WO2022271108A1 - Eau de rose sous forme de poudre et son procédé de production - Google Patents

Eau de rose sous forme de poudre et son procédé de production Download PDF

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Publication number
WO2022271108A1
WO2022271108A1 PCT/TR2021/050641 TR2021050641W WO2022271108A1 WO 2022271108 A1 WO2022271108 A1 WO 2022271108A1 TR 2021050641 W TR2021050641 W TR 2021050641W WO 2022271108 A1 WO2022271108 A1 WO 2022271108A1
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WO
WIPO (PCT)
Prior art keywords
rose water
powder form
form according
rose
comparison
Prior art date
Application number
PCT/TR2021/050641
Other languages
English (en)
Inventor
Abdi Nuri ERÇETİN
Esma ÖZUSTA
Original Assignee
Erçeti̇n Gülyaği Sanayi̇ Ve Ti̇caret Anoni̇m Şi̇rketi̇
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Erçeti̇n Gülyaği Sanayi̇ Ve Ti̇caret Anoni̇m Şi̇rketi̇ filed Critical Erçeti̇n Gülyaği Sanayi̇ Ve Ti̇caret Anoni̇m Şi̇rketi̇
Priority to PCT/TR2021/050641 priority Critical patent/WO2022271108A1/fr
Publication of WO2022271108A1 publication Critical patent/WO2022271108A1/fr

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Classifications

    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/73Rosaceae (Rose family), e.g. strawberry, chokeberry, blackberry, pear or firethorn
    • A61K36/738Rosa (rose)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/10General cosmetic use

Definitions

  • Invention relates to rose water in powder form and its production method.
  • the invention particularly relates to conversion of rose water into powder form by means of an effective and simple method in order to increase stabilization of rose water and facilitate easy use thereof.
  • Rose is the name designated to multi-year close seed and nice smelling woody plant species of Rosa Damascena of Rosaceae family. Homeland of most rose types is Asia. Few number of them grow in Europe, North America and North-west Africa. Roses are mostly grown for their beauties and smells and have cultural essence in several societies. Vitamins, antioxidants and nice smells of them are other factors making this delicate flower popular.
  • rose Because of being natural and having strong antiseptic features, rose is used in several areas today and particularly is commonly used in medicine, cosmetics and gastronomy fields.
  • TR application numbered 2020/07882 discloses a method for rose water and rose oil extraction from rose and use of them in hand sanitizer composition.
  • Another invention is a Chinese application numbered CN112126524 (A).
  • the invention relates to rose essence distillation method.
  • a cutting and grinding device are used for rose essence distillation method.
  • the present invention relates to rose water in powder form and its production method meeting the needs mentioned above, eliminating all disadvantages, and providing some additional advantages, and a manufacturing method for the powder.
  • Primary aim of the invention is to provide an effective method to obtain rose water converted into powder form correctly in powder form having high stability.
  • Another aim of the invention is to create process steps applied during method used to obtain rose water in powder form are convenient and provide efficient results without deforming rose water content.
  • a further aim of the invention is to provide easy use of rose water in powder form obtained by said method in cosmetics and food sector and use it to give natural smell, aroma not containing chemical agents.
  • the invention aims to provide conversion of rose water into powder form by means of an effective and simple method in order to increase stabilization of rose water and facilitate easy use thereof in several sectors.
  • the invention is a method to obtain rose water in powder form and comprises steps listed below. a) adding maltodextrin and/or inulin and/or gum Arabic and/or xanthan gum into rose water concentrate or rose water and then adding water into this mixture to form emulsion, b) drying obtained emulsion in spray dryer and converting into powder.
  • Rose water in powder form disclosed under this present invention is produced by means of applying required pre-treatment to rose water at convenient conditions and drying it. Upon vaporization of water in the dried product as a result of drying the product remains in powder. Antioxidants, active agents in rose water in natural powder form are protected similar to its fresh natural form and thus can be stored in stable for long periods.
  • the invention is a method to obtain rose water in powder form and characterized by process steps of a) adding maltodextrin and/or inulin and/or gum Arabic and/or xanthan gum into rose water concentrate or into rose water and then adding water into this mixture to form emulsion, b) drying obtained emulsion in spray dryer and converting into powder.
  • a maltodextrin and/or inulin and/or gum Arabic and/or xanthan gum is added into rose water concentrate or rose water in order to form a structure on outer surface of rose water concentrate or rose water outer surface. Water is added to this mixture, and emulsion is obtained. All process steps are performed at room temperature of 20 °C.
  • said rose water concentrate is obtained by passing rose water through ion exchange resin.
  • Rose water concentrate provides shorter process step when compared to use of rose water.
  • inulin, gum Arabic and maltodextrin is added into rose water concentrate or rose water in process step a.
  • maltodextrin and gum Arabic are added into rose water concentrate or rose water in process step a.
  • inulin and gum Arabic are added into rose water concentrate or rose water in process step a.
  • xanthan gum, gum Arabic and maltodextrin are added into rose water concentrate or rose water in process step a.
  • mechanical stirrer is used as mixer in process step a.
  • homogenizer or magnetic stirrer is used as mixer in process step a.
  • emulsifier are agents sused in process step a when forming emulsion.
  • Emulsifier are agents mixed in order to provide mixture of two or more phases not mixing with each other.
  • Maltodextrin is an agent in polysaccharide class. It is used safely in several sectors such as cosmetics, medicine, food. It has high melting point. Maltodextrin is used to form a shell on outer surface of rose water concentrate in the invention.
  • Inulin is a natural group of polysaccharide produced by several plant types. It is used safely in several sectors such as cosmetics, medicine, food. It is used to form a shell on outer surface of rose water concentrate in the invention.
  • Gum Arabic is also known as acacin, Senegal gum, Indian gum. Gum arabic is a complex mixture of glycoprotein comprising commonly arabinose and galactose, and polysaccharide. It is an agent soluble in water and can safely be used in many sectors. Gum arabic is used to form a film around rose water concentrate in the present invention.
  • Xanthan gum is a polysaccharide obtained from fermentation of Xantnomonas campestris bacteria from glucose or sucrose. It is preferred in several sectors for its solid stabilization and durable against environmental conditions. It is used to form a film around rose water concentrate in the present invention.
  • emulsion is kept in spray dryer for 40 minutes at process step b. After average 40 minutes, about 25 g powder is obtained.
  • Inlet temperature of emulsion at spray dryer is between 110°C and 180°C. Moisture rate of product increases at low inlet temperature and rose water volatile oils may escape from air outlet at high temperature. For that reason, inlet temperature is important.
  • inlet temperature of emulsion at spray dryer is preferably 150°C in process step b.
  • outlet temperature of emulsion at spray dryer is preferably 90 - 98°C in process step b.
  • Outlet temperature may vary subject to several parameters such as inlet air relative humidity, inlet air temperature, spray gas flow, feeding rate, emulsion solid concentrate and use of organic solvent in emulsion.
  • Spray dryer parameters are as follows; aspirator rate 100 %, pump rate 10-30 %, inlet air feeding 30-40 mmHg.
  • rose water concentrate quantity is between 1 % and 20 % by weight in comparison to total composition. This amount is preferably 8 % in comparison to total composition by weight.
  • maltodextrin quantity is between 25 % and 65 % by weight in comparison to total composition. This amount is preferably 30 % in comparison to total composition by weight.
  • inulin quantity is between 10 % and 50 % by weight in comparison to total composition. This amount is preferably 16 % in comparison to total composition by weight.
  • gum arabic quantity is between 25 % and 50 % by weight in comparison to total composition. This amount is preferably 46 % in comparison to total composition by weight.
  • xanthan gum quantity is between 0.1 % and 5 % by weight in comparison to total composition. This amount is preferably 0.2 % in comparison to total composition by weight.
  • quantity of emulsifier that can be used optionally is between 0.1 % and 3 % by weight in comparison to total composition.
  • quantity of emulsifier that can be used optionally is between 0.1 % and 3 % by weight in comparison to total composition.
  • rose water in powder form can stay stabile for long time period on shelf and provides easy to use by dissolving in water when desired, and thus area of use can also be considerably wide.
  • rose water in powder form is mixed with water and rose water can be obtained easily.
  • rose water in powder form can be used as raw material or compound in food, cosmetic sectors.
  • cosmetic sector for instance, it is added into cream or shampoo products or in products of food sector directly thus antioxidants available in rose and nice smell can be added to the products as a natural component. It can also be used as food additive or aroma.
  • Example 1 rose water composition converted into powder form accurately
  • Example 2 rose water composition converted into powder form accurately
  • Example 3 rose water composition converted into powder form accurately
  • Example 4 rose water composition converted into powder form accurately

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • General Health & Medical Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • Mycology (AREA)
  • Engineering & Computer Science (AREA)
  • Epidemiology (AREA)
  • Microbiology (AREA)
  • Botany (AREA)
  • Biotechnology (AREA)
  • Dermatology (AREA)
  • Birds (AREA)
  • Chemical & Material Sciences (AREA)
  • Alternative & Traditional Medicine (AREA)
  • Medical Informatics (AREA)
  • Medicinal Chemistry (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Medicinal Preparation (AREA)

Abstract

L'Invention concerne de l'eau de rose sous forme de poudre et son procédé de production. L'invention concerne en particulier la conversion d'eau de rose en poudre au moyen d'un procédé efficace et simple afin d'augmenter la stabilisation de l'eau de rose et de permettre une utilisation aisée de celle-ci.
PCT/TR2021/050641 2021-06-23 2021-06-23 Eau de rose sous forme de poudre et son procédé de production WO2022271108A1 (fr)

Priority Applications (1)

Application Number Priority Date Filing Date Title
PCT/TR2021/050641 WO2022271108A1 (fr) 2021-06-23 2021-06-23 Eau de rose sous forme de poudre et son procédé de production

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PCT/TR2021/050641 WO2022271108A1 (fr) 2021-06-23 2021-06-23 Eau de rose sous forme de poudre et son procédé de production

Publications (1)

Publication Number Publication Date
WO2022271108A1 true WO2022271108A1 (fr) 2022-12-29

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Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/TR2021/050641 WO2022271108A1 (fr) 2021-06-23 2021-06-23 Eau de rose sous forme de poudre et son procédé de production

Country Status (1)

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WO (1) WO2022271108A1 (fr)

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1998019652A1 (fr) * 1996-11-06 1998-05-14 The Boots Company Plc Poudre sechee par pulverisation contenant au moins une proteine et un amidon hydrolyse, et son utilisation dans des compositions topiques
KR100730792B1 (ko) * 2005-12-29 2007-06-21 김병갑 식물조직에서 분리한 신선한 탈수액 분무건조물의 제조방법
CN112126524A (zh) * 2020-09-23 2020-12-25 合肥蓝胖子生物技术有限公司 一种玫瑰精华液蒸馏提取方法

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1998019652A1 (fr) * 1996-11-06 1998-05-14 The Boots Company Plc Poudre sechee par pulverisation contenant au moins une proteine et un amidon hydrolyse, et son utilisation dans des compositions topiques
KR100730792B1 (ko) * 2005-12-29 2007-06-21 김병갑 식물조직에서 분리한 신선한 탈수액 분무건조물의 제조방법
CN112126524A (zh) * 2020-09-23 2020-12-25 合肥蓝胖子生物技术有限公司 一种玫瑰精华液蒸馏提取方法

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
AHMED YASMEEN, SHAKIR JAMIL S, HASHIMI AYSHAH, SIRAJ MANTASHA BINTH, JAHANGIR UMAR: "Rosa Damascene Mill. (Rose): A versatile herb in cosmetology", vol. 9, no. 4, 1 January 2019 (2019-01-01), XP093020793, DOI: 10.5667/tang.2019.0017 *
ETZBACH LARA, MEINERT MESSINA, FABER THILO, KLEIN CAROLIN, SCHIEBER ANDREAS, WEBER FABIAN: "Effects of carrier agents on powder properties, stability of carotenoids, and encapsulation efficiency of goldenberry (Physalis peruviana L.) powder produced by co-current spray drying", CURRENT RESEARCH IN FOOD SCIENCE, vol. 3, 1 November 2020 (2020-11-01), pages 73 - 81, XP093020796, ISSN: 2665-9271, DOI: 10.1016/j.crfs.2020.03.002 *

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