WO2016141754A1 - Nerve-soothing and sleep-aiding patch and preparation method therefor - Google Patents
Nerve-soothing and sleep-aiding patch and preparation method therefor Download PDFInfo
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- WO2016141754A1 WO2016141754A1 PCT/CN2015/099071 CN2015099071W WO2016141754A1 WO 2016141754 A1 WO2016141754 A1 WO 2016141754A1 CN 2015099071 W CN2015099071 W CN 2015099071W WO 2016141754 A1 WO2016141754 A1 WO 2016141754A1
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/70—Web, sheet or filament bases ; Films; Fibres of the matrix type containing drug
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/53—Lamiaceae or Labiatae (Mint family), e.g. thyme, rosemary or lavender
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/73—Rosaceae (Rose family), e.g. strawberry, chokeberry, blackberry, pear or firethorn
- A61K36/738—Rosa (rose)
Definitions
- the invention relates to a soothing sleep aid.
- the invention also relates to a preparation method of a soothing sleep aid paste.
- insomnia In daily life, with the rapid pace of life, discomfort in labor, etc., insomnia often occurs, affecting physical and mental health and normal working life.
- the drug-assisted mainly is the hospital to prescribe sleeping pills. Taking a small amount of sleeping pills can help the insomniacs to sleep, but taking long-term sleeping pills has certain damage to the body itself.
- the way of aromatherapy requires a certain method and the price is relatively expensive, so the quick and effective way of assisting sleep is temporarily blank in the market, and the market for soothing and sleeping is filling the gap in the market.
- the technical problem to be solved by the present invention is to provide a soothing sleep aid.
- the technical problem still to be solved by the present invention is to provide a preparation method of the soothing sleep aid paste.
- the soothing sleep aid paste comprises a body of the soothing sleep aid, wherein the body of the soothing sleep aid is composed of a backing layer, a polymer gel layer and a release layer, and the release layer is located on the upper layer of the polymer gel layer.
- the backing layer is located in the lower layer of the polymer gel layer, and the composition of the polymer gel layer is: polymer gel material: 30-32%; galaluminum: 0.07-0.08%; Lavender essential oil: 0.5-1.5%; rose essential oil: 0.5-1.5%; purified water: added to 100%.
- the release layer is composed of a polyethylene film.
- the polymer gel material comprises sorbitol, glycerin, crospovidone, polyvinylpyrrolidone, sodium polyacrylate, the sorbitol is a dispersing agent, the glycerin is a humectant, and the crospovidone is A crosslinking agent, the polyvinylpyrrolidone is an adhesion agent, and the sodium polyacrylate is a thickener.
- the preparation method of the soothing sleep aid paste comprises the following steps: (1) adding 24.5-25% glycerin, 0.07-0.08% glycol aluminum in the raw material 2.7-3.1% sodium polyacrylate and stirring for 20 min;
- the invention has the advantages that the production process is relatively convenient, the product is convenient to use, and meets the needs of daily life.
- the soothing sleep aid paste comprises a body of the soothing sleep aid, wherein the body of the soothing sleep aid is composed of a backing layer, a polymer gel layer and a release layer, and the release layer is located on the upper layer of the polymer gel layer.
- the backing layer is located under the polymer gel layer, and the composition of the polymer gel layer is as follows:
- Polymer gel material 30%;
- Lavender essential oil 0.5%
- Purified water added to 100%.
- the release layer is composed of a polyethylene film.
- the polymer gel material comprises sorbitol, glycerin, crospovidone, polyvinylpyrrolidone, sodium polyacrylate, the sorbitol is a dispersing agent, the glycerin is a humectant, and the crospovidone is A crosslinking agent, the polyvinylpyrrolidone is an adhesion agent, and the sodium polyacrylate is a thickener.
- the preparation method of the soothing sleep aid paste comprises the following steps: (1) adding 24.5% glycerin, 0.07% galaluminum in the 2.7% sodium polyacrylate of the raw material and stirring for 20 min;
- the soothing sleep aid paste comprises a body of the soothing sleep aid, wherein the body of the soothing sleep aid is composed of a backing layer, a polymer gel layer and a release layer, and the release layer is located on the upper layer of the polymer gel layer.
- the backing layer is located under the polymer gel layer, and the composition of the polymer gel layer is as follows:
- Polymer gel material 32%;
- Purified water added to 100%.
- the release layer is composed of a polyethylene film.
- the polymer gel material comprises sorbitol, glycerin, crospovidone, polyvinylpyrrolidone, sodium polyacrylate, the sorbitol is a dispersing agent, the glycerin is a humectant, and the crospovidone is A crosslinking agent, the polyvinylpyrrolidone is an adhesion agent, and the sodium polyacrylate is a thickener.
- the preparation method of the soothing sleep aid paste comprises the following steps: (1) adding 25% glycerin, 0.08% galaluminum in the raw material 3.1% sodium polyacrylate and stirring for 20 min;
- the soothing sleep aid paste comprises a body of the soothing sleep aid, wherein the body of the soothing sleep aid is composed of a backing layer, a polymer gel layer and a release layer, and the release layer is located on the upper layer of the polymer gel layer.
- the backing layer is located under the polymer gel layer, and the composition of the polymer gel layer is as follows:
- Polymer gel material 31%;
- Glycol aluminum 0.075%
- Lavender essential oil 1%
- Purified water added to 100%.
- the release layer is composed of a polyethylene film.
- the polymer gel material comprises sorbitol, glycerin, crospovidone, polyvinylpyrrolidone, sodium polyacrylate, the sorbitol is a dispersing agent, the glycerin is a humectant, and the crospovidone is A crosslinking agent, the polyvinylpyrrolidone is an adhesion agent, and the sodium polyacrylate is a thickener.
- the preparation method of the soothing sleep aid paste comprises the following steps: (1) adding 24.8% glycerin and 0.075% galaluminum in the 2.8% sodium polyacrylate of the raw material and stirring for 20 min;
- the production process of the invention is relatively convenient, and the product is convenient to use and meets the needs of daily life.
Abstract
A nerve-soothing and sleep-aiding patch, consisting of a back lining layer, a polymer gel layer and an anti-sticking layer. The anti-sticking layer is formed by a polyethylene film and is located at an upper layer of the polymer gel layer. The back lining layer is located at a lower layer of the polymer gel layer. The polymer gel layer comprises the following components in percentage by weight: 30 to 32 percent of polymer gel material, 0.07 to 0.08 percent of aluminum glycinate, 0.5 to 1.5 percent of lavender essential oil, 0.5 to 1.5 percent of rose essential oil and the balance of pure water. The polymer gel material comprises a dispersing agent, a moisturizer, a cross-linking agent, an adhesive and a thickener. Also disclosed is a preparation method for the nerve-soothing and sleep-aiding patch, comprising: adding 24.5 to 25 percent of glycerol and 0.07 to 0.08 percent of aluminum glycinate into 2.7 to 3.1 percent of sodium polyacrylate, and performing stirring for 20min; adding 0.2 to 0.4 percent of cross-linked polyvinylpolypyrrolidone, 2.3 to 3 percent of polyvinylpyrrolidone, 0.3 to 0.5 percent of sorbitol and pure water, and performing vacuum stirring for 5 to 8min; and adding 0.5 to 1.5 percent of lavender essential oil and 0.5 to 1.5 percent of rose essential oil, and performing vacuum stirring for 5min.
Description
本发明涉及一种安神助眠贴。The invention relates to a soothing sleep aid.
本发明还涉及一种安神助眠贴的制备方法。The invention also relates to a preparation method of a soothing sleep aid paste.
目前,在日常生活中,随着生活节奏的变快,劳役不适度等,常常会有失眠的情况发生,影响身心健以及正常的工作生活。现在市面上治疗失眠的方法主要分为药物辅助和香薰两种方式,药物辅助主要是医院开具安眠药,服用少量的安眠药可以帮助失眠者睡眠,但是长期服用安眠药对身体本身是有一定的伤害,而香薰的方式需要一定的方式方法,价格也相对昂贵,所以快捷有效的助眠方式在市场上暂时是空白,安神助眠贴的面市,填补了市场上的这一空白。At present, in daily life, with the rapid pace of life, discomfort in labor, etc., insomnia often occurs, affecting physical and mental health and normal working life. Nowadays, the methods for treating insomnia on the market are mainly divided into two methods: drug-assisted and aromatherapy. The drug-assisted mainly is the hospital to prescribe sleeping pills. Taking a small amount of sleeping pills can help the insomniacs to sleep, but taking long-term sleeping pills has certain damage to the body itself. The way of aromatherapy requires a certain method and the price is relatively expensive, so the quick and effective way of assisting sleep is temporarily blank in the market, and the market for soothing and sleeping is filling the gap in the market.
发明内容Summary of the invention
本发明需要解决的技术问题是提供一种安神助眠贴。The technical problem to be solved by the present invention is to provide a soothing sleep aid.
本发明还需要解决的技术问题是提供一种安神助眠贴的制备方法。The technical problem still to be solved by the present invention is to provide a preparation method of the soothing sleep aid paste.
本发明采用的技术方案是:The technical solution adopted by the invention is:
安神助眠贴,包括安神助眠贴本体,所述安神助眠贴本体由背衬层、高分子凝胶层和防粘层组成,所述防粘层位于高分子凝胶层的上层,所述背衬层位于高分子凝胶层的下层,所述高分子凝胶层的组成按重量百分比为:高分子凝胶材料:30-32%;甘羟铝:0.07-0.08%;
薰衣草精油:0.5-1.5%;玫瑰精油:0.5-1.5%;纯化水:加至100%。The soothing sleep aid paste comprises a body of the soothing sleep aid, wherein the body of the soothing sleep aid is composed of a backing layer, a polymer gel layer and a release layer, and the release layer is located on the upper layer of the polymer gel layer. The backing layer is located in the lower layer of the polymer gel layer, and the composition of the polymer gel layer is: polymer gel material: 30-32%; galaluminum: 0.07-0.08%;
Lavender essential oil: 0.5-1.5%; rose essential oil: 0.5-1.5%; purified water: added to 100%.
所述防粘层由聚乙烯薄膜组成。The release layer is composed of a polyethylene film.
所述高分子凝胶材料包括山梨醇、甘油、交联聚维酮、聚乙烯吡咯烷酮、聚丙烯酸钠,所述山梨醇为分散剂,所述甘油为保湿剂,所述交联聚维酮为交联剂,所述聚乙烯吡咯烷酮为黏附剂,所述聚丙烯酸钠为增稠剂。The polymer gel material comprises sorbitol, glycerin, crospovidone, polyvinylpyrrolidone, sodium polyacrylate, the sorbitol is a dispersing agent, the glycerin is a humectant, and the crospovidone is A crosslinking agent, the polyvinylpyrrolidone is an adhesion agent, and the sodium polyacrylate is a thickener.
所述的安神助眠贴的制备方法,包括以下步骤:(1)在原料2.7-3.1%的聚丙烯酸钠中加入24.5-25%的甘油、0.07-0.08%甘羟铝并搅拌20min;The preparation method of the soothing sleep aid paste comprises the following steps: (1) adding 24.5-25% glycerin, 0.07-0.08% glycol aluminum in the raw material 2.7-3.1% sodium polyacrylate and stirring for 20 min;
(2)在(1)材料中加入0.2-0.4%的交联聚维酮、2.3-3%聚乙烯吡咯烷酮、0.3-0.5%山梨醇、纯化水,并且真空搅拌5-8min;(2) adding 0.2-0.4% crospovidone, 2.3-3% polyvinylpyrrolidone, 0.3-0.5% sorbitol, purified water to the material (1), and stirring under vacuum for 5-8 min;
(3)在(2)材料中加入活性物:0.5-1.5%玫瑰精油、0.5-1.5%薰衣草精油,并且真空搅拌5min。(3) The active substance was added to the (2) material: 0.5-1.5% rose essential oil, 0.5-1.5% lavender essential oil, and stirred under vacuum for 5 min.
本发明的优点是:生产过程比较便捷,产品使用方便,符合日常生活所需。The invention has the advantages that the production process is relatively convenient, the product is convenient to use, and meets the needs of daily life.
实施例1Example 1
安神助眠贴,包括安神助眠贴本体,所述安神助眠贴本体由背衬层、高分子凝胶层和防粘层组成,所述防粘层位于高分子凝胶层的上层,所述背衬层位于高分子凝胶层的下层,所述高分子凝胶层的组成按重量百分比为:The soothing sleep aid paste comprises a body of the soothing sleep aid, wherein the body of the soothing sleep aid is composed of a backing layer, a polymer gel layer and a release layer, and the release layer is located on the upper layer of the polymer gel layer. The backing layer is located under the polymer gel layer, and the composition of the polymer gel layer is as follows:
高分子凝胶材料:30%;
Polymer gel material: 30%;
甘羟铝:0.07%;Glycol aluminum: 0.07%;
薰衣草精油:0.5%;Lavender essential oil: 0.5%;
玫瑰精油:0.5%;Rose essential oil: 0.5%;
纯化水:加至100%。Purified water: added to 100%.
所述防粘层由聚乙烯薄膜组成。The release layer is composed of a polyethylene film.
所述高分子凝胶材料包括山梨醇、甘油、交联聚维酮、聚乙烯吡咯烷酮、聚丙烯酸钠,所述山梨醇为分散剂,所述甘油为保湿剂,所述交联聚维酮为交联剂,所述聚乙烯吡咯烷酮为黏附剂,所述聚丙烯酸钠为增稠剂。The polymer gel material comprises sorbitol, glycerin, crospovidone, polyvinylpyrrolidone, sodium polyacrylate, the sorbitol is a dispersing agent, the glycerin is a humectant, and the crospovidone is A crosslinking agent, the polyvinylpyrrolidone is an adhesion agent, and the sodium polyacrylate is a thickener.
所述的安神助眠贴的制备方法,包括以下步骤:(1)在原料2.7%的聚丙烯酸钠中加入24.5%的甘油、0.07%甘羟铝并搅拌20min;The preparation method of the soothing sleep aid paste comprises the following steps: (1) adding 24.5% glycerin, 0.07% galaluminum in the 2.7% sodium polyacrylate of the raw material and stirring for 20 min;
(2)在(1)材料中加入0.2%的交联聚维酮、2.3%聚乙烯吡咯烷酮、0.3%山梨醇、纯化水加至100%,并且真空搅拌5-8min;(2) adding 0.2% crospovidone, 2.3% polyvinylpyrrolidone, 0.3% sorbitol, purified water to 100%, and vacuum stirring for 5-8 min;
(3)在(2)材料中加入活性物:0.5%玫瑰精油、0.5%薰衣草精油,并且真空搅拌5min。(3) The active substance was added to the (2) material: 0.5% rose essential oil, 0.5% lavender essential oil, and stirred under vacuum for 5 min.
实施例2Example 2
安神助眠贴,包括安神助眠贴本体,所述安神助眠贴本体由背衬层、高分子凝胶层和防粘层组成,所述防粘层位于高分子凝胶层的上层,所述背衬层位于高分子凝胶层的下层,所述高分子凝胶层的组成按重量百分比为:The soothing sleep aid paste comprises a body of the soothing sleep aid, wherein the body of the soothing sleep aid is composed of a backing layer, a polymer gel layer and a release layer, and the release layer is located on the upper layer of the polymer gel layer. The backing layer is located under the polymer gel layer, and the composition of the polymer gel layer is as follows:
高分子凝胶材料:32%;Polymer gel material: 32%;
甘羟铝:0.08%;
Glycol aluminum: 0.08%;
薰衣草精油:1.5%;Lavender essential oil: 1.5%;
玫瑰精油:1.5%;Rose essential oil: 1.5%;
纯化水:加至100%。Purified water: added to 100%.
所述防粘层由聚乙烯薄膜组成。The release layer is composed of a polyethylene film.
所述高分子凝胶材料包括山梨醇、甘油、交联聚维酮、聚乙烯吡咯烷酮、聚丙烯酸钠,所述山梨醇为分散剂,所述甘油为保湿剂,所述交联聚维酮为交联剂,所述聚乙烯吡咯烷酮为黏附剂,所述聚丙烯酸钠为增稠剂。The polymer gel material comprises sorbitol, glycerin, crospovidone, polyvinylpyrrolidone, sodium polyacrylate, the sorbitol is a dispersing agent, the glycerin is a humectant, and the crospovidone is A crosslinking agent, the polyvinylpyrrolidone is an adhesion agent, and the sodium polyacrylate is a thickener.
所述的安神助眠贴的制备方法,包括以下步骤:(1)在原料3.1%的聚丙烯酸钠中加入25%的甘油、0.08%甘羟铝并搅拌20min;The preparation method of the soothing sleep aid paste comprises the following steps: (1) adding 25% glycerin, 0.08% galaluminum in the raw material 3.1% sodium polyacrylate and stirring for 20 min;
(2)在(1)材料中加入0.4%的交联聚维酮、3%聚乙烯吡咯烷酮、0.5%山梨醇、纯化水加至100%,并且真空搅拌5-8min;(2) Adding 0.4% crospovidone, 3% polyvinylpyrrolidone, 0.5% sorbitol, purified water to 100% in (1) material, and stirring under vacuum for 5-8 min;
(3)在(2)材料中加入活性物:1.5%玫瑰精油、1.5%薰衣草精油,并且真空搅拌5min。(3) The active substance was added to the (2) material: 1.5% rose essential oil, 1.5% lavender essential oil, and stirred under vacuum for 5 min.
实施例3Example 3
安神助眠贴,包括安神助眠贴本体,所述安神助眠贴本体由背衬层、高分子凝胶层和防粘层组成,所述防粘层位于高分子凝胶层的上层,所述背衬层位于高分子凝胶层的下层,所述高分子凝胶层的组成按重量百分比为:The soothing sleep aid paste comprises a body of the soothing sleep aid, wherein the body of the soothing sleep aid is composed of a backing layer, a polymer gel layer and a release layer, and the release layer is located on the upper layer of the polymer gel layer. The backing layer is located under the polymer gel layer, and the composition of the polymer gel layer is as follows:
高分子凝胶材料:31%;Polymer gel material: 31%;
甘羟铝:0.075%;Glycol aluminum: 0.075%;
薰衣草精油:1%;
Lavender essential oil: 1%;
玫瑰精油:1%;Rose essential oil: 1%;
纯化水:加至100%。Purified water: added to 100%.
所述防粘层由聚乙烯薄膜组成。The release layer is composed of a polyethylene film.
所述高分子凝胶材料包括山梨醇、甘油、交联聚维酮、聚乙烯吡咯烷酮、聚丙烯酸钠,所述山梨醇为分散剂,所述甘油为保湿剂,所述交联聚维酮为交联剂,所述聚乙烯吡咯烷酮为黏附剂,所述聚丙烯酸钠为增稠剂。The polymer gel material comprises sorbitol, glycerin, crospovidone, polyvinylpyrrolidone, sodium polyacrylate, the sorbitol is a dispersing agent, the glycerin is a humectant, and the crospovidone is A crosslinking agent, the polyvinylpyrrolidone is an adhesion agent, and the sodium polyacrylate is a thickener.
所述的安神助眠贴的制备方法,包括以下步骤:(1)在原料2.8%的聚丙烯酸钠中加入24.8%的甘油、0.075%甘羟铝并搅拌20min;The preparation method of the soothing sleep aid paste comprises the following steps: (1) adding 24.8% glycerin and 0.075% galaluminum in the 2.8% sodium polyacrylate of the raw material and stirring for 20 min;
(2)在(1)材料中加入0.3%的交联聚维酮、2.7%聚乙烯吡咯烷酮、0.4%山梨醇、纯化水加至100%,并且真空搅拌5-8min;(2) adding (3) material to the mixture of 0.3% crospovidone, 2.7% polyvinylpyrrolidone, 0.4% sorbitol, purified water to 100%, and vacuum stirring for 5-8min;
(3)在(2)材料中加入活性物:1%玫瑰精油、1%薰衣草精油,并且真空搅拌5min。(3) The active substance was added to the (2) material: 1% rose essential oil, 1% lavender essential oil, and stirred under vacuum for 5 min.
本发明的生产过程比较便捷,产品使用方便,符合日常生活所需。
The production process of the invention is relatively convenient, and the product is convenient to use and meets the needs of daily life.
Claims (4)
- 安神助眠贴,包括安神助眠贴本体,其特征在于:所述安神助眠贴本体由背衬层、高分子凝胶层和防粘层组成,所述防粘层位于高分子凝胶层的上层,所述背衬层位于高分子凝胶层的下层,所述高分子凝胶层的组成按重量百分比为:The soothing sleep aid paste includes the body of the soothing sleep aid, wherein the body of the soothing sleep aid is composed of a backing layer, a polymer gel layer and a release layer, and the release layer is located on the polymer gel layer. The upper layer, the backing layer is located in the lower layer of the polymer gel layer, and the composition of the polymer gel layer is in weight percentage:
- 根据权利要求1所述的安神助眠贴,其特征在于:所述防粘层由聚乙烯薄膜组成。The soothing sleep aid according to claim 1, wherein the release layer is composed of a polyethylene film.
- 根据权利要求1所述的安神助眠贴,其特征在于:所述高分子凝胶材料包括山梨醇、甘油、交联聚维酮、聚乙烯吡咯烷酮、聚丙烯酸钠,所述山梨醇为分散剂,所述甘油为保湿剂,所述交联聚维酮为交联剂,所述聚乙烯吡咯烷酮为黏附剂,所述聚丙烯酸钠为增稠剂。The soothing sleep aid according to claim 1, wherein the polymer gel material comprises sorbitol, glycerin, crospovidone, polyvinylpyrrolidone, sodium polyacrylate, and the sorbitol is a dispersing agent. The glycerin is a humectant, the crospovidone is a crosslinking agent, the polyvinylpyrrolidone is an adhesion agent, and the sodium polyacrylate is a thickener.
- 一种如权利要求1所述的安神助眠贴的制备方法,其特征在于:包括以下步骤:(1)在原料2.7-3.1%的聚丙烯酸钠中加入24.5-25%的甘油、0.07-0.08%甘羟铝并搅拌20min;A method for preparing a soothing sleep aid according to claim 1, comprising the steps of: (1) adding 24.5-25% glycerin, 0.07-0.08 to the raw material 2.7-3.1% sodium polyacrylate. % galaluminum and stirred for 20 min;(2)在(1)材料中加入0.2-0.4%的交联聚维酮、2.3-3%聚乙烯吡咯烷酮、0.3-0.5%山梨醇、纯化水,并且真空搅拌5-8min; (2) adding 0.2-0.4% crospovidone, 2.3-3% polyvinylpyrrolidone, 0.3-0.5% sorbitol, purified water to the material (1), and stirring under vacuum for 5-8 min;(3)在(2)材料中加入活性物:0.5-1.5%玫瑰精油、0.5-1.5%薰衣草精油,并且真空搅拌5min。 (3) The active substance was added to the (2) material: 0.5-1.5% rose essential oil, 0.5-1.5% lavender essential oil, and stirred under vacuum for 5 min.
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CN110693940A (en) * | 2019-09-24 | 2020-01-17 | 李友谊 | Dampness-expelling and fat-reducing essence and preparation method thereof |
CN110522816A (en) * | 2019-10-21 | 2019-12-03 | 健民药业集团股份有限公司 | A kind of cow-bezoar infantile umbilical paste and preparation method thereof |
CN114642655A (en) * | 2022-04-22 | 2022-06-21 | 杭州师范大学 | Brain-nourishing mind-tranquilizing gel navel paste and preparation method thereof |
CN115137779B (en) * | 2022-06-01 | 2024-03-19 | 品高生物科技(广州)有限公司 | Sleep-aiding plant essential oil and preparation method thereof |
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