WO2021253838A1 - 一种高效节能自动溶铜技术 - Google Patents

一种高效节能自动溶铜技术 Download PDF

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WO2021253838A1
WO2021253838A1 PCT/CN2021/074566 CN2021074566W WO2021253838A1 WO 2021253838 A1 WO2021253838 A1 WO 2021253838A1 CN 2021074566 W CN2021074566 W CN 2021074566W WO 2021253838 A1 WO2021253838 A1 WO 2021253838A1
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fixedly installed
tank
liquid pipe
stirring
pipe
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French (fr)
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陈晓东
陈泽仁
黄国和
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江西鑫铂瑞科技有限公司
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    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27BFURNACES, KILNS, OVENS, OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
    • F27B15/00Fluidised-bed furnaces; Other furnaces using or treating finely-divided materials in dispersion
    • F27B15/02Details, accessories, or equipment peculiar to furnaces of these types
    • F27B15/10Arrangements of air or gas supply devices
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/20Mixing gases with liquids
    • B01F23/23Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids
    • B01F23/233Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids using driven stirrers with completely immersed stirring elements
    • B01F23/2331Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids using driven stirrers with completely immersed stirring elements characterised by the introduction of the gas along the axis of the stirrer or along the stirrer elements
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/20Mixing gases with liquids
    • B01F23/23Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids
    • B01F23/233Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids using driven stirrers with completely immersed stirring elements
    • B01F23/2331Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids using driven stirrers with completely immersed stirring elements characterised by the introduction of the gas along the axis of the stirrer or along the stirrer elements
    • B01F23/23314Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids using driven stirrers with completely immersed stirring elements characterised by the introduction of the gas along the axis of the stirrer or along the stirrer elements through a hollow stirrer element
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/40Static mixers
    • B01F25/45Mixers in which the materials to be mixed are pressed together through orifices or interstitial spaces, e.g. between beads
    • B01F25/452Mixers in which the materials to be mixed are pressed together through orifices or interstitial spaces, e.g. between beads characterised by elements provided with orifices or interstitial spaces
    • B01F25/4523Mixers in which the materials to be mixed are pressed together through orifices or interstitial spaces, e.g. between beads characterised by elements provided with orifices or interstitial spaces the components being pressed through sieves, screens or meshes which obstruct the whole diameter of the tube
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/05Stirrers
    • B01F27/07Stirrers characterised by their mounting on the shaft
    • B01F27/072Stirrers characterised by their mounting on the shaft characterised by the disposition of the stirrers with respect to the rotating axis
    • B01F27/0726Stirrers characterised by their mounting on the shaft characterised by the disposition of the stirrers with respect to the rotating axis having stirring elements connected to the stirrer shaft each by a single radial rod, other than open frameworks
    • B01F27/07261Stirrers characterised by their mounting on the shaft characterised by the disposition of the stirrers with respect to the rotating axis having stirring elements connected to the stirrer shaft each by a single radial rod, other than open frameworks of the anchor type, i.e. the stirring elements being connected to the rods by one end and extending parallel to the shaft axis
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    • B01F33/00Other mixers; Mixing plants; Combinations of mixers
    • B01F33/86Mixing heads comprising a driven stirrer
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/45Closures or doors specially adapted for mixing receptacles; Operating mechanisms therefor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/90Heating or cooling systems
    • B01F35/91Heating or cooling systems using gas or liquid injected into the material, e.g. using liquefied carbon dioxide or steam
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006Controlling or regulating processes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006Controlling or regulating processes
    • B01J19/0013Controlling the temperature of the process
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0066Stirrers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0073Sealings
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00Feed or outlet devices; Feed or outlet control devices
    • B01J4/001Feed or outlet devices as such, e.g. feeding tubes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00Feed or outlet devices; Feed or outlet control devices
    • B01J4/001Feed or outlet devices as such, e.g. feeding tubes
    • B01J4/002Nozzle-type elements
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00Feed or outlet devices; Feed or outlet control devices
    • B01J4/001Feed or outlet devices as such, e.g. feeding tubes
    • B01J4/004Sparger-type elements
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00Feed or outlet devices; Feed or outlet control devices
    • B01J4/008Feed or outlet control devices
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G3/00Compounds of copper
    • C01G3/10Sulfates
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F2101/00Mixing characterised by the nature of the mixed materials or by the application field
    • B01F2101/45Mixing in metallurgical processes of ferrous or non-ferrous materials
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/20Mixing gases with liquids
    • B01F23/23Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids
    • B01F23/237Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids characterised by the physical or chemical properties of gases or vapours introduced in the liquid media
    • B01F23/2376Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids characterised by the physical or chemical properties of gases or vapours introduced in the liquid media characterised by the gas being introduced
    • B01F23/23761Aerating, i.e. introducing oxygen containing gas in liquids
    • B01F23/237612Oxygen
    • BPERFORMING OPERATIONS; TRANSPORTING
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    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2204/00Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices
    • B01J2204/002Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices the feeding side being of particular interest
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2204/00Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices
    • B01J2204/005Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices the outlet side being of particular interest
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00121Controlling the temperature by direct heating or cooling
    • B01J2219/00123Controlling the temperature by direct heating or cooling adding a temperature modifying medium to the reactants
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G1/00Methods of preparing compounds of metals not covered by subclasses C01B, C01C, C01D, or C01F, in general
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
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    • Y02P20/10Process efficiency
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
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Abstract

一种高效节能自动溶铜技术,包括外设(1),外设(1)包含作为主体的罐体(101),罐体(101)的底部周边固定安装有底座(102),底座(102)的底部固定安装有支撑(103),罐体(101)的顶部盖接有上搅拌装置(2),上搅拌装置(2)的顶部安装的是顶盖(201),顶盖(201)的下方固定安装有密封垫(202),密封垫(202)的中间部位固定安装有搅拌电机(203),搅拌电机(203)的中间部位固定安装有立柱(204),立柱(204)的周围边缘固定安装有搅拌辊(205),罐体(101)内部的上半部位放置有测头(3),测头(3)的末端固定安装有电线(4),电线(4)的一侧末端并联连接有空气悬浮风机(5),电线(4)的另一侧末端固定连接有DCS检测装置(6),罐体(101)的内部中间部位固定安装有筛板(7),罐体(101)的左侧边固定安装有风管(8),罐体(101)的右侧边固定安装有液管(9),风管(8)的末端固定安装有风管搅拌器(10),液管(9)的右端固定安装有液管搅拌器(11),风管搅拌器(10)与液管搅拌器(11)固定安装于罐体(101)内部的底端。

Description

一种高效节能自动溶铜技术 技术领域
本实用新型涉及硫酸铜制备技术领域,具体为一种高效节能自动溶铜技术。
背景技术
把铜线或电解铜块在硫酸的作用下制成CuSO4溶液必须具备空气、水、铜料、温度。
反应式:2Cu+2H2SO4+O2 加热  CuSO4+H2O
那么空气提供氧就至关重要,铜首先要和氧气产生氧化反应,然后CuO再和硫酸反应生成CuSO4,铜氧化的速度越快,生成CuSO4就越快;供氧靠溶铜罐底部的风管、液管提供,供液里含O2越多越均匀,溶铜速度就越快,采用气液对向喷射的方式使氧气充分和溶液混合,再通过筛板均匀细密的流通孔能使空气中的氧气进一步充分混合在溶液里面,通过溶液的向上流动使氧和铜料表面充分接触,使铜料表面充分氧化,达到简单高效溶铜的效果。
但是现有技术在制备铜盐的过程中,样式多元化,使用过程中会出现不同程度供风不均、溶铜效果差、能耗大、数据滞后、过程控制波动大、自动化程度差的现象,非常不利于稳定生产,高效节能。
为此我们提出一种高效节能自动溶铜技术用于解决上述问题。
技术问题
本发明的目的在于提供一种高效节能自动溶铜技术,以解决上述背景技术中提出的问题。
技术解决方案
为实现上述目的,本发明提供如下技术方案:一种高效节能自动溶铜技术,包括外设,所述外设包含作为主体的罐体,所述罐体的底部周边固定安装有底座的底部固定安装有支撑,所述罐体的顶部盖接有上搅拌装置,所述上搅拌装置的顶部安装的是顶盖,所述顶盖的下方固定安装有密封垫,所述密封垫的中间部位固定安装有搅拌电机,所述搅拌电机的中间部位固定安装有立柱,所述立柱的周围边缘固定安装有搅拌辊,所述罐体内部的上半部为放置有测头,所述测头的末端固定安装有电线,所述电线的一侧末端并联连接有空气悬浮风机,所述电线的另一侧末端固定连接有DCS检测装置,所述罐体的内部中间部位固定安装有筛板,所述罐体的左侧边固定安装有风管,所述罐体的右侧边固定安装有液管,所述风管的末端固定安装有风管搅拌器,所述液管的右端固定安装有液管搅拌器,所述风管搅拌器与所述液管搅拌器固定安装于所述罐体内部的底端。
优选的一种实施案例,所述液管的末端外接有冲液泵,所述罐体内部的顶端固定安装有出料泵,所述罐体的底部固定安装有进料泵。
优选的一种实施案例,所述液管搅拌器的进口处固定安装有不锈钢,所述不锈钢的末端固定安装有转接头,所述转接头的末端固定安装有L管,所述L管的末端固定安装有轴承,所述轴承通过密封垫密封安装在球腔的内部,所述球腔的底部周边导通安装有若干个搅拌棒,所述搅拌棒的外圈固定安装有环,所述搅拌棒与所述环的表面开设有若干个孔,所述球腔远离所述转接头的一侧固定焊接安装有联轴器,所述联轴器的末端固定安装有混合电机。
优选的一种实施案例,所述不锈钢的外表固定安装有海绵保温层,所述筛板的内部开设有均匀密布的筛孔,筛孔的直径为1mm。
优选的一种实施案例,所述风管的末端安装与所述液管末端相同的搅拌器,即所述风管搅拌器与所述液管搅拌器的结构形状尺寸一致,所述风管搅拌器与所述液管搅拌器之间保留10cm的对冲空间。
有益效果
与现有技术相比,本发明的有益效果是:
本技术的气液对向喷射能使氧气充分均匀混合,结构简单高效,达到溶铜速度400kg/h的能力;充分利用空气悬浮风机20000转/分钟转动产生90℃-120℃温度的热空气对溶液进行加热,节省了锅炉蒸汽或电锅炉热水对溶液的加热,节省了锅炉或热水锅炉44.9万元的设备投资,运行电费节省了约16716元/天;用设备代替人工调整,实现稳定生产、工厂智能化。
附图说明
图1为本发明结构示意图;
图2为本发明的结构简图;
图3为本发明搅拌器的结构示意图。
图中:1外设、101罐体、102底座、103支撑、2上搅拌装置、201顶盖、202密封垫、203搅拌电机、204立柱、205搅拌辊、3测头、4电线、5空气悬浮风机、6DNS检测装置、7筛板、8风管、9液管、10风管搅拌器、11液管搅拌器、12混合电机、13充液泵、14除料泵、15进料泵、1101304不锈钢、1102转接头、1103316L管、1104轴承、1105球腔、1106搅拌棒、1107孔、1108环、1109联轴器。
本发明的最佳实施方式
下面将结合本发明实施例中的附图,对本发明实施例中的技术方案进行清楚、完整地描述,显然,所描述的实施例仅仅是本发明的一部分实施例,而不是全部的实施例。基于本发明中的实施例,本领域普通技术人员在没有做出创造性劳动前提下所获得的所有其他实施例,都属于本发明保护的范围。
请参阅图1-3,本发明提供一种技术方案:一种高效节能自动溶铜技术,包括外设1,外设1包含作为主体的罐体101,罐体101的底部周边固定安装有底座102的底部固定安装有支撑103;
为了使得装置内部的铜块搅拌的更加充分,本装置设置了搅拌器装置,具体为:罐体101的顶部盖接有上搅拌装置2,上搅拌装置2的顶部安装的是用于装置密封盖接的顶盖201,顶盖201的下方固定安装有防止泄露的密封垫202,密封垫202的中间部位固定安装有驱动装置搅拌电机203,搅拌电机203的中间部位固定安装有转轴装置立柱204,立柱204的周围边缘固定安装有搅拌辊205,搅拌辊205可以直接实现对装置内部的铜片进行均匀的搅拌。
本装置外接了国际先进的铜离子检测装置,通过控制空气悬浮风机5的转速,进而控制风管8的进气温度,使得装置内部的气液混合速率发生改变,进而实时的控制装置内部的反应速率,保证反应的平衡。为了保证检测的准确性,罐体101内部的上半部为放置有测头3,测头3的末端固定安装有电线4,电线4的一侧末端并联连接有空气悬浮风机5,空气悬浮电机5可以通过扇叶搅动空气而形成90℃到140℃的温度,为化学反应提供相应的反应温度;电线4的另一侧末端固定连接有用于终端检测DCS检测装置6;
为了增加气液混合的混合度,罐体101的内部中间部位固定安装有筛板7,液体在被推出筛板7的过程中会出现打泡的现象,进一步的增进了氧气的溶解;装置的两端分别作为进料的主部位,罐体101的左侧边固定安装有风管8,为反应提供足量的氧气和温度;罐体101的右侧边固定安装有液管9,为反应提供足量的水;为了实现气液混合更加的充分,风管8的末端固定安装有风管搅拌器10,液管9的右端固定安装有液管搅拌器11,风管搅拌器9与液管搅拌器11固定安装于罐体101内部的底端;
液管搅拌器11的进口处固定安装有304不锈钢1101,304不锈钢1101的末端固定安装有转接头1102,转接头1102的末端固定安装有316L管1103,目的是防止腐蚀的出现;为了分隔转动与静止,316L管1103的末端固定安装有轴承1104,轴承1104通过密封垫密封安装在收纳装置球腔1105的内部;为了实现搅拌器的搅拌功能,球腔1105的底部周边导通安装有若干个搅拌棒1106,搅拌棒1106的外圈固定安装有固定限位装置环1108,搅拌棒1106与环1108的表面开设有若干个孔1107-孔位之间的空气与液体相互对喷,实现气液的充分混合。球腔1105远离转接头1102的一侧固定焊接安装有联轴器1109,联轴器1109的末端固定安装有混合电机12。。
液管9的末端外接有冲液泵13,罐体101内部的顶端固定安装有出料泵14,罐体101的底部固定安装有进料泵15。
304不锈钢1101的外表固定安装有海绵保温层,筛板7的内部开设有均匀密布的筛孔,筛孔的直径为1mm。
风管8的末端安装与液管9末端相同的搅拌器,即风管搅拌器10与液管搅拌器11的结构形状尺寸一致,风管搅拌器10与液管搅拌器11之间保留10cm的对冲空间。
工作原理:
外设1包含作为主体的罐体101,罐体101的底部周边固定安装有底座102的底部固定安装有支撑103;
为了使得装置内部的铜块搅拌的更加充分,本装置设置了搅拌器装置,具体为:罐体101的顶部盖接有上搅拌装置2,上搅拌装置2的顶部安装的是用于装置密封盖接的顶盖201,顶盖201的下方固定安装有防止泄露的密封垫202,密封垫202的中间部位固定安装有驱动装置搅拌电机203,搅拌电机203的中间部位固定安装有转轴装置立柱204,立柱204的周围边缘固定安装有搅拌辊205,搅拌辊205可以直接实现对装置内部的铜片进行均匀的搅拌。
本装置外接了国际先进的铜离子检测装置,通过控制空气悬浮风机5的转速,进而控制风管8的进气温度,使得装置内部的气液混合速率发生改变,进而实时的控制装置内部的反应速率,保证反应的平衡。为了保证检测的准确性,罐体101内部的上半部为放置有测头3,测头3的末端固定安装有电线4,电线4的一侧末端并联连接有空气悬浮风机5,空气悬浮电机5可以通过扇叶搅动空气而形成90℃到140℃的温度,为化学反应提供相应的反应温度;电线4的另一侧末端固定连接有用于终端检测DCS检测装置6;
为了增加气液混合的混合度,罐体101的内部中间部位固定安装有筛板7,液体在被推出筛板7的过程中会出现打泡的现象,进一步的增进了氧气的溶解;装置的两端分别作为进料的主部位,罐体101的左侧边固定安装有风管8,为反应提供足量的氧气和温度;罐体101的右侧边固定安装有液管9,为反应提供足量的水;为了实现气液混合更加的充分,风管8的末端固定安装有风管搅拌器10,液管9的右端固定安装有液管搅拌器11,风管搅拌器9与液管搅拌器11固定安装于罐体101内部的底端;液管搅拌器11的进口处固定安装有304不锈钢1101,304不锈钢1101的末端固定安装有转接头1102,转接头1102的末端固定安装有316L管1103,目的是防止腐蚀的出现;为了分隔转动与静止,316L管1103的末端固定安装有轴承1104,轴承1104通过密封垫密封安装在收纳装置球腔1105的内部;为了实现搅拌器的搅拌功能,球腔1105的底部周边导通安装有若干个搅拌棒1106,搅拌棒1106的外圈固定安装有固定限位装置环1108,搅拌棒1106与环1108的表面开设有若干个孔1107-孔位之间的空气与液体相互对喷,实现气液的充分混合。球腔1105远离转接头1102的一侧固定焊接安装有联轴器1109,联轴器1109的末端固定安装有混合电机12。。
液管9的末端外接有冲液泵13,罐体101内部的顶端固定安装有出料泵14,罐体101的底部固定安装有进料泵15。304不锈钢1101的外表固定安装有海绵保温层,筛板7的内部开设有均匀密布的筛孔,筛孔的直径为1mm。风管8的末端安装与液管9末端相同的搅拌器,即风管搅拌器10与液管搅拌器11的结构形状尺寸一致,风管搅拌器10与液管搅拌器11之间保留10cm的对冲空间。
总结:铜线或铜料必须在60℃-85℃的温度范围内生成CuSO4溶液的速度最快,利用供氧(空气)空气悬浮风机20000转/分钟的高转速,风机叶片和空气摩擦产生大量的热能使空气升温到90℃-120℃,通风管采用304不锈钢(外层加保温),进入溶铜罐采用316L管(防腐蚀),满足生成CuSO4溶液的温度条件。
采用国际先进的铜/酸离子在线检测仪在线实时检测数据,并把数据传入DCS控制系统,DCS控制系统根据设定的范围及数据分析,然后对送风机进行频率的调整,调整风量的大小或关停/开启,以空气中的含氧量控制铜的氧化速度,从而控制硫酸铜的生成速度,达到铜离子的生成和损耗平衡。
尽管已经示出和描述了本实用新型的实施例,对于本领域的普通技术人员而言,可以理解在不脱离本实用新型的原理和精神的情况下可以对这些实施例进行多种变化、修改、替换和变型,本实用新型的范围由所附权利要求及其等同物限定。

Claims (5)

  1. [根据细则26改正16.03.2021] 
    1.一种高效节能自动溶铜技术,包括外设(1),其特征在于:所述外设(1)包含作为主体的罐体(101),所述罐体(101)的底部周边固定安装有底座(102)的底部固定安装有支撑(103),所述罐体(101)的顶部盖接有上搅拌装置(2),所述上搅拌装置(2)的顶部安装的是顶盖(201),所述顶盖(201)的下方固定安装有密封垫(202),所述密封垫(202)的中间部位固定安装有搅拌电机(203),所述搅拌电机(203)的中间部位固定安装有立柱(204),所述立柱(204)的周围边缘固定安装有搅拌辊(205),所述罐体(101)内部的上半部为放置有测头(3),所述测头(3)的末端固定安装有电线(4),所述电线(4)的一侧末端并联连接有空气悬浮风机(5),所述电线(4)的另一侧末端固定连接有DCS检测装置(6),所述罐体(101)的内部中间部位固定安装有筛板(7),所述罐体(101)的左侧边固定安装有风管(8),所述罐体(101)的右侧边固定安装有液管(9),所述风管(8)的末端固定安装有风管搅拌器(10),所述液管(9)的右端固定安装有液管搅拌器(11),所述风管搅拌器(9)与所述液管搅拌器(11)固定安装于所述罐体(101)内部的底端。
  2. 2.根据权利要求1所述的一种高效节能自动溶铜技术,其特征在于:所述液管(9)的末端外接有冲液泵(13),所述罐体(101)内部的顶端固定安装有出料泵(14),所述罐体(101)的底部固定安装有进料泵(15)。
  3. 3.根据权利要求1所述的一种高效节能自动溶铜技术,其特征在于:所述液管搅拌器(11)的进口处固定安装有304不锈钢(1101),所述304不锈钢(1101)的末端固定安装有转接头(1102),所述转接头(1102)的末端固定安装有316L管(1103),所述316L管(1103)的末端固定安装有轴承(1104),所述轴承(1104)通过密封垫密封安装在球腔(1105)的内部,所述球腔(1105)的底部周边导通安装有若干个搅拌棒(1106),所述搅拌棒(1106)的外圈固定安装有环(1108),所述搅拌棒(1106)与所述环(1108)的表面开设有若干个孔(1107),所述球腔(1105)远离所述转接头(1102)的一侧固定焊接安装有联轴器(1109),所述联轴器(1109)的末端固定安装有混合电机(12)。
  4. 4.根据权利要求1所述的一种高效节能自动溶铜技术,其特征在于:所述304不锈钢(1101)的外表固定安装有海绵保温层,所述筛板(7)的内部开设有均匀密布的筛孔,筛孔的直径为1mm。
  5. 5.根据权利要求1所述的一种高效节能自动溶铜技术,其特征在于:所述风管(8)的末端安装与所述液管(9)末端相同的搅拌器,即所述风管搅拌器(10)与所述液管搅拌器(11)的结构形状尺寸一致,所述风管搅拌器(10)与所述液管搅拌器(11)之间保留10cm的对冲空间。
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