WO2019214117A1 - 一种加快发酵过程的陶瓷及其制备方法 - Google Patents

一种加快发酵过程的陶瓷及其制备方法 Download PDF

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WO2019214117A1
WO2019214117A1 PCT/CN2018/104913 CN2018104913W WO2019214117A1 WO 2019214117 A1 WO2019214117 A1 WO 2019214117A1 CN 2018104913 W CN2018104913 W CN 2018104913W WO 2019214117 A1 WO2019214117 A1 WO 2019214117A1
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parts
corn
rare earth
powder
degrees celsius
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French (fr)
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高伟
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淄博名堂教育科技有限公司
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Definitions

  • the invention relates to special ceramics, in particular to a ceramic which accelerates the fermentation process.
  • Ceramics have a long history in China and are now widely used all over the world. Ceramics are made of clay, clay and china clay, which are made of clay, clay, and clay. The history of ceramics development is an important part of the history of Chinese civilization. As one of the four ancient civilizations, China has made outstanding contributions to the progress and development of human society. The invention and development of ceramics have unique meanings. Each generation of Chinese history has different artistic styles and different technical characteristics.
  • Fermentation refers to the process of preparing microbial cells themselves, or direct metabolites or secondary metabolites by means of the life activities of microorganisms under aerobic or anaerobic conditions. It is a biochemical reaction that humans contact earlier, and now in food. It is widely used in the industrial, biological and chemical industries, and it is also the basic process of bioengineering, namely fermentation engineering. Fermentation is also used in many people's lives and production. Winemaking is one of them. It is well known that the cycle of winemaking is long, resulting in a long payback period. People are also using microwave and electromagnetic energy to accelerate the fermentation process and shorten the fermentation time. Technology equipment costs are high and requires a large site, which imposes restrictions on its application.
  • the present invention provides the following technical solutions:
  • a ceramic for accelerating the fermentation process comprising the following raw materials by weight: spinel 8-13 parts, rare earth compound 1.6-3 parts, polytetrafluoroethylene fine powder 5-8 parts, diamond fine powder 3-6 parts, nano zinc oxide 1.5-2.4 parts, 4-8 parts of magnetic wave, 4-5 parts of gelatin, 6-10 parts of olivine, 0.8-1.5 parts of purple sand, 4-6 parts of mica and 5-10 parts of corn.
  • the rare earth compound includes at least one of a rare earth nitrate, a rare earth carbonate, a rare earth sulfate, and a rare earth phosphate.
  • the particle diameter of the polytetrafluoroethylene fine powder is 30-65 um
  • the particle diameter of the diamond fine powder is 12-25 um
  • the particle diameter of the nano zinc oxide is 45-80 nm.
  • Step one the corn is squeezed into juice and enzymatically hydrolyzed for 5-8 hours in an environment of 30-45 degrees Celsius and a pH of 4.5-6. After the end of enzymatic hydrolysis, the enzyme is killed to obtain a corn fermentation broth, and the corn broth is equally divided into two. Share
  • the spinel, the rare earth compound, the magnetic wave, the olivine, the purple sand and the mica are respectively pulverized to 100-150 mesh, and used;
  • the spinel powder, the polytetrafluoroethylene micropowder, the olivine powder, the purple sand powder and a corn fermentation broth are ball milled uniformly in a ball mill at 50-60 degrees Celsius to obtain a first mixture;
  • Step 4 the magnetic wave powder, the diamond micropowder, the nano zinc oxide, the mica powder and the rare earth compound are uniformly stirred in a high-mixer, then calcined at 520-580 degrees Celsius for 90-135 minutes, naturally cooled to 40-55 degrees Celsius, and ground. And adding another corn fermentation broth while grinding, the corn broth is added for 2-4 minutes, and the corn broth is completely added and the grinding is continued for 60-80 minutes to obtain a second mixture;
  • Step 5 the gelatin is dissolved in hot water 2-3 times its weight to obtain a gelatin solution, and the first mixture, the second mixture and the gelatin solution are ball milled in a ball mill rotating at 3600-4500 rpm for 50-75 minutes to obtain the first Three mixtures;
  • step 6 the third mixture is added to the extruder, extruded to obtain a semi-finished product, and the semi-finished product is maintained in a sintering furnace at 850-920 degrees Celsius for 2-4 hours, and then heated to 1350 at a rate of 15-20 degrees Celsius/minute. At 1560 degrees Celsius and for 7-10 hours, the product is cooled by natural cooling.
  • the ball mill ratio of the step three ball mill is 45-60:1, and the ball milling speed is 90-150 rpm.
  • the invention has the beneficial effects that the raw material of the invention has wide sources and reduces the production cost, and the prepared product can be accelerated by adopting different preparation processes of different raw materials and secondary sintering of various raw materials.
  • the Brownian movement of the wine molecule shortens the brewing cycle of the wine, improves the economic efficiency of the brewer, and has a good use effect; the product can also be applied to other fermentation fields and has a wide range of uses.
  • a ceramic for accelerating the fermentation process comprising the following raw materials by weight: 8 parts of spinel, 1.6 parts of rare earth compound, 5 parts of polytetrafluoroethylene micropowder, 3 parts of diamond micropowder, 1.5 parts of nano zinc oxide, 4 parts of magnetic wave, 4 parts of gelatin, 6 parts of olivine, 0.8 parts of purple sand, 4 parts of mica and 5 parts of corn.
  • the rare earth compound includes a mixture of a rare earth nitrate and a rare earth phosphate.
  • Step one the corn is squeezed into juice and enzymatically hydrolyzed for 6 hours at 38 degrees Celsius and a pH of 4.7. After the end of enzymatic hydrolysis, the enzyme is deactivated to obtain a corn fermentation broth, and the corn broth is equally divided into two portions;
  • the spinel, the rare earth compound, the magnetic wave, the olivine, the purple sand and the mica are respectively pulverized to 120 mesh, and used;
  • the spinel powder, the polytetrafluoroethylene micropowder, the olivine powder, the purple sand powder and a corn fermentation broth are ball milled uniformly in a ball mill at 54 degrees Celsius to obtain a first mixture;
  • Step 4 the magnetic wave powder, the diamond micro powder, the nano zinc oxide, the mica powder and the rare earth compound are uniformly stirred in a high-mixer, then calcined at 560 ° C for 125 minutes, naturally cooled to 48 ° C, ground and uniformly added while grinding. Another corn fermentation broth, the corn broth was added for 3 minutes, and the corn broth was completely added and the grinding was continued for 66 minutes to obtain a second mixture;
  • Step 5 the gelatin is dissolved in hot water of 2 times its weight to obtain a gelatin solution, and the first mixture, the second mixture and the gelatin solution are ball milled in a ball mill rotating at 3900 rpm for 65 minutes to obtain a third mixture;
  • step 6 the third mixture is added to the extruder, extruded to obtain a semi-finished product, and the semi-finished product is kept in a sintering furnace at 870 ° C for 3 hours, and then heated to 1480 ° C at a rate of 18 ° C / min for 8 hours. The product is obtained by cooling.
  • Example 1 The product of Example 1 was used as a container, and the pure liquor distilled from the winery was sealed, and the same white wine was sealed in a common porcelain bottle for comparison; after sealing for 30 days, the seal was opened, and the alcohol of Example 1 was softened.
  • the aroma is rich and the taste is long, which is equivalent to the effect of one year of storage.
  • the contrast of the new wine is strong, hot and short, and the quality of the wine is not changed. It is sealed again and kept for 50 days.
  • the wine of Example 1 is equivalent to the effect of hiding for 3 years, and the quality of the comparative wine has not changed much.
  • a ceramic for accelerating the fermentation process comprising the following raw materials by weight: 10 parts of spinel, 2.2 parts of rare earth compound, 6.4 parts of polytetrafluoroethylene powder, 3.8 parts of diamond powder, 1.9 parts of nano zinc oxide, 5.5 parts of magnetic wave, 4.3 parts of gelatin, 7.2 parts of olivine, 1.1 parts of purple sand, 4.8 parts of mica and 7 parts of corn.
  • the particle size of the polytetrafluoroethylene micropowder is 48 um
  • the particle size of the diamond micropowder is 16 um
  • the particle size of the nano zinc oxide is 70 nm.
  • Step one the corn is squeezed into juice and enzymatically hydrolyzed for 7 hours at 38 degrees Celsius and a pH of 5.2. After the end of enzymatic hydrolysis, the enzyme is deactivated to obtain a corn fermentation broth, and the corn broth is equally divided into two portions;
  • the spinel, the rare earth compound, the magnetic wave, the olivine, the purple sand and the mica are respectively pulverized to 140 mesh, and used;
  • the spinel powder, the polytetrafluoroethylene micropowder, the olivine powder, the purple sand powder and a corn fermentation broth are ball milled uniformly in a ball mill at 56 degrees Celsius to obtain a first mixture;
  • step 4 the magnetic wave powder, the diamond micropowder, the nano zinc oxide, the mica powder and the rare earth compound are uniformly stirred in a high-mixer, then calcined at 540 ° C for 115 minutes, naturally cooled to 44 ° C, ground and uniformly added while grinding.
  • Another corn fermentation broth the corn broth was added for 3 minutes, and the corn broth was completely added and the milling was continued for 75 minutes to obtain a second mixture;
  • Step 5 the gelatin is dissolved in hot water of 3 times its weight to obtain a gelatin solution, and the first mixture, the second mixture and the gelatin solution are ball milled in a ball mill rotating at 3900 rpm for 68 minutes to obtain a third mixture;
  • step six the third mixture is added to the extruder, extruded to obtain a semi-finished product, and the semi-finished product is kept in a sintering furnace at 900 degrees Celsius for 3.5 hours, and then heated to 1530 degrees Celsius at a rate of 19 degrees Celsius/minute for 8 hours. The product is obtained by cooling.
  • Example 2 The product of Example 2 was used as a container, and the pure liquor distilled from the winery was sealed, and the same white wine was sealed in a common porcelain bottle for comparison; after sealing for 34 days, the seal was opened, and the alcohol of Example 2 was softened. It has a rich aroma and a long aftertaste, which is equivalent to a one-year effect.
  • the contrasting new wine has a strong smell, a hot and short aftertaste, and the quality of the wine has not changed. It is sealed again and kept for 60 days, and the seal is opened again.
  • the wine of Example 2 is equivalent to the effect of hiding for 3 years, and the quality of the proportioned wine has not changed much.
  • a ceramic for accelerating the fermentation process comprising the following raw materials by weight: 12 parts of spinel, 2.6 parts of rare earth compound, 7.2 parts of polytetrafluoroethylene powder, 5.5 parts of diamond powder, 2.2 parts of nano zinc oxide, 7 parts of magnetic wave, 4.7 parts of gelatin, 9.5 parts of olivine, 1.4 parts of purple sand, 5.6 parts of mica and 9 parts of corn.
  • the rare earth compound includes a mixture of a rare earth nitrate, a rare earth sulfate, and a rare earth phosphate.
  • Step one the corn is squeezed into juice and enzymatically hydrolyzed for 7 hours in an environment of 42 degrees Celsius and a pH of 5.5. After the end of enzymatic hydrolysis, the enzyme is inactivated to obtain a corn fermentation broth, and the corn broth is equally divided into two portions;
  • the spinel, the rare earth compound, the magnetic wave, the olivine, the purple sand and the mica are respectively pulverized to 120 mesh, and used;
  • the spinel powder, the polytetrafluoroethylene powder, the olivine powder, the purple sand powder and a corn fermentation broth are uniformly milled at a ball mill of 58 degrees Celsius and a ball ratio of 50:1, and the ball milling speed is 120 rpm.
  • the magnetic wave powder, the diamond micro powder, the nano zinc oxide, the mica powder and the rare earth compound are uniformly stirred in a high-mixer, then calcined at 555 degrees Celsius for 130 minutes, naturally cooled to 48 degrees Celsius, ground and uniformly added while grinding.
  • Step 5 the gelatin is dissolved in hot water of 3 times its weight to obtain a gelatin solution, and the first mixture, the second mixture and the gelatin solution are ball milled in a ball mill rotating at 4200 rpm for 60 minutes to obtain a third mixture;
  • step six the third mixture is added to the extruder, extruded to obtain a semi-finished product, and the semi-finished product is kept in a sintering furnace at 910 ° C for 3 hours, and then heated to 1390 ° C at a rate of 18 ° C / min for 10 hours. The product is obtained by cooling.
  • Example 3 The product of Example 3 was used as a container, and the pure liquor distilled from the winery was sealed, and the same white wine was sealed in a common porcelain bottle for comparison; after sealing for 25 days, the seal was opened, and the wine of Example 3 was softened. It has a rich aroma and a long aftertaste, which is equivalent to the effect of one year of storage. The contrasting new wine has a strong smell, a hot and short aftertaste, and the quality of the wine has not changed. It is sealed again and kept for 45 days, and the seal is opened again. The wine of Example 3 is equivalent to the effect of three years of storage, and the quality of the proportioned wine has not changed much.
  • a ceramic for accelerating the fermentation process comprising the following raw materials by weight: 13 parts of spinel, 3 parts of rare earth compound, 8 parts of polytetrafluoroethylene micropowder, 6 parts of diamond micropowder, 2.4 parts of nano zinc oxide, 8 parts of magnetic wave, 5 parts of gelatin, 10 parts of olivine, 1.5 parts of purple sand, 6 parts of mica and 10 parts of corn.
  • the rare earth compound includes a mixture of a rare earth nitrate, a rare earth carbonate, a rare earth sulfate, and a rare earth phosphate.
  • the particle size of the polytetrafluoroethylene micropowder was 55 ⁇ m
  • the particle size of the diamond micropowder was 20 ⁇ m
  • the particle size of the nano zinc oxide was 70 nm.
  • the corn is squeezed into juice and digested for 6 hours in an environment of 40 degrees Celsius and a pH of 5.2.
  • the enzyme is deactivated to obtain a corn fermentation broth, and the corn broth is divided into two parts on average;
  • the spinel, the rare earth compound, the magnetic wave, the olivine, the purple sand and the mica are respectively pulverized to 120 mesh, and used;
  • the spinel powder, the polytetrafluoroethylene powder, the olivine powder, the purple sand powder and a corn fermentation broth are uniformly milled at a ball mill of 55 degrees Celsius and a ball ratio of 60:1, and the ball milling speed is 135 rpm.
  • Step 4 the magnetic wave powder, the diamond micro powder, the nano zinc oxide, the mica powder and the rare earth compound are uniformly stirred in a high-mixer, then calcined at 550 ° C for 120 minutes, naturally cooled to 48 ° C, ground and uniformly added while grinding. Another corn fermentation broth, the corn broth was added for 4 minutes, and the corn broth was completely added and the milling was continued for 75 minutes to obtain a second mixture;
  • Step 5 the gelatin is dissolved in hot water of 3 times its weight to obtain a gelatin solution, and the first mixture, the second mixture and the gelatin solution are ball milled in a ball mill rotating at 3600 rpm for 68 minutes to obtain a third mixture;
  • Step 6 Add the third mixture to the extruder, extrude to obtain the semi-finished product, and then hold the semi-finished product in a sintering furnace at 860 ° C for 3 hours, then raise the temperature to 1550 ° C at 15 ° C / min for 8 hours. The product is obtained by cooling.
  • Example 4 The product of Example 4 was used as a container, and the pure liquor distilled from the winery was sealed, and the same white wine was sealed in a common porcelain bottle for comparison; after sealing for 40 days, the seal was opened, and the wine of Example 4 was softened.
  • the aroma is rich and the taste is long, which is equivalent to the effect of one year of storage; while the new wine has a strong smell, dryness and short aftertaste, the quality of the wine has not changed, and it is sealed again and kept for 70 days, and the seal is opened again.
  • the wine of Example 4 is equivalent to the effect of hiding for 3 years, and the quality of the comparative wine has not changed much.
  • the corn is fermented, the olivine, the spinel and the like are modified by using the corn fermentation liquid to improve the activity of the functional group, and the rare earth compound is first calcined and then ground uniformly by the corn fermentation liquid, and then various kinds of The raw materials are prepared by secondary sintering, and the rare earth elements and magnetic waves can release infrared rays and form a magnetic field, accelerate the Brownian motion of the alcohol molecules, promote the fermentation process, shorten the fermentation time, and thereby greatly shorten the brewing cycle of the wine.

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Abstract

一种加快发酵过程的陶瓷及其制备方法,包括以下重量份的原料:尖晶石8-13份、稀土化合物1.6-3份、聚四氟乙烯微粉5-8份、金刚石微粉3-6份、纳米氧化锌1.5-2.4份、磁波石4-8份、明胶4-5份、橄榄石6-10份、紫砂0.8-1.5份、云母4-6份和玉米5-10份。

Description

一种加快发酵过程的陶瓷及其制备方法 技术领域
本发明涉及特种陶瓷,具体是一种加快发酵过程的陶瓷。
背景技术
陶瓷在中国有悠久的历史,如今已在全世界范围内广泛使用,陶瓷是用陶土和瓷土这两种不同性质的粘土为原料,经过配料、成型、干燥、焙烧等工艺流程制成的器物,陶瓷的发展史是中华文明史的一个重要的组成部分,中国作为四大文明古国之一,为人类社会的进步和发展做出了卓越的贡献,其中陶瓷的发明和发展更具有独特的意义,中国历史上各朝各代有着不同艺术风格和不同技术特点。
发酵指人们借助微生物在有氧或无氧条件下的生命活动来制备微生物菌体本身、或者直接代谢产物或次级代谢产物的过程,是人类较早接触的一种生物化学反应,如今在食品工业、生物和化学工业中均有广泛应用,其也是生物工程的基本过程,即发酵工程。发酵在人们的生活和生产中也有许多应用,酿酒就是其中一种,众所周知,酿酒的周期长,导致回报周期长,人们目前也采用微波、电磁能的方法加快发酵过程从而缩短发酵时间,但是这些技术的设备成本高,需要场地大,这就为其应用带来了限制。
发明内容
本发明的目的在于提供一种加快发酵过程的陶瓷,以解决上述背景技术中提出的问题。
为实现上述目的,本发明提供如下技术方案:
一种加快发酵过程的陶瓷,包括以下重量份的原料:尖晶石8-13份、稀土化合物1.6-3份、聚四氟乙烯微粉5-8份、金刚石微粉3-6份、纳米氧化锌1.5-2.4份、磁波石4-8份、明胶4-5份、橄榄石6-10份、紫砂0.8-1.5份、云母4-6份和玉米5-10份。
作为本发明进一步的方案:稀土化合物包括稀土硝酸盐、稀土碳酸盐、稀土硫酸盐以及稀土磷酸盐中的至少一种。
作为本发明进一步的方案:聚四氟乙烯微粉的粒径为30-65um,金刚石微粉的粒径为12-25um,纳米氧化锌的粒径为45-80nm。
所述加快发酵过程的陶瓷的制备方法,具体步骤如下:
步骤一,将玉米榨成汁并且在30-45摄氏度以及PH值为4.5-6的环境下酶解5-8小时,酶解结束后灭酶,得到玉米发酵液,将玉米发酵液平均分成两份;
步骤二,将尖晶石、稀土化合物、磁波石、橄榄石、紫砂和云母分别粉碎至100-150目,备用;
步骤三,将尖晶石粉末、聚四氟乙烯微粉、橄榄石粉末、紫砂粉末以及一份玉米发酵液在50-60摄氏度下的球磨机中球磨均匀,得到第一混合物;
步骤四,将磁波石粉末、金刚石微粉、纳米氧化锌、云母粉末以及稀土化合物在高混机中搅拌均匀,然后在520-580摄氏度下煅烧90-135分钟,自然冷却至40-55摄氏度,研磨并且边研磨边匀速加入另一份玉米发酵液,玉米发酵液加入的时间为2-4分钟,完全加入玉米发酵液后继续研磨60-80分钟,得到第二混合物;
步骤五,将明胶溶于其重量2-3倍的热水中,得到明胶溶液,将第一混合物、第二混合物以及明胶溶液在转速为3600-4500rpm的球磨机中球磨50-75分钟,得到第三混合物;
步骤六,将第三混合物加入挤压机中,挤压得到半成品,再将半成品在850-920摄氏度的烧结炉中保持2-4小时,然后以15-20摄氏度/分钟的速度升温至1350-1560摄氏度并且保持7-10小时,自然冷却即得到成品。
作为本发明进一步的方案:步骤三球磨机的球料比为45-60:1,球磨速度为90-150rpm。
与现有技术相比,本发明的有益效果是:本发明原料来源广泛,降低了生产成本,通过将不同的原料采用不同的制备工艺并且将各种原料进行二次烧结,制备的成品可以加快酒分子的布朗运动,缩短酒的酿造周期,提高了酿酒者的经济效益,使用效果好;本产品还可以适用于其他发酵领域,使用范围广。
具体实施方式
下面结合具体实施方式对本专利的技术方案作进一步详细地说明。
实施例1
一种加快发酵过程的陶瓷,包括以下重量份的原料:尖晶石8份、稀土化合物1.6份、聚四氟乙烯微粉5份、金刚石微粉3份、纳米氧化锌1.5份、磁波石4份、明胶4份、橄榄石6份、紫砂0.8份、云母4份和玉米5份。稀土化合物包 括稀土硝酸盐以及稀土磷酸盐的混合物。
所述加快发酵过程的陶瓷的制备方法,具体步骤如下:
步骤一,将玉米榨成汁并且在38摄氏度以及PH值为4.7的环境下酶解6小时,酶解结束后灭酶,得到玉米发酵液,将玉米发酵液平均分成两份;
步骤二,将尖晶石、稀土化合物、磁波石、橄榄石、紫砂和云母分别粉碎至120目,备用;
步骤三,将尖晶石粉末、聚四氟乙烯微粉、橄榄石粉末、紫砂粉末以及一份玉米发酵液在54摄氏度下的球磨机中球磨均匀,得到第一混合物;
步骤四,将磁波石粉末、金刚石微粉、纳米氧化锌、云母粉末以及稀土化合物在高混机中搅拌均匀,然后在560摄氏度下煅烧125分钟,自然冷却至48摄氏度,研磨并且边研磨边匀速加入另一份玉米发酵液,玉米发酵液加入的时间为3分钟,完全加入玉米发酵液后继续研磨66分钟,得到第二混合物;
步骤五,将明胶溶于其重量2倍的热水中,得到明胶溶液,将第一混合物、第二混合物以及明胶溶液在转速为3900rpm的球磨机中球磨65分钟,得到第三混合物;
步骤六,将第三混合物加入挤压机中,挤压得到半成品,再将半成品在870摄氏度的烧结炉中保持3小时,然后以18摄氏度/分钟的速度升温至1480摄氏度并且保持8小时,自然冷却即得到成品。
将实施例1的产品作为容器,将酒厂刚蒸馏出来的原浆白酒进行密封,同时将同样的白酒装入普通瓷瓶密封作为对比;密封30天之后开启密封,实施例1的酒绵柔醇和、香味浓郁,后味长,相当于窖藏1年的效果;而对比样新酒气味浓,燥辣、后味短,酒的品质没有发生改变,再次密封并继续保存50天,再次开启密封,实施例1的酒相当于窖藏3年的效果,对比例酒的品质没有太大改变。
实施例2
一种加快发酵过程的陶瓷,包括以下重量份的原料:尖晶石10份、稀土化合物2.2份、聚四氟乙烯微粉6.4份、金刚石微粉3.8份、纳米氧化锌1.9份、磁波石5.5份、明胶4.3份、橄榄石7.2份、紫砂1.1份、云母4.8份和玉米7份。聚四氟乙烯微粉的粒径为48um,金刚石微粉的粒径为16um,纳米氧化锌的粒径为 70nm。
所述加快发酵过程的陶瓷的制备方法,具体步骤如下:
步骤一,将玉米榨成汁并且在38摄氏度以及PH值为5.2的环境下酶解7小时,酶解结束后灭酶,得到玉米发酵液,将玉米发酵液平均分成两份;
步骤二,将尖晶石、稀土化合物、磁波石、橄榄石、紫砂和云母分别粉碎至140目,备用;
步骤三,将尖晶石粉末、聚四氟乙烯微粉、橄榄石粉末、紫砂粉末以及一份玉米发酵液在56摄氏度下的球磨机中球磨均匀,得到第一混合物;
步骤四,将磁波石粉末、金刚石微粉、纳米氧化锌、云母粉末以及稀土化合物在高混机中搅拌均匀,然后在540摄氏度下煅烧115分钟,自然冷却至44摄氏度,研磨并且边研磨边匀速加入另一份玉米发酵液,玉米发酵液加入的时间为3分钟,完全加入玉米发酵液后继续研磨75分钟,得到第二混合物;
步骤五,将明胶溶于其重量3倍的热水中,得到明胶溶液,将第一混合物、第二混合物以及明胶溶液在转速为3900rpm的球磨机中球磨68分钟,得到第三混合物;
步骤六,将第三混合物加入挤压机中,挤压得到半成品,再将半成品在900摄氏度的烧结炉中保持3.5小时,然后以19摄氏度/分钟的速度升温至1530摄氏度并且保持8小时,自然冷却即得到成品。
将实施例2的产品作为容器,将酒厂刚蒸馏出来的原浆白酒进行密封,同时将同样的白酒装入普通瓷瓶密封作为对比;密封34天之后开启密封,实施例2的酒绵柔醇和、香味浓郁,后味长,相当于窖藏1年的效果;而对比样新酒气味浓,燥辣、后味短,酒的品质没有发生改变,再次密封并继续保存60天,再次开启密封,实施例2的酒相当于窖藏3年的效果,对比例酒的品质没有太大改变
实施例3
一种加快发酵过程的陶瓷,包括以下重量份的原料:尖晶石12份、稀土化合物2.6份、聚四氟乙烯微粉7.2份、金刚石微粉5.5份、纳米氧化锌2.2份、磁波石7份、明胶4.7份、橄榄石9.5份、紫砂1.4份、云母5.6份和玉米9份。稀土化合物包括稀土硝酸盐、稀土硫酸盐以及稀土磷酸盐的混合物。
所述加快发酵过程的陶瓷的制备方法,具体步骤如下:
步骤一,将玉米榨成汁并且在42摄氏度以及PH值为5.5的环境下酶解7小时,酶解结束后灭酶,得到玉米发酵液,将玉米发酵液平均分成两份;
步骤二,将尖晶石、稀土化合物、磁波石、橄榄石、紫砂和云母分别粉碎至120目,备用;
步骤三,将尖晶石粉末、聚四氟乙烯微粉、橄榄石粉末、紫砂粉末以及一份玉米发酵液在58摄氏度下和球料比为50:1的球磨机中球磨均匀,球磨速度为120rpm,得到第一混合物;
步骤四,将磁波石粉末、金刚石微粉、纳米氧化锌、云母粉末以及稀土化合物在高混机中搅拌均匀,然后在555摄氏度下煅烧130分钟,自然冷却至48摄氏度,研磨并且边研磨边匀速加入另一份玉米发酵液,玉米发酵液加入的时间为3分钟,完全加入玉米发酵液后继续研磨70分钟,得到第二混合物;
步骤五,将明胶溶于其重量3倍的热水中,得到明胶溶液,将第一混合物、第二混合物以及明胶溶液在转速为4200rpm的球磨机中球磨60分钟,得到第三混合物;
步骤六,将第三混合物加入挤压机中,挤压得到半成品,再将半成品在910摄氏度的烧结炉中保持3小时,然后以18摄氏度/分钟的速度升温至1390摄氏度并且保持10小时,自然冷却即得到成品。
将实施例3的产品作为容器,将酒厂刚蒸馏出来的原浆白酒进行密封,同时将同样的白酒装入普通瓷瓶密封作为对比;密封25天之后开启密封,实施例3的酒绵柔醇和、香味浓郁,后味长,相当于窖藏1年的效果;而对比样新酒气味浓,燥辣、后味短,酒的品质没有发生改变,再次密封并继续保存45天,再次开启密封,实施例3的酒相当于窖藏3年的效果,对比例酒的品质没有太大改变
实施例4
一种加快发酵过程的陶瓷,包括以下重量份的原料:尖晶石13份、稀土化合物3份、聚四氟乙烯微粉8份、金刚石微粉6份、纳米氧化锌2.4份、磁波石8份、明胶5份、橄榄石10份、紫砂1.5份、云母6份和玉米10份。稀土化合物包括稀土硝酸盐、稀土碳酸盐、稀土硫酸盐以及稀土磷酸盐的混合物。聚四氟乙烯微 粉的粒径为55um,金刚石微粉的粒径为20um,纳米氧化锌的粒径为70nm。
所述加快发酵过程的陶瓷的制备方法,具体步骤如下:
步骤一,将玉米榨成汁并且在40摄氏度以及PH值为5.2的环境下酶解6小时,酶解结束后灭酶,得到玉米发酵液,将玉米发酵液平均分成两份;
步骤二,将尖晶石、稀土化合物、磁波石、橄榄石、紫砂和云母分别粉碎至120目,备用;
步骤三,将尖晶石粉末、聚四氟乙烯微粉、橄榄石粉末、紫砂粉末以及一份玉米发酵液在55摄氏度下和球料比为60:1的球磨机中球磨均匀,球磨速度为135rpm,得到第一混合物;
步骤四,将磁波石粉末、金刚石微粉、纳米氧化锌、云母粉末以及稀土化合物在高混机中搅拌均匀,然后在550摄氏度下煅烧120分钟,自然冷却至48摄氏度,研磨并且边研磨边匀速加入另一份玉米发酵液,玉米发酵液加入的时间为4分钟,完全加入玉米发酵液后继续研磨75分钟,得到第二混合物;
步骤五,将明胶溶于其重量3倍的热水中,得到明胶溶液,将第一混合物、第二混合物以及明胶溶液在转速为3600rpm的球磨机中球磨68分钟,得到第三混合物;
步骤六,将第三混合物加入挤压机中,挤压得到半成品,再将半成品在860摄氏度的烧结炉中保持3小时,然后以15摄氏度/分钟的速度升温至1450摄氏度并且保持8小时,自然冷却即得到成品。
将实施例4的产品作为容器,将酒厂刚蒸馏出来的原浆白酒进行密封,同时将同样的白酒装入普通瓷瓶密封作为对比;密封40天之后开启密封,实施例4的酒绵柔醇和、香味浓郁,后味长,相当于窖藏1年的效果;而对比样新酒气味浓,燥辣、后味短,酒的品质没有发生改变,再次密封并继续保存70天,再次开启密封,实施例4的酒相当于窖藏3年的效果,对比例酒的品质没有太大改变。
本发明的产品中将玉米进行发酵,将橄榄石、尖晶石等采用玉米发酵液进行改性,提高官能团的活性,同时将稀土化合物等先煅烧再采用玉米发酵液研磨均匀,再将各种原料采用二次烧结制备成品,利用稀土元素、磁波石等可以释放红外线并且形成磁场,加快酒分子的布朗运动,促进发酵过程,缩短发酵时间, 从而大大缩短了酒的酿造周期。
对于本领域技术人员而言,显然本发明不限于上述示范性实施例的细节,而且在不背离本发明的精神或基本特征的情况下,能够以其他的具体形式实现本发明。因此,无论从哪一点来看,均应将实施例看作是示范性的,而且是非限制性的,本发明的范围由所附权利要求而不是上述说明限定,因此旨在将落在权利要求的等同要件的含义和范围内的所有变化囊括在本发明内。
此外,应当理解,虽然本说明书按照实施方式加以描述,但并非每个实施方式仅包含一个独立的技术方案,说明书的这种叙述方式仅仅是为清楚起见,本领域技术人员应当将说明书作为一个整体,各实施例中的技术方案也可以经适当组合,形成本领域技术人员可以理解的其他实施方式。

Claims (5)

  1. 一种加快发酵过程的陶瓷,其特征在于,包括以下重量份的原料:尖晶石8-13份、稀土化合物1.6-3份、聚四氟乙烯微粉5-8份、金刚石微粉3-6份、纳米氧化锌1.5-2.4份、磁波石4-8份、明胶4-5份、橄榄石6-10份、紫砂0.8-1.5份、云母4-6份和玉米5-10份。
  2. 根据权利要求1所述的加快发酵过程的陶瓷,其特征在于,所述稀土化合物包括稀土硝酸盐、稀土碳酸盐、稀土硫酸盐以及稀土磷酸盐中的至少一种。
  3. 根据权利要求1所述的加快发酵过程的陶瓷,其特征在于,所述聚四氟乙烯微粉的粒径为30-65um,金刚石微粉的粒径为12-25um,纳米氧化锌的粒径为45-80nm。
  4. 一种如权利要求1-3任一所述的加快发酵过程的陶瓷的制备方法,其特征在于,具体步骤如下:
    步骤一,将玉米榨成汁并且在30-45摄氏度以及PH值为4.5-6的环境下酶解5-8小时,酶解结束后灭酶,得到玉米发酵液,将玉米发酵液平均分成两份;
    步骤二,将尖晶石、稀土化合物、磁波石、橄榄石、紫砂和云母分别粉碎至100-150目,备用;
    步骤三,将尖晶石粉末、聚四氟乙烯微粉、橄榄石粉末、紫砂粉末以及一份玉米发酵液在50-60摄氏度下的球磨机中球磨均匀,得到第一混合物;
    步骤四,将磁波石粉末、金刚石微粉、纳米氧化锌、云母粉末以及稀土化合物在高混机中搅拌均匀,然后在520-580摄氏度下煅烧90-135分钟,自然冷却至40-55摄氏度,研磨并且边研磨边匀速加入另一份玉米发酵液,玉米发酵液加入的时间为2-4分钟,完全加入玉米发酵液后继续研磨60-80分钟,得到第二混合物;
    步骤五,将明胶溶于其重量2-3倍的热水中,得到明胶溶液,将第一混合物、第二混合物以及明胶溶液在转速为3600-4500rpm的球磨机中球磨50-75分钟,得到第三混合物;
    步骤六,将第三混合物加入挤压机中,挤压得到半成品,再将半成品在850-920摄氏度的烧结炉中保持2-4小时,然后以15-20摄氏度/分钟的速度升温至1350-1560摄氏度并且保持7-10小时,自然冷却即得到成品。
  5. 根据权利要求4所述的加快发酵过程的陶瓷的制备方法,其特征在于, 所述步骤三球磨机的球料比为45-60:1,球磨速度为90-150rpm。
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