them. In addition, a sintered body manufactured using raw material powder that is a combination of one or two or more of these ceramic materials will naturally have a composition that can be produced from these materials. The mass ratio of the ceramic raw material powder in the raw material paste may be generally 20 mass % or more and 85 mass % or less, and preferably 30 mass % or more and 75 mass % or less, based on the mass of the entire paste.
 セッターは、全体が単一の組成で形成されていてもよいし、異なる複数の組成から形成された部分の組み合わせでもよい。一実施形態において、全体が単一種の材料で一体的に形成されたセッターを用いてもよい。
 以降においては、セッターがメッシュ状部位を含むセラミックスシートである場合の製造方法を中心に説明するが、これ以外のセッターについても以降の説明に準じた手法により製造され得ることを当業者は理解するであろう。
The setter may be made entirely of a single composition or may be a combination of parts made of different compositions, in one embodiment, a setter may be used that is integrally made entirely of a single type of material.
Hereinafter, we will mainly explain the manufacturing method when the setter is a ceramic sheet including a mesh-like portion, but those skilled in the art will understand that other setters can also be manufactured by methods similar to those explained below.
 セッターがメッシュ状部位を含むセラミックスシートである実施形態において、メッシュ状部位の第1線条部層と第2線条部層とが、あるいは各線条部層の異なる部分同士が単一の組成から形成されていてよい。他の一実施態様において、メッシュ状部位の第1線条部層と第2線条部層とが、あるいは各線条部層の異なる部分同士が異なる複数の組成から形成されていてよい。一実施形態において、全体が単一種の材料で一体的に形成されたメッシュ状のセラミックスシート焼結体であるセッターを用いてもよい。このようなセッターを用いることにより、セラミックスシート全体の強度が非常に高くなり、またセッターの効率的な製造にもつながる。 In an embodiment in which the setter is a ceramic sheet including a mesh-like portion, the first and second striated layers of the mesh-like portion, or different portions of each striated layer, may be formed from a single composition. In another embodiment, the first and second striated layers of the mesh-like portion, or different portions of each striated layer may be formed from a plurality of different compositions. In one embodiment, a setter may be used that is a mesh-like ceramic sheet sintered body integrally formed as a whole from a single type of material. Use of such a setter significantly increases the strength of the entire ceramic sheet and also leads to efficient manufacture of the setter.
 原料ペーストに用いられるセラミックス原料粉の平均粒径は、通常0.1~20μmの範囲であってよく、好ましくは0.2~10μmの範囲であってよい。ここでのセラミックス原料粉の平均粒径は、レーザ回折・散乱法による体積累積中位径 (D50)の値である。セラミックス原料粉の平均粒径が上記範囲内であることによって、焼成後の構造的な強度・安定性が増大し、崩壊の可能性が低減された焼結体を得ることが可能になる。 The average particle size of the ceramic raw material powder used in the raw material paste may usually be in the range of 0.1 to 20 μm, and preferably in the range of 0.2 to 10 μm. The average particle size of the ceramic raw material powder here is the volume cumulative median diameter (D50) value measured by the laser diffraction/scattering method. By having the average particle size of the ceramic raw material powder within the above range, it is possible to obtain a sintered body with increased structural strength and stability after firing and reduced possibility of collapse.
 メッシュ状部位の第1線条部層および第2線条部層の前駆体である成形体を作成するための原料ペーストの媒体としては、通常、水が用いられる。水以外の媒体としては、アルコール、アセトンおよび酢酸エチルなども用いられる。これらの媒体を2種類以上混合してもよい。原料ペーストにおける媒体の質量割合は、ペースト全体の質量に対して、通常10質量%以上60質量%以下であってよく、15質量%以上55質量%以下であることが好ましい。 Water is usually used as the medium of the raw material paste for producing a molded body that is a precursor of the first and second striated layers of the mesh-like portion. As a medium other than water, alcohol, acetone, ethyl acetate, etc. can also be used. Two or more of these media may be mixed. The mass ratio of the medium in the raw material paste may usually be 10% by mass or more and 60% by mass or less, and preferably 15% by mass or more and 55% by mass or less, based on the mass of the entire paste.
 メッシュ状部位の第1線条部層および第2線条部層の前駆体である成形体を作成するための原料ペーストは、任意選択で公知のいずれかの焼結助剤を適当量で含んでいてよい。また、原料ペーストは公知のいずれかの結合剤を含んでよい。原料ペーストにおける結合剤の質量割合は、原料ペーストの全質量に対して、例えば0質量%以上40質量%以下であってよく、1質量%以上40質量%以下であることが好ましい。 The raw material paste for producing the molded body that is the precursor of the first and second striated layers of the mesh-like portion may optionally contain an appropriate amount of any known sintering aid. The raw material paste may also contain any known binder. The mass proportion of the binder in the raw material paste may be, for example, 0% by mass or more and 40% by mass or less, and is preferably 1% by mass or more and 40% by mass or less, relative to the total mass of the raw material paste.
 原料ペーストの粘度は、線条塗工体の塗布時の温度において高粘度であることが、線条塗工体を首尾よく製造し得る点から好ましい。原料ペーストの粘度は、特に限定されないが、塗布時の温度(典型的には約25℃等の室温)において1.5MPa・s以上5.0MPa・s以下であることが好ましい。ここでの原料ペーストの粘度は、コーンプレート型回転式粘度計またはレオメーターを用いて、回転数0.3rpmにて測定開始後4分時の測定値を指す。原料ペーストには、粘性調整剤として、公知のいずれかの増粘剤、凝集剤、チクソトロピック剤などを含有させることができる。 It is preferable that the viscosity of the raw material paste is high at the temperature when the linear coated body is applied, in order to be able to successfully manufacture the linear coated body. The viscosity of the raw material paste is not particularly limited, but is preferably 1.5 MPa·s or more and 5.0 MPa·s or less at the temperature when it is applied (typically room temperature, such as about 25°C). The viscosity of the raw material paste here refers to the measured value 4 minutes after the start of measurement at a rotation speed of 0.3 rpm using a cone-plate type rotational viscometer or rheometer. The raw material paste may contain any known thickener, flocculating agent, thixotropic agent, etc. as a viscosity adjusting agent.
 メッシュ状部位の第1線条部層および第2線条部層の前駆体である成形体を得るための吐出装置からの吐出量を安定させるため、原料ペーストは、例えば、公知のいずれかの可塑剤、潤滑剤、分散剤、沈降抑制剤、pH調整剤などを含んでもよい。 In order to stabilize the amount of material discharged from the discharge device to obtain a molded body that is a precursor of the first and second striated layers of the mesh-like portion, the raw material paste may contain, for example, any known plasticizer, lubricant, dispersant, settling inhibitor, pH adjuster, etc.
 このようにして得られた原料ペーストを吐出装置から平坦な基板上に吐出することによって、所与の間隔で配置された各条が一方向に延伸された複数条の第1線条塗工体を形成する。第1線条塗工体はメッシュ状部位の第2線条部に対応するものである。
 吐出装置としては、例えば小型押し出し機や印刷機などの公知の種々の装置を用いることができる。これらの吐出装置は、典型的に、ノズルを有するディスペンサを備えていてよい。第1線条塗工体が吐出された後、第1線条塗工体に含まれている媒体を除去して乾燥させ、粘度を高める操作を行うことができる。媒体除去操作後の第1線条塗工体における媒体の割合は、好ましくは50質量%以下、より好ましくは30質量%以下にまで低減されていてよい。
The raw material paste thus obtained is discharged from a discharge device onto a flat substrate to form a first linear coated body having a plurality of stripes arranged at given intervals and each stripe extending in one direction. The first linear coated body corresponds to the second linear portion of the mesh-like portion.
As the discharge device, various known devices such as a small extruder or a printer can be used. These discharge devices may typically include a dispenser having a nozzle. After the first striated coated body is discharged, an operation can be performed to remove the medium contained in the first striated coated body, dry it, and increase the viscosity. The ratio of the medium in the first striated coated body after the medium removal operation may be reduced to preferably 50% by mass or less, more preferably 30% by mass or less.
 次いで原料ペーストを用いて、第1線条塗工体の各条の上に接してこれと交差するように所与の間隔で配置された、各条が一方向に延伸された複数条の第2線条塗工体を形成する。第2線条塗工体は、メッシュ状部位の第1線条部に対応するものである。第2線条塗工体を形成するための原料ペーストは、第1線条塗工体を形成するための原料ペーストと同一であっても異なっていてよいが、線条塗工体形成の効率性、ならびに、生産するセラミックスシート焼結体の構造および物性の一体性の観点から、同一であることがより好ましい。 Then, using the raw material paste, a second filamentary coated body is formed, each filament extending in one direction and arranged at a given interval so as to contact and intersect with each filament of the first filamentary coated body. The second filamentary coated body corresponds to the first filamentary portion of the mesh-like portion. The raw material paste for forming the second filamentary coated body may be the same as or different from the raw material paste for forming the first filamentary coated body, but it is more preferable that they are the same from the viewpoints of efficiency in forming the filamentary coated body and integrity of the structure and physical properties of the ceramic sheet sintered body to be produced.
 成形体として形成される複数条の第1線条塗工体および複数条の第2線条塗工体の具体的な形状は、上述した種々のメッシュ状部位の所望の形状に適合させるように構築することができる。 The specific shapes of the first multiple filamentary coated body and the second multiple filamentary coated body formed as a molded body can be constructed to match the desired shapes of the various mesh-like portions described above.
 追加の一実施形態において、原料ペーストを用いて、第2線条塗工体の各条の上に接して第1線条塗工体および第2線条塗工体と交差するように所与の間隔で配置された、各条が一方向に延伸された複数条の第3線条塗工体を任意選択的に形成してもよい。任意選択の第3線条塗工体を形成するための原料ペーストは、第1/第2線条塗工体を形成するための原料ペーストと同一であっても異なっていてよいが、線条塗工体形成の効率性、ならびに、生産するメッシュ状部位の構造および物性の一体性の観点から、同一であることがより好ましい。 In an additional embodiment, the raw material paste may be used to optionally form a third filamentary coating body having multiple stripes that are arranged at given intervals so as to contact each stripe of the second filamentary coating body and intersect with the first and second filamentary coating bodies, each stripe being stretched in one direction. The raw material paste for forming the optional third filamentary coating body may be the same as or different from the raw material paste for forming the first and second filamentary coating bodies, but it is more preferable that they are the same from the viewpoints of efficiency in forming the filamentary coating body and integrity of the structure and physical properties of the mesh-like portion produced.
 このようにして得られた複数条の第1線条塗工体および複数条の第2線条塗工体を含む成形体を基板(成形体の形成作業台)から剥離して焼成治具(焼成炉)内に配置し、焼成することによって、目的とするメッシュ状部位が得られる。焼成により、複数条の第1線条部で構成される第1線条部層、および複数条の第2線条部で構成される第2線条部層を含むメッシュ状部位は、通常、各部材の接着剤による物理的結合を含まない一体的な構造物である焼結体として構築される。 The molded body thus obtained, including the multiple first filamentary coated bodies and the multiple second filamentary coated bodies, is peeled off from the substrate (the workbench on which the molded bodies are formed) and placed in a firing jig (firing furnace), where it is fired to obtain the desired mesh-like portion. Through firing, the mesh-like portion including the first filamentary layer made up of the multiple first filamentary portions and the second filamentary layer made up of the multiple second filamentary portions is usually constructed as a sintered body, which is an integrated structure that does not involve physical bonding of the individual components by adhesive.
 メッシュ状部位を得るための焼成プロセスは、必要に応じて、大気雰囲気中(大気圧下)で行ってもよいし、例えば窒素などの不活性ガスによる加圧下にて行ってもよい。焼成温度は、セラミックス素材の原料粉の種類に応じて適切な温度を選択すればよい。焼成時間に関しても同様である。焼成温度の非限定的な例としては、500℃以上、800℃以上、または1000℃以上であってよく、4000℃以下、3500℃以下、または3000℃以下であってよい。焼成時間の非限定的な例としては、30分以上、1時間以上または2時間以上であってよく、24時間以下、12時間以下、または6時間以下であってよい。 The firing process to obtain the mesh-like portion may be carried out in an air atmosphere (atmospheric pressure) as necessary, or may be carried out under pressure with an inert gas such as nitrogen. The firing temperature may be selected appropriately depending on the type of raw powder of the ceramic material. The same applies to the firing time. Non-limiting examples of the firing temperature may be 500°C or more, 800°C or more, or 1000°C or more, and 4000°C or less, 3500°C or less, or 3000°C or less. Non-limiting examples of the firing time may be 30 minutes or more, 1 hour or more, or 2 hours or more, and 24 hours or less, 12 hours or less, or 6 hours or less.
 セッターの一部または全部がメッシュ状部位を含むセラミックスシートである実施形態では、メッシュ状部位において、第2線条部層の第1線条部層に対する接面がセッターの敷板に対する近接面Sをなし、第1線条部層を構成する第1線条部がセッターの凸部をなすから、凸部を別途形成する必要はない。 In an embodiment in which part or all of the setter is a ceramic sheet including a mesh-like portion, the contact surface of the second striated portion layer with the first striated portion layer in the mesh-like portion forms the adjacent surface S with respect to the base plate of the setter, and the first striated portion constituting the first striated portion layer forms the convex portion of the setter, so there is no need to form the convex portion separately.
 メッシュ状部位を含むセラミックスシート以外のセッターにおいては、セッターのセラミックスシート表面の平坦面上に、長手方向に略均一な断面を備える凸部を別途形成する必要がある。この場合、セラミックスシート(凸部以外の基部)とその表面の平坦面上に設けられる凸部とは、同じ原料(すなわち同じセラミックス原料粉および添加剤の混合物を含む原料)から形成されていても、異なる原料から形成されていてもよい。セラミックスシート(凸部以外の基部)とその表面の平坦面上に設けられる凸部とは、焼成時の加熱・冷却の熱履歴(膨張・収縮の繰り返し)による接合強度の低下およびこれに起因する凸部のシートからの剥離を抑制する観点から、同じ原料から形成されていることがより好ましい。 In setters other than ceramic sheets that include mesh-like portions, it is necessary to separately form convex portions with a substantially uniform cross section in the longitudinal direction on the flat surface of the ceramic sheet surface of the setter. In this case, the ceramic sheet (base portion other than the convex portions) and the convex portions provided on the flat surface of the surface may be formed from the same raw material (i.e., raw material containing the same mixture of ceramic raw material powder and additives) or from different raw materials. It is more preferable that the ceramic sheet (base portion other than the convex portions) and the convex portions provided on the flat surface of the surface of the ceramic sheet be formed from the same raw material, from the viewpoint of preventing a decrease in bonding strength due to the thermal history of heating and cooling during firing (repeated expansion and contraction) and the resulting peeling of the convex portions from the sheet.
 例えば、表面の平坦面上に長手方向に略均一な断面を備える凸部が別途形成されたセッターのセラミックスシートは、プレス型、鋳込み成形、振動成形などの公知のいずれかの成型方法で、一体の成形体を形成した後に、メッシュ状部位の焼成プロセスについて上述したものと同様の条件にて焼成することによって製造することができる。
 別法として、表面の平坦面上に長手方向に略均一な断面を備える凸部が別途形成されたセッターのセラミックスシートの製造のため、メッシュ状部位を含むセラミックスシートを製造する際に上記原料ペーストを吐出装置から平坦な基板上に吐出して第1線条塗工体を形成し次いで焼成するのと同様の手法を採用することができる。あるいは、表面の平坦面上に長手方向に略均一な断面を備える凸部が別途形成されたセッターのセラミックスシートは、セラミックスシート(凸部以外)およびその表面の平坦面上に設けられる凸部のそれぞれの成形体の形成および焼成を個別に行った後、セラミックスシート(凸部以外)の焼結体の上面の所定の領域に凸部の焼結物を、公知のいずれかのセラミックス用接着剤などで接合することもできる。このようなセラミックス用接着剤の非限定的な例としては、ポリイミド系樹脂、エポキシ系樹脂またはポリアミドイミド系樹脂を含む接着剤組成物や、アルミナなどの耐火性セラミックスおよび無機ポリマーを主成分とする無機系接着剤組成物(例えば、東亜合成株式会社製「アロンセラミック」等)などを挙げることができる。
 また、更なる別法として、表面の平坦面上に長手方向に略均一な断面を備える凸部が別途形成されたセッターのセラミックスシートは、セラミックスシート(凸部以外)の成形体を形成した後、あるいはこの成形体を焼成して焼結体を製造した後に、その表面に機械加工を施して凸部を形成することによって得ることもできる。このような機械加工の例としては、特に限定されないが、ドリルやヤスリなどの刃物工具を用いた切削、研磨加工等を挙げることができる。
For example, a setter ceramic sheet having a convex portion having a substantially uniform cross section in the longitudinal direction formed separately on the flat surface of the front surface can be manufactured by forming an integral molded body using any of the known molding methods such as press molding, slip casting, vibration molding, etc., and then firing the body under conditions similar to those described above for the firing process of the mesh-like portion.
Alternatively, for the manufacture of a ceramic sheet for a setter in which a convex portion having a substantially uniform cross section in the longitudinal direction is separately formed on the flat surface of the front surface, a similar method to that used for manufacturing a ceramic sheet including a mesh-like portion can be adopted, in which the raw material paste is discharged from a discharge device onto a flat substrate to form a first filament coating body and then fired. Alternatively, for a ceramic sheet for a setter in which a convex portion having a substantially uniform cross section in the longitudinal direction is separately formed on the flat surface of the front surface, the ceramic sheet (other than the convex portion) and the convex portion provided on the flat surface of the front surface are separately formed and fired, and then the sintered product of the convex portion can be bonded to a predetermined region on the upper surface of the sintered product of the ceramic sheet (other than the convex portion) with any known ceramic adhesive. Non-limiting examples of such ceramic adhesives include adhesive compositions containing polyimide resins, epoxy resins, or polyamideimide resins, and inorganic adhesive compositions mainly composed of fire-resistant ceramics such as alumina and inorganic polymers (for example, "Aron Ceramic" manufactured by Toa Gosei Co., Ltd.).
As another alternative method, the ceramic sheet of the setter having a convex portion having a substantially uniform cross section in the longitudinal direction formed separately on the flat surface of the front surface can be obtained by forming a molded body of the ceramic sheet (other than the convex portion) or by sintering this molded body to produce a sintered body, and then machining the surface to form the convex portion. Examples of such machining include, but are not limited to, cutting and polishing using cutting tools such as drills and files.
 本発明に係る焼成治具を構成する敷板の製造方法は、セッターに対する近接面の一部に上記要件を満たす条溝部を含む敷板を製造することが可能である限りは、特に限定されない。
 敷板を製造するためのセラミックス原料粉および添加剤は、セッターについて上述された事項の中から同様に適宜選択され得る。例えば、敷板のセラミックス原料粉は、アルミナ(Al)、ジルコニア(ZrO)、酸化マグネシウム(MgO)、ムライト(3Al-2SiO)、炭化ケイ素(SiC)、窒化ケイ素(Si)、窒化アルミニウム(AlN)、炭化ホウ素(BC)、コージェライト(MgO/Al/SiO)、チタン酸アルミニウム(AlTiO)、チタン酸マグネシウム(MgTiO)、二硼化チタン(TiB)などの1種または2種以上の組み合わせであってよい。
The method for manufacturing the base plate constituting the firing jig according to the present invention is not particularly limited, so long as it is possible to manufacture a base plate including a groove portion satisfying the above requirements on a portion of the surface adjacent to the setter.
The ceramic raw material powder and additives for producing the base plate can be appropriately selected from the items described above for the setter. For example, the ceramic raw material powder for the base plate can be one or a combination of two or more of alumina (Al 2 O 3 ), zirconia (ZrO 2 ), magnesium oxide (MgO), mullite (3Al 2 O 3 -2SiO 2 ), silicon carbide (SiC), silicon nitride (Si 3 N 4 ), aluminum nitride (AlN), boron carbide (B 4 C), cordierite (MgO/Al 2 O 3 /SiO 2 ), aluminum titanate (Al 2 TiO 5 ), magnesium titanate (MgTiO 3 ), titanium diboride (TiB 2 ), etc.
 条溝部を含む敷板は、プレス型、鋳込み成形、振動成形などの公知のいずれかの成型方法で、表面に所望の断面形状および長手方向の長さを有する条溝が穿たれた一体の成形体を形成した後に、メッシュ状部位の焼成プロセスについて上述したものと同様の条件にて焼成することによって製造することができる。
 別法として、条溝部を含む敷板は、敷板の基材部(条溝を有しないもの)の成形体を形成した後、あるいは敷板の基材部の成形体を焼成して焼結体を製造した後に、その表面に機械加工を施して条溝を形成することによって得ることもできる。このような機械加工の例としては、特に限定されないが、ドリルやヤスリなどの刃物工具を用いた切削、研磨加工等を挙げることができる。
The base plate including the groove portion can be manufactured by forming an integral molded body having grooves with the desired cross-sectional shape and longitudinal length on its surface using any known molding method such as press molding, cast molding, vibration molding, etc., and then firing the body under conditions similar to those described above for the firing process of the mesh-like portion.
Alternatively, the floor plate including the grooves can be obtained by forming a molded body of the base plate (one without grooves) or by sintering the molded body of the base plate to produce a sintered body, and then machining the surface to form the grooves. Examples of such machining include, but are not limited to, cutting and polishing using cutting tools such as drills and files.
メッシュ状セラミックスシート1のセッターの製造
(1)線条塗工体形成用のペーストの調製
 平均粒径0.8μmの3モル%イットリア添加部分安定化ジルコニア粉65.3部と、水系結合剤としてヒドロキシプロピルメチルセルロース(平均重合度:30万g/mol)5.0部と、可塑剤として、グリセリン2.5部と、ポリカルボン酸系分散剤(分子量12000)1.1部と、水26.1部とを混合し、脱泡してペーストを調製した。ペーストの粘度は25℃において2.3MPa・sであった。
(2)線条塗工体の形成
 前記のペーストを原料とし、直径4.0mmの断面円形ノズルを有するディスペンサを用いて樹脂基板上に線条第1塗工体を形成した。次いでドライヤーを用いて線条第1塗工体に熱風を吹き付け水を除去して線条第1塗工体を乾燥させた。乾燥後の線条第1塗工体の水の含有量は10%であった。引き続き線条第1塗工体に交差する線条第2塗工体を形成した。両線条塗工体の交差角度は90度とした。ドライヤーを用いて線条第2塗工体に熱風を吹き付け、水を除去して線条第2塗工体を乾燥させた。乾燥後の線条第2塗工体の水の含有量は8%であった。これらの操作によって、垂直に交差した第1線条体(線条第2塗工体の乾燥物)と第2線条体(線条第1塗工体の乾燥物)からなる格子状前駆体を得た。
(3)焼成工程
 乾燥後の格子状前駆体を樹脂基板から剥離した後、大気焼成炉内に載置した。この焼成炉内で脱脂および焼成を行って、ジルコニア製のメッシュ状セラミックスシート1を得た。焼成温度は1450℃とし、焼成時間は3時間とした。メッシュ状セラミックスシート1においては、第1線条部(断面形状は略円形である)と第2線条部(断面形状は略円形の一部が直線状に切断された形状)とは、それらの交差部において点接触していた。得られたメッシュ状ジルコニア製シート1における第1線条部の最大幅員(平面視における設計方向である長手方向に対して垂直方向の長さ、すなわち第1線条部の長手方向に垂直な断面の、セッターの敷板に対する近接面に平行な方向の最大幅員)Wcは4.0mmであった。また第1線条部の断面形状は略円形であったから、第1線条部の最大高さ(第1線条部の長手方向に垂直な断面の、セッターの敷板に対する近接面に垂直な方向の最大高さ)Hcは、Wcと同じ4.0mmであると見積もられた。第1線条部間の間隔は0.1mmであった。すなわち、メッシュ状セラミックスシート1における貫通孔の寸法(目開き寸法)は0.1mm□であり、貫通孔の面積は0.01mmであった。メッシュ状セラミックスシート1における各線条部と辺部との角度は45°であり、第1線条部と第2線条部との交差角は90°であった。メッシュ状セラミックスシート1の外形寸法は、縦300mm×横300mmであった。従って、本例において、セッターであるメッシュ状セラミックスシート1の敷板(後述)に対する近接面の輪郭内体積bは90000mmであった(セッターの敷板への戴置の際に近接面Sを垂直視するとき、敷板の輪郭からはみ出る領域が生じないように後述の敷板を設計した)。メッシュ状セラミックスシート1の第1線条部の最大幅員Wcに対する第1線条部の長手方向の両端部間の長さLc(ここではシートの縦横寸法と同一の長さをもって代表的な両端部間の長さと定義する)のアスペクト比Lc/Wcは75であり、第1線条部の最大高さHcに対する第1線条部の最大幅員Wcの比率Wc/Hcは1.0と見積もられた。また、メッシュ状セラミックスシート1が敷板(後述)に戴置されるときに、全ての凸部(第1線条部)が敷板(後述)の条溝部に収容され得るように設計されていることを前提とした場合、条溝部に収容される凸部の投影面積の合計aは、デジタルマイクロスコープ(キーエンス製、商品名「VHX-5000」)を用いた画像解析により69600mmであった。
 本セッターの縦横の外形寸法およびこれによって決定されるセッターの輪郭内面積b、ならびに、第1線条部の最大幅員Wc(と最大高さHc)、第1線条部間の間隔、およびこれらを調整することによって決定される凸部の投影面積の合計aを表1に示す。
Manufacturing of a setter for a mesh-like ceramic sheet 1 (1) Preparation of a paste for forming a filamentary coating body 65.3 parts of 3 mol% yttria-added partially stabilized zirconia powder with an average particle size of 0.8 μm, 5.0 parts of hydroxypropylmethylcellulose (average degree of polymerization: 300,000 g/mol) as an aqueous binder, 2.5 parts of glycerin as a plasticizer, 1.1 parts of a polycarboxylic acid-based dispersant (molecular weight 12,000), and 26.1 parts of water were mixed and degassed to prepare a paste. The viscosity of the paste was 2.3 MPa·s at 25°C.
(2) Formation of a linear coated body Using the above paste as a raw material, a first linear coated body was formed on a resin substrate using a dispenser having a circular nozzle with a diameter of 4.0 mm. Next, hot air was blown onto the first linear coated body using a dryer to remove water and dry the first linear coated body. The water content of the first linear coated body after drying was 10%. Subsequently, a second linear coated body intersecting the first linear coated body was formed. The intersection angle of both linear coated bodies was 90 degrees. Hot air was blown onto the second linear coated body using a dryer to remove water and dry the second linear coated body. The water content of the second linear coated body after drying was 8%. Through these operations, a lattice-shaped precursor consisting of a first linear body (dried product of the second linear coated body) and a second linear body (dried product of the first linear coated body) perpendicularly intersecting each other was obtained.
(3) Firing process The dried lattice-shaped precursor was peeled off from the resin substrate and then placed in an air firing furnace. Degreasing and firing were performed in this firing furnace to obtain a mesh-shaped ceramic sheet 1 made of zirconia. The firing temperature was 1450°C, and the firing time was 3 hours. In the mesh-shaped ceramic sheet 1, the first linear portion (having a substantially circular cross-sectional shape) and the second linear portion (having a cross-sectional shape in which a portion of the substantially circular shape is cut linearly) were in point contact at their intersections. The maximum width Wc of the first linear portion in the obtained mesh-shaped zirconia sheet 1 (length in a direction perpendicular to the longitudinal direction, which is the design direction in a plan view, i.e., the maximum width Wc of the cross section perpendicular to the longitudinal direction of the first linear portion in a direction parallel to the adjacent surface of the setter's floor plate) was 4.0 mm. In addition, since the cross-sectional shape of the first filamentary portion was approximately circular, the maximum height Hc of the first filamentary portion (the maximum height of the cross section perpendicular to the longitudinal direction of the first filamentary portion in the direction perpendicular to the adjacent surface of the setter to the floor plate) was estimated to be 4.0 mm, the same as Wc. The interval between the first filamentary portions was 0.1 mm. That is, the size (opening size) of the through hole in the mesh-like ceramic sheet 1 was 0.1 mm□, and the area of the through hole was 0.01 mm2. The angle between each filamentary portion and the side portion in the mesh-like ceramic sheet 1 was 45°, and the intersection angle between the first filamentary portion and the second filamentary portion was 90°. The outer dimensions of the mesh-like ceramic sheet 1 were 300 mm long x 300 mm wide. Therefore, in this example, the volume b within the contour of the adjacent surface of the mesh-like ceramic sheet 1 relative to the base plate (described later) serving as the setter was 90,000 mm2 (the base plate described later was designed so that when the adjacent surface S is viewed vertically when the setter is placed on the base plate, no area protrudes from the contour of the base plate). The aspect ratio Lc/Wc of the length Lc between both ends of the first filamentary portion in the longitudinal direction to the maximum width Wc of the first filamentary portion of the mesh-like ceramic sheet 1 (here, the length is defined as a representative length between both ends that is the same as the length and width of the sheet) was 75, and the ratio Wc/Hc of the maximum width Wc of the first filamentary portion to the maximum height Hc of the first filamentary portion was estimated to be 1.0. In addition, assuming that the mesh-like ceramic sheet 1 is designed so that all of the convex portions (first linear portions) can be accommodated in the groove portions of the base plate (described later) when the mesh-like ceramic sheet 1 is placed on the base plate (described later), the total projected area a of the convex portions accommodated in the groove portions was 69,600 mm2 as determined by image analysis using a digital microscope (manufactured by Keyence, product name "VHX-5000").
Table 1 shows the length and width external dimensions of this setter and the outline inner area b of the setter determined thereby, as well as the maximum width Wc (and maximum height Hc) of the first filamentary portions, the spacing between the first filamentary portions, and the total projected area a of the convex portions determined by adjusting these.
メッシュ状セラミックスシート2~4および6~8のセッター、ならびに比較用セラミックスシート9のセッターの製造
 セッターの縦横の外形寸法およびこれによって決定されるセッターの輪郭内面積b、ならびに、第1線条部の最大幅員Wc、第1線条部間の間隔、およびこれらを調整することによって決定される凸部の投影面積の合計aを表1に示すように変更した以外は、セッター用メッシュ状セラミックスシート1と同様に、セラミックスシート2~4および6~8ならびに比較用セラミックスシート9のセッターを製造した。
 これらのセッターの縦横の外形寸法およびこれによって決定されるセッターの輪郭内面積b、ならびに、第1線条部の最大幅員Wc、第1線条部間の間隔、およびこれらを調整することによって決定される凸部の投影面積の合計aを表1に示す。
Manufacturing of setters for mesh-like ceramic sheets 2 to 4 and 6 to 8, and setter for comparative ceramic sheet 9 Setters for ceramic sheets 2 to 4 and 6 to 8, and comparative ceramic sheet 9 were manufactured in the same manner as for mesh-like ceramic sheet 1 for setters, except that the length and width external dimensions of the setter and the outline inner area b of the setter determined thereby, as well as the maximum width Wc of the first filamentary portion, the spacing between the first filamentary portions, and the total projected area a of the convex portions determined by adjusting these were changed as shown in Table 1.
Table 1 shows the vertical and horizontal external dimensions of these setters and the outline inner area b of the setters determined thereby, as well as the maximum width Wc of the first filamentary portions, the spacing between the first filamentary portions, and the total projected area a of the convex portions determined by adjusting these.
セラミックスシート5のセッターの製造
 上記セラミックスシート1についての線条塗工体形成用のペーストと同一組成の原料を用いて、縦寸法150mm×横寸法150mm(輪郭内面積b=22500mm)のセラミックス成形体を用意した。このセラミックス成形体の表面の平坦面上に、直径1.0mmの断面円形ノズルを有するディスペンサを用いて、同原料で148mmの間隔を空けて2本の線条塗工体を形成し、次いで上記セラミックスシート1と同一条件にて焼成工程を行い、セラミックスシート5のセッターを得た。
 この線条塗工体から得られたセッターの凸部の長手方向に垂直な断面の、セッターの敷板に対する近接面に平行な方向の最大幅員Wcは1.0mmであった。凸部の断面形状は略円形の一部がシートの平坦面により直線状に切断された形状であった。凸部の最大高さ(凸部の長手方向に垂直な断面の、セッターの敷板に対する近接面に垂直な方向の最大高さ)Hcは、0.5mmと見積もられた。また、セラミックスシート5の凸部の最大幅員Wcに対する凸部の長手方向の両端部間の長さLcのアスペクト比Lc/Wcは150であり、凸部の最大高さHcに対する凸部の最大幅員Wcの比率Wc/Hcは2.0と見積もられた。
 本セッターの縦横の外形寸法およびこれによって決定されるセッターの輪郭内面積b、ならびに、凸部の最大幅員Wc、凸部間の間隔、およびこれらを調整することによって決定される凸部の投影面積の合計aを表1に示す。
A ceramic molded body having a length of 150 mm and a width of 150 mm (inner contour area b = 22,500 mm2 ) was prepared using raw materials having the same composition as the paste for forming the linear coating body for the ceramic sheet 1. On the flat surface of the front surface of this ceramic molded body, two linear coating bodies were formed with the same raw materials at an interval of 148 mm using a dispenser having a circular nozzle with a diameter of 1.0 mm, and then a firing process was carried out under the same conditions as for the ceramic sheet 1, to obtain a setter for ceramic sheet 5.
The maximum width Wc of the cross section perpendicular to the longitudinal direction of the convex portion of the setter obtained from this linear coating body in the direction parallel to the adjacent surface of the setter to the sole plate was 1.0 mm. The cross-sectional shape of the convex portion was a shape in which a part of an approximately circular shape was cut linearly by the flat surface of the sheet. The maximum height Hc of the convex portion (the maximum height of the cross section perpendicular to the longitudinal direction of the convex portion in the direction perpendicular to the adjacent surface of the setter to the sole plate) was estimated to be 0.5 mm. In addition, the aspect ratio Lc/Wc of the length Lc between both ends of the convex portion in the longitudinal direction to the maximum width Wc of the convex portion of the ceramic sheet 5 was 150, and the ratio Wc/Hc of the maximum width Wc of the convex portion to the maximum height Hc of the convex portion was estimated to be 2.0.
Table 1 shows the vertical and horizontal external dimensions of this setter and the outline inner area b of the setter determined thereby, as well as the maximum width Wc of the convex portions, the spacing between the convex portions, and the total projected area a of the convex portions determined by adjusting these.
Figure JPOXMLDOC01-appb-T000001
Figure JPOXMLDOC01-appb-T000001
敷板1の製造
 原料として、アルミナを65質量部、シリカを35質量部にバインダーとしてポリビニルアルコール(PVA)を含む混合材料を用いて前駆体となる成形体を得た後、焼成温度1700℃、焼成時間4時間の焼成条件にて矩形状の敷板1を得た。敷板1の周縁全体に高さ3mm、頂部幅7mmの矩形状の周壁部を設け、これによって敷板1の表面に縦300mm×横300mmのメッシュ状セラミックスシート1が戴置されるとき、シートの全体が収まると共に、敷板の全周にわたりシートの端部と矩形状の周壁部との間に3mmの間隙が付与されるようにこれらの寸法取りを行った。
 成形体にプレス型で加工を施すことによって、敷板1の周壁部を除く表面の全体に、セラミックスシート1の第1線条部である凸部の全てが収容され得るようにV字型の条溝部を設けた。この敷板1のV字型のプレス加工は、表2に示すように、敷板の条溝部の深さDg(平均深さDg・av:上述の定義に従い、この場合は任意の10個の深さの平均値)が1.00mmであり、条溝部の最大幅員Wp(条溝部の長手方向に垂直な断面の、敷板のセッターに対する近接面Pに平行な方向の最大幅員)が4.00mmであり、条溝部間の垂直最短距離Ig(この場合は各条溝部間の垂直最短距離の平均値)が0.1mmであり、比率Ig/Dg・avが0.1であるように行った。
A precursor molded body was obtained using a mixed material containing 65 parts by mass of alumina, 35 parts by mass of silica, and polyvinyl alcohol (PVA) as a binder as the raw material for manufacturing the floor plate 1 , and then the material was fired at 1700° C. for 4 hours to obtain a rectangular floor plate 1. A rectangular peripheral wall portion 3 mm high and 7 mm wide at the top was provided around the entire periphery of the floor plate 1, and the dimensions were measured so that when a mesh-like ceramic sheet 1 measuring 300 mm long and 300 mm wide was placed on the surface of the floor plate 1, the entire sheet would fit therein and a gap of 3 mm would be provided between the edge of the sheet and the rectangular peripheral wall portion around the entire periphery of the floor plate.
By processing the molded body with a press mold, a V-shaped groove was provided so that all of the protrusions, which are the first linear portions of the ceramic sheet 1, could be accommodated on the entire surface of the floor plate 1 except for the peripheral wall portion. The V-shaped press processing of the floor plate 1 was performed so that the depth Dg (average depth Dg·av: according to the above definition, in this case the average value of the depth of any 10 pieces) of the floor plate was 1.00 mm, the maximum width Wp of the groove was 4.00 mm (the maximum width of the cross section perpendicular to the longitudinal direction of the groove in the direction parallel to the adjacent surface P of the floor plate relative to the setter), the vertical shortest distance Ig between the grooves was 0.1 mm (in this case the average value of the vertical shortest distance between each groove) and the ratio Ig/Dg·av was 0.1, as shown in Table 2.
 このようにV字型の条溝部が表面に設けられた敷板1および下記の例による敷板に、凸部を有するセラミックスシートが収容される際の敷板の条溝部の深さDgeと、セッターの凸部の長手方向に垂直な断面の、セッターの敷板に対する近接面に垂直な方向の最大高さHceとの関係の概略を図10に例示する。この図にて、7eはセッターの本体(基部)、7Seは、セッターの敷板に対する近接面、8eはセッターの凸部、9eは敷板の本体(基部)、9Peは敷板のセッターに対する近接面、10eは敷板のV字型条溝、Hceはセッターの凸部の最大高さ、Dgeは敷板の条溝部の深さ、Dg’は敷板のセッターに対する近接面9Peから凸部8eの最低位置までの距離を意味する。
 この敷板1および下記の例による敷板のようにV字型の条溝部が表面に設けられている場合には、セッターの凸部8eが敷板の条溝部10eに収容される際、図10に示すように、セッターの凸部8eの垂直方向における最低位置と条溝部10eの垂直方向における最低位置とが接触していない。
 従って、この敷板1については、敷板の条溝部の深さDgeのセッターの凸部の最大高さHceに対する比率Dge/Hceが十分な大きさとなるように、敷板のセッターに対する近接面9Peから凸部8eの最低位置までの距離をDg’のHceに対する比率Dg’/Hceが0.1以上の範囲を満たすように条溝部の設計を行った。Dg’は、凸部の最大高さHceから、セッターの敷板に対する近接面7Seと敷板のセッターに対する近接面9Peとの間(セッターの本体7eと敷板の本体9eの隙間)の垂直距離を引いて算出することができる。
The relationship between the depth Dge of the groove of the sole plate when a ceramic sheet having a convex portion is accommodated in the sole plate 1 having the V-shaped groove portion on the surface thereof and the sole plate according to the following example, and the maximum height Hce of the setter in the direction perpendicular to the adjacent surface of the setter to the sole plate, in a cross section perpendicular to the longitudinal direction of the convex portion of the setter, is illustrated in Fig. 10. In this figure, 7e is the main body (base) of the setter, 7Se is the adjacent surface of the setter to the sole plate, 8e is the convex portion of the setter, 9e is the main body (base) of the sole plate, 9Pe is the adjacent surface of the sole plate to the setter, 10e is the V-shaped groove of the sole plate, Hce is the maximum height of the convex portion of the setter, Dge is the depth of the groove of the sole plate, and Dg' is the distance from the adjacent surface 9Pe of the sole plate to the setter to the lowest position of the convex portion 8e.
When a V-shaped groove portion is provided on the surface, as in this floor plate 1 and the floor plate in the example below, when the convex portion 8e of the setter is accommodated in the groove portion 10e of the floor plate, as shown in Figure 10, the lowest vertical position of the convex portion 8e of the setter and the lowest vertical position of the groove portion 10e are not in contact.
Therefore, for this sole plate 1, the grooves were designed so that the ratio Dge/Hce of the depth Dge of the sole plate to the maximum height Hce of the convex part of the setter is sufficiently large, and the ratio Dg'/Hce of the distance from the proximal surface 9Pe of the sole plate to the setter to the lowest position of the convex part 8e to Hce is in the range of 0.1 or more. Dg' can be calculated by subtracting the vertical distance between the proximal surface 7Se of the setter to the sole plate and the proximal surface 9Pe of the sole plate to the setter (the gap between the main body 7e of the setter and the main body 9e of the sole plate) from the maximum height Hce of the convex part.
敷板2~8および比較用敷板9の製造
 セッターであるセラミックスシート2~8および比較用セラミックスシート9のそれぞれの全体が収まると共に、敷板の全周にわたり上記周壁部を設けた矩形状とし、プレス型での加工によって表2に示す形状(深さDg(平均深さDg・av)、最大幅員Wp、垂直最短距離Ig、比率Ig/Dg・av)の条溝部を設けた以外は敷板1と同様に、敷板2~8および比較用敷板9を製造した。
 なお、敷板2~6および比較用敷板9については、敷板1と同様に比率Dg’/Hceが0.1以上の範囲を満たすように条溝部の設計を行った(図10を再度参照)。敷板7および敷板8については、それぞれ、比率Dg’/Hceが0.05以上および0.02以上の範囲を満たすように条溝部の設計を行った。
Plates 2 to 8 and comparative plate 9 were manufactured in the same manner as plate 1, except that the ceramic sheets 2 to 8 and comparative ceramic sheet 9, which are manufacturing setters, were made to fit the entirety of each sheet and had the above-mentioned peripheral wall portion around the entire circumference of the plate, and groove portions of the shape shown in Table 2 (depth Dg (average depth Dg・av), maximum width Wp, shortest vertical distance Ig, ratio Ig/Dg・av) were formed by processing using a press mold.
For plates 2 to 6 and comparative plate 9, the grooves were designed so that the ratio Dg'/Hce was in the range of 0.1 or more, as in plate 1 (see FIG. 10 again). For plates 7 and 8, the grooves were designed so that the ratio Dg'/Hce was in the range of 0.05 or more and 0.02 or more, respectively.
Figure JPOXMLDOC01-appb-T000002
Figure JPOXMLDOC01-appb-T000002
実施例1~8および比較例1:焼成治具による摺動防止性評価
 セッターの上記セラミックスシート1~8および比較用セラミックスシート9を、それらの各々に対応する上記敷板1~8および比較用敷板9の上に、敷板の周壁部を除く表面の全体にシートの凸部の全てが収容されるように戴置し、セッターと敷板とが組み合わせられた実施例1~8および比較例1の焼成治具を構成した。
 実施例1~8および比較例1の焼成治具の各々について、セッターの凸部と敷板の条溝部との関係を表3に示す。
Examples 1 to 8 and Comparative Example 1: Evaluation of anti-slip properties using a firing jig The ceramic sheets 1 to 8 and comparative ceramic sheet 9 of the setter were placed on the corresponding base plates 1 to 8 and comparative base plate 9, respectively, so that all of the convex parts of the sheets were contained on the entire surface except for the peripheral wall parts of the base plates, thereby forming the firing jigs of Examples 1 to 8 and Comparative Example 1 in which the setter and base plates were combined.
For each of the baking jigs of Examples 1 to 8 and Comparative Example 1, the relationship between the convex portion of the setter and the groove portion of the bottom plate is shown in Table 3.
Figure JPOXMLDOC01-appb-T000003
Figure JPOXMLDOC01-appb-T000003
 実施例1~8および比較例1の焼成治具の各々を、下記の敷板傾斜試験および敷板振動試験に供した。 Each of the firing jigs in Examples 1 to 8 and Comparative Example 1 was subjected to the following base plate tilt test and base plate vibration test.
敷板傾斜試験
 上記実施例1~8および比較例1にて得られた敷板およびその上に戴置されたセラミックスシートのセッターの組み合わせからなる焼成治具について、凸部および条溝部の長手方向に対する45°の角度を有する片端部をゆっくりと上昇させていき、セッターが敷板上で摺動を始めた際の敷板の傾き角度(°)を測定し、これを敷板傾斜時のセッターの移動開始角度と定義した。本試験の角度測定機器として、アイリス株式会社製の商品名「アズワン」型番BB01Bの角度計を用いた。
 敷板傾斜時のセッターの移動開始角度の評価基準は、以下のとおりとした。
 AA(最良):60°以上
 A(良):40°以上60°未満
 B(可):20°以上40°未満
 C(不可):20°未満
Plate inclination test For the firing tool consisting of the plate obtained in Examples 1 to 8 and Comparative Example 1 and the ceramic sheet setter placed on it, one end having an angle of 45° with respect to the longitudinal direction of the convex portion and the groove portion was slowly raised, and the inclination angle (°) of the plate was measured when the setter started to slide on the plate, and this was defined as the start angle of the setter's movement when the plate was inclined. As an angle measuring device for this test, a goniometer with the product name "AS ONE" model number BB01B manufactured by Iris Corporation was used.
The evaluation criteria for the setter's movement start angle when the floor plate was inclined were as follows:
AA (best): 60° or more A (good): 40° or more and less than 60° B (acceptable): 20° or more and less than 40° C (unacceptable): Less than 20°
敷板振動試験
 上記実施例1~8および比較例1にて得られた敷板およびその上に戴置されたセラミックスシートのセッターの組み合わせからなる焼成治具を振動試験機にセットし、レベル10の強度で振動させ、セッターが敷板上で3mm摺動するまでの時間(秒)を測定し、これを敷板振動時のセッターの移動開始時間(セッター保持時間)と定義した。60Hzの振動試験機として、SINFONIA TECHNOLOGY社製の商品名「VIBRATORY PACKER,TYPE VP-40」を用いた。
 敷板振動時のセッターの移動開始時間の評価基準は、以下のとおりとした。
 AA(最良):50秒以上以上
 A(良):30秒以上50秒未満
 B(可):10秒以上30秒未満
 C(不可):10秒未満
Plate Vibration Test The firing jig consisting of the plate obtained in Examples 1 to 8 and Comparative Example 1 and the ceramic sheet setter placed thereon was set in a vibration tester and vibrated at a level of 10. The time (seconds) until the setter slid 3 mm on the plate was measured and defined as the time when the setter started to move when the plate was vibrating (setter retention time). A 60 Hz vibration tester, manufactured by SINFONIA TECHNOLOGY under the trade name "VIBRATORY PACKER, TYPE VP-40", was used.
The evaluation criteria for the time when the setter started to move when the base plate was vibrated were as follows:
AA (best): 50 seconds or more A (good): 30 seconds or more but less than 50 seconds B (passable): 10 seconds or more but less than 30 seconds C (unacceptable): Less than 10 seconds
 上記実施例1~8および比較例1の各々について、敷板傾斜時のセッターの移動開始角度および敷板振動時のセッターの移動開始時間ならびにこれらの評価結果を表4に示す。 For each of the above Examples 1 to 8 and Comparative Example 1, the setter start angle when the floor plate is tilted and the time when the setter start moving when the floor plate is vibrated, as well as the evaluation results, are shown in Table 4.
Figure JPOXMLDOC01-appb-T000004
Figure JPOXMLDOC01-appb-T000004
 これらの結果から、本発明に係る焼成治具によれば、セッターの輪郭内面積に対する凸部の投影面積の比率を特定範囲内に制御することにより、セッターの敷板上での摺動を十分に防止することが可能になることが分かった。
 また、セッターの凸部の最大高さHcに対する凸部が収容される条溝部の深さDgの比率を特定範囲内に制御することによって、摺動防止効果を更に高めることが可能になることも分かった。
From these results, it was found that with the firing jig of the present invention, it is possible to sufficiently prevent the setter from sliding on the base plate by controlling the ratio of the projected area of the convex portion to the inner contour area of the setter within a specific range.
It was also found that the anti-slip effect can be further improved by controlling the ratio of the depth Dg of the groove portion in which the convex portion is accommodated to the maximum height Hc of the convex portion of the setter within a specific range.
 なお、本発明に包含され得る諸態様または諸実施形態は、以下のとおり要約される。
[1].
 セッターと、このセッターが戴置される敷板とからなる焼成治具であって、
 前記セッターは、前記敷板に対する近接面Sの一部に、長手方向に略均一な断面を備える1つまたは複数の線条をなす凸部を含み、
 前記敷板は、前記セッターに対する近接面Pの一部に、長手方向に略均一な断面を備える1つまたは複数の条溝部を含み、
 前記セッターが前記敷板に戴置されるとき、前記セッターの凸部の少なくとも1つが前記敷板の条溝部の少なくとも1つに収容されるように、前記凸部および前記条溝部が形成されており、
 ここで、
 前記セッターの近接面Sの輪郭内面積(ただし、前記セッターの前記敷板への戴置の際に、前記近接面Sを垂直視するとき、敷板の輪郭からはみ出る領域の面積を除く)をbとし、
 前記セッターが前記敷板に戴置されるときに、前記条溝部に収容される前記凸部の投影面積(ただし、ここでの投影面積は、前記セッターの近接面Sに平行な面における当該凸部の最大断面積を指す)の合計をaとするとき、
 0.5≦(a/b)*100≦90(式A)の関係を満たす、
 焼成治具。
[2],
 前記セッターの凸部が略平行に2つ以上形成されており、かつ前記敷板の条溝部が略平行に2つ以上形成されており、前記セッターの前記敷板への戴置の際、前記凸部の過半数が前記敷板の条溝部に収容されるように前記凸部および前記条溝部が形成されている、上記[1]項に記載の焼成治具。
[3],
 前記セッターの凸部が3つ以上の場合にはこれらの凸部は略等間隔で形成されており、および/または、前記敷板の条溝部が3つ以上の場合にはこれらの条溝部は略等間隔で形成されている、上記[2]項に記載の焼成治具。
[4],
 前記セッターの凸部の少なくとも1つの長手方向に垂直な断面の前記近接面Sに平行な方向の最大幅員Wcと、前記セッターの前記敷板への戴置の際、この凸部が収容される前記条溝部の長手方向に垂直な断面の前記近接面Pに平行な方向の最大幅員Wpとの割合Wc/Wpが2以下である、上記[1]~[3]項のいずれか1項に記載の焼成治具。
[5],
 前記敷板の条溝部の平均深さ(前記条溝部の長手方向に垂直な断面の前記近接面Pから垂直方向の最低位置までの長さについて各条溝部の平均値を指す)Dg・avに対する、当該条溝部間の垂直最短距離(条溝部が3つ以上形成されている場合は、複数の垂直最短距離の平均値を指す)Igの比率Ig/Dg・avが0.05以上600以下である、上記[2]または[3]項に記載の焼成治具。
[6],
 前記セッターの凸部の少なくとも1つについて、その長手方向に垂直な断面の前記近接面Sに平行な方向の最大幅員Wcに対する、その長手方向の両端部間の長さLcのアスペクト比Lc/Wcが10以上である、上記[1]~[5]項のいずれか1項に記載の焼成治具。
[7],
 前記セッターの凸部の少なくとも1つの長手方向に垂直な断面の前記近接面Sに垂直な方向の最大高さHcに対する、前記セッターの前記敷板への戴置の際、この凸部が収容される前記条溝部の長手方向に垂直な断面の前記近接面Pから垂直方向の最低位置までの深さDgの比率Dg/Hcが0.1以上である、上記[1]~[6]項のいずれか1項に記載の焼成治具。
[8],
 前記セッターの凸部の少なくとも1つの長手方向に垂直な断面の前記近接面Sに垂直な方向の最大高さHcに対する、この凸部の長手方向に垂直な断面の前記近接面Sに平行な方向の最大幅員Wcの比率Wc/Hcが0.3以上4以下である、上記[1]~[7]項のいずれか1項に記載の焼成治具。
[9],
 前記セッターが、その少なくとも一部にメッシュ状セラミックスシートを含み、
 このメッシュ状セラミックスシートは、所与の間隔で配置された各条が一方向に延伸された複数条の第1線条部で構成される第1線条部層、および、前記第1線条部の各条の上に接してこれと交差するように所与の間隔で配置された、各条が一方向に延伸された複数条の第2線条部で構成される第2線条部層を含み、前記第1線条部層と前記第2線条部層とが一体的に形成されているセラミックスシート焼結体であり、
 前記第2線条部層の前記第1線条部層に対する接面が、前記セッターの近接面Sをなしており、前記第1線条部層を構成する第1線条部が、前記セッターの凸部をなしている、
 上記[1]~[8]項のいずれか1項に記載の焼成治具。
Various aspects or embodiments that can be included in the present invention are summarized as follows.
[1]
A firing jig consisting of a setter and a base plate on which the setter is placed,
The setter includes one or more linear protrusions having a substantially uniform cross section in the longitudinal direction on a portion of a surface S adjacent to the base plate,
The base plate includes one or more grooves having a substantially uniform cross section in the longitudinal direction on a portion of a surface P adjacent to the setter,
the protrusions and the grooves are formed so that at least one of the protrusions of the setter is received in at least one of the grooves of the base plate when the setter is placed on the base plate,
here,
The area within the contour of the proximity surface S of the setter (excluding the area of the region that protrudes from the contour of the sole plate when the proximity surface S is viewed vertically when the setter is placed on the sole plate) is b,
When the setter is placed on the base plate, the total projected area of the convex portion accommodated in the groove portion (wherein the projected area here refers to the maximum cross-sectional area of the convex portion in a plane parallel to the adjacent surface S of the setter) is a,
The relationship of 0.5≦(a/b)*100≦90 (Formula A) is satisfied.
Firing fixture.
[2]
The firing jig described in item [1] above, wherein the setter has two or more convex portions formed approximately parallel to each other, and the base plate has two or more groove portions formed approximately parallel to each other, and the convex portions and the groove portions are formed so that when the setter is placed on the base plate, the majority of the convex portions are accommodated in the groove portions of the base plate.
[3]
The firing jig described in item [2] above, wherein when the setter has three or more convex portions, these convex portions are formed at approximately equal intervals, and/or when the base plate has three or more groove portions, these groove portions are formed at approximately equal intervals.
[4]
A firing jig described in any one of items [1] to [3] above, in which the ratio Wc/Wp of the maximum width Wc in a direction parallel to the proximity surface S of a cross section perpendicular to the longitudinal direction of at least one of the convex portions of the setter to the maximum width Wp in a direction parallel to the proximity surface P of a cross section perpendicular to the longitudinal direction of the groove portion in which the convex portion is accommodated when the setter is placed on the base plate is 2 or less.
[5]
The firing jig described in item [2] or [3] above, in which the ratio Ig/Dg・av of the vertical shortest distance Ig between the groove portions (if three or more groove portions are formed, this refers to the average value of multiple vertical shortest distances) to the average depth Dg・av of the groove portions of the base plate (which refers to the average value of each groove portion for the length from the adjacent surface P to the lowest vertical position in a cross section perpendicular to the longitudinal direction of the groove portions) is 0.05 or more and 600 or less.
[6]
The firing tool according to any one of items [1] to [5] above, wherein for at least one of the convex portions of the setter, the aspect ratio Lc/Wc of the length Lc between both ends in the longitudinal direction to the maximum width Wc in a direction parallel to the adjacent surface S of a cross section perpendicular to the longitudinal direction is 10 or more.
[7]
A firing jig described in any one of items [1] to [6] above, wherein the ratio Dg/Hc of the depth Dg from the proximity surface P to the lowest vertical position of a cross section perpendicular to the longitudinal direction of the groove portion in which the convex portion is accommodated when the setter is placed on the base plate to the maximum height Hc in the direction perpendicular to the proximity surface S of at least one of the convex portions of the setter is 0.1 or more.
[8]
A firing jig as described in any one of items [1] to [7] above, wherein the ratio Wc/Hc of the maximum height Hc of at least one of the convex portions of the setter in a direction perpendicular to the longitudinal direction of the convex portion in a direction perpendicular to the adjacent surface S to the maximum width Wc of the cross section perpendicular to the longitudinal direction of the convex portion in a direction parallel to the adjacent surface S is 0.3 or more and 4 or less.
[9]
the setter includes a mesh-like ceramic sheet in at least a portion thereof,
This mesh-like ceramic sheet includes a first linear portion layer composed of a plurality of first linear portions, each of which is arranged at a given interval and extends in one direction, and a second linear portion layer composed of a plurality of second linear portions, each of which is arranged at a given interval so as to be in contact with and intersect with each of the first linear portions, and is a ceramic sheet sintered body in which the first linear portion layer and the second linear portion layer are integrally formed,
A contact surface of the second filamentary portion layer with respect to the first filamentary portion layer forms a proximity surface S of the setter, and a first filamentary portion constituting the first filamentary portion layer forms a convex portion of the setter.
The firing jig according to any one of the above items [1] to [8].
 C:被焼成物
 A:セッター
 B:多段積みで積層された敷板
 M:多段積みの焼成治具(上記符号C、A、B、Mは公知例を示す図1に関する。)
 1:焼成治具(組み合わせ)
 2:メッシュ状セラミックスシートのセッター
 2S:セッターの敷板に対する近接面(図2の紙面裏側)
 3:敷板
 3P:敷板のセッターに対する近接面
 4:敷板の基材部
 5:敷板の周壁部(リブ)
 6:セッターの凸部(図2に図示せず)に対応する敷板の条溝部
 HL:敷板の開口部
 7:セッターの本体(基部)
 7S:セッターの敷板に対する近接面
 8:セッターの凸部
 9:敷板の本体(基部)
 9P:敷板のセッターに対する近接面
 10:敷板の条溝部
 a1:図3中左側の凸部の投影面積
 a2:図3中右側の凸部の投影面積
 Σa:凸部の投影面積aの合計
 b:セッターの敷板に対する近接面の輪郭内の面積
 Wc:セッターの凸部の最大幅員
 Wp:敷板の条溝部の最大幅員
 Dg・av:敷板の条溝部の平均深さ
 Ig:敷板の条溝部間の垂直最短距離
 Lc:セッターの凸部の長手方向の両端部間の長さ
 Hc:セッターの凸部の最大高さ
 Dg:敷板の条溝部の深さ
 11:メッシュ状部位
 12:第1線条部
 13:第2線条部
 7e:セッターの本体(基部)
 7Se:セッターの敷板に対する近接面
 8e:セッターの凸部
 9e:敷板の本体(基部)
 9Pe:敷板のセッターに対する近接面
 10e:敷板の条溝部(V字型条溝)
 Hce:セッターの凸部の最大高さ
 Dge:敷板の条溝部の深さ
 Dg’:敷板のセッターに対する近接面から凸部の最低位置までの距離(上記7e以降は、実施例における概略図を示す。)
C: object to be fired A: setter B: base plates stacked in multiple layers M: multi-layer firing jig (the above symbols C, A, B, and M refer to FIG. 1 showing a known example).
1: Firing jig (combination)
2: Mesh-like ceramic sheet setter 2S: Close surface of the setter to the base plate (back side of the paper in FIG. 2)
3: Sole plate 3P: Surface of sole plate adjacent to setter 4: Base material of sole plate 5: Peripheral wall of sole plate (rib)
6: A groove portion of the bottom plate corresponding to the convex portion of the setter (not shown in FIG. 2) HL: An opening portion of the bottom plate 7: A main body (base) of the setter
7S: surface of the setter adjacent to the sole plate 8: protruding part of the setter 9: main body (base) of the sole plate
9P: surface of the base plate adjacent to the setter 10: grooved portion of the base plate a1: projected area of the convex portion on the left side in FIG. 3 a2: projected area of the convex portion on the right side in FIG. 3 Σa x : total projected area a x of the convex portions b: area within the contour of the surface of the setter adjacent to the base plate Wc: maximum width of the convex portion of the setter Wp: maximum width of the grooved portion of the base plate Dg·av: average depth of the grooved portion of the base plate Ig: shortest vertical distance between the grooved portions of the base plate Lc: length between both ends of the convex portion of the setter in the longitudinal direction Hc: maximum height of the convex portion of the setter Dg: depth of the grooved portion of the base plate 11: mesh-like portion 12: first linear portion 13: second linear portion 7e: main body (base) of the setter
7Se: surface of the setter adjacent to the sole plate 8e: protruding portion of the setter 9e: main body (base) of the sole plate
9Pe: surface of the base plate adjacent to the setter 10e: groove portion of the base plate (V-shaped groove)
Hce: maximum height of the convex part of the setter Dge: depth of the groove part of the sole plate Dg': distance from the surface of the sole plate close to the setter to the lowest position of the convex part (7e and the following are schematic diagrams of the examples).

Claims (9)

  1.  セッターと、このセッターが戴置される敷板とからなる焼成治具であって、
     前記セッターは、前記敷板に対する近接面Sの一部に、長手方向に略均一な断面を備える1つまたは複数の線条をなす凸部を含み、
     前記敷板は、前記セッターに対する近接面Pの一部に、長手方向に略均一な断面を備える1つまたは複数の条溝部を含み、
     前記セッターが前記敷板に戴置されるとき、前記セッターの凸部の少なくとも1つが前記敷板の条溝部の少なくとも1つに収容されるように、前記凸部および前記条溝部が形成されており、
     ここで、
     前記セッターの近接面Sの輪郭内面積(ただし、前記セッターの前記敷板への戴置の際に、前記近接面Sを垂直視するとき、敷板の輪郭からはみ出る領域の面積を除く)をbとし、
     前記セッターが前記敷板に戴置されるときに、前記条溝部に収容される前記凸部の投影面積(ただし、ここでの投影面積は、前記セッターの近接面Sに平行な面における当該凸部の最大断面積を指す)の合計をaとするとき、
     0.5≦(a/b)*100≦90(式A)の関係を満たす、
     焼成治具。
    A firing jig consisting of a setter and a base plate on which the setter is placed,
    The setter includes one or more linear protrusions having a substantially uniform cross section in the longitudinal direction on a portion of a surface S adjacent to the base plate,
    The base plate includes one or more grooves having a substantially uniform cross section in the longitudinal direction on a portion of a surface P adjacent to the setter,
    the protrusions and the grooves are formed so that at least one of the protrusions of the setter is received in at least one of the grooves of the base plate when the setter is placed on the base plate,
    here,
    The area within the contour of the proximity surface S of the setter (excluding the area of the region that protrudes from the contour of the sole plate when the proximity surface S is viewed vertically when the setter is placed on the sole plate) is b,
    When the setter is placed on the base plate, the total projected area of the convex portion accommodated in the groove portion (wherein the projected area here refers to the maximum cross-sectional area of the convex portion in a plane parallel to the adjacent surface S of the setter) is a,
    The relationship of 0.5≦(a/b)*100≦90 (Formula A) is satisfied.
    Firing fixture.
  2.  前記セッターの凸部が略平行に2つ以上形成されており、かつ前記敷板の条溝部が略平行に2つ以上形成されており、前記セッターの前記敷板への戴置の際、前記凸部の過半数が前記敷板の条溝部に収容されるように前記凸部および前記条溝部が形成されている、請求項1に記載の焼成治具。 The firing jig according to claim 1, wherein the setter has two or more generally parallel convex portions, the base plate has two or more generally parallel groove portions, and the convex portions and the groove portions are formed so that the majority of the convex portions are accommodated in the groove portions of the base plate when the setter is placed on the base plate.
  3.  前記セッターの凸部が3つ以上の場合にはこれらの凸部は略等間隔で形成されており、および/または、前記敷板の条溝部が3つ以上の場合にはこれらの条溝部は略等間隔で形成されている、請求項2に記載の焼成治具。 The firing jig according to claim 2, wherein when the setter has three or more protruding portions, these protruding portions are formed at approximately equal intervals, and/or when the base plate has three or more grooved portions, these grooved portions are formed at approximately equal intervals.
  4.  前記セッターの凸部の少なくとも1つの長手方向に垂直な断面の前記近接面Sに平行な方向の最大幅員Wcと、前記セッターの前記敷板への戴置の際、この凸部が収容される前記条溝部の長手方向に垂直な断面の前記近接面Pに平行な方向の最大幅員Wpとの割合Wc/Wpが2以下である、請求項1~3のいずれか1項に記載の焼成治具。 The firing jig according to any one of claims 1 to 3, wherein the ratio Wc/Wp between the maximum width Wc of at least one of the protruding parts of the setter in a direction parallel to the adjacent surface S of a cross section perpendicular to the longitudinal direction of the setter and the maximum width Wp of the groove part in which the protruding part is accommodated in a cross section perpendicular to the longitudinal direction of the setter when the setter is placed on the base plate, in a direction parallel to the adjacent surface P, is 2 or less.
  5.  前記敷板の条溝部の平均深さ(前記条溝部の長手方向に垂直な断面の前記近接面Pから垂直方向の最低位置までの長さについて各条溝部の平均値を指す)Dg・avに対する、当該条溝部間の垂直最短距離(条溝部が3つ以上形成されている場合は、複数の垂直最短距離の平均値を指す)Igの比率Ig/Dg・avが0.05以上600以下である、請求項2または3に記載の焼成治具。 The firing jig according to claim 2 or 3, in which the ratio Ig/Dg・av of the shortest vertical distance Ig between the groove sections (if three or more groove sections are formed, the average of the shortest vertical distances) to the average depth Dg・av of the groove sections of the base plate (the average value of each groove section for the length from the adjacent surface P to the lowest vertical position in a cross section perpendicular to the longitudinal direction of the groove sections) is 0.05 or more and 600 or less.
  6.  前記セッターの凸部の少なくとも1つについて、その長手方向に垂直な断面の前記近接面Sに平行な方向の最大幅員Wcに対する、その長手方向の両端部間の長さLcのアスペクト比Lc/Wcが10以上である、請求項1~3のいずれか1項に記載の焼成治具。 The firing jig according to any one of claims 1 to 3, wherein for at least one of the convex parts of the setter, the aspect ratio Lc/Wc of the length Lc between both ends in the longitudinal direction to the maximum width Wc in the direction parallel to the adjacent surface S of the cross section perpendicular to the longitudinal direction is 10 or more.
  7.  前記セッターの凸部の少なくとも1つの長手方向に垂直な断面の前記近接面Sに垂直な方向の最大高さHcに対する、前記セッターの前記敷板への戴置の際、この凸部が収容される前記条溝部の長手方向に垂直な断面の前記近接面Pから垂直方向の最低位置までの深さDgの比率Dg/Hcが0.1以上である、請求項1~3のいずれか1項に記載の焼成治具。 The firing jig according to any one of claims 1 to 3, wherein the ratio Dg/Hc of the depth Dg from the proximity surface P to the lowest position in the vertical direction of the cross section perpendicular to the longitudinal direction of the groove portion in which the protrusion is housed when the setter is placed on the base plate to the maximum height Hc in the direction perpendicular to the proximity surface S of at least one of the protrusions of the setter in the longitudinal direction of the cross section, is 0.1 or more.
  8.  前記セッターの凸部の少なくとも1つの長手方向に垂直な断面の前記近接面Sに垂直な方向の最大高さHcに対する、この凸部の長手方向に垂直な断面の前記近接面Sに平行な方向の最大幅員Wcの比率Wc/Hcが0.3以上4以下である、請求項1~3のいずれか1項に記載の焼成治具。 The firing jig according to any one of claims 1 to 3, wherein the ratio Wc/Hc of the maximum height Hc of at least one of the protruding parts of the setter in a direction perpendicular to the longitudinal direction of the protruding part in a cross section perpendicular to the longitudinal direction of the protruding part in a direction parallel to the adjacent surface S to the maximum height Hc in a direction perpendicular to the longitudinal direction of the protruding part is 0.3 or more and 4 or less.
  9.  前記セッターが、その少なくとも一部にメッシュ状セラミックスシートを含み、
     このメッシュ状セラミックスシートは、所与の間隔で配置された各条が一方向に延伸された複数条の第1線条部で構成される第1線条部層、および、前記第1線条部の各条の上に接してこれと交差するように所与の間隔で配置された、各条が一方向に延伸された複数条の第2線条部で構成される第2線条部層を含み、前記第1線条部層と前記第2線条部層とが一体的に形成されているセラミックスシート焼結体であり、
     前記第2線条部層の前記第1線条部層に対する接面が、前記セッターの近接面Sをなしており、前記第1線条部層を構成する第1線条部が、前記セッターの凸部をなしている、
     請求項1~3のいずれか1項に記載の焼成治具。
     
    the setter includes a mesh-like ceramic sheet in at least a portion thereof,
    This mesh-like ceramic sheet includes a first linear portion layer composed of a plurality of first linear portions, each of which is arranged at a given interval and extends in one direction, and a second linear portion layer composed of a plurality of second linear portions, each of which is arranged at a given interval so as to be in contact with and intersect with each of the first linear portions, and is a ceramic sheet sintered body in which the first linear portion layer and the second linear portion layer are integrally formed,
    A contact surface of the second filamentary portion layer with respect to the first filamentary portion layer forms a proximity surface S of the setter, and a first filamentary portion constituting the first filamentary portion layer forms a convex portion of the setter.
    The firing jig according to any one of claims 1 to 3.
PCT/JP2023/039647 2022-12-13 2023-11-02 Firing jig comprising setter and bottom plate WO2024127845A1 (en)

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JPH0262399U (en) * 1988-10-28 1990-05-09
JP2005029462A (en) * 2003-06-17 2005-02-03 Mino Ceramic Co Ltd Method for manufacturing ceramic plate, ceramic plate and setter made of ceramic
JP2011052909A (en) * 2009-09-02 2011-03-17 Ngk Insulators Ltd Kiln tool plate for ceramic firing
KR20130082325A (en) * 2012-01-11 2013-07-19 주식회사 아모텍 Light setter for ferrite sintering and method of ferrite sintering used light setter
CN203837497U (en) * 2013-06-20 2014-09-17 广东风华高新科技股份有限公司 Bearing and burning jig for ceramic electronic elements
WO2015008503A1 (en) * 2013-07-16 2015-01-22 三井金属鉱業株式会社 Firing tool
WO2016009849A1 (en) * 2014-07-18 2016-01-21 株式会社村田製作所 Heat treatment jig
WO2017204061A1 (en) * 2016-05-24 2017-11-30 三井金属鉱業株式会社 Ceramic lattice
WO2021033375A1 (en) * 2019-08-16 2021-02-25 日本碍子株式会社 Firing rack and firing tool

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0262399U (en) * 1988-10-28 1990-05-09
JP2005029462A (en) * 2003-06-17 2005-02-03 Mino Ceramic Co Ltd Method for manufacturing ceramic plate, ceramic plate and setter made of ceramic
JP2011052909A (en) * 2009-09-02 2011-03-17 Ngk Insulators Ltd Kiln tool plate for ceramic firing
KR20130082325A (en) * 2012-01-11 2013-07-19 주식회사 아모텍 Light setter for ferrite sintering and method of ferrite sintering used light setter
CN203837497U (en) * 2013-06-20 2014-09-17 广东风华高新科技股份有限公司 Bearing and burning jig for ceramic electronic elements
WO2015008503A1 (en) * 2013-07-16 2015-01-22 三井金属鉱業株式会社 Firing tool
WO2016009849A1 (en) * 2014-07-18 2016-01-21 株式会社村田製作所 Heat treatment jig
WO2017204061A1 (en) * 2016-05-24 2017-11-30 三井金属鉱業株式会社 Ceramic lattice
WO2021033375A1 (en) * 2019-08-16 2021-02-25 日本碍子株式会社 Firing rack and firing tool

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