WO2022246933A1 - Multi-mode measurement method and measurement system based on near-field non-porous probe - Google Patents
Multi-mode measurement method and measurement system based on near-field non-porous probe Download PDFInfo
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- WO2022246933A1 WO2022246933A1 PCT/CN2021/100992 CN2021100992W WO2022246933A1 WO 2022246933 A1 WO2022246933 A1 WO 2022246933A1 CN 2021100992 W CN2021100992 W CN 2021100992W WO 2022246933 A1 WO2022246933 A1 WO 2022246933A1
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- 239000000835 fiber Substances 0.000 claims description 89
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01Q—SCANNING-PROBE TECHNIQUES OR APPARATUS; APPLICATIONS OF SCANNING-PROBE TECHNIQUES, e.g. SCANNING PROBE MICROSCOPY [SPM]
- G01Q60/00—Particular types of SPM [Scanning Probe Microscopy] or microscopes; Essential components thereof
- G01Q60/18—SNOM [Scanning Near-Field Optical Microscopy] or apparatus therefor, e.g. SNOM probes
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- the invention belongs to the field of near-field optical imaging of micro-nano structure, shape measurement and optical fiber waveguide, and relates to a multi-mode measurement method and a measurement system based on a near-field non-porous probe.
- near-field optical technology has broken the bottleneck of the optical diffraction limit and realized optical high-resolution measurement.
- the structure of the probe it is mainly divided into hole-type and non-hole-type probes. Since the non-hole-type probe can achieve higher measurement resolution, it has been widely studied and applied.
- the commonly used measurement method based on the non-porous probe is the scattering measurement optical path.
- a beam of spatial light is irradiated at the point where the probe tip interacts with the sample, and then the light scattered by the near-field of the tip is collected at a distance, and finally used for optical imaging.
- this method is suitable for the measurement of most samples, there is only one method for excitation and collection of optical signals, which has great limitations, which limits the measurement of optical properties of various types of samples, and is not conducive to the field of near-field optical measurement. develop.
- Scattering measurement optical path is more complex, difficult to adjust and difficult to integrate. If the above measurement problems can be solved, it will bring great convenience to scientific research and promote the development of measuring instruments.
- the purpose of the present invention is to propose a multi-mode measurement method and measurement system based on a near-field non-porous probe.
- the present invention can realize a variety of different measurement modes, and the measurement system uses optical fiber As the carrier of light propagation, the entire optical path is very flexible, which is convenient for optical path debugging during the measurement process.
- a multi-mode measurement system based on a near-field non-porous probe including a first laser, a first detector, a second laser, a second detector, a first fiber coupler, a second fiber coupler, and a probe fiber , focusing lens group, first optical fiber, second optical fiber, third optical fiber, fourth optical fiber and fifth optical fiber;
- Both the first fiber coupler and the second fiber coupler include an input port, a first output port, a second output port, a first reflector, a beam splitter, a second reflector and a third reflector, and the first reflector is set On the optical path of the incident light at the input end, the beam splitter and the first output end are both located on the optical path of the reflected light of the first reflector, the coated side of the beam splitter faces the first output end, and the second reflector is located at the beam splitter The optical path of the reflected light on the side of the mirror with coating, the third reflector is located on the optical path of the reflected light of the second reflector, the second output end is located on the optical path of the reflected light of the third reflector, and the transmittance ratio of the beam splitter is different. less than 1;
- the first optical fiber, the second optical fiber, and the probe optical fiber are respectively connected to the input end, the second output end, and the first output end of the first optical fiber coupler, the first optical fiber of the first optical fiber coupler is connected to the first laser, and the first optical fiber is connected to the first laser.
- Two optical fibers are connected to the first detector;
- the third optical fiber, the fourth optical fiber, and the fifth optical fiber are respectively connected to the input end, the second output end, and the first output end of the second fiber coupler, the third optical fiber is connected to the second laser, and the fourth optical fiber is connected to the second detector. , the fifth optical fiber is connected to the focusing lens group;
- the axis of the probe tip of the probe fiber is coaxial with the axis of the focusing lens group.
- the probe tip of the probe fiber is located at the focal point of the focusing lens group.
- the first laser and the second laser are identical.
- the first detector and the second detector are identical.
- the probe tip of the probe fiber is a tapered tip structure.
- the multi-mode measurement system based on the near-field non-porous probe of the present invention also includes a three-dimensional mobile platform, a clamping mechanism capable of three-dimensional movement is provided on the three-dimensional mobile platform, and one end of the probe fiber with a probe tip is installed on the clamping mechanism.
- the present invention also provides a multi-mode measurement method based on a near-field non-porous probe, which is carried out by using the multi-mode measurement system based on the near-field non-porous probe of the present invention as described above, including:
- Measurement mode 1 the first laser emits laser light, the laser light emitted by the first laser emits on the surface of the sample to be tested through the first optical fiber, the first optical fiber coupler, and the probe tip of the probe fiber, and the probe tip of the probe fiber receives the The reflected light reflected by the surface of the sample to be tested enters the first detector through the probe fiber, the first fiber coupler and the second fiber;
- Measurement mode two the first laser emits laser light, the laser light emitted by the first laser emits on the surface of the sample to be tested through the first optical fiber, the first optical fiber coupler, and the probe tip of the probe optical fiber, and the fifth optical fiber receives it through the focusing lens group Measure the transmitted light of the sample, and the transmitted light enters the second detector through the fifth optical fiber, the second optical fiber coupler and the fourth optical fiber;
- Measurement mode three the second laser emits laser light, and the laser emitted by the second laser emits on the surface of the sample to be measured through the third optical fiber, the second optical fiber coupler, the fifth optical fiber, and the focusing lens group, and the focusing lens group receives the laser light passing through the surface of the sample to be measured The reflected reflected light enters the second detector through the fifth optical fiber, the second optical fiber coupler, and the fourth optical fiber;
- Measurement mode four the second laser emits laser light, and the laser light emitted by the second laser emits on the surface of the sample to be measured through the third optical fiber, the second optical fiber coupler, the fifth optical fiber, and the focusing lens group, and the probe tip of the probe optical fiber receives the laser light to be tested.
- the transmitted light of the sample is measured, and the transmitted light enters the first detector through the probe fiber, the first fiber coupler and the second fiber.
- measurement mode 1, measurement mode 2, measurement mode 3, measurement mode 4, measurement mode 1 and measurement mode 2 are carried out simultaneously, or measurement mode 3 and measurement mode 4 are carried out simultaneously. way to measure.
- the probe tip of the probe fiber is located at the focal point of the focusing lens group;
- the probe tip of the probe fiber is located at the focal point of the focusing lens group.
- measurement mode 1 is used for measurement.
- the multi-mode measurement system based on the near-field non-porous probe of the present invention can realize multiple different measurement modes, and study the physical and optical properties of the sample to be measured from different aspects.
- the multiple different measurement modes include: 1) using the first laser and the first detector. At this time, the near-field light on the surface of the sample to be measured is emitted by the probe tip, and the collected light is returned by the needle tip; 2) the first laser and the second detector are used.
- the needle tip is emitted, and the collected light is collected by the optical fiber under the sample to be tested; 3) Using the second laser and the first detector, the near-field light on the surface of the sample to be tested is incident on the probe tip from the bottom of the sample to be tested and interacts with the sample to be tested , the collected light is collected by the probe tip; 4) using the second laser and the second detector, the near-field light on the surface of the sample to be tested is incident on the probe tip and the sample to be tested from the bottom of the sample to be tested, and the collected light It is collected by the optical fiber below the sample to be tested.
- the measurement system of the present invention uses the first, second, third and fourth optical fibers as carriers for light propagation, which makes the entire optical path very flexible and facilitates the adjustment of the optical path during the measurement process.
- Fig. 1 is a schematic structural diagram of a multi-mode measurement system based on a near-field non-porous probe according to the present invention
- Fig. 2 is a schematic diagram of the working principle of the optical fiber coupler of the present invention, wherein the light entered by a can only exit through port b, and the light entered by b can only exit through port c;
- Fig. 3 is a partially enlarged schematic diagram of the tip of the fiber optic probe needle of the present invention.
- Fig. 4 is a schematic structural view of the lens group connected to the end of the optical fiber according to the present invention. After the light passes through the lens group, the outgoing light energy converges at one point;
- Fig. 5 is a near-field optical image of grid scattering measured by a first laser and a first detector in an embodiment of the present invention
- Fig. 6 is a grid transmission near-field optical image measured by a first laser and a second detector
- Fig. 7 is a schematic diagram of the optical path structure of the fiber coupler used in the present invention.
- 1 the first laser, 2 the first detector, 3 the second laser, 4 the second detector, 5 the first fiber, 6 the second fiber, 7 the third fiber, 8 the fourth fiber, 9 the first fiber coupling Device, 10 second fiber coupler, 11 probe fiber, 12 clamping mechanism, 13 sample to be tested, 14 lens group, 15 fifth fiber, 16 probe tip, 17 fiber tail, 18 focusing lens group, 19 fiber Coupler, 20 beam splitter, 21 first reflector, 22 second reflector, 23 third reflector, 24 input end, 25 first output end, 26 second output end.
- the multi-mode measurement system based on the near-field non-porous probe of the present invention includes a first laser 1, a first detector 2, a second laser 3, a second detector 4, a first A fiber coupler 9, a second fiber coupler 10, a probe fiber 11, a focusing lens group 18, a first fiber 5, a second fiber 6, a third fiber 7, a fourth fiber 8 and a fifth fiber 15;
- the first Both the fiber coupler 9 and the second fiber coupler 10 include an input port 24, a first output port 25, a second output port 26, a first reflector 21, a beam splitter 20, a second reflector 22 and a third reflector 23.
- the first reflector 21 is set on the optical path of the incident light at the input end 24, the beam splitter 20 and the first output end 25 are both located on the optical path of the light reflected by the first reflector 21, and the side of the beam splitter 20 is coated Towards the first output end 25, the second reflector 22 is located on the optical path of the reflected light on the coated side of the beam splitter 20, the third reflector 23 is located on the optical path of the reflected light from the second reflector 22, and the second output end 26 is located on the optical path of the light reflected by the third reflector 23, and the transmittance-reflectance ratio of the beam splitter 20 is not less than 1, that is, the amount of light transmitted by the beam splitter 20 is not less than the amount of reflected light. Referring to Fig.
- the arrow Indicates the direction of the optical path
- the incident from port a ie input port
- port b ie the first output port 25
- port c ie the second output port 26
- the transmittance ratio of the beam splitter can be 1:1, 3:1, 9:1, 99:1, 99.9:1.
- the first optical fiber 5, the second optical fiber 6, and the probe optical fiber 11 are respectively connected to the input end, the second output end, and the first output end of the first optical fiber coupler 9, and the first
- the first fiber 5 is connected to the first laser 1
- the second fiber 6 is connected to the first detector 2
- the third fiber 7, the fourth fiber 8 and the fifth fiber 15 are respectively connected to the second fiber coupler
- the connection between the input end, the second output end and the first output end of 10 is connected with the second laser 3
- the fourth optical fiber 8 is connected with the second detector 4
- the fifth optical fiber 15 is connected with the focusing lens group 18
- the axis of the probe tip 16 of the probe fiber 11 is coaxial with the axis of the focusing lens group 18 .
- the probe tip 16 of the probe fiber 11 is located at the focal point of the focusing lens group 18 .
- the first laser 1 and the second laser 3 are identical.
- the first detector 2 and the second detector 4 are identical.
- the probe tip 16 of the probe fiber 11 is a tapered tip structure.
- the multi-mode measurement system based on the near-field non-porous probe of the present invention also includes a three-dimensional mobile platform.
- a clamping mechanism 12 capable of three-dimensional movement is provided on the three-dimensional mobile platform.
- One end with a probe tip 16 is mounted on the clamping mechanism 12 .
- the focusing lens group 18 is clamped by a conventional fixed bracket and fixed on the other side of the sample.
- the clamping mechanism 12 moves the adjustable needle point with the probe tip 16 to the focus of the focusing lens group 18 , and then the clamping mechanism 12 does not move, and the focusing lens group 18 does not move all the time.
- both the probe 16 and the lens group 18 are stationary, and the sample stage carries the sample for three-dimensional movement for measurement.
- the present invention also provides a multi-mode measurement method based on a near-field non-porous probe, which is carried out by using the multi-mode measurement system based on the near-field non-porous probe of the present invention as described above, including:
- the sample 13 to be tested is arranged between the probe tip 16 and the focusing lens group 18;
- the probe tip of 11 receives the reflected light reflected by the surface of the sample 13 to be tested, and the reflected light enters the first detector 2 through the probe optical fiber 11, the first optical fiber coupler 9, and the second optical fiber 6;
- Measurement mode two the first laser 1 emits laser light, and the laser light emitted by the first laser 1 hits the surface of the sample 13 to be tested through the first optical fiber 5, the first optical fiber coupler 9, and the probe tip of the probe optical fiber 11, and the fifth optical fiber 15 Receive the transmitted light of the sample 13 to be measured through the focusing lens group 18, and the transmitted light enters the second detector 4 through the fifth optical fiber 15, the second optical fiber coupler 10 and the fourth optical fiber 8;
- Measurement mode three the second laser 3 emits laser light, and the laser light emitted by the second laser 3 passes through the third optical fiber 7, the second optical fiber coupler 10, the fifth optical fiber 15, and the focusing lens group 18 on the surface of the sample 13 to be measured, and the focusing lens
- the group 18 receives the reflected light reflected by the surface of the sample 13 to be tested, and the reflected light enters the second detector 4 through the fifth optical fiber 15, the second optical fiber coupler 10, and the fourth optical fiber 8;
- Measurement mode four the second laser 3 emits laser light, and the laser light emitted by the second laser 3 passes through the third optical fiber 7, the second optical fiber coupler 10, the fifth optical fiber 15, and the focusing lens group 18 on the surface of the sample 13 to be measured.
- the probe tip of the optical fiber 11 receives the transmitted light of the sample 13 to be tested, and the transmitted light enters the first detector 2 through the probe optical fiber 11 , the first optical fiber coupler 9 and the second optical fiber 6 .
- measurement mode one, measurement mode two, measurement mode three, measurement mode four, measurement mode one and measurement mode two are carried out simultaneously or measurement mode three and Measuring Mode Four Simultaneous measurement is carried out.
- the probe tip 16 of the probe fiber 11 when using measurement mode two to measure, is located at the focus of the focusing lens group 18; when using measurement mode four to measure, the probe tip 16 of the probe fiber 11 The needle tip 16 is located at the focal point of a focusing lens group 18 .
- measurement mode 1 is used for measurement.
- the probe used in the present invention is a non-porous fiber optic probe, and four different measurement modes can be realized by selectively adopting the method of emitting laser light or collecting laser light on the upper and lower surfaces of the sample to be measured.
- the measurement system uses optical fiber as the carrier of light propagation, which makes the entire optical path very flexible and facilitates optical path debugging during the measurement process.
- the technical solution of the present invention is to provide two identical lasers and detectors respectively.
- the emitted light of the laser and the collected light of the detector can be emitted or collected by the upper surface or the lower surface of the sample, so four different measurement modes can be obtained.
- the fiber with the probe tip is always on the upper surface of the sample
- the fiber with the tail lens set is always on the lower surface of the sample.
- the near-field light on the sample surface is emitted by the probe tip, and the collected light is also returned by the needle tip;
- the selected optical path of the laser is located on the upper surface of the sample and the optical path of the detector is located under the sample
- the near-field light on the sample surface is emitted by the probe tip, and the collected light is collected by the optical fiber under the sample;
- the selected laser optical path is located on the lower surface of the sample and the detector optical path is located on the upper surface of the sample, the near-field light on the sample surface is incident from below the sample
- the selected laser and detector optical path are located on the side of the lower surface of the sample, the near-field light on the sample surface is incident from the bottom of the sample to the probe tip and the sample interaction , the collected light is collected by the optical fiber below the sample.
- the present invention provides two methods for forming focused light spots at the probe tip in near-field optical measurement, and provides two methods for collecting near-field scattering signals, so four different measurement modes can be realized.
- the light-transmitting sample to be tested can realize the measurement and imaging of near-field scattered light and transmitted light at the same time on the upper and lower detectors, and can improve the signal-to-noise ratio of near-field signals.
- the measurement system uses optical fiber as the carrier of light propagation, which is flexible in operation, easy to adjust and integrate.
- the multi-mode measurement system based on the near-field non-porous probe in this embodiment uses two identical lasers, namely the first laser 1 and the second laser 3, and two identical detectors, namely the first For the detector 2 and the first detector 4, both the laser and the detector are selected during operation, and only one is selected for use.
- Both the laser and the detector are connected with optical fibers (5, 6, 7, 8), and the first optical fiber coupler 9 couples one end of the first optical fiber 5, the second optical fiber 6 and the probe optical fiber 11 together, and the second optical fiber coupler
- the device 10 couples and connects one end of the third optical fiber 7, the fourth optical fiber 8 and the fifth optical fiber 15 together.
- the needle tip at the tail end of the probe fiber 11 can move three-dimensionally under the drive of the clamping mechanism 12.
- the fiber tail 17 of the fifth fiber 15 is connected to the lens group 14, and the lens group 14 can converge the light at one point.
- the center between the needle point at the end of the probe fiber 11 and the lens group 14 is the placement area for the sample 13 to be tested, and the sample also divides the optical path into upper and lower sides.
- the first optical fiber coupler 9 needs to satisfy that the light output by the first optical fiber 5 can only enter the probe optical fiber 11, and the light output by the probe optical fiber 11 can only enter the second optical fiber 6; the second optical fiber coupler 10 needs to The light output by the third optical fiber 7 can only enter the fifth optical fiber 15 , and the light output by the fifth optical fiber 15 can only enter the second optical fiber 8 .
- each mode also fixes the measurement optical path used.
- the first is to use the first laser 1 and the first detector 2; the second is to use the first A laser 1 and a second detector 4; the third is to use the second laser 3 and the first detector 2; the first is to use the second laser 3 and the second detector 4.
- the specific measurement methods for each mode are:
- the near-field light on the sample surface is emitted by the probe tip, and the collected light is collected by the optical fiber under the sample;
- the near-field light on the sample surface is incident on the probe tip and the sample from below the sample, and the collected light is collected by the probe tip;
- the second laser 3 and the second detector 4 are used. At this time, the near-field light on the sample surface is incident on the probe tip and the sample from below the sample, and the collected light is collected by the optical fiber below the sample.
- the probe fiber 11 is used in conjunction with the fifth fiber 15, the central axes of the two fibers should coincide and the needle tip at the tail end of the probe fiber 11 should be adjusted to the upper focal point of the lens group 14. Time signal collection is the highest.
- the sample 13 to be tested is a light-transmitting sample
- four different modes can be used for near-field optical measurement.
- the first is to use the first laser 1 and the first detector 2; the second is to use the first laser 1 and the second detector 4; the third is to use the second laser 3 and the first detector 2; the fourth One is to use a second laser 3 and a second detector 4 .
- the first and the second can be used at the same time to measure scattered light and transmitted light, that is, the first laser 1 and the second detector 2 and the second detector 4; the third and the fourth can be used at the same time to measure Scattered light and transmitted light, that is, the second laser 3 and the first detector 2 and the second detector 4 .
- the difference between the two is that the incident light is irradiated from the upper surface or the lower surface of the sample.
- sample 13 to be tested is a non-transparent sample, then select the first laser 1 and the first detector 2 to be used together.
- the present invention carries out the near-field optical imaging test of the first and second modes simultaneously for a grid structure, the central axes of the probe fiber 11 and the fifth fiber 15 are coincident and the tip of the probe fiber 11 tail end is adjusted to At the focal point above the lens group 14, the scattering near-field optical image (as shown in FIG. 5 ) and the transmission near-field optical image (as shown in FIG. 6 ) of the sample are simultaneously obtained.
- the signal of the two images is The noise ratios are all high, and can be compared with each other to confirm the accuracy of the results.
- the multi-mode measurement method and measurement system based on the near-field non-porous probe involved in the present invention has very prominent features and advantages, including the following points:
- the measurement resolution of each mode can reach the highest resolution of current near-field optical measurement.
- optical fiber optical path is used together with the optical fiber probe, the optical path is very flexible, which provides great convenience for the experimental operation.
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Abstract
A multi-mode measurement method and measurement system based on a near-field non-porous probe. First and second optical fibers (5, 6) are coupled to a probe optical fiber (11) by means of a first optical fiber coupler (9), the first optical fiber (5) is connected to a first laser (1), and the second optical fiber (6) is connected to a first detector (2). Third and fourth optical fibers (7, 8) are coupled to a fifth optical fiber (15) by means of a second optical fiber coupler (10), the third optical fiber (7) is connected to a second laser (3), the fourth optical fiber (8) is connected to a second detector (4), and the fifth optical fiber (15) is connected to a focusing lens group (18). Light that is output from the first optical fiber (5) can only enter the probe optical fiber (11), light that is output from the probe optical fiber (11) can only enter the second optical fiber (6), light that is output from the third optical fiber (7) can only enter the fifth optical fiber (15), and light that is output from the fifth optical fiber (15) can only enter the fourth optical fiber (8). An axis of a probe tip (16) of the probe optical fiber (11) is coaxial with an axis of the focusing lens group (18). By means of the measurement method, different measurement modes can be realized, and for a measurement system, optical fibers are used as carriers for optical propagation, which makes the entire optical path flexible, thereby facilitating optical path debugging during a measurement process.
Description
本发明属于微纳米结构近场光学成像、形貌测量和光纤波导光路领域,涉及一种基于近场无孔式探针的多模式测量方法及测量系统。The invention belongs to the field of near-field optical imaging of micro-nano structure, shape measurement and optical fiber waveguide, and relates to a multi-mode measurement method and a measurement system based on a near-field non-porous probe.
近场光学技术的出现打破了光学衍射极限的瓶颈,实现了光学高分辨测量。研究人员通过将探针放置在样品表面百纳米区域以内,成功的探测到了样品近场倏逝波,在这其中使用一根合适的探针是近场测量的关键所在。根据探针的结构不同,主要分为有孔式和无孔式探针,其中由于无孔式探针可以实现更高的测量分辨率,所以得到了更广的研究和应用。The emergence of near-field optical technology has broken the bottleneck of the optical diffraction limit and realized optical high-resolution measurement. The researchers successfully detected the near-field evanescent wave of the sample by placing the probe within a hundred nanometers of the sample surface, and using a suitable probe is the key to the near-field measurement. According to the structure of the probe, it is mainly divided into hole-type and non-hole-type probes. Since the non-hole-type probe can achieve higher measurement resolution, it has been widely studied and applied.
目前,基于无孔式探针常用的测量方法为散射式测量光路,通常为一束空间光照射在探针针尖与样品作用处,再在远处收集由针尖近场散射的光,最后用于光学成像。该方法虽然适用于大部分样品的测量,但是在光信号的激发和收集上只有一种方式,有很大的局限性,限制了多类样品光学性质的测量,不利于近场光学测量领域的发展。散射式测量光路较为复杂,调节难度高,难以集成。如果可以解决上述测量问题,定会带来很大的科研便利,推进测量仪器的发展。At present, the commonly used measurement method based on the non-porous probe is the scattering measurement optical path. Usually, a beam of spatial light is irradiated at the point where the probe tip interacts with the sample, and then the light scattered by the near-field of the tip is collected at a distance, and finally used for optical imaging. Although this method is suitable for the measurement of most samples, there is only one method for excitation and collection of optical signals, which has great limitations, which limits the measurement of optical properties of various types of samples, and is not conducive to the field of near-field optical measurement. develop. Scattering measurement optical path is more complex, difficult to adjust and difficult to integrate. If the above measurement problems can be solved, it will bring great convenience to scientific research and promote the development of measuring instruments.
发明内容Contents of the invention
为解决现有技术中存在的问题,本发明的目的在于提出一种基于近场无孔式探针的多模式测量方法及测量系统,本发明能够实现多种不同的测量模式,测量系统使用光纤作为光传播的载体,让整个光路十分灵活,便于测量过程中的光路调试。In order to solve the problems existing in the prior art, the purpose of the present invention is to propose a multi-mode measurement method and measurement system based on a near-field non-porous probe. The present invention can realize a variety of different measurement modes, and the measurement system uses optical fiber As the carrier of light propagation, the entire optical path is very flexible, which is convenient for optical path debugging during the measurement process.
本发明采用的技术方案如下:The technical scheme that the present invention adopts is as follows:
一种基于近场无孔式探针的多模式测量系统,包括第一激光器、第一探测器、第二激光器、 第二探测器、第一光纤耦合器、第二光纤耦合器、探针光纤、聚焦透镜组、第一光纤、第二光纤、第三光纤、第四光纤和第五光纤;A multi-mode measurement system based on a near-field non-porous probe, including a first laser, a first detector, a second laser, a second detector, a first fiber coupler, a second fiber coupler, and a probe fiber , focusing lens group, first optical fiber, second optical fiber, third optical fiber, fourth optical fiber and fifth optical fiber;
第一光纤耦合器和第二光纤耦合器均包括输入端、第一输出端、第二输出端、第一反射镜、分束镜、第二反射镜和第三反射镜,第一反射镜设置于输入端入射光的光路上,分束镜和第一输出端均位于第一反射镜反射光的光路上,分束镜有镀膜的一侧朝向第一输出端,第二反射镜位于分束镜有镀膜的一侧的反射光的光路上,第三反射镜位于第二反射镜反射光的光路上,第二输出端位于第三反射镜反射光的光路上,分束镜的透反比不小于1;Both the first fiber coupler and the second fiber coupler include an input port, a first output port, a second output port, a first reflector, a beam splitter, a second reflector and a third reflector, and the first reflector is set On the optical path of the incident light at the input end, the beam splitter and the first output end are both located on the optical path of the reflected light of the first reflector, the coated side of the beam splitter faces the first output end, and the second reflector is located at the beam splitter The optical path of the reflected light on the side of the mirror with coating, the third reflector is located on the optical path of the reflected light of the second reflector, the second output end is located on the optical path of the reflected light of the third reflector, and the transmittance ratio of the beam splitter is different. less than 1;
第一光纤、第二光纤和探针光纤分别与第一光纤耦合器的输入端、第二输出端和第一输出端连接,第一光纤耦合器的,第一光纤与第一激光器连接,第二光纤与第一探测器连接;The first optical fiber, the second optical fiber, and the probe optical fiber are respectively connected to the input end, the second output end, and the first output end of the first optical fiber coupler, the first optical fiber of the first optical fiber coupler is connected to the first laser, and the first optical fiber is connected to the first laser. Two optical fibers are connected to the first detector;
第三光纤、第四光纤和第五光纤分别与第二光纤耦合器的输入端、第二输出端和第一输出端的连接,第三光纤与第二激光器连接,第四光纤第二探测器连接,第五光纤与聚焦透镜组连接;The third optical fiber, the fourth optical fiber, and the fifth optical fiber are respectively connected to the input end, the second output end, and the first output end of the second fiber coupler, the third optical fiber is connected to the second laser, and the fourth optical fiber is connected to the second detector. , the fifth optical fiber is connected to the focusing lens group;
探针光纤的探针针尖的轴线与聚焦透镜组的轴线同轴。The axis of the probe tip of the probe fiber is coaxial with the axis of the focusing lens group.
优选的,探针光纤的探针针尖位于聚焦透镜组的焦点上。Preferably, the probe tip of the probe fiber is located at the focal point of the focusing lens group.
优选的,第一激光器和第二激光器相同。Preferably, the first laser and the second laser are identical.
优选的,第一探测器和第二探测器相同。Preferably, the first detector and the second detector are identical.
优选的,探针光纤的探针针尖为一锥形尖端结构。Preferably, the probe tip of the probe fiber is a tapered tip structure.
优选的,本发明基于近场无孔式探针的多模式测量系统还包括三维移动平台,三维移动平台上设有能够进行三维移动的夹持机构,探针光纤上具有探针针尖的一端安装于所述夹持机构上。Preferably, the multi-mode measurement system based on the near-field non-porous probe of the present invention also includes a three-dimensional mobile platform, a clamping mechanism capable of three-dimensional movement is provided on the three-dimensional mobile platform, and one end of the probe fiber with a probe tip is installed on the clamping mechanism.
本发明还提供了一种基于近场无孔式探针的多模式测量方法,该测量方法采用本发明如上所述的基于近场无孔式探针的多模式测量系统进行,包括:The present invention also provides a multi-mode measurement method based on a near-field non-porous probe, which is carried out by using the multi-mode measurement system based on the near-field non-porous probe of the present invention as described above, including:
将待测样品设置于探针针尖与聚焦透镜组之间;Set the sample to be tested between the probe tip and the focusing lens group;
以及采用如下至少一种测量模式进行测量:And take measurements using at least one of the following measurement modes:
测量模式一:第一激光器发射激光,第一激光器发射的激光经第一光纤、第一光纤耦合器、探针光纤的探针针尖射于待测样品表面,探针光纤的探针针尖接收经待测样品表面反射的反射光,该反射光经探针光纤、第一光纤耦合器、第二光纤进入第一探测器;Measurement mode 1: the first laser emits laser light, the laser light emitted by the first laser emits on the surface of the sample to be tested through the first optical fiber, the first optical fiber coupler, and the probe tip of the probe fiber, and the probe tip of the probe fiber receives the The reflected light reflected by the surface of the sample to be tested enters the first detector through the probe fiber, the first fiber coupler and the second fiber;
测量模式二:第一激光器发射激光,第一激光器发射的激光经第一光纤、第一光纤耦合器、探针光纤的探针针尖射于待测样品表面,第五光纤经聚焦透镜组接收待测样品的透射光,该透射光经第五光纤、第二光纤耦合器和第四光纤进入第二探测器;Measurement mode two: the first laser emits laser light, the laser light emitted by the first laser emits on the surface of the sample to be tested through the first optical fiber, the first optical fiber coupler, and the probe tip of the probe optical fiber, and the fifth optical fiber receives it through the focusing lens group Measure the transmitted light of the sample, and the transmitted light enters the second detector through the fifth optical fiber, the second optical fiber coupler and the fourth optical fiber;
测量模式三:第二激光器发射激光,第二激光器发射的激光经第三光纤、第二光纤耦合器、第五光纤、聚焦透镜组射于待测样品表面,聚焦透镜组接收经待测样品表面反射的反射光,该反射光经第五光纤、第二光纤耦合器、第四光纤进入第二探测器;Measurement mode three: the second laser emits laser light, and the laser emitted by the second laser emits on the surface of the sample to be measured through the third optical fiber, the second optical fiber coupler, the fifth optical fiber, and the focusing lens group, and the focusing lens group receives the laser light passing through the surface of the sample to be measured The reflected reflected light enters the second detector through the fifth optical fiber, the second optical fiber coupler, and the fourth optical fiber;
测量模式四:第二激光器发射激光,第二激光器发射的激光经第三光纤、第二光纤耦合器、第五光纤、聚焦透镜组射于待测样品表面,探针光纤的探针针尖接收待测样品的透射光,该透射光经探针光纤、第一光纤耦合器、第二光纤进入第一探测器。Measurement mode four: the second laser emits laser light, and the laser light emitted by the second laser emits on the surface of the sample to be measured through the third optical fiber, the second optical fiber coupler, the fifth optical fiber, and the focusing lens group, and the probe tip of the probe optical fiber receives the laser light to be tested. The transmitted light of the sample is measured, and the transmitted light enters the first detector through the probe fiber, the first fiber coupler and the second fiber.
优选的,当待测样品为透光样品时,采用测量模式一、测量模式二、测量模式三、测量模式四、测量模式一和测量模式二同时进行或者测量模式三与测量模式四同时进行的方式进行测量。Preferably, when the sample to be measured is a light-transmitting sample, measurement mode 1, measurement mode 2, measurement mode 3, measurement mode 4, measurement mode 1 and measurement mode 2 are carried out simultaneously, or measurement mode 3 and measurement mode 4 are carried out simultaneously. way to measure.
优选的:当采用测量模式二进行测量时,探针光纤的探针针尖位于聚焦透镜组的焦点上;Preferably: when the measurement mode 2 is used for measurement, the probe tip of the probe fiber is located at the focal point of the focusing lens group;
当采用测量模式四进行测量时,探针光纤的探针针尖位于聚焦透镜组的焦点上。When measuring with measurement mode 4, the probe tip of the probe fiber is located at the focal point of the focusing lens group.
优选的,当待测样品为非透光样品时,采用测量模式一进行测量。Preferably, when the sample to be tested is a non-transparent sample, measurement mode 1 is used for measurement.
本发明具有如下有益效果:The present invention has following beneficial effect:
本发明基于近场无孔式探针的多模式测量系统能够实现多种不同的测量模式,从不同方面 研究待测样品的物理光学性质,多种不同的测量模式包括:1)使用第一激光器和第一探测器,此时待测样品表面近场光由探针针尖发出,收集光由针尖返回;2)使用第一激光器和第二探测器,此时待测样品表面近场光由探针针尖发出,收集光被待测样品下方光纤收集;3)使用第二激光器和第一探测器,此时待测样品表面近场光由待测样品下方入射到探针针尖和待测样品作用处,收集光被探针针尖收集;4)使用第二激光器和第二探测器,此时待测样品表面近场光由待测样品下方入射到探针针尖和待测样品作用处,收集光被待测样品下方光纤收集。本发明测量系统使用第一、第二、第三、第四光纤作为光传播的载体,让整个光路十分灵活,便于测量过程中的光路调试。The multi-mode measurement system based on the near-field non-porous probe of the present invention can realize multiple different measurement modes, and study the physical and optical properties of the sample to be measured from different aspects. The multiple different measurement modes include: 1) using the first laser and the first detector. At this time, the near-field light on the surface of the sample to be measured is emitted by the probe tip, and the collected light is returned by the needle tip; 2) the first laser and the second detector are used. The needle tip is emitted, and the collected light is collected by the optical fiber under the sample to be tested; 3) Using the second laser and the first detector, the near-field light on the surface of the sample to be tested is incident on the probe tip from the bottom of the sample to be tested and interacts with the sample to be tested , the collected light is collected by the probe tip; 4) using the second laser and the second detector, the near-field light on the surface of the sample to be tested is incident on the probe tip and the sample to be tested from the bottom of the sample to be tested, and the collected light It is collected by the optical fiber below the sample to be tested. The measurement system of the present invention uses the first, second, third and fourth optical fibers as carriers for light propagation, which makes the entire optical path very flexible and facilitates the adjustment of the optical path during the measurement process.
图1是本发明所述基于近场无孔式探针多模式测量系统结构示意图;Fig. 1 is a schematic structural diagram of a multi-mode measurement system based on a near-field non-porous probe according to the present invention;
图2是本发明所述光纤耦合器的工作原理示意图,其中由a进入的光只能从b口出,由b进入的光只能从c口出;Fig. 2 is a schematic diagram of the working principle of the optical fiber coupler of the present invention, wherein the light entered by a can only exit through port b, and the light entered by b can only exit through port c;
图3是本发明所述光纤探针针尖端局部放大后的示意图;Fig. 3 is a partially enlarged schematic diagram of the tip of the fiber optic probe needle of the present invention;
图4是本发明所述光纤尾端连接透镜组的结构示意图,光经过透镜组后,出射的光能会聚于一点;Fig. 4 is a schematic structural view of the lens group connected to the end of the optical fiber according to the present invention. After the light passes through the lens group, the outgoing light energy converges at one point;
图5是本发明实施例中采用第一激光器和第一探测器测量的栅格散射近场光学图像;Fig. 5 is a near-field optical image of grid scattering measured by a first laser and a first detector in an embodiment of the present invention;
图6是采用第一激光器和第二探测器测量的栅格透射近场光学图像;Fig. 6 is a grid transmission near-field optical image measured by a first laser and a second detector;
图7为本发明采用的光纤耦合器的光路结构示意图。Fig. 7 is a schematic diagram of the optical path structure of the fiber coupler used in the present invention.
图中:1第一激光器、2第一探测器、3第二激光器、4第二探测器、5第一光纤、6第二光纤、7第三光纤、8第四光纤、9第一光纤耦合器、10第二光纤耦合器、11探针光纤、12夹持机构、13待测样品、14透镜组、15第五光纤、16探针针尖、17光纤尾端、18聚焦透镜组,19光纤耦合器、20分束镜、21第一反射镜、22第二反射镜、23第三反射镜、24输入端、25 第一输出端、26第二输出端。In the figure: 1 the first laser, 2 the first detector, 3 the second laser, 4 the second detector, 5 the first fiber, 6 the second fiber, 7 the third fiber, 8 the fourth fiber, 9 the first fiber coupling Device, 10 second fiber coupler, 11 probe fiber, 12 clamping mechanism, 13 sample to be tested, 14 lens group, 15 fifth fiber, 16 probe tip, 17 fiber tail, 18 focusing lens group, 19 fiber Coupler, 20 beam splitter, 21 first reflector, 22 second reflector, 23 third reflector, 24 input end, 25 first output end, 26 second output end.
下面将结合附图和具体实施方法对本发明做清楚、具体的说明。The present invention will be clearly and specifically described below in conjunction with the accompanying drawings and specific implementation methods.
参照图1、图2和图7,本发明基于近场无孔式探针的多模式测量系统,包括第一激光器1、第一探测器2、第二激光器3、第二探测器4、第一光纤耦合器9、第二光纤耦合器10、探针光纤11、聚焦透镜组18、第一光纤5、第二光纤6、第三光纤7、第四光纤8和第五光纤15;第一光纤耦合器9和第二光纤耦合器10均包括输入端24、第一输出端25、第二输出端26、第一反射镜21、分束镜20、第二反射镜22和第三反射镜23,第一反射镜21设置于输入端24入射光的光路上,分束镜20和第一输出端25均位于第一反射镜21反射光的光路上,分束镜20有镀膜的一侧朝向第一输出端25,第二反射镜22位于分束镜20有镀膜的一侧的反射光的光路上,第三反射镜23位于第二反射镜22反射光的光路上,第二输出端26位于第三反射镜23反射光的光路上,分束镜20的透反比不小于1,即分束镜20的透光量不小于其反射光量,参照图1、图2和图7,箭头表示光路方向,从a口(即输入端)入射可以到b口(即第一输出端25)射出,b口(即第一输出端25)入射则从c口(即第二输出端26)射出,此时a口也会有少量光射出,该光为无用光,不考虑,分束镜的透反比可选1:1、3:1、9:1、99:1、99.9:1,一般选用9:1即可满足使用要求;第一光纤5、第二光纤6和探针光纤11分别与第一光纤耦合器9的输入端、第二输出端和第一输出端连接,第一光纤耦合器9的,第一光纤5与第一激光器1连接,第二光纤6与第一探测器2连接;第三光纤7、第四光纤8和第五光纤15分别与第二光纤耦合器10的输入端、第二输出端和第一输出端的连接,第三光纤7与第二激光器3连接,第四光纤8第二探测器4连接,第五光纤15与聚焦透镜组18连接;;参照图1,探针光纤11的探针针尖16的轴线与聚焦透镜组18的轴线同轴。Referring to Fig. 1, Fig. 2 and Fig. 7, the multi-mode measurement system based on the near-field non-porous probe of the present invention includes a first laser 1, a first detector 2, a second laser 3, a second detector 4, a first A fiber coupler 9, a second fiber coupler 10, a probe fiber 11, a focusing lens group 18, a first fiber 5, a second fiber 6, a third fiber 7, a fourth fiber 8 and a fifth fiber 15; the first Both the fiber coupler 9 and the second fiber coupler 10 include an input port 24, a first output port 25, a second output port 26, a first reflector 21, a beam splitter 20, a second reflector 22 and a third reflector 23. The first reflector 21 is set on the optical path of the incident light at the input end 24, the beam splitter 20 and the first output end 25 are both located on the optical path of the light reflected by the first reflector 21, and the side of the beam splitter 20 is coated Towards the first output end 25, the second reflector 22 is located on the optical path of the reflected light on the coated side of the beam splitter 20, the third reflector 23 is located on the optical path of the reflected light from the second reflector 22, and the second output end 26 is located on the optical path of the light reflected by the third reflector 23, and the transmittance-reflectance ratio of the beam splitter 20 is not less than 1, that is, the amount of light transmitted by the beam splitter 20 is not less than the amount of reflected light. Referring to Fig. 1, Fig. 2 and Fig. 7, the arrow Indicates the direction of the optical path, the incident from port a (ie input port) can be emitted to port b (ie the first output port 25), and the incident from port b (ie the first output port 25) is incident from port c (ie the second output port 26) At this time, a small amount of light will also be emitted from the a port. This light is useless light. Regardless, the transmittance ratio of the beam splitter can be 1:1, 3:1, 9:1, 99:1, 99.9:1. Generally, 9:1 can be used to meet the requirements; the first optical fiber 5, the second optical fiber 6, and the probe optical fiber 11 are respectively connected to the input end, the second output end, and the first output end of the first optical fiber coupler 9, and the first For the fiber coupler 9, the first fiber 5 is connected to the first laser 1, and the second fiber 6 is connected to the first detector 2; the third fiber 7, the fourth fiber 8 and the fifth fiber 15 are respectively connected to the second fiber coupler The connection between the input end, the second output end and the first output end of 10, the third optical fiber 7 is connected with the second laser 3, the fourth optical fiber 8 is connected with the second detector 4, and the fifth optical fiber 15 is connected with the focusing lens group 18; Referring to FIG. 1 , the axis of the probe tip 16 of the probe fiber 11 is coaxial with the axis of the focusing lens group 18 .
作为本发明优选的实施方案,参照图1、图3和图4,探针光纤11的探针针尖16位于聚 焦透镜组18的焦点上。As a preferred embodiment of the present invention, referring to FIG. 1 , FIG. 3 and FIG. 4 , the probe tip 16 of the probe fiber 11 is located at the focal point of the focusing lens group 18 .
作为本发明优选的实施方案,第一激光器1和第二激光器3相同。As a preferred embodiment of the invention, the first laser 1 and the second laser 3 are identical.
作为本发明优选的实施方案,第一探测器2和第二探测器4相同。As a preferred embodiment of the present invention, the first detector 2 and the second detector 4 are identical.
作为本发明优选的实施方案,参照图3,探针光纤11的探针针尖16为一锥形尖端结构。As a preferred embodiment of the present invention, referring to FIG. 3 , the probe tip 16 of the probe fiber 11 is a tapered tip structure.
作为本发明优选的实施方案,本发明基于近场无孔式探针的多模式测量系统还包括三维移动平台,三维移动平台上设有能够进行三维移动的夹持机构12,探针光纤11上具有探针针尖16的一端安装于所述夹持机构12上。聚焦透镜组18用常规的固定支架夹持保持不动并安装在样品另一侧。夹持机构12带着探针针尖16移动可调节针尖至聚焦透镜组18的焦点上,然后夹持机构12不移动,聚焦透镜组18始终不动。在具体测量样品时,探针16和透镜组18都是不动的,样品台承载样品进行三维移动进行测量。As a preferred embodiment of the present invention, the multi-mode measurement system based on the near-field non-porous probe of the present invention also includes a three-dimensional mobile platform. A clamping mechanism 12 capable of three-dimensional movement is provided on the three-dimensional mobile platform. On the probe optical fiber 11 One end with a probe tip 16 is mounted on the clamping mechanism 12 . The focusing lens group 18 is clamped by a conventional fixed bracket and fixed on the other side of the sample. The clamping mechanism 12 moves the adjustable needle point with the probe tip 16 to the focus of the focusing lens group 18 , and then the clamping mechanism 12 does not move, and the focusing lens group 18 does not move all the time. When measuring a sample, both the probe 16 and the lens group 18 are stationary, and the sample stage carries the sample for three-dimensional movement for measurement.
本发明还提供了一种基于近场无孔式探针的多模式测量方法,该多模式测量方法采用本发明如上所述的基于近场无孔式探针的多模式测量系统进行,包括:The present invention also provides a multi-mode measurement method based on a near-field non-porous probe, which is carried out by using the multi-mode measurement system based on the near-field non-porous probe of the present invention as described above, including:
参照图1,将待测样品13设置于探针针尖16与聚焦透镜组18之间;Referring to Fig. 1, the sample 13 to be tested is arranged between the probe tip 16 and the focusing lens group 18;
采用如下至少一种测量模式进行测量:Take measurements using at least one of the following measurement modes:
测量模式一:第一激光器1发射激光,第一激光器1发射的激光经第一光纤5、第一光纤耦合器9、探针光纤11的探针针尖射于待测样品13表面,探针光纤11的探针针尖接收经待测样品13表面反射的反射光,该反射光经探针光纤11、第一光纤耦合器9、第二光纤6进入第一探测器2;Measurement mode one: the first laser 1 emits laser light, and the laser light emitted by the first laser 1 hits the surface of the sample 13 to be tested through the first optical fiber 5, the first optical fiber coupler 9, and the probe tip of the probe optical fiber 11, and the probe optical fiber The probe tip of 11 receives the reflected light reflected by the surface of the sample 13 to be tested, and the reflected light enters the first detector 2 through the probe optical fiber 11, the first optical fiber coupler 9, and the second optical fiber 6;
测量模式二:第一激光器1发射激光,第一激光器1发射的激光经第一光纤5、第一光纤耦合器9、探针光纤11的探针针尖射于待测样品13表面,第五光纤15经聚焦透镜组18接收待测样品13的透射光,该透射光经第五光纤15、第二光纤耦合器10和第四光纤8进入第二探测器4;Measurement mode two: the first laser 1 emits laser light, and the laser light emitted by the first laser 1 hits the surface of the sample 13 to be tested through the first optical fiber 5, the first optical fiber coupler 9, and the probe tip of the probe optical fiber 11, and the fifth optical fiber 15 Receive the transmitted light of the sample 13 to be measured through the focusing lens group 18, and the transmitted light enters the second detector 4 through the fifth optical fiber 15, the second optical fiber coupler 10 and the fourth optical fiber 8;
测量模式三:第二激光器3发射激光,第二激光器3发射的激光经第三光纤7、第二光纤耦合器10、第五光纤15、聚焦透镜组18射于待测样品13表面,聚焦透镜组18接收经待测样品13表面反射的反射光,该反射光经第五光纤15、第二光纤耦合器10、第四光纤8进入第二探测器4;Measurement mode three: the second laser 3 emits laser light, and the laser light emitted by the second laser 3 passes through the third optical fiber 7, the second optical fiber coupler 10, the fifth optical fiber 15, and the focusing lens group 18 on the surface of the sample 13 to be measured, and the focusing lens The group 18 receives the reflected light reflected by the surface of the sample 13 to be tested, and the reflected light enters the second detector 4 through the fifth optical fiber 15, the second optical fiber coupler 10, and the fourth optical fiber 8;
测量模式四:第二激光器3发射激光,第二激光器3发射的激光经第三光纤7、第二光纤耦合器10、第五光纤15、聚焦透镜组18射于待测样品13表面,探针光纤11的探针针尖接收待测样品13的透射光,该透射光经探针光纤11、第一光纤耦合器9、第二光纤6进入第一探测器2。Measurement mode four: the second laser 3 emits laser light, and the laser light emitted by the second laser 3 passes through the third optical fiber 7, the second optical fiber coupler 10, the fifth optical fiber 15, and the focusing lens group 18 on the surface of the sample 13 to be measured. The probe tip of the optical fiber 11 receives the transmitted light of the sample 13 to be tested, and the transmitted light enters the first detector 2 through the probe optical fiber 11 , the first optical fiber coupler 9 and the second optical fiber 6 .
作为本发明优选的实施方案,当待测样品13为透光样品时,采用测量模式一、测量模式二、测量模式三、测量模式四、测量模式一和测量模式二同时进行或者测量模式三与测量模式四同时进行的方式进行测量。As a preferred embodiment of the present invention, when the sample 13 to be tested is a light-transmitting sample, measurement mode one, measurement mode two, measurement mode three, measurement mode four, measurement mode one and measurement mode two are carried out simultaneously or measurement mode three and Measuring Mode Four Simultaneous measurement is carried out.
作为本发明优选的实施方案:当采用测量模式二进行测量时,探针光纤11的探针针尖16位于聚焦透镜组18的焦点上;当采用测量模式四进行测量时,探针光纤11的探针针尖16位于聚焦透镜组18的焦点上。As a preferred embodiment of the present invention: when using measurement mode two to measure, the probe tip 16 of the probe fiber 11 is located at the focus of the focusing lens group 18; when using measurement mode four to measure, the probe tip 16 of the probe fiber 11 The needle tip 16 is located at the focal point of a focusing lens group 18 .
作为本发明优选的实施方案,当待测样品13为非透光样品时,采用测量模式一进行测量。As a preferred embodiment of the present invention, when the sample 13 to be tested is a non-transparent sample, measurement mode 1 is used for measurement.
本发明所使用的探针为无孔式的光纤探针,通过在待测样品的上下表面选择性采用发射激光或收集激光的方式,可以实现四种不同的测量模式。测量系统使用光纤作为光传播的载体,让整个光路十分灵活,便于测量过程中的光路调试。The probe used in the present invention is a non-porous fiber optic probe, and four different measurement modes can be realized by selectively adopting the method of emitting laser light or collecting laser light on the upper and lower surfaces of the sample to be measured. The measurement system uses optical fiber as the carrier of light propagation, which makes the entire optical path very flexible and facilitates optical path debugging during the measurement process.
本发明的技术方案为分别提供两个相同的激光器和探测器,激光器的出射光和探测器的收集光均可由样品的上表面或下表面发射或收集,于是便可得到四种不同的测量模式,其中具有探针尖端的光纤始终位于样品上表面,具有尾端透镜组的光纤始终位于样品下表面。当选取的激光器和探测器光路位于样品上表面一侧时,样品表面近场光由探针针尖发出,收集光也由针 尖返回;当选取的激光器光路位于样品上表面而探测器光路位于样品下表面时,样品表面近场光由探针针尖发出,收集光被样品下方光纤收集;当选取的激光器光路位于样品下表面而探测器光路位于样品上表面时,样品表面近场光由样品下方入射到探针针尖和样品作用处,收集光被探针针尖收集;当选取的激光器和探测器光路位于样品下表面一侧时,样品表面近场光由样品下方入射到探针针尖和样品作用处,收集光被样品下方光纤收集。The technical solution of the present invention is to provide two identical lasers and detectors respectively. The emitted light of the laser and the collected light of the detector can be emitted or collected by the upper surface or the lower surface of the sample, so four different measurement modes can be obtained. , where the fiber with the probe tip is always on the upper surface of the sample, and the fiber with the tail lens set is always on the lower surface of the sample. When the optical path of the selected laser and detector is located on the side of the upper surface of the sample, the near-field light on the sample surface is emitted by the probe tip, and the collected light is also returned by the needle tip; when the selected optical path of the laser is located on the upper surface of the sample and the optical path of the detector is located under the sample When the surface is on the surface, the near-field light on the sample surface is emitted by the probe tip, and the collected light is collected by the optical fiber under the sample; when the selected laser optical path is located on the lower surface of the sample and the detector optical path is located on the upper surface of the sample, the near-field light on the sample surface is incident from below the sample When the probe tip and the sample interact, the collected light is collected by the probe tip; when the selected laser and detector optical path are located on the side of the lower surface of the sample, the near-field light on the sample surface is incident from the bottom of the sample to the probe tip and the sample interaction , the collected light is collected by the optical fiber below the sample.
本发明在近场光学测量中提供了两种在探针针尖处形成聚焦光斑方法,同时对于近场散射信号的收集也给出了两种方式,因此可以实现四种不同的测量模式。透光的待测样品可以在上下两个探测器同时实现近场散射光和透射光的测量成像,并且能提升近场信号的信噪比。测量系统采用光纤作为光传播的载体,操作灵活,便于调节和集成。The present invention provides two methods for forming focused light spots at the probe tip in near-field optical measurement, and provides two methods for collecting near-field scattering signals, so four different measurement modes can be realized. The light-transmitting sample to be tested can realize the measurement and imaging of near-field scattered light and transmitted light at the same time on the upper and lower detectors, and can improve the signal-to-noise ratio of near-field signals. The measurement system uses optical fiber as the carrier of light propagation, which is flexible in operation, easy to adjust and integrate.
实施例Example
如图1所示,本实施例基于近场无孔式探针的多模式测量系统采用两个相同的激光器,即第一激光器1和第二激光器3,两个相同的探测器,即第一探测器2和第一探测器4,工作时激光器与探测器均选取且只选取一个使用即可。激光器和探测器均连接有光纤(5、6、7、8),第一光纤耦合器9将第一光纤5、第二光纤6和探针光纤11的一端耦合连接在一起,第二光纤耦合器10则将第三光纤7第四光纤8和第五光纤15的一端耦合连接在一起。探针光纤11尾端针尖在夹持机构12的带动下可实现三维移动,第五光纤15的光纤尾端17连接透镜组14,透镜组14可将光会聚在一点。探针光纤11尾端针尖与透镜组14的中间为待测样品13的放置区,同时样品也将光路分为了上下两侧。参照图2,第一光纤耦合器9需要满足第一光纤5输出的光只能进入探针光纤11,探针光纤11输出的光只能进入第二光纤6中;第二光纤耦合器10需满足第三光纤7输出的光只能进入第五光纤15,第五光纤15输出的光只能进入第二光纤8中。As shown in Figure 1, the multi-mode measurement system based on the near-field non-porous probe in this embodiment uses two identical lasers, namely the first laser 1 and the second laser 3, and two identical detectors, namely the first For the detector 2 and the first detector 4, both the laser and the detector are selected during operation, and only one is selected for use. Both the laser and the detector are connected with optical fibers (5, 6, 7, 8), and the first optical fiber coupler 9 couples one end of the first optical fiber 5, the second optical fiber 6 and the probe optical fiber 11 together, and the second optical fiber coupler The device 10 couples and connects one end of the third optical fiber 7, the fourth optical fiber 8 and the fifth optical fiber 15 together. The needle tip at the tail end of the probe fiber 11 can move three-dimensionally under the drive of the clamping mechanism 12. The fiber tail 17 of the fifth fiber 15 is connected to the lens group 14, and the lens group 14 can converge the light at one point. The center between the needle point at the end of the probe fiber 11 and the lens group 14 is the placement area for the sample 13 to be tested, and the sample also divides the optical path into upper and lower sides. Referring to Fig. 2, the first optical fiber coupler 9 needs to satisfy that the light output by the first optical fiber 5 can only enter the probe optical fiber 11, and the light output by the probe optical fiber 11 can only enter the second optical fiber 6; the second optical fiber coupler 10 needs to The light output by the third optical fiber 7 can only enter the fifth optical fiber 15 , and the light output by the fifth optical fiber 15 can only enter the second optical fiber 8 .
根据选取激光器和探测器的不同,有四种测量模式,每种模式也就固定了所使用的测量光 路,第一种为使用第一激光器1和第一探测器2;第二种为使用第一激光器1和第二探测器4;第三种为使用第二激光器3和第一探测器2;第一种为使用第二激光器3和第二探测器4。每种模式的具体测量方式为:According to the choice of laser and detector, there are four measurement modes, and each mode also fixes the measurement optical path used. The first is to use the first laser 1 and the first detector 2; the second is to use the first A laser 1 and a second detector 4; the third is to use the second laser 3 and the first detector 2; the first is to use the second laser 3 and the second detector 4. The specific measurement methods for each mode are:
1)使用第一激光器1和第一探测器2,此时样品表面近场光由探针针尖发出,收集光也由针尖返回;1) Use the first laser 1 and the first detector 2. At this time, the near-field light on the sample surface is emitted by the probe tip, and the collected light is also returned by the needle tip;
2)使用第一激光器1和第二探测器4,此时样品表面近场光由探针针尖发出,收集光被样品下方光纤收集;2) Using the first laser 1 and the second detector 4, at this time, the near-field light on the sample surface is emitted by the probe tip, and the collected light is collected by the optical fiber under the sample;
3)使用第二激光器3和第一探测器2,此时样品表面近场光由样品下方入射到探针针尖和样品作用处,收集光被探针针尖收集;3) Using the second laser 3 and the first detector 2, at this time, the near-field light on the sample surface is incident on the probe tip and the sample from below the sample, and the collected light is collected by the probe tip;
4)使用第二激光器3和第二探测器4,此时样品表面近场光由样品下方入射到探针针尖和样品作用处,收集光被样品下方光纤收集。4) The second laser 3 and the second detector 4 are used. At this time, the near-field light on the sample surface is incident on the probe tip and the sample from below the sample, and the collected light is collected by the optical fiber below the sample.
其中,第二种和第三种模式下,探针光纤11与第五光纤15连用,两个光纤中心轴要重合且探针光纤11尾端针尖要调至透镜组14的上方焦点处,此时光信号的收集量最高。Wherein, under the second and third modes, the probe fiber 11 is used in conjunction with the fifth fiber 15, the central axes of the two fibers should coincide and the needle tip at the tail end of the probe fiber 11 should be adjusted to the upper focal point of the lens group 14. Time signal collection is the highest.
如果待测样品13为透光样品,则可以采用四种不同的模式来进行近场光学测量。第一种为使用第一激光器1和第一探测器2;第二种为使用第一激光器1和第二探测器4;第三种为使用第二激光器3和第一探测器2;第四种为使用第二激光器3和第二探测器4。其中第一种和第二种可同时使用,测量散射光和透射光,即第一激光器1和探第二测器2、第二探测器4;第三种和第四种可同时使用,测量散射光和透射光,即第二激光器3和第一探测器2、第二探测器4。两者区别在于入射光从样品的上表面或下表面照射。If the sample 13 to be tested is a light-transmitting sample, four different modes can be used for near-field optical measurement. The first is to use the first laser 1 and the first detector 2; the second is to use the first laser 1 and the second detector 4; the third is to use the second laser 3 and the first detector 2; the fourth One is to use a second laser 3 and a second detector 4 . Among them, the first and the second can be used at the same time to measure scattered light and transmitted light, that is, the first laser 1 and the second detector 2 and the second detector 4; the third and the fourth can be used at the same time to measure Scattered light and transmitted light, that is, the second laser 3 and the first detector 2 and the second detector 4 . The difference between the two is that the incident light is irradiated from the upper surface or the lower surface of the sample.
如果待测样品13的为非透光样品,那么选择第一激光器1和第一探测器2连用。If the sample 13 to be tested is a non-transparent sample, then select the first laser 1 and the first detector 2 to be used together.
本发明针对一个栅格结构,同时进行了第一种和第二种方式的近场光学成像测试,将探针光纤11与第五光纤15的中心轴重合且探针光纤11尾端针尖调至透镜组14的上方焦点处,同 时得到了样品的散射近场光学图像(如图5所示)和透射近场光学图像(如图6所示),从结果可以看出,两幅图的信噪比都很高,且能相互比对证实结果准确性。The present invention carries out the near-field optical imaging test of the first and second modes simultaneously for a grid structure, the central axes of the probe fiber 11 and the fifth fiber 15 are coincident and the tip of the probe fiber 11 tail end is adjusted to At the focal point above the lens group 14, the scattering near-field optical image (as shown in FIG. 5 ) and the transmission near-field optical image (as shown in FIG. 6 ) of the sample are simultaneously obtained. As can be seen from the results, the signal of the two images is The noise ratios are all high, and can be compared with each other to confirm the accuracy of the results.
综上,本发明所涉及的基于近场无孔式探针的多模式测量方法及测量系统与当前的近场测量光路相比,特点和优势非常突出,有以下几点:To sum up, compared with the current near-field measurement optical path, the multi-mode measurement method and measurement system based on the near-field non-porous probe involved in the present invention has very prominent features and advantages, including the following points:
1)可实现四种不同的测量模式,从四种不同方面研究待测样品的物理光学性质。1) Four different measurement modes can be realized, and the physical optical properties of the sample to be tested can be studied from four different aspects.
2)每种模式的测量分辨率都可达目前近场光学测量的最高分辨率。2) The measurement resolution of each mode can reach the highest resolution of current near-field optical measurement.
3)采用光纤光路并搭配光纤探针,光路十分灵活,给实验操作提供很大的便利。3) The optical fiber optical path is used together with the optical fiber probe, the optical path is very flexible, which provides great convenience for the experimental operation.
Claims (10)
- 一种基于近场无孔式探针的多模式测量系统,其特征在于,包括第一激光器(1)、第一探测器(2)、第二激光器(3)、第二探测器(4)、第一光纤耦合器(9)、第二光纤耦合器(10)、探针光纤(11)、聚焦透镜组(18)、第一光纤(5)、第二光纤(6)、第三光纤(7)、第四光纤(8)和第五光纤(15);A multi-mode measurement system based on a near-field non-porous probe, characterized in that it includes a first laser (1), a first detector (2), a second laser (3), and a second detector (4) , the first fiber coupler (9), the second fiber coupler (10), the probe fiber (11), the focusing lens group (18), the first fiber (5), the second fiber (6), the third fiber (7), the fourth optical fiber (8) and the fifth optical fiber (15);第一光纤耦合器(9)和第二光纤耦合器(10)均包括输入端(24)、第一输出端(25)、第二输出端(26)、第一反射镜(21)、分束镜(20)、第二反射镜(22)和第三反射镜(23),第一反射镜(21)设置于输入端(24)入射光的光路上,分束镜(20)和第一输出端(25)均位于第一反射镜(21)反射光的光路上,分束镜(20)有镀膜的一侧朝向第一输出端(25),第二反射镜(22)位于分束镜(20)有镀膜的一侧的反射光的光路上,第三反射镜(23)位于第二反射镜(22)反射光的光路上,第二输出端(26)位于第三反射镜(23)反射光的光路上,分束镜(20)的透反比不小于1;Both the first fiber coupler (9) and the second fiber coupler (10) include an input port (24), a first output port (25), a second output port (26), a first reflector (21), a splitter The beam mirror (20), the second reflector (22) and the third reflector (23), the first reflector (21) is arranged on the optical path of the input end (24) incident light, the beam splitter (20) and the third One output end (25) is located on the optical path of the reflected light of the first reflector (21), the coated side of the beam splitter (20) faces the first output end (25), and the second reflector (22) is located at the splitter On the optical path of the reflected light on the side of the beam mirror (20) with coating, the third reflector (23) is located on the optical path of the reflected light of the second reflector (22), and the second output terminal (26) is located on the third reflector (23) On the optical path of the reflected light, the transmittance ratio of the beam splitter (20) is not less than 1;第一光纤(5)、第二光纤(6)和探针光纤(11)分别与第一光纤耦合器(9)的输入端、第二输出端和第一输出端连接,第一光纤耦合器(9)的,第一光纤(5)与第一激光器(1)连接,第二光纤(6)与第一探测器(2)连接;The first optical fiber (5), the second optical fiber (6) and the probe optical fiber (11) are respectively connected with the input end, the second output end and the first output end of the first optical fiber coupler (9), and the first optical fiber coupler (9), the first optical fiber (5) is connected to the first laser (1), and the second optical fiber (6) is connected to the first detector (2);第三光纤(7)、第四光纤(8)和第五光纤(15)分别与第二光纤耦合器(10)的输入端、第二输出端和第一输出端的连接,第三光纤(7)与第二激光器(3)连接,第四光纤(8)第二探测器(4)连接,第五光纤(15)与聚焦透镜组(18)连接;The third optical fiber (7), the fourth optical fiber (8) and the fifth optical fiber (15) are respectively connected with the input end, the second output end and the first output end of the second optical fiber coupler (10), and the third optical fiber (7) ) is connected with the second laser (3), the fourth optical fiber (8) is connected with the second detector (4), and the fifth optical fiber (15) is connected with the focusing lens group (18);探针光纤(11)的探针针尖(16)的轴线与聚焦透镜组(18)的轴线同轴。The axis of the probe tip (16) of the probe fiber (11) is coaxial with the axis of the focusing lens group (18).
- 根据权利要求1所述的一种基于近场无孔式探针的多模式测量系统,其特征在于,探针光纤(11)的探针针尖(16)位于聚焦透镜组(18)的焦点上。The multi-mode measurement system based on a near-field non-porous probe according to claim 1, wherein the probe tip (16) of the probe fiber (11) is located at the focal point of the focusing lens group (18) .
- 根据权利要求1所述的一种基于近场无孔式探针的多模式测量系统,其特征在于,第一激光器(1)和第二激光器(3)相同。The multi-mode measurement system based on near-field non-porous probe according to claim 1, characterized in that the first laser (1) and the second laser (3) are the same.
- 根据权利要求1所述的一种基于近场无孔式探针的多模式测量系统,其特征在于,第一探测器(2)和第二探测器(4)相同。The multi-mode measurement system based on near-field non-porous probe according to claim 1, characterized in that the first detector (2) and the second detector (4) are the same.
- 根据权利要求1所述的一种基于近场无孔式探针的多模式测量系统,其特征在于,探针光纤(11)的探针针尖(16)为一锥形尖端结构。The multi-mode measurement system based on a near-field non-porous probe according to claim 1, characterized in that the probe tip (16) of the probe fiber (11) is a tapered tip structure.
- 根据权利要求1-5任意一项所述的一种基于近场无孔式探针的多模式测量系统,其特征在于,还包括三维移动平台,三维移动平台上设有能够进行三维移动的夹持机构(12),探针光纤(11)上具有探针针尖(16)的一端安装于所述夹持机构(12)上。A multi-mode measurement system based on a near-field non-porous probe according to any one of claims 1-5, characterized in that it also includes a three-dimensional mobile platform, and a clamp capable of three-dimensional movement is provided on the three-dimensional mobile platform. A holding mechanism (12), one end of the probe fiber (11) having a probe tip (16) is installed on the holding mechanism (12).
- 一种基于近场无孔式探针的多模式测量方法,其特征在于,采用权利要求1-6任意一项所述的基于近场无孔式探针的多模式测量系统进行,包括:A multi-mode measurement method based on a near-field non-porous probe, characterized in that the multi-mode measurement system based on a near-field non-porous probe according to any one of claims 1-6 is used, including:将待测样品(13)设置于探针针尖(16)与聚焦透镜组(18)之间;The sample to be measured (13) is arranged between the probe tip (16) and the focusing lens group (18);采用如下至少一种测量模式进行测量:Take measurements using at least one of the following measurement modes:测量模式一:第一激光器(1)发射激光,第一激光器(1)发射的激光经第一光纤(5)、第一光纤耦合器(9)、探针光纤(11)的探针针尖射于待测样品(13)表面,探针光纤(11)的探针针尖接收经待测样品(13)表面反射的反射光,该反射光经探针光纤(11)、第一光纤耦合器(9)、第二光纤(6)进入第一探测器(2);Measurement mode 1: the first laser (1) emits laser light, and the laser light emitted by the first laser (1) is emitted through the probe tip of the first optical fiber (5), the first optical fiber coupler (9), and the probe optical fiber (11). On the surface of the sample to be measured (13), the probe tip of the probe fiber (11) receives the reflected light reflected from the surface of the sample to be measured (13), and the reflected light passes through the probe fiber (11), the first fiber coupler ( 9), the second optical fiber (6) enters the first detector (2);测量模式二:第一激光器(1)发射激光,第一激光器(1)发射的激光经第一光纤(5)、第一光纤耦合器(9)、探针光纤(11)的探针针尖射于待测样品(13)表面,第五光纤(15)经聚焦透镜组(18)接收待测样品(13)的透射光,该透射光经第五光纤(15)、第二光纤耦合器(10)和第四光纤(8)进入第二探测器(4);Measurement mode 2: the first laser (1) emits laser light, and the laser light emitted by the first laser (1) is emitted through the probe tip of the first optical fiber (5), the first optical fiber coupler (9), and the probe optical fiber (11). On the surface of the sample to be measured (13), the fifth optical fiber (15) receives the transmitted light of the sample to be measured (13) through the focusing lens group (18), and the transmitted light passes through the fifth optical fiber (15), the second fiber coupler ( 10) and the fourth optical fiber (8) enter the second detector (4);测量模式三:第二激光器(3)发射激光,第二激光器(3)发射的激光经第三光纤(7)、第二光纤耦合器(10)、第五光纤(15)、聚焦透镜组(18)射于待测样品(13)表面,聚焦透镜组(18)接收经待测样品(13)表面反射的反射光,该反射光经第五光纤(15)、第二光纤 耦合器(10)、第四光纤(8)进入第二探测器(4);Measurement mode three: the second laser (3) emits laser light, and the laser light emitted by the second laser (3) passes through the third optical fiber (7), the second optical fiber coupler (10), the fifth optical fiber (15), and the focusing lens group ( 18) emit on the surface of the sample to be measured (13), the focusing lens group (18) receives the reflected light reflected by the surface of the sample to be measured (13), and the reflected light passes through the fifth optical fiber (15), the second optical fiber coupler (10 ), the fourth optical fiber (8) enters the second detector (4);测量模式四:第二激光器(3)发射激光,第二激光器(3)发射的激光经第三光纤(7)、第二光纤耦合器(10)、第五光纤(15)、聚焦透镜组(18)射于待测样品(13)表面,探针光纤(11)的探针针尖接收待测样品(13)的透射光,该透射光经探针光纤(11)、第一光纤耦合器(9)、第二光纤(6)进入第一探测器(2)。Measurement mode four: the second laser (3) emits laser light, and the laser light emitted by the second laser (3) passes through the third optical fiber (7), the second optical fiber coupler (10), the fifth optical fiber (15), and the focusing lens group ( 18) shoot on the surface of the sample to be measured (13), the probe tip of the probe fiber (11) receives the transmitted light of the sample to be measured (13), and the transmitted light passes through the probe fiber (11), the first fiber coupler ( 9), the second optical fiber (6) enters the first detector (2).
- 根据权利要求7所述的一种基于近场无孔式探针的多模式测量方法,其特征在于,当待测样品(13)为透光样品时,采用测量模式一、测量模式二、测量模式三、测量模式四、测量模式一和测量模式二同时进行或者测量模式三与测量模式四同时进行的方式进行测量。The multi-mode measurement method based on a near-field non-porous probe according to claim 7, wherein when the sample to be measured (13) is a light-transmitting sample, measurement mode one, measurement mode two, measurement mode Mode 3, measurement mode 4, measurement mode 1 and measurement mode 2 at the same time, or measurement mode 3 and measurement mode 4 at the same time.
- 根据权利要求7或8所述的一种基于近场无孔式探针的多模式测量方法,其特征在于:A kind of multi-mode measurement method based on near-field non-porous probe according to claim 7 or 8, characterized in that:当采用测量模式二进行测量时,探针光纤(11)的探针针尖(16)位于聚焦透镜组(18)的焦点上;When using measurement mode two to measure, the probe tip (16) of the probe fiber (11) is located at the focal point of the focusing lens group (18);当采用测量模式四进行测量时,探针光纤(11)的探针针尖(16)位于聚焦透镜组(18)的焦点上。When measurement is carried out in measurement mode four, the probe tip (16) of the probe fiber (11) is located at the focal point of the focusing lens group (18).
- 根据权利要求7所述的一种基于近场无孔式探针的多模式测量方法,其特征在于,当待测样品(13)为非透光样品时,采用测量模式一进行测量。The multi-mode measurement method based on near-field non-porous probe according to claim 7, characterized in that, when the sample to be measured (13) is a non-transparent sample, measurement mode 1 is used for measurement.
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