WO2017158864A1 - 導電性複合材料の検査方法及び導電性複合材料の検査装置 - Google Patents
導電性複合材料の検査方法及び導電性複合材料の検査装置 Download PDFInfo
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- WO2017158864A1 WO2017158864A1 PCT/JP2016/073832 JP2016073832W WO2017158864A1 WO 2017158864 A1 WO2017158864 A1 WO 2017158864A1 JP 2016073832 W JP2016073832 W JP 2016073832W WO 2017158864 A1 WO2017158864 A1 WO 2017158864A1
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N27/00—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means
- G01N27/72—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating magnetic variables
- G01N27/82—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating magnetic variables for investigating the presence of flaws
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N27/00—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means
- G01N27/72—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating magnetic variables
Definitions
- the present disclosure relates to a conductive composite material inspection method and a conductive composite material inspection apparatus.
- This application is based on Japanese Patent Application No. 2016-052606 filed on March 16, 2016, and claims the benefit of priority to them, the entire contents of which are referred to Which is incorporated herein by reference.
- the conductive composite material includes a plurality of laminated prepregs.
- the prepreg is a conductive fiber woven fabric.
- the conductive composite material is obtained by impregnating a carbon fiber woven fabric with a thermosetting resin or a thermoplastic resin.
- carbon fibers are oriented in a predetermined direction in the resin. The orientation of the carbon fibers affects the mechanical properties of the conductive composite material. Therefore, in the manufacturing process of the conductive composite material, the orientation state of the carbon fiber may be inspected.
- the disorder of the orientation of the conductive fibers is in the thickness direction (that is, the out-of-plane direction) of the conductive composite material and in the direction intersecting the thickness direction (that is, the in-plane direction). Including turbulence. Therefore, in the manufacturing process of the conductive composite material, the disorder of orientation in the out-of-plane direction and the disorder of orientation in the in-plane direction are inspected. For the inspection of the alignment disorder in the out-of-plane direction, for example, an ultrasonic flaw detection method described in Patent Document 1 is used.
- a method of cutting a flat conductive composite material and observing the cut surface, or cutting the conductive composite material finely and using X-rays, the conductive fiber A method of detecting turbulence is used. Further, for example, a method for detecting a meandering fiber of a conductive composite material described in Patent Document 2 is also used for inspecting the alignment disorder in the in-plane direction.
- the conductive composite material When a conductive composite material is applied to industrial uses such as aircraft parts, the conductive composite material may be required to have high mechanical properties. Disturbance of the orientation of the conductive fiber affects the mechanical properties. Accordingly, the present disclosure describes a conductive composite material inspection method and inspection apparatus that can reliably detect disorder in the orientation of conductive fibers.
- One form of the present disclosure is a method for inspecting a conductive composite material including conductive fibers, in which a first magnetic field measurement unit that acquires a magnetic field strength in a direction along a first detection axis is connected to the conductive composite material. And a step of arranging the first detection axis so as to be parallel to the set orientation direction of the conductive fibers at a position facing the main surface of the test body including the magnetic field strength in the direction along the second detection axis.
- a step of acquiring a magnetic field strength of 1 and a second magnetic field measuring unit with respect to the main surface Obtaining the second magnetic field strength output from the second magnetic field measurement unit while relatively moving, and using the first magnetic field strength and the second magnetic field strength, the orientation of the conductive fibers Detecting a portion in which the orientation of the conductive fiber is disturbed, and correcting the first magnetic field strength using the second magnetic field strength.
- the conductive composite material inspection method and inspection apparatus can reliably detect disorder of the orientation of the conductive fibers.
- Part (a) of FIG. 1 is a perspective view illustrating a structure of a conductive composite material to be inspected by the conductive composite material inspection method according to the present disclosure.
- Part (b) of FIG. 1 and part (c) of FIG. 1 are perspective views for explaining meandering that may occur in the conductive composite material.
- FIG. 2 is a block diagram illustrating a configuration of a conductive composite material inspection apparatus for performing the conductive composite material inspection method according to the present disclosure.
- Part (a) of FIG. 3 and part (b) of FIG. 3 are diagrams showing the relationship between the magnetic field sensor and the conductive fiber and the relationship between the magnetic field sensor and the magnetic field.
- FIG. 4 is a flowchart showing the main steps of the conductive composite inspection method according to the present disclosure.
- FIG. 5 is a diagram for explaining the positional relationship between the specimen and the magnetic field sensor.
- FIG. 6 is a diagram for explaining the test body according to the example.
- Part (a) of FIG. 7 is a diagram showing the magnetic field strength proportional to the current value generated in the test body shown in FIG. Part (b) of FIG. 7 is a diagram showing the magnetic field strength for detecting disturbance in the orientation of the conductive fibers generated in the test body shown in FIG. Part (a) of FIG. 8 is a diagram showing a result of correcting the magnetic field intensity shown in part (b) of FIG. Part (b) of FIG. 8 is a diagram for illustrating the effect of correction.
- One form of the present disclosure is a method for inspecting a conductive composite material including conductive fibers, in which a first magnetic field measurement unit that acquires a magnetic field strength in a direction along a first detection axis is connected to the conductive composite material. And a step of arranging the first detection axis so as to be parallel to the set orientation direction of the conductive fibers at a position facing the main surface of the test body including the magnetic field strength in the direction along the second detection axis.
- a step of acquiring a magnetic field strength of 1 and a second magnetic field measuring unit with respect to the main surface Obtaining the second magnetic field strength output from the second magnetic field measurement unit while relatively moving, and using the first magnetic field strength and the second magnetic field strength, the orientation of the conductive fibers Detecting a portion in which the orientation of the conductive fiber is disturbed, and correcting the first magnetic field strength using the second magnetic field strength.
- the orientation of the conductive fiber may deviate from a preset orientation direction.
- a state in which the actual orientation direction of the conductive fibers is deviated from the set orientation direction is a state in which the orientation of the conductive fibers is disturbed.
- a magnetic field is generated when the current is applied through the conductive fiber.
- the magnetic field is orthogonal to the direction of current flow. Since the current flows through the conductive fiber, the direction in which the current flows coincides with the actual orientation direction of the conductive fiber. Therefore, the magnetic field is orthogonal to the actual orientation direction of the conductive fibers.
- the direction of the magnetic field is inclined at an angle that is not orthogonal to the set orientation direction.
- the magnetic field strength can be affected by the current value.
- the first magnetic field measurement unit Since the first magnetic field measurement unit is arranged so that the first detection axis is parallel to the set orientation direction, the first magnetic field measurement unit acquires the first magnetic field strength along the set orientation direction. When there is no disturbance in the orientation of the conductive fibers, the magnetic field is orthogonal to the set orientation direction. Therefore, the first magnetic field strength is zero. On the other hand, when the orientation of the conductive fibers is disturbed, the magnetic field is tilted with respect to the set orientation direction, so the first magnetic field strength is a predetermined value. That is, according to the step of acquiring the first magnetic field strength, the first magnetic field strength including the influence caused by the disorder of the orientation of the conductive fibers and the influence of the current value is obtained.
- the second magnetic field measurement unit is arranged so that the second detection axis intersects the set orientation direction. Therefore, the second magnetic field measurement unit obtains the second magnetic field strength along the direction intersecting the set orientation direction.
- the second magnetic field strength is proportional to the current value. That is, according to the step of obtaining the second magnetic field strength, the second magnetic field strength including the influence of the current value is obtained.
- a correction coefficient is obtained using the second magnetic field strength.
- the correction coefficient reduces the influence of the current value included in the first magnetic field strength. Therefore, by correcting the first magnetic field strength using the correction coefficient, the influence of the current value included in the first magnetic field strength is reduced. Therefore, according to the step of detecting the portion where the orientation of the conductive fiber is disturbed using the corrected first magnetic field strength, the disorder of the orientation of the conductive fiber can be reliably detected.
- obtaining the correction coefficient includes obtaining an average value of the second magnetic field strength, calculating a correction coefficient using the second magnetic field strength and the average value, and But you can. According to the step, a suitable correction coefficient can be obtained.
- obtaining the corrected first magnetic field strength may divide the first magnetic field strength by a correction factor. According to the step, the first magnetic field strength excluding the influence of the current value can be suitably obtained.
- Another aspect of the present disclosure is an apparatus for inspecting a conductive composite material including conductive fibers, which acquires a magnetic field strength in a direction along a first detection axis, and includes a test body including the conductive composite material.
- a first magnetic field measuring unit arranged so that the first detection axis is parallel to the set orientation direction of the conductive fiber at a position facing the main surface; and a magnetic field in a direction along the second detection axis
- a second magnetic field measurement unit that obtains the strength and is arranged so that the second detection axis intersects the set orientation direction of the conductive fiber at a position facing the main surface of the specimen, and the conductive fiber
- a current applying unit that applies a current between one end and the other end of the test body, and a moving mechanism unit that moves the first magnetic field measuring unit and the second magnetic field measuring unit relative to the main surface And the first magnetic field intensity output from the first magnetic field measurement unit and the second magnetic field measurement unit.
- a correction coefficient acquisition unit that acquires a correction coefficient for correcting the first magnetic field strength
- a signal correction unit that acquires a corrected first magnetic field strength using the correction coefficient
- a corrected first And a meandering inspection unit that detects a portion where the orientation of the conductive fibers is disturbed by using the magnetic field strength.
- the test body S has a rectangular parallelepiped shape in which a plurality of prepregs (S1, S3,..., Sn-1), (S2, S4,... Sn-2, Sn) are stacked.
- Each prepreg is obtained by impregnating a conductive fiber woven fabric SS with a thermoplastic resin or a thermosetting resin.
- the orientation directions of the conductive fibers SE included in the prepreg are 90 ° different from each other. Therefore, the test body S has two orientation directions.
- the terms “set orientation direction” and “actual orientation direction” are used for the orientation direction.
- the “set orientation direction” is a preset direction and is always constant.
- the “real orientation direction” is a direction in which the conductive fibers SE are actually oriented, and is distinguished from the set orientation direction.
- “Disturbance of alignment” and “meandering” mean that the actual alignment direction is not parallel to the set alignment direction. That is, “disturbance of alignment” and “meandering” mean a state in which the actual alignment direction is inclined with respect to the set alignment direction.
- the conductive fibers SE are oriented along a predetermined direction.
- the orientation of the conductive fiber SE may change due to heating or cooling in the molding process.
- the state in which the orientation of the conductive fiber SE is changed is called fiber orientation disorder or fiber meandering.
- the meandering of the fiber may have two forms.
- the meandering of the fiber is meandering along the thickness direction of the specimen S (see (b) part of FIG. 1), meandering along the main surface Sa of the specimen S (see (c) part of FIG. 1), including.
- the inspection method and inspection apparatus according to the present disclosure have the meandering shown in part (c) of FIG.
- the fiber meander inspection device 1 (conductive composite material inspection device) includes a stage 2 (movement mechanism unit), a driver 3, a current application device 4 (current application unit), and a magnetic field sensor. 6 and a computer 7 (data processing unit).
- the fiber meandering inspection device 1 may include a desired device (for example, a lock-in amplifier 8) necessary for processing a signal output from the magnetic field sensor 6.
- the lock-in amplifier 8 detects the output of the magnetic field sensor 6 using the output of the current application device 4 as a reference signal. In the lock-in amplifier 8, the phase of the output of the magnetic field sensor 6 with respect to the phase of the output signal of the current application device 4 is adjusted so that the detection signal input to the computer 7 is maximized.
- the stage 2 which is a moving mechanism unit moves the magnetic field sensor 6 relative to the main surface Sa of the specimen S.
- Stage 2 is a biaxial stage. The two movement axes of the stage 2 form a plane parallel to the main surface Sa.
- the magnetic field sensor 6 is fixed, and the test body S is moved with respect to the magnetic field sensor 6.
- the moving mechanism unit may be configured such that the specimen S is fixed and the magnetic field sensor 6 is moved relative to the specimen S.
- the operation of the stage 2 is controlled by a control signal input from the driver 3.
- the driver 3 is connected to the stage 2 and the computer 7.
- the driver 3 generates a signal for controlling the operation of the stage 2 based on the control signal input from the computer 7.
- the current application device 4 is connected to the specimen S, the computer 7 and the lock-in amplifier 8.
- the current application device 4 applies a current to the specimen S.
- the prepregs S2, S4,..., Sn have a set orientation direction B.
- the current application device 4 applies a current along the set orientation direction B of the conductive fibers SE in the plurality of prepregs S2, S4,.
- the current application device 4 has a pair of electrodes 9. When a plurality of prepregs S2, S4,..., Sn are to be inspected, the electrode 9 is attached to the end of the specimen S that intersects the set orientation direction B of the prepregs S2, S4,.
- the magnetic field sensor 6 is disposed on the main surface Sa of the specimen S.
- the magnetic field sensor 6 acquires the magnetic field strength.
- the magnetic field sensor 6 includes a detection magnetic field measurement unit 6a (first magnetic field measurement unit) and a correction magnetic field measurement unit 6b (second magnetic field measurement unit).
- the detection magnetic field measurement unit 6a acquires the magnetic field strength along the direction of the first detection axis D1.
- the correction magnetic field measurement unit 6b acquires the magnetic field strength along the direction of the second detection axis D2.
- the magnetic field sensor 6 has two detection axes (a first detection axis D1 and a second detection axis D2).
- the magnetic field sensor 6 outputs a signal corresponding to the magnetic field intensity along the direction of the detection axis as a voltage value to the lock-in amplifier 8.
- the magnetic field sensor 6 includes an MI (Magneto Impedance) sensor, a GMR (Giant Magneto Resistance) sensor, a TMR (Tunnel Magneto Resistance) sensor, an AMR (Anisotropic Magneto Resistance) sensor, an FG (Flux Gate) sensor, a Hall element, and a SQUID (Superconducting).
- MI Magnetic Impedance
- GMR Global Magneto Resistance
- TMR Tunnelnel Magneto Resistance
- AMR Anisotropic Magneto Resistance
- FG Fluor Gate
- SQUID Superconducting
- the current E When the current E is supplied to the test body S, the current E flows between one end and the other end of the test body S through the conductive fiber SE. A magnetic field M is generated by the current E. Therefore, the output of the magnetic field sensor 6 is affected by the current value caused by the current E.
- the direction of the magnetic field M is orthogonal to the direction of the current E. In other words, the direction of the magnetic field M is orthogonal to the actual orientation direction C in which the conductive fibers SE are arranged.
- the actual orientation direction C deviates from the set orientation direction B (see part (b) in FIG. 3)
- the direction of the magnetic field M is not orthogonal to the set orientation direction B.
- the direction of the magnetic field M is not orthogonal to the set orientation direction B. Therefore, the direction of the magnetic field M is inclined with respect to the set orientation direction B.
- the output of the magnetic field sensor 6 is affected by the actual orientation direction C. In other words, the output of the magnetic field sensor 6 includes the influence of the current value caused by the current E and the influence of the actual orientation direction C.
- the computer 7 will be described with reference to FIG.
- the computer 7 includes a main control unit 11, an input / output unit 12, a signal processing unit 13, and a memory 14.
- the computer 7 controls the operation of the stage 2 and the operation of the current application device 4.
- the computer 7 performs meandering inspection using the output signal of the magnetic field sensor 6.
- the computer 7 is connected to the driver 3, the current application device 4, and the lock-in amplifier 8.
- the main control unit 11 controls the overall operation of the computer 7.
- the main control unit 11 displays the processing result of the signal processing unit 13.
- the main control unit 11 controls the operation of the stage 2 and the operation of the current application device 4.
- the main control unit 11 is connected to the input / output unit 12 and outputs a control signal to the input / output unit 12.
- the main control unit 11 is connected to the signal processing unit 13 and receives a processing signal from the signal processing unit 13.
- the main control unit 11 is connected to the memory 14 and reads various setting values stored in the memory 14.
- the main control unit 11 includes a display control unit 11a, a current control unit 11b, and a stage control unit 11c.
- the display control unit 11a, the current control unit 11b, and the stage control unit 11c are functional components realized by a program stored in the memory 14 of the computer 7 being executed by a CPU or the like.
- the display control unit 11a is connected to the signal processing unit 13 and displays the processing signal received from the signal processing unit 13 on a display device such as a display.
- the current control unit 11 b is connected to the input / output unit 12 and outputs a control signal for controlling the operation of the current application device 4 to the input / output unit 12.
- the control signal of the current control unit 11b controls, for example, the start and stop of current application and the frequency and current value of the current E output from the current application device 4.
- the stage control unit 11 c is connected to the input / output unit 12 and outputs a control signal for controlling the operation of the stage 2 to the input / output unit 12.
- the stage control unit 11c outputs the position information of the stage 2 using the control signal.
- the position information may be generated by another component. The specific operation of stage 2 will be described later.
- the input / output unit 12 receives a signal input from a device such as the lock-in amplifier 8.
- the input / output unit 12 outputs a signal for controlling operations of the devices such as the driver 3 and the current application device 4.
- the input / output unit 12 is connected to the driver 3, the current application device 4, and the lock-in amplifier 8.
- the input / output unit 12 includes a digitizer 12a and a controller 12b.
- a digitizer 12 a that is a so-called analog-digital conversion device is connected to the lock-in amplifier 8, the signal processing unit 13, and the memory 14.
- the digitizer 12a converts the analog signal input from the lock-in amplifier 8 into a digital signal.
- the digitizer 12 a outputs the digital signal to the signal processing unit 13 or the memory 14.
- the controller 12 b is connected to the driver 3 and the main control unit 11.
- the controller 12 b generates a control signal to be given to the driver 3 using the control signal given from the main control unit 11.
- the controller 12b outputs a
- the signal processing unit 13 is connected to the main control unit 11, the input / output unit 12, and the memory 14.
- the signal processing unit 13 uses the information input from the input / output unit 12 or the information read from the memory 14 to inspect for meandering.
- the inspection related to the meander includes an inspection related to the presence of meandering and an inspection related to the degree of meandering. For example, the signal processing unit 13 determines the presence or absence of meandering. When the signal processing unit 13 determines that meandering is present, the signal processing unit 13 quantitatively calculates the degree of meandering. The signal processing unit 13 may determine whether or not the meandering is acceptable using an amount indicating the degree of meandering.
- the signal processing unit 13 includes a filter processing unit 13a, an average intensity acquisition unit 13b, a reference intensity acquisition unit 13c, a correction coefficient acquisition unit 13d, a signal correction unit 13e, and a meander inspection unit 13f.
- a program stored in the memory 14 of the computer 7 is executed by the CPU or the like. It is a functional component realized by this.
- the filter processing unit 13a is connected to the digitizer 12a, the average intensity acquisition unit 13b, the signal correction unit 13e, and the memory 14 of the input / output unit 12.
- the filter processing unit 13a performs desired filter processing (for example, band-pass filter processing) on the digital signal input from the digitizer 12a or information read from the memory 14.
- the filtered signal is output to the average intensity acquisition unit 13b and the signal correction unit 13e.
- the average intensity acquisition unit 13b is connected to the filter processing unit 13a and the reference intensity acquisition unit 13c.
- the average intensity acquisition unit 13b calculates a plurality of average intensities using the filtered signal and outputs the average intensity to the reference intensity acquisition unit 13c. The specific operation of the average intensity acquisition unit 13b will be described later.
- the reference intensity acquisition unit 13c is connected to the average intensity acquisition unit 13b and the correction coefficient acquisition unit 13d.
- the reference intensity acquisition unit 13c selects a reference intensity from a plurality of average intensities and outputs the reference intensity to the correction coefficient acquisition unit 13d. The specific operation of the reference strength acquisition unit 13c will be described later.
- the correction coefficient acquisition unit 13d is connected to the reference intensity acquisition unit 13c and the signal correction unit 13e.
- the correction coefficient acquisition unit 13d calculates a correction coefficient using the reference intensity and the average intensity, and outputs the correction coefficient to the signal correction unit 13e. The specific operation of the correction coefficient acquisition unit 13d will be described later.
- the signal correction unit 13e is connected to the filter processing unit 13a, the correction coefficient acquisition unit 13d, and the meandering inspection unit 13f.
- the signal correction unit 13e corrects the magnetic field intensity input from the filter processing unit 13a using the correction coefficient input from the correction coefficient acquisition unit 13d and outputs the corrected magnetic field strength to the meandering inspection unit 13f. The operation of the signal correction unit 13e will be described later.
- the meandering inspection unit 13f is connected to the signal correction unit 13e.
- the meandering inspection unit 13f performs processing for obtaining the presence / absence of the meandering and the degree of meandering using the corrected magnetic field intensity input from the signal correction unit 13e.
- the meandering inspection unit 13 f outputs the processing result to the main control unit 11 and the memory 14.
- the memory 14 holds various set values and various data used for meander detection processing.
- Various data used for the meandering detection process may include information on the acquired magnetic field strength and a correction coefficient.
- the memory 14 is configured to be readable and writable from the main control unit 11, the input / output unit 12, and the signal processing unit 13.
- the memory 14 stores information relating to the magnetic field strength in association with position information between the stage 2 and the magnetic field sensor 6.
- Information regarding the magnetic field strength is output from the digitizer 12 a of the input / output unit 12.
- the position information is information indicating the positional relationship between the stage 2 and the magnetic field sensor 6 output from the stage control unit 11 c of the main control unit 11.
- the association between the information on the magnetic field strength and the position information may be performed in a component other than the memory 14.
- a meandering inspection method using the fiber meandering inspection apparatus 1 will be described. Hereinafter, after describing the principle of the inspection method, detailed steps will be described.
- the detection magnetic field strength (M1) is affected by the current value. That is, as the current value increases, the detection magnetic field strength (M1) also increases. On the other hand, when the current value decreases, the detection magnetic field strength (M1) also decreases. Therefore, the detection magnetic field strength (M1) includes the influence of the current value and the influence of the direction in which the conductive fibers SE are arranged (actual orientation direction C).
- the actual orientation direction C is a main item to be inspected in the inspection method of the present disclosure.
- Step T1 for preparing the specimen S is executed.
- the electrode 9 is attached to the specimen S.
- the electrode 9 is attached to each of one end Sb and the other end Sc intersecting the set orientation direction B (see FIG. 5).
- the width of the electrode 9 is determined empirically in consideration of meandering detectability and workability. As an example, the width of the electrode 9 may be determined from the viewpoint of suppressing a decrease in the density of the current E flowing through the test body S. For example, when the length of the one end Sb is 300 mm, the length of the electrode 9 may be 100 mm. When the length of the one end Sb is 600 mm, the length of the electrode 9 may be 100 mm.
- the specimen S to which the electrode 9 is attached is placed on the stage 2.
- Step T2 for arranging the magnetic field sensor 6 is executed.
- the magnetic field sensor 6 includes a detection magnetic field measurement unit 6a and a correction magnetic field measurement unit 6b. Therefore, Step T2 includes Step T2a for arranging the magnetic field measuring unit 6a for detection and Step T2b for arranging the magnetic field measuring unit 6b for correction.
- the magnetic field sensor 6 is disposed at a position facing the main surface Sa of the test body S.
- the magnetic field sensor 6 may be brought into contact with the main surface Sa or may be separated from the main surface Sa by a predetermined distance. When separating, for example, the distance between the magnetic field sensor 6 and the main surface Sa is 5 mm or less.
- the first detection axis D1 is parallel to the set orientation direction B.
- the second detection axis D2 is orthogonal to the set orientation direction B (see part (a) of FIG. 3).
- the first detection axis D1 and the second detection axis D2 are orthogonal to each other. Therefore, if the first detection axis D1 is arranged so as to be parallel to the set orientation direction B, the second detection axis D2 is necessarily arranged so as to be orthogonal to the set orientation direction B.
- Step T3 in which current E is applied.
- the current E is continuously applied to the specimen S until step T6 for stopping the current E to be executed later.
- Step T3 is executed by the current application device 4 and the current controller 11b of the computer 7.
- the computer 7 outputs a control signal to operate the current application device 4.
- the control signal includes a command for starting the output of the current E from the current application device 4.
- the control signal includes instructions regarding the frequency of the current E and the intensity of the current E.
- the control signal includes a command for setting the frequency of the current E to 100 kHz and a command for setting the intensity of the current E to 200 mA.
- Step T4 for acquiring the magnetic field strength is executed.
- data relating to the magnetic field strength is acquired while the position of the magnetic field sensor 6 is moved relative to the specimen S.
- the data regarding the magnetic field strength includes two-dimensional position information (x, y) of the magnetic field sensor 6 with respect to the test body S and information on the magnetic field strength at the position.
- the magnetic field strength information includes a detection magnetic field strength (M1) (first magnetic field strength) and a correction magnetic field strength (M2) (second magnetic field strength).
- the data regarding the magnetic field strength is “when the magnetic field sensor 6 is at the position (x, y) on the main surface Sa of the test body S, the detection magnetic field strength (M1) is the value (V1), and the correction magnetic field is The intensity (M2) is a value (V2) ".
- step T4 the movement of the specimen S is executed by the stage 2, the driver 3, the stage control unit 11c, and the controller 12b.
- step T4 acquisition of data regarding the magnetic field strength is executed by the magnetic field sensor 6, the lock-in amplifier 8, the digitizer 12a, the filter processing unit 13a, and the memory 14.
- the stage control unit 11c outputs a control signal for controlling the stage 2 so as to move the test body S along a preset movement course.
- the control signal is output to the stage 2 via the controller 12b and the driver 3.
- the stage 2 moves the specimen S in the X-axis direction and the Y-axis direction according to the control signal.
- the computer 7 controls the stage 2 so that the magnetic field sensor 6 is arranged at the corner of the specimen S. This point is now called the first starting point R1.
- the first start point R1 is indicated by coordinate information (0, 0).
- the computer 7 controls the stage 2 so that the magnetic field sensor 6 moves along the X-axis direction from the first start point R1 to the first end point R2.
- the first end point R2 is indicated by coordinate information (X, 0).
- the magnetic field sensor 6 outputs the detection magnetic field strength (M1) and the correction magnetic field strength (M2) to the lock-in amplifier 8.
- the stage controller 11c outputs position information indicating the position of the magnetic field sensor 6 with respect to the stage 2 to the memory 14 based on the control signal.
- the memory 14 of the computer 7 stores the positional information (x, y) and the detection magnetic field strength (M1) in association with each other.
- the memory 14 stores the positional information (x, y) and the correction magnetic field strength (M2) in association with each other.
- step T4 the magnetic field intensity for detection (M1) and the magnetic field intensity for correction (M2) along the line L1 are obtained (steps T4a and T4b).
- the computer 7 executes Step T5.
- the computer 7 controls the stage 2 so that the magnetic field sensor 6 moves from the first end point R2 to the second start point R3.
- the second start point R3 is indicated by coordinate information (0, y1). While the magnetic field sensor 6 moves from the first end point R2 to the second start point R3, the magnetic field intensity output from the magnetic field sensor 6 may be stored in the memory 14 in association with the position information.
- the computer 7 executes Step T4 again.
- the computer 7 controls the stage 2 so that the magnetic field sensor 6 moves along the X-axis direction from the second start point R3 to the second end point R4.
- the second end point R4 is indicated by coordinate information (X, y1). While the magnetic field sensor 6 moves from the second start point R3 to the second end point R4, the magnetic field sensor 6, the lock-in amplifier 8, the digitizer 12a, the filter processing unit 13a, and the memory 14 acquire data related to the magnetic field strength. I do.
- step T4 the magnetic field intensity for detection (M1) and the magnetic field intensity for correction (M2) along the line L2 are obtained.
- the detection magnetic field strength (M1) and the correction along the lines L1, L2, L3, L4, L5, L6, and L7 as data on the magnetic field strength are corrected by repeatedly performing Step T4 and Step T5.
- the first detection axis D1 is along the main surface Sa and parallel to the set orientation direction B. Therefore, when the direction in which the conductive fibers SE are arranged and the set orientation direction B coincide with each other, the detection magnetic field strength (M1) is zero. In other words, when the actual orientation direction C and the set orientation direction B coincide, the detection magnetic field strength (M1) is zero. In other words, when the conductive fiber SE meanders, the detection magnetic field strength (M1) is a predetermined value that is not zero.
- the second detection axis D2 is orthogonal to the first detection axis D1. That is, the second detection axis D2 is along the main surface Sa and is orthogonal to the set orientation direction B. Therefore, when the actual orientation direction C coincides with the set orientation direction B, the correction magnetic field strength (M2) is a predetermined value that is not zero. In other words, when the conductive fiber SE does not meander, the correction magnetic field strength (M2) is a predetermined value that is not zero. On the other hand, when the actual orientation direction C does not coincide with the set orientation direction B, the correction magnetic field strength (M2) decreases to a value smaller than the predetermined value. In other words, when the conductive fiber SE meanders, the correction magnetic field strength (M2) decreases to a value smaller than the predetermined value.
- step T7 a portion where the orientation of the conductive fiber SE is disturbed (a meandering portion) is detected using data on the magnetic field strength.
- Step T7 includes a step T8 for obtaining a correction coefficient, a step T9 for correcting the magnetic field intensity for detection (M1) using the correction coefficient, and a step T10 for determining the presence or absence of meandering.
- Step T8 for obtaining the correction coefficient will be described.
- Step T8 is executed by the signal processing unit 13.
- the correction coefficient (a) is calculated using the position information (x, y) and the correction magnetic field strength (M2) associated with the position information. More specifically, step T8 includes a step T8a for obtaining an average value (Hm) of the correction magnetic field strength (M2), a step T8b for selecting a reference strength (Href), and a step for calculating a correction coefficient (a). T8c.
- step T8a for obtaining the average value (Hm) the average value (M2) of the correction magnetic field strength (M2) is obtained using the position information (x, y) and the correction magnetic field strength (M2) associated with the information. Hm) is acquired (see equation (1)).
- Step T8a is executed by the memory 14 and the average intensity acquisition unit 13b.
- the average intensity acquisition unit 13b takes out the correction magnetic field intensity (M2) associated with the information whose Y coordinate is (0) from the memory 14.
- the average intensity acquisition unit 13b calculates an average value (Hm) of the extracted correction magnetic field intensity (M2).
- Step T8a for calculating the average value (Hm) is executed for each of the lines L1, L2, L3, L4, L5, L6, and L7 for which the correction magnetic field strength (M2) has already been acquired. Therefore, when the correction magnetic field strength (M2) is acquired for the seven lines L1, L2, L3, L4, L5, L6, and L7, the average strength acquisition unit 13b determines the seven average values (Hm ) Is calculated.
- Hm Average value of magnetic field intensity for correction in the nth line
- M2 Magnetic field intensity for correction
- k Number of samples of magnetic field intensity for correction n: Line number
- FIG. 7 (a) is a contour diagram showing the distribution of the second magnetic field strength that is proportional to the current value in the specimen S.
- FIG. The color shading corresponds to the current value.
- the dark portion is a portion where the current value is relatively high.
- a light-colored portion is a portion having a relatively low current value.
- the region K1 is a region sandwiched between the electrodes 9. As shown in part (a) of FIG. 7, the current value distribution in the specimen S is not two-dimensionally uniform. Specifically, in the region K1 of the test body S, the current value changes along the direction from one electrode 9 toward the other electrode 9 (that is, the set orientation direction B).
- the current value in the vicinity of the electrode 9 tends to be larger than the current value in the vicinity of the center of the pair of electrodes 9.
- the range used for calculating the average value (Hm) is limited to a region (region K3) that does not include the region in the vicinity of the electrode 9. That is, the average value (Hm) is calculated using the correction magnetic field strength (M2) acquired in the region K3. In other words, the correction magnetic field strength (M2) acquired in the region near the electrode 9 not included in the region K3 is not used for calculating the average value (Hm).
- Step T8b selects the standard strength (Href).
- one reference intensity (Href) serving as a correction reference is selected from the seven average values (Hm).
- Step T8b is executed by the reference intensity acquisition unit 13c.
- the reference strength acquisition unit 13c selects the maximum value among the plurality of average values (Hm) as the reference strength (Href).
- the reference strength acquisition unit 13 c uses the average value (Hm) in the region closest to the side edge as the reference strength.
- Select as (Href) selects the average value (Hm) of the line L1 as the reference strength (Href).
- the reference strength acquisition unit 13c may select an average value (Hm) in a region having a relatively high current value in the test body S as the reference strength (Href).
- the reference strength acquisition unit 13c may select the reference strength (Href) based on other criteria.
- step T8c for obtaining the correction coefficient (a) the correction coefficient (a) is calculated.
- Step T8c is executed by the correction coefficient acquisition unit 13d. Specifically, the correction coefficient acquisition unit 13d divides each of the plurality of average values (Hm) by the reference intensity (Href) (see Expression (2)).
- the correction coefficient (a) is stored in the memory 14 in association with the line L number.
- Step T9 is executed.
- the detection magnetic field strength (M1) is corrected using the correction coefficient (a).
- Step T9 is executed by the signal correction unit 13e.
- the signal correction unit 13e takes out the detection magnetic field strength (M1) and the correction coefficient (a) corresponding to the nth line L from the memory 14 using the position information (y) corresponding to the nth line L as a trigger. .
- the signal correction unit 13e divides the detection magnetic field strength (M1) by the correction coefficient (a) (see Expression (3)), and corrects the detected magnetic field strength (M3) (first corrected magnetic field strength). ) Division processing is correction processing.
- (M3) n magnetic field intensity for detection after correction in the nth line
- n magnetic field intensity for detection before correction in the nth line
- n correction coefficient in the nth line
- Steps T8a, T8b, T8c, and T9 the corrected magnetic field intensity (M3) after the current value variation is suppressed is obtained.
- step T10 an inspection relating to meandering is performed using the corrected magnetic field strength for detection (M3).
- Step T10 is executed by the meandering inspection unit 13f.
- the meandering inspection unit 13 f reads the corrected magnetic field intensity for detection (M3) from the memory 14.
- the meandering inspection unit 13f performs inspection related to meandering.
- the inspection related to meandering includes determination of presence / absence of meandering and determination of a position where meandering occurs. The presence or absence of meandering may be determined according to a desired standard. For example, the peak value in the corrected magnetic field intensity (M3) can be adopted as a desired reference.
- a magnetic field intensity having a wavelength narrower than the predetermined threshold and having an absolute value larger than the predetermined threshold it may be determined that a change in the magnetic field M has occurred. If it is determined that a change in the magnetic field M has occurred, it is determined that meandering is present. Alternatively, it is determined that a change in the magnetic field M has occurred when the waveform included in the corrected magnetic field strength for detection (M3) is disturbed and the variation in the waveform period exceeds a predetermined threshold. You can do it. If it is determined that a change in the magnetic field M has occurred, it is determined that meandering is present.
- the corrected magnetic field strength for detection (M3) is associated with the position information (x, y). Therefore, the position where the meander exists can be acquired by referring to the position information (x, y) corresponding to the information determined that the meander exists.
- the result of step T10 is stored in the memory 14.
- Step T11 displays the corrected magnetic field intensity for detection (M3) obtained by executing Step T9 and the result of the inspection relating to meandering obtained in Step T10.
- Step T11 is executed by the display control unit 11a. If it is determined that there is no problem in the result, the mounting position of the electrode 9 is changed (step T12).
- FIG. 7 (a) is a contour diagram showing a second magnetic field intensity proportional to the current value on the main surface Sa of the test body S.
- FIG. The color shading corresponds to the current value.
- the dark portion is a portion where the current value is relatively high.
- a light-colored portion is a portion having a relatively low current value.
- Part (b) of FIG. 7 is a contour diagram showing the detection magnetic field strength (M1) on the main surface Sa of the specimen S.
- the color shading indicates the strength of the magnetic field strength for detection (M1).
- the dark portion is a portion where the magnetic field strength is relatively strong.
- the light-colored portion is a portion where the magnetic field strength is relatively weak.
- Part (a) of FIG. 7 and part (b) of FIG. 7 are results obtained in an example described later. A detailed description of the embodiment in which the parts (a) and (b) of FIG. 7 are acquired will be described later.
- the detection magnetic field strength (M1) is disturbed in the region where the meandering occurs. If the degree of meandering is constant with respect to the direction intersecting the set orientation direction B (Y-axis direction), the magnetic field strength should be constant with respect to the Y-axis direction. However, as in the region K4 shown in FIG. 7B, the magnetic field intensity generated by meandering is not constant along the direction (Y-axis direction).
- the current value distribution in the specimen S is not two-dimensionally uniform, as shown in part (a) of FIG. Specifically, the current value distribution changes along the direction (Y-axis direction) intersecting the set orientation direction B in the specimen S.
- the current value is distributed in the Y-axis direction intersecting the set orientation direction B.
- the current E flows linearly between the pair of electrodes 9 and the other electrode 9, but passes through a region K ⁇ b> 2 where the current E is not sandwiched between the electrodes 9 as it approaches the other side. Then flow. Therefore, the current value is expected to be distributed in the Y-axis direction intersecting the set orientation direction B.
- the orientation of the conductive fiber SE may deviate from a preset orientation direction. As described above, a state in which the actual orientation direction of the conductive fiber SE is deviated from the set orientation direction is a state in which the orientation of the conductive fiber SE is disturbed.
- step T3 in which the current E is applied when the current E is applied through the conductive fiber SE, a magnetic field M is generated.
- the magnetic field M is orthogonal to the direction in which the current E flows. Since the current E flows through the conductive fiber SE, the direction in which the current E flows matches the actual orientation direction of the conductive fiber SE. Therefore, the magnetic field M is orthogonal to the actual orientation direction of the conductive fiber SE. If the actual orientation direction of the conductive fibers SE is deviated from the set orientation direction, the magnetic field M tilts at an angle that is not orthogonal to the set orientation direction.
- the magnetic field strength can be affected by the current value.
- the detection magnetic field measurement unit 6a Since the detection magnetic field measurement unit 6a is arranged so that the first detection axis D1 is parallel to the set orientation direction, the detection magnetic field strength (M1) along the set orientation direction is acquired. To do. Therefore, when there is no disturbance in the orientation of the conductive fibers SE, the magnetic field M is orthogonal to the set orientation direction, and thus the detection magnetic field strength (M1) is zero. On the other hand, when the orientation of the conductive fiber SE is disturbed, the magnetic field M is inclined with respect to the set orientation direction, and therefore the detection magnetic field strength (M1) is a predetermined value. That is, according to step T4a for obtaining the magnetic field strength for detection (M1), the magnetic field strength for detection (M1) including the influence due to the disorder of the orientation of the conductive fiber SE and the influence of the current value is obtained. .
- the correction magnetic field measuring unit 6b Since the correction magnetic field measuring unit 6b is arranged so that the second detection axis D2 intersects the set orientation direction, the correction magnetic field strength (M2) along the direction intersecting the set orientation direction is set. ) To get.
- the correction magnetic field strength (M2) is proportional to the current value. That is, according to step T4b for obtaining the correction magnetic field strength (M2), the correction magnetic field strength (M2) including the influence of the current value is obtained.
- step T10 in which the inspection relating to meandering is performed, the correction coefficient (a) is acquired using the correction magnetic field strength (M2).
- the correction coefficient (a) reduces the influence of the current value included in the detection magnetic field strength (M1). Accordingly, by correcting the detection magnetic field strength (M1) using the correction coefficient (a), the influence of the current value included in the detection magnetic field strength (M1) is reduced. Therefore, according to step T10, disorder of the orientation of the conductive fiber SE can be reliably detected.
- a test body S in which meandering was intentionally introduced was prepared.
- the test body S is made of a conductive composite material.
- the test body S has a plate shape with a length (X-axis direction) of 298 mm and a width (Y-axis direction) of 235 mm.
- the test body S has a meandering introduction portion 21 extending in the width direction in the vicinity of the approximate center in the vertical direction.
- the meandering introduction portion 21 has a first region 21a and a second region 21b.
- the first region 21a has a width of 90 mm.
- the first region 21a includes a plurality of prepregs in which meandering is introduced.
- the second region 21b has a width of 145 mm.
- the second region 21b has fewer prepregs in which meandering is introduced than the first region 21a.
- the inspection range 22 in the test body S is rectangular. Specifically, the inspection range 22 in the test body S has a length of 270 mm and a width of 235 mm. A pair of electrodes 9 was attached so as to sandwich the first region 21a in the vertical direction. The length of the electrode 9 is 100 mm in the width direction.
- an AMR sensor having a sensing axis in two directions of the X axis and the Y axis was used as the magnetic field sensor.
- the frequency of the current E supplied to the test body S was 100 kHz.
- the magnetic field sensor was scanned along a trajectory as shown in FIG. The scanning speed is 50 mm / sec.
- the scan pitch in the vertical direction (X-axis direction) is 0.5 mm.
- the recording pitch in the width direction (Y-axis direction) is 1.0 mm.
- (A) part of Drawing 7 shows distribution of the 2nd magnetic field strength proportional to an electric current value. The color shading corresponds to the current value.
- Part (b) of FIG. 7 shows the distribution of the magnetic field intensity for detection (M1). As shown in part (a) of FIG. 7, it was found that the current value changed along the width direction (Y-axis direction) of the specimen S. It was found that the detection magnetic field strength (M1) shown in part (b) of FIG. 7 also changed along the width direction (Y-axis direction) of the specimen S so as to correspond to the change in the current value. (See region K4).
- FIG. 8 (a) shows the result of correcting the detection magnetic field strength (M1) shown in FIG. 7 (b) using the inspection method according to the present disclosure. That is, part (a) of FIG. 8 shows the corrected magnetic field intensity (M3). As shown in part (a) of FIG. 8, it can be seen that the change along the width direction (Y-axis direction) is suppressed in the magnetic field change portion (region K4A) indicating the presence of meandering.
- a graph G1 shows the distribution of the magnetic field intensity for detection (M1) before correction in the region K4 in part (b) of FIG.
- a graph G2 shows the distribution of the corrected magnetic field strength (M3) in the region K4A in FIG.
- the horizontal axis corresponds to the width direction of the specimen S.
- the vertical axis corresponds to the normalized amplitude.
- a plurality of prepregs (S1, S3,..., Sn-1), (S2, S4,..., Sn) whose fiber orientation directions are different from each other by 90 ° are alternately laminated. It was.
- a plurality of prepregs whose fiber orientation directions are plus or minus 45 ° may be alternately laminated.
- a plurality of prepregs whose fiber orientation directions are all the same may be laminated.
- the inspection process may be executed every time one intensity history is acquired.
- the individual processes constituting the intensity acquisition and the intensity process may be combined in a desired order.
- the conductive composite material inspection method and inspection apparatus can reliably detect disorder of the orientation of the conductive fibers.
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Abstract
Description
M2 :補正用磁界強度
k :補正用磁界強度のサンプル数
n :ラインの番号
(Hm)n:n番目のラインに対応する平均値
Href :基準強度
(M1)n:n番目のラインにおける補正前の検出用磁界強度
(a)n :n番目のラインにおける補正係数
2 ステージ
3 ドライバ
4 電流印加装置
6 磁界センサ
6a 検出用磁界測定部(第1の磁界測定部)
6b 補正用磁界測定部(第2の磁界測定部)
7 コンピュータ(データ処理部)
8 ロックインアンプ
9 電極
11 主制御部
12 入出力部
13 信号処理部
14 メモリ
11a 表示制御部
11c ステージ制御部
11b 電流制御部
12a デジタイザ
12b コントローラ
13a フィルタ処理部
13b 平均強度取得部
13c 基準強度取得部
13d 補正係数取得部
13e 信号補正部
13f 蛇行検査部
B 設定配向方向
C 実配向方向
D1 第1の検出軸
D2 第2の検出軸
E 電流
Hm 平均値
Href 基準強度
M 磁界
M1 検出用磁界強度(第1の磁界強度)
M2 補正用磁界強度(第2の磁界強度)
M3 補正後の検出用磁界強度
S 試験体
Sa 主面
SE 導電性繊維
Sb 一端
Sc 他端
Claims (5)
- 導電性繊維を含む導電性複合材料の検査方法であって、
第1の検出軸に沿った方向の磁界強度を取得する第1の磁界測定部を、前記導電性複合材料を含む試験体の主面と対向する位置において前記第1の検出軸が前記導電性繊維の設定された配向方向と平行になるように配置するステップと、
第2の検出軸に沿った方向の磁界強度を取得する第2の磁界測定部を、前記試験体の主面と対向する位置において前記第2の検出軸が前記導電性繊維の設定された配向方向と交差するように配置するステップと、
前記導電性繊維を介して前記試験体の一端と他端との間に電流を印加するステップと、
前記主面に対して前記第1の磁界測定部を相対的に移動させながら、前記第1の磁界測定部から出力される第1の磁界強度を取得するステップと、
前記主面に対して前記第2の磁界測定部を相対的に移動させながら、前記第2の磁界測定部から出力される第2の磁界強度を取得するステップと、
前記第1の磁界強度と前記第2の磁界強度とを利用して、前記導電性繊維の配向が乱れている部分を検出するステップと、を有し、
前記導電性繊維の配向が乱れている部分を検出するステップは、
前記第2の磁界強度を利用して、前記第1の磁界強度を補正するための補正係数を取得するステップと、
前記補正係数を利用して、補正された前記第1の磁界強度を取得するステップと、
補正された前記第1の磁界強度を利用して、前記導電性繊維の配向が乱れている部分を検出するステップと、を含む導電性複合材料の検査方法。 - 前記補正係数を取得するステップは、
前記第2の磁界強度の平均値を取得するステップと、
前記第2の磁界強度及び前記平均値を利用して、前記補正係数を算出するステップと、
を含む、請求項1に記載の導電性複合材料の検査方法。 - 前記補正された前記第1の磁界強度を取得するステップは、
前記第1の磁界強度を前記補正係数によって除算する、請求項1に記載の導電性複合材料の検査方法。 - 前記補正された前記第1の磁界強度を取得するステップは、
前記第1の磁界強度を前記補正係数によって除算する、請求項2に記載の導電性複合材料の検査方法。 - 導電性繊維を含む導電性複合材料の検査装置であって、
第1の検出軸に沿った方向の磁界強度を取得すると共に、前記導電性複合材料を含む試験体の主面と対向する位置において前記第1の検出軸が前記導電性繊維の設定された配向方向と平行になるように配置される第1の磁界測定部と、
第2の検出軸に沿った方向の磁界強度を取得すると共に、前記試験体の主面と対向する位置において前記第2の検出軸が前記導電性繊維の設定された配向方向と交差するように配置される第2の磁界測定部と、
前記導電性繊維を介して前記試験体の一端と他端との間に電流を印加する電流印加部と、
前記主面に対して前記第1の磁界測定部及び前記第2の磁界測定部を相対的に移動させる移動機構部と、
前記第1の磁界測定部から出力される第1の磁界強度と前記第2の磁界測定部から出力される第2の磁界強度とを利用して、前記導電性繊維の配向が乱れている部分を検出するデータ処理部と、を備え、
前記データ処理部は、
前記第2の磁界強度を利用して、前記第1の磁界強度を補正するための補正係数を取得する補正係数取得部と、
前記補正係数を利用して、補正された前記第1の磁界強度を取得する信号補正部と、
補正された前記第1の磁界強度を利用して、前記導電性繊維の配向が乱れている部分を検出する蛇行検査部と、を含む、導電性複合材料の検査装置。
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JP6428962B2 (ja) | 2018-11-28 |
CA3015868C (en) | 2020-06-16 |
JPWO2017158864A1 (ja) | 2018-06-21 |
EP3431981A4 (en) | 2019-11-20 |
EP3431981A1 (en) | 2019-01-23 |
CA3015868A1 (en) | 2017-09-21 |
US10605777B2 (en) | 2020-03-31 |
CN108369212B (zh) | 2021-08-13 |
CN108369212A (zh) | 2018-08-03 |
RU2696339C1 (ru) | 2019-08-01 |
EP3431981B1 (en) | 2021-10-06 |
US20190072521A1 (en) | 2019-03-07 |
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