WO2021200783A9 - アミデート化合物及びその製造方法、ブロック剤解離触媒並びに熱硬化性樹脂組成物 - Google Patents

アミデート化合物及びその製造方法、ブロック剤解離触媒並びに熱硬化性樹脂組成物 Download PDF

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WO2021200783A9
WO2021200783A9 PCT/JP2021/013184 JP2021013184W WO2021200783A9 WO 2021200783 A9 WO2021200783 A9 WO 2021200783A9 JP 2021013184 W JP2021013184 W JP 2021013184W WO 2021200783 A9 WO2021200783 A9 WO 2021200783A9
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WIPO (PCT)
Prior art keywords
blocking
resin composition
production method
curable resin
method therefor
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PCT/JP2021/013184
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English (en)
French (fr)
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WO2021200783A1 (ja
Inventor
元嘉 宮城
光貴 小野田
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広栄化学株式会社
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Application filed by 広栄化学株式会社 filed Critical 広栄化学株式会社
Priority to EP21780685.0A priority Critical patent/EP4129984A4/en
Priority to US17/914,995 priority patent/US20230202988A1/en
Priority to JP2022512184A priority patent/JPWO2021200783A1/ja
Priority to CN202180025102.7A priority patent/CN115397814A/zh
Priority to KR1020227034722A priority patent/KR20220161344A/ko
Publication of WO2021200783A1 publication Critical patent/WO2021200783A1/ja
Publication of WO2021200783A9 publication Critical patent/WO2021200783A9/ja

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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/42—Polycondensates having carboxylic or carbonic ester groups in the main chain
    • C08G18/4236—Polycondensates having carboxylic or carbonic ester groups in the main chain containing only aliphatic groups
    • C08G18/4238—Polycondensates having carboxylic or carbonic ester groups in the main chain containing only aliphatic groups derived from dicarboxylic acids and dialcohols
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D233/00—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings
    • C07D233/54—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having two double bonds between ring members or between ring members and non-ring members
    • C07D233/64—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having two double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms, e.g. histidine
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D233/00—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings
    • C07D233/54—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having two double bonds between ring members or between ring members and non-ring members
    • C07D233/66—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having two double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D233/90—Carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
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    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
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    • C08G18/08—Processes
    • C08G18/16—Catalysts
    • C08G18/18—Catalysts containing secondary or tertiary amines or salts thereof
    • C08G18/20—Heterocyclic amines; Salts thereof
    • C08G18/2009—Heterocyclic amines; Salts thereof containing one heterocyclic ring
    • C08G18/2027—Heterocyclic amines; Salts thereof containing one heterocyclic ring having two nitrogen atoms in the ring
    • C—CHEMISTRY; METALLURGY
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    • C08G18/2805—Compounds having only one group containing active hydrogen
    • C08G18/2895—Compounds containing active methylene groups
    • C—CHEMISTRY; METALLURGY
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    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
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    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/42—Polycondensates having carboxylic or carbonic ester groups in the main chain
    • C—CHEMISTRY; METALLURGY
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    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/72—Polyisocyanates or polyisothiocyanates
    • C08G18/721—Two or more polyisocyanates not provided for in one single group C08G18/73 - C08G18/80
    • C08G18/725—Combination of polyisocyanates of C08G18/78 with other polyisocyanates
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
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    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/72—Polyisocyanates or polyisothiocyanates
    • C08G18/73—Polyisocyanates or polyisothiocyanates acyclic
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    • C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/72—Polyisocyanates or polyisothiocyanates
    • C08G18/74—Polyisocyanates or polyisothiocyanates cyclic
    • C08G18/76—Polyisocyanates or polyisothiocyanates cyclic aromatic
    • C08G18/7614—Polyisocyanates or polyisothiocyanates cyclic aromatic containing only one aromatic ring
    • C08G18/7621—Polyisocyanates or polyisothiocyanates cyclic aromatic containing only one aromatic ring being toluene diisocyanate including isomer mixtures
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/72—Polyisocyanates or polyisothiocyanates
    • C08G18/74—Polyisocyanates or polyisothiocyanates cyclic
    • C08G18/76—Polyisocyanates or polyisothiocyanates cyclic aromatic
    • C08G18/7657—Polyisocyanates or polyisothiocyanates cyclic aromatic containing two or more aromatic rings
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    • C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/72—Polyisocyanates or polyisothiocyanates
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    • C08G18/76—Polyisocyanates or polyisothiocyanates cyclic aromatic
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    • C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/72—Polyisocyanates or polyisothiocyanates
    • C08G18/77—Polyisocyanates or polyisothiocyanates having heteroatoms in addition to the isocyanate or isothiocyanate nitrogen and oxygen or sulfur
    • C08G18/78—Nitrogen
    • C08G18/7806—Nitrogen containing -N-C=0 groups
    • C08G18/7818—Nitrogen containing -N-C=0 groups containing ureum or ureum derivative groups
    • C08G18/7831—Nitrogen containing -N-C=0 groups containing ureum or ureum derivative groups containing biuret groups
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    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/72—Polyisocyanates or polyisothiocyanates
    • C08G18/80—Masked polyisocyanates
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    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/72—Polyisocyanates or polyisothiocyanates
    • C08G18/80—Masked polyisocyanates
    • C08G18/8061—Masked polyisocyanates masked with compounds having only one group containing active hydrogen
    • C08G18/807—Masked polyisocyanates masked with compounds having only one group containing active hydrogen with nitrogen containing compounds
    • C08G18/8077—Oximes
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    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/72—Polyisocyanates or polyisothiocyanates
    • C08G18/80—Masked polyisocyanates
    • C08G18/8061—Masked polyisocyanates masked with compounds having only one group containing active hydrogen
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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Polyurethanes Or Polyureas (AREA)

Abstract

本発明は、下記式（１）（式中、Ｒ１～Ｒ５は、明細書に定義される通りである。） で表されるイミダゾリウムカルボン酸塩と下記式（２）（式中、Ａ、ｘは、明細書に定義される通りである） で表されるポリイソシアネート化合物を反応させる工程を含む、下記式（３）（式中、ｙ、ｚ、Ａ、Ｒ１～Ｒ５は、明細書に定義される通りである。） で表されるアミデート化合物の製造方法を提供するものである。
PCT/JP2021/013184 2020-03-30 2021-03-29 アミデート化合物及びその製造方法、ブロック剤解離触媒並びに熱硬化性樹脂組成物 WO2021200783A1 (ja)

Priority Applications (5)

Application Number Priority Date Filing Date Title
EP21780685.0A EP4129984A4 (en) 2020-03-30 2021-03-29 AMIDATE COMPOUND, PRODUCTION METHOD THEREFOR, BLOCKING AGENT DISSOCIATION CATALYST, AND THERMOSETTING RESIN COMPOSITION
US17/914,995 US20230202988A1 (en) 2020-03-30 2021-03-29 Amidate compound, production method therefor, blocking-agent dissociation catalyst, and thermally curable resin composition
JP2022512184A JPWO2021200783A1 (ja) 2020-03-30 2021-03-29
CN202180025102.7A CN115397814A (zh) 2020-03-30 2021-03-29 酰胺化物化合物及其制造方法、封端剂解离催化剂以及热固性树脂组合物
KR1020227034722A KR20220161344A (ko) 2020-03-30 2021-03-29 아미데이트 화합물 및 그 제조 방법, 블록제 해리 촉매 그리고 열경화성 수지 조성물

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Application Number Priority Date Filing Date Title
JP2020-061166 2020-03-30
JP2020061166 2020-03-30

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WO2021200783A1 WO2021200783A1 (ja) 2021-10-07
WO2021200783A9 true WO2021200783A9 (ja) 2021-11-11

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US (1) US20230202988A1 (ja)
EP (1) EP4129984A4 (ja)
JP (1) JPWO2021200783A1 (ja)
KR (1) KR20220161344A (ja)
CN (1) CN115397814A (ja)
TW (1) TW202200549A (ja)
WO (1) WO2021200783A1 (ja)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20230004717A (ko) * 2020-04-30 2023-01-06 고에이 가가쿠 가부시키가이샤 블록 이소시아네이트 조성물, 열경화성 수지 조성물, 경화물 및 그 제조 방법, 아미데이트 화합물 및 블록 이소시아네이트용 블록제 해리 촉매

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2018025970A1 (ja) * 2016-08-04 2018-02-08 広栄化学工業株式会社 アミデート化合物、ポリウレタン製造用触媒及びポリウレタン樹脂の製造方法
WO2018181753A1 (ja) * 2017-03-31 2018-10-04 広栄化学工業株式会社 アミデート化合物の製造方法
JP6665355B2 (ja) * 2017-09-29 2020-03-13 関西ペイント株式会社 カチオン電着塗料組成物
KR20200060367A (ko) 2017-09-29 2020-05-29 고에이 가가쿠 고교 가부시키가이샤 블록 이소시아네이트용 블록제 해리 촉매 및 그 블록제 해리 촉매를 함유하는 열 경화성 조성물
KR20210068012A (ko) * 2018-09-28 2021-06-08 고에이 가가쿠 가부시키가이샤 아미데이트 화합물의 제조 방법 및 아미데이트 화합물
TW202136217A (zh) * 2020-02-03 2021-10-01 日商廣榮化學股份有限公司 羧酸鹽化合物的製造方法及醯胺鹽化合物的製造方法

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Publication number Publication date
JPWO2021200783A1 (ja) 2021-10-07
CN115397814A (zh) 2022-11-25
EP4129984A1 (en) 2023-02-08
KR20220161344A (ko) 2022-12-06
WO2021200783A1 (ja) 2021-10-07
TW202200549A (zh) 2022-01-01
US20230202988A1 (en) 2023-06-29
EP4129984A4 (en) 2024-04-03

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