WO2015196390A1 - 一种静态乳化敏化无装药泵的乳化炸药连续生产方法 - Google Patents

一种静态乳化敏化无装药泵的乳化炸药连续生产方法 Download PDF

Info

Publication number
WO2015196390A1
WO2015196390A1 PCT/CN2014/080735 CN2014080735W WO2015196390A1 WO 2015196390 A1 WO2015196390 A1 WO 2015196390A1 CN 2014080735 W CN2014080735 W CN 2014080735W WO 2015196390 A1 WO2015196390 A1 WO 2015196390A1
Authority
WO
WIPO (PCT)
Prior art keywords
static
sensitization
emulsification
inner core
sensitizer
Prior art date
Application number
PCT/CN2014/080735
Other languages
English (en)
French (fr)
Inventor
唐秋明
郭紫卿
王木申
张爱军
Original Assignee
石家庄成功机电有限公司
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 石家庄成功机电有限公司 filed Critical 石家庄成功机电有限公司
Priority to AU2014399172A priority Critical patent/AU2014399172B2/en
Priority to US15/322,289 priority patent/US10759718B2/en
Priority to EP14895829.1A priority patent/EP3162785B1/en
Priority to PCT/CN2014/080735 priority patent/WO2015196390A1/zh
Publication of WO2015196390A1 publication Critical patent/WO2015196390A1/zh

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C06—EXPLOSIVES; MATCHES
    • C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
    • C06B21/00—Apparatus or methods for working-up explosives, e.g. forming, cutting, drying
    • C06B21/0008—Compounding the ingredient
    • C—CHEMISTRY; METALLURGY
    • C06—EXPLOSIVES; MATCHES
    • C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
    • C06B23/00—Compositions characterised by non-explosive or non-thermic constituents
    • C06B23/002—Sensitisers or density reducing agents, foam stabilisers, crystal habit modifiers
    • C—CHEMISTRY; METALLURGY
    • C06—EXPLOSIVES; MATCHES
    • C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
    • C06B47/00—Compositions in which the components are separately stored until the moment of burning or explosion, e.g. "Sprengel"-type explosives; Suspensions of solid component in a normally non-explosive liquid phase, including a thickened aqueous phase
    • C06B47/14—Compositions in which the components are separately stored until the moment of burning or explosion, e.g. "Sprengel"-type explosives; Suspensions of solid component in a normally non-explosive liquid phase, including a thickened aqueous phase comprising a solid component and an aqueous phase
    • C06B47/145—Water in oil emulsion type explosives in which a carbonaceous fuel forms the continuous phase

Definitions

  • the invention relates to the field of emulsion explosive production, and in particular to a continuous production method of an emulsion explosive static emulsification sensitized drug-free pump.
  • the present invention is directed to a method for producing an emulsion explosive static emulsification sensitized drug-free pump to achieve intrinsic safety in the production of emulsion explosives.
  • the present invention is achieved by the following technical solution (see FIG. 1),
  • Continuous production method of emulsion emulsifying sensitization-sensitized drug-free pump in the emulsion sensitization process, a continuous production method of static emulsification and static sensitization is adopted, wherein the static emulsifier and the static sensitizer are static mixers. At least one of the orifice plate, the jet stream, and the venturi tube method; the emulsification sensitizing device is directly connected to the injection tube, and after emulsification sensitization, the sensitization directly enters the charging process to complete the charging.
  • the static emulsifier comprises an oil phase inlet, a water phase inlet, an outer casing and an inner core, and the inner wall of the outer casing is provided with a split port, and the inner core is composed of an injection port and an orifice plate.
  • Each inner core corresponds to one splitting port, and the water phase enters the corresponding inner core from each splitting port.
  • the injection port of the inner core is arranged on the inner wall of the inner core, the orifice plate is arranged at the tail end of the inner core, the water phase is passed through the injection port and then enters the inner core through the injection port, and is mixed with the oil phase which enters the inner core through the oil phase inlet and is emulsified. Then enter the next core through the orifice plate.
  • the inner core is three or more, preferably five.
  • the static sensitizer includes a housing, a sensitizer feed port, an inner core, and a perforated plate.
  • the inner core is more than one, preferably three, and the sensitizing mode of the static sensitizer is that after the sensitizer passes through the sensitizer feeding port, it enters under the action of the sensitizer ejection port on the core of the first stage.
  • the latex matrix is mixed with the sensitizer through the first-stage porous plate, and then mixed through the second-stage, third-stage, and the like.
  • the apertures of the perforated plate may be circular, square, conical and/or petal shaped.
  • Static emulsification sensitization method can also add static sensitization plus static sensitization to static colostrum. Static sensitization is the same equipment as static condensate.
  • the oil phase self-oil phase tank enters the first-stage coarse milk mixer by the oil phase pump according to the full proportion of the explosive; the water phase self-water phase tank is divided into the explosive ratio by the water phase pump, and enters the multi-stage coarse milk mixer through the multi-stage splitting multiple times.
  • the emulsification is completed by the final grade of the coarse blender.
  • Milk The latex matrix enters the static sensitizer and the sensitizer enters the static sensitizer to complete the sensitization.
  • the drug then enters the injection tube.
  • the injection tube is wrapped in a tubular film, and the material is uniformly filled in the tubular film by a safe material pump instead of a dangerous gel pump or an explosive pump.
  • the filled medicine roll is sealed and then cooled into the cooling water. After the cooling is completed, it is packed through the conveyor belt and then stored in the warehouse.
  • the invention does not need mechanical agitation shearing and colloid/dynamite pumping device, and the water phase is mixed with the oil phase through the multi-stage coarse milk mixer through the flow regulation control to make the oil phase each time and a small amount of water phase. It can be thoroughly mixed, and after multiple additions of the aqueous phase, the final and all oil phases are uniformly mixed under low pressure conditions to obtain a colloidal matrix having a particle size of about 1 micrometer. Since the apparatus mixes the aqueous phase with the oil phase in the desired proportion, the conventional one-time mixing is improved to multiple mixing, which greatly reduces the amount of the drug, without mechanical agitation and shear emulsification.
  • the sensitization mode of the mechanical mixing type is eliminated, and the full static high temperature sensitization is performed, thereby improving the safety of the sensitization process.
  • the filling pump of the traditional production line is also eliminated, and the injection tube is directly entered, which reduces the dangerous point in the production process and the online drug storage amount, and realizes the intrinsic safety of the pharmaceutical and the charging.
  • Figure 1 is a process flow diagram of the method of the present invention
  • Figure 2 is a static emulsifier introduced by the present invention.
  • oil phase port 2 water phase port 3; outer casing 4: inner core 5 outlet
  • Figure 3 is a static sensitizer introduced by the present invention.
  • Feed port 2 Sensitizer feed port 3: Discharge port (fine plate) 4: Inner core 5: Housing
  • Figure 4 is a static emulsion sensitization combination diagram introduced by the present invention
  • Static emulsifier 2 Static sensitizer (with static emulsion)
  • the 5-stage emulsification equipment is subjected to 5-stage emulsification; the full-scale oil phase enters from the beginning of the static emulsifier, and some of the water phase flows from the lateral self-dividing port, and is ejected from the jet hole at a certain flow rate, impinging on the oil phase.
  • the mixture is sprayed through the orifice plate at a certain flow rate to form a first-stage crude milk; the effluent is further connected to the splitting port, and the second portion of the water phase sprayed through the jet orifice at a certain flow rate collides and mixes, and the mixture is further mixed
  • the orifice plate is sprayed at a certain flow rate to form a secondary coarse emulsion; the sprayed material is further connected to the splitting port, and the third portion of the aqueous phase sprayed through the jet orifice at a certain flow velocity collides and mixes, and the mixture is passed through the orifice plate.
  • Spraying at a certain flow rate to form a three-stage crude milk the effluent is again connected to the splitting port, and the fourth part of the water phase sprayed through the jet orifice at a certain flow rate collides and mixes, and the mixture is sprayed through the orifice plate at a certain flow rate.
  • the effluent is further connected to the splitting port, and the fifth part of the water phase sprayed through the jet hole at a certain flow rate collides and mixes, and the mixture is sprayed through the orifice plate at a certain flow rate to form five Grade coarse milk.
  • the effluent is finally sprayed through the fine orifice plate from the jet orifice at a certain flow rate to complete the emulsification process.
  • the latex matrix enters the static sensitizer, and the sensitizer enters the colloidal cavity at a speed of not less than lm/s through the sensitizer feed port under the action of the first-stage inner sensitizer ejection port.
  • the first stage of the multi-well plate is mixed with the sensitizer, Then, it is mixed through the second stage, the third stage, and the like.
  • the static concentrate is passed through the last stage of the static sensitizer, and after completion, it enters the injection tube of the heat sealing machine, or directly enters the common injection tube without passing through the static essence.
  • the injection tube is wrapped in a tubular film to achieve uniform filling of the material in the tubular film. It is best (or not necessary) to fill the medicine roll.
  • the cloth roll mechanism is S-shaped on the buffer adjustment machine.
  • Each punching machine installed on the rotating platform of the punching machine rotates the medicine roll with the platform, and sequentially seals, cuts and throws the plastic medicine roll (other general punching and sealing machine can also be used).
  • the drug roll then enters the cooling water for cooling. After cooling is completed, it is packed and stored in storage.
  • Example 1 The oil phase from the oil phase tank is entered into the first-stage coarse milk mixer by the oil phase pump according to the full proportion of the explosive; the water phase self-water phase tank is replaced by the water phase pump according to the explosive ratio, and the multi-stage splitting is entered into the multi-stage coarse multiple times. Milk mixer; emulsification is completed by the final grade of the coarse blender. The latex matrix density was measured to be 1.37 g/cm 3 . After emulsification, the latex matrix enters the static sensitizer, and the sensitizer enters the sensitizer feed port at a rate of not less than 3 m/s through the sensitizer feed port at a rate of 0.3%.
  • the latex matrix is mixed with the sensitizer through the first-stage porous plate, and then mixed through the second-stage, third-stage, and the like.
  • the sensitization temperature was 80 ° C
  • the explosive density was measured to be 1.07 g/cm 3 .
  • the injection tube is wrapped in a tubular film, and the material is uniformly filled in the tubular film by controlling the heat sealing machine.
  • the filled medicine roll is S-shaped on the buffer adjustment machine through the cloth winding mechanism.
  • Each punching machine installed on the rotating platform of the punching machine rotates the medicine roll with the platform, and sequentially seals, cuts and throws the plastic medicine roll.
  • the drug roll then enters the cooling water for cooling. After the cooling is completed, it is packed through the conveyor belt, and then stored in the warehouse. At this time, the density of the medicine roll is: 1.10g/cm 3 , and the medicine temperature is 25 °C.
  • Example 2 The oil phase from the oil phase tank is entered into the first-stage coarse milk mixer by the oil phase pump according to the full proportion of the explosive; the water phase self-water phase tank is replaced by the water phase pump according to the explosive ratio, and the multi-stage splitting is used to enter the multi-stage coarse multiple times.
  • the milk blender after the final stage of the coarse milk blender, the crude milk was completed, at which time the substrate density was 1.35 g/cm 3 .
  • the crude matrix enters the static sensitizer, and the sensitizer enters the sensitizer feed port at a rate of not less than 3 m/s through the sensitizer feed port at a rate of 0.3%.
  • the crude milk matrix is mixed with the sensitizer through the first-stage porous plate, and then mixed through the second-stage, third-stage, and the like.
  • the static concentrate was subjected to the last stage of the perforated plate of the static sensitizer, and the density was measured to be 1.08 g/cm 3 .
  • the injection tube is wrapped in a tubular film, and the material is uniformly filled in the tubular film by controlling the heat sealing machine.
  • the filled medicine roll is S-shaped on the buffer adjustment machine through the cloth winding mechanism.
  • Each punching machine installed on the rotating platform of the punching machine rotates the medicine roll with the platform, and sequentially seals, cuts and throws the plastic medicine roll.
  • the drug roll then enters the cooling water for cooling. After the cooling is completed, it is packed through the conveyor belt, and then stored in the warehouse. At this time, the density of the medicine roll is: 1. lOg/cm 3 , and the medicine temperature is 25 ° C.
  • Example 3 The oil phase from the oil phase tank is entered into the first-stage crude milk mixer by the oil phase pump according to the full proportion of the explosive; the water phase self-water phase tank is replaced by the water phase pump according to the proportion of the explosive, and the multi-stage splitting is used to enter the multi-stage coarse multiple times.
  • Milk mixer after the last stage of the coarse milk mixer, it is finished In the form of a crude milk, the substrate density was 1.35 g/cm 3 at this time.
  • the crude matrix enters the static sensitizer, and the sensitizer enters the emulsification cavity at a rate of not less than 3 m/s through the sensitizer feed port at a dose of 0.3%, and then is mixed by a static mixer to detect the density.
  • the injection tube of the heat sealing machine When finished, enter the injection tube of the heat sealing machine.
  • the injection tube is wrapped in a tubular film, and the material is uniformly filled in the tubular film by controlling the heat sealing machine.
  • the filled medicine roll is S-shaped on the buffer adjustment machine through the cloth winding mechanism.
  • Each punching machine installed on the rotating platform of the punching machine rotates the medicine roll with the platform, and sequentially seals, cuts and throws the plastic medicine roll.
  • the drug roll then enters the cooling water for cooling. After the cooling is completed, it is packed through the conveyor belt, and then stored in the warehouse. At this time, the density of the medicine roll is: 1.10g/cm 3 and the medicine temperature is 25 °C.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Colloid Chemistry (AREA)

Abstract

一种乳化炸药静态乳化敏化无装药泵的生产方法，水、油相进入静态乳化器中进行乳化后，乳胶基质进入静态敏化器；敏化剂通过敏化剂进料口进入静态敏化器，乳胶基质和敏化剂在静态敏化器中混合，敏化后药体直接进入到注药管中进行装药工序。采用静态乳化器与静态敏化器将传统的一次混合改进为多次混合，大大减少了存药量，生产过程无机械搅拌剪切乳化，同时取消了机械混拌式的敏化方式，进行全静态的高温敏化，提高了敏化工序的安全性。取消了传统生产线的灌装泵，敏化后直接进入注药管，减少了生产过程中的危险点和在线存药量，实现了制药、装药的本质安全。

Description

一种静态乳化敏化无装药泵的乳化炸药连续生产方法 技术领域：
本发明涉及乳化炸药生产领域，具体涉及一种乳化炸药静态乳化敏化无装药泵的连续生产 方法。
发明背景：
近年来连续发生的乳化炸药生产线爆炸， 究其原因都与生产设备的机械运动有关， 因此研 制全静态乳化敏化第二代乳化炸药生产线， 以静态分散替代动态乳化； 以静态分散替代动态 敏化， 以无装药泵代替有装药泵， 淘汰落后的、 安全隐患明显的现有第一代生产线， 对于大 幅提高生产本质安全水平， 减少甚至避免爆炸发生具有十分重大意义。
发明内容- 本发明旨在提供一种乳化炸药静态乳化敏化无装药泵的生产方法，以达到乳化炸药生产过 程中的本质安全。
本发明通过以下的技术方案 （见附图 1 ) 实现，
一种乳化炸药静态乳化敏化无装药泵的连续生产方法：在乳化敏化工序，采用的是静态乳 化与静态敏化的连续生产方法， 其中静态乳化器、 静态敏化器为静态混合器、 孔板、 射流、 文丘里管方式中至少一种； 乳化敏化装置与注药管直接连接， 乳化敏化后由敏化直接进入装 药工序完成装药。
静态乳化器包含油相进口、水相进口、 外壳和内芯， 外壳内壁设有分流口， 内芯由喷射口 和孔板构成。 每个内芯分别对应一个分流口， 水相从各个分流口进入对应的内芯。 内芯的喷 射口设置在内芯的管壁上， 孔板设置在内芯的管尾， 水相由分流口再经喷射口进入内芯， 与 经油相进口进入内芯的油相混合乳化，再经孔板进入下一个内芯。内芯为 3个以上，优选为 5 个。
静态敏化器包括外壳、 敏化剂加料口、 内芯、 多孔板。 内芯为 1个以上， 优选为 3个， 静 态敏化器的敏化方式为， 敏化剂通过敏化剂加料口后， 在第一级内芯上的敏化剂喷射口作用 下， 进入胶体腔体中， 乳胶基质通过第一级多孔板时与敏化剂相混合， 之后经过第二级， 第 三级等多孔板进行混匀。 多孔板的小孔， 可以为圆形、 方形、 锥形和 /或花瓣形。
静态乳化敏化方式，还可以为静态初乳加静态敏化加静态精乳，静态敏化与静态精乳为同 一设备。
油相自油相罐由油相泵按炸药全比例进入一级粗乳混合器；水相自水相罐由水相泵按炸药 比例， 通过多级分流分多次进入多级粗乳混合器； 经最后一级粗乳混合器， 便完成乳化。 乳 化之后乳胶基质进入静态敏化器， 同时敏化剂进入静态敏化器， 完成敏化。 之后药体进入到 注药管中。 注药管被包裹于筒状薄膜中， 由安全的原料泵而非危险的胶体泵或炸药泵， 实现 物料在筒状薄膜中均匀灌装。 灌装好的药卷封口后进入冷却水中进行冷却。 冷却完成后经过 输送皮带进行装箱， 之后入库储存。
本发明无需机械搅拌剪切和胶体 /炸药泵送装置， 通过多级粗乳混合器将水相通过流量 调节的控制分多次同油相混合，使油相每次和较少量的水相能充分混合，经过多次水相添加， 最终和全部的油相实现低压条件下均匀的混合， 得到颗粒约 1微米的胶体基质。 由于该方法 设备将水相按所需比例分次同油相混合， 将传统的一次混合改进为多次混合， 大大减少了存 药量， 无机械搅拌剪切乳化。 同时取消了机械混拌式的敏化方式， 进行全静态的高温敏化， 提高了敏化工序的安全性。 如此， 还取消了传统生产线的灌装泵， 而直接进入注药管， 减少 了生产过程中的危险点， 和在线存药量， 实现了制药、 装药的本质安全。
附图说明：
1. 附图 1为本发明所介绍方法的工艺流程图
2. 附图 2为本发明所介绍的一种静态乳化器
1： 油相口 2: 水相口 3 ;外壳 4: 内芯 5出口
3. 附图 3为本发明所介绍的一种静态敏化器
1： 进料口 2: 敏化剂加料口 3: 出料口 （精乳孔板） 4: 内芯 5: 外壳
4. 附图 4为本发明所介绍的一种静态乳化敏化组合图
1： 静态乳化器 2: 静态敏化器 （可带静态精乳）
具体实施方式：
如附图 2所示 5级乳化设备， 进行 5级乳化； 全比例油相自静态乳化器起始端进入， 部分 水相自侧向自分流口， 以一定流速由射流孔喷出， 撞击油相， 其混合物再经孔板， 以一定流 速喷出， 形成一级粗乳； 喷出物再与分流口来， 并经射流孔以一定流速喷出的第二部分水相 碰撞混合， 此混合物再经孔板， 以一定流速喷出， 形成二级粗乳； 喷出物再与分流口来， 并 经射流孔以一定流速喷出的第三部分水相碰撞混合， 此混合物再经孔板， 以一定流速喷出， 形成三级粗乳； 喷出物再与分流口来， 并经射流孔以一定流速喷出的第四部分水相碰撞混合， 此混合物再经孔板， 以一定流速喷出， 形成四级粗乳； 喷出物再与分流口来， 并经射流孔以 一定流速喷出的第五部分水相碰撞混合， 此混合物再经孔板， 以一定流速喷出， 形成五级粗 乳。 喷出物最后经精乳孔板， 由射流孔， 以一定流速喷出， 完成乳化过程。
之后乳胶基质进入静态敏化器，同时敏化剂通过敏化剂加料口在第一级内芯上敏化剂喷射 口作用下， 以不低于 lm/s的速度进入胶体腔中， 基质通过第一级多孔板时与敏化剂相混合， 之后经过第二级， 第三级等多孔板进行混匀。 混合完成之后， 通过静态敏化器最后一级多孔 板进行静态精乳， 完成后， 进入到热合机的注药管中， 或者不经过静态精乳， 直接进入到常 用的注药管中。 注药管被包裹于筒状薄膜中， 实现物料在筒状薄膜中均匀灌装。 灌装好的药 卷最好 （也可不进行该步骤） 经布卷机构呈 S型布在缓存调节机上。 安装在打卡机旋转平台 上的各打卡机随平台转动牵引药卷， 并依次完成塑料药卷的封口、 切断和抛卷 （也可采用其 他通用打卡封口机）。 之后药卷进入冷却水中进行冷却。 冷却完成后装箱， 入库储存。
为了更好的解释本发明， 下面通过具体实施例对本发明进行详细举例说明。
实例一： 油相自油相罐由油相泵按炸药全比例进入一级粗乳混合器； 水相自水相罐由水 相泵按炸药比例， 通过多级分流分多次进入多级粗乳混合器； 经最后一级粗乳混合器， 便完 成乳化。 检测乳胶基质密度为 1.37g/cm3。 乳化之后乳胶基质进入静态敏化器， 同时敏化剂 按照 0.3%的用量通过敏化剂加料口在第一级内芯上敏化剂喷射口作用下， 以不低于 3m/s的 速度进入乳化腔体中， 乳胶基质通过第一级多孔板时与敏化剂相混合， 之后经过第二级， 第 三级等多孔板进行混匀。 敏化温度为 80°C之后， 检测炸药密度为 1.07g/cm3。 进入到热合机 的注药管中。注药管被包裹于筒状薄膜中， 通过对热合机的控制以实现物料在筒状薄膜中均 匀灌装。灌装好的药卷经布卷机构呈 S型布在缓存调节机上。安装在打卡机旋转平台上的各 打卡机随平台转动牵引药卷， 并依次完成塑料药卷的封口、切断和抛卷。之后药卷进入冷却 水中进行冷却。 冷却完成后经过输送皮带进行装箱， 之后入库储存， 此时药卷密度为： 1. 10g/cm3, 药温为 25°C。
实例二： 油相自油相罐由油相泵按炸药全比例进入一级粗乳混合器；水相自水相罐由水 相泵按炸药比例， 通过多级分流分多次进入多级粗乳混合器； 经最后一级粗乳混合器， 便完 成粗乳，此时基质密度为 1.35g/cm3。 之后粗乳基质进入静态敏化器， 同时敏化剂按照 0.3%的 用量通过敏化剂加料口在第一级内芯上敏化剂喷射口作用下，以不低于 3m/s的速度进入乳化 腔体中， 粗乳基质通过第一级多孔板时与敏化剂相混合， 之后经过第二级， 第三级等多孔板 进行混匀。 混合完成之后， 通过静态敏化器最后一级多孔板进行静态精乳， 检测密度为 1.08g/cm3。 完成后， 进入到热合机的注药管中。 注药管被包裹于筒状薄膜中， 通过对热合机 的控制以实现物料在筒状薄膜中均匀灌装。 灌装好的药卷经布卷机构呈 S型布在缓存调节机 上。安装在打卡机旋转平台上的各打卡机随平台转动牵引药卷， 并依次完成塑料药卷的封口、 切断和抛卷。 之后药卷进入冷却水中进行冷却。 冷却完成后经过输送皮带进行装箱， 之后入 库储存，此时药卷密度为： 1. lOg/cm3,药温为 25°C。
实例三： 油相自油相罐由油相泵按炸药全比例进入一级粗乳混合器；水相自水相罐由水 相泵按炸药比例， 通过多级分流分多次进入多级粗乳混合器； 经最后一级粗乳混合器， 便完 成粗乳，此时基质密度为 1.35g/cm3。 之后粗乳基质进入静态敏化器， 同时敏化剂按照 0.3%的 用量通过敏化剂加料口， 以不低于 3m/s的速度进入乳化腔体中， 再通过静态混合器混合， 检 测密度为 1.20g/cm3。 完成后， 进入到热合机的注药管中。 注药管被包裹于筒状薄膜中， 通过 对热合机的控制以实现物料在筒状薄膜中均匀灌装。 灌装好的药卷经布卷机构呈 S型布在缓 存调节机上。 安装在打卡机旋转平台上的各打卡机随平台转动牵引药卷， 并依次完成塑料药 卷的封口、 切断和抛卷。 之后药卷进入冷却水中进行冷却。 冷却完成后经过输送皮带进行装 箱， 之后入库储存，此时药卷密度为： 1. 10g/cm3，药温为 25°C。
显然， 上述实施例仅仅是为清楚地说明所作的举例， 而并非对实施方式的限定。 对于所 属领域的普通技术人员来说， 在上述说明的基础上还可以做出其它不同形式的变化或变动。 这里无需也无法对所有的实施方式予以穷举。 而由此所引伸出的显而易见的变化或变动仍处 于本发明创造的保护范围之中。

Claims

1、 一种乳化炸药静态乳化敏化无装药泵的连续生产方法， 包括乳化， 敏化， 装药， 其 特征在于：
( 1 )在乳化敏化工序， 采用的是静态乳化与静态敏化的连续生产方法， 其中静态乳化 器、 静态敏化器为静态混合器、 孔板、 射流、 文丘里管方式中至少一种；
( 2 ) 乳化敏化后由敏化直接进入装药工序完成装药。
2、 根据权利要求 1所述的乳化炸药静态乳化敏化无装药泵的连续生产方法， 其特征在 于， 所述的静态乳化器包含油相进口、 水相进口、 外壳和内芯， 外壳内壁设有分流口， 内芯 由喷射口和孔板构成。
3、 根据权利要求 2所述的乳化炸药静态乳化敏化无装药泵的连续生产方法， 其特征在 于， 所述内芯分别对应一个分流口， 水相从各个分流口进入对应的内芯。
4、 根据权利要求 2所述的乳化炸药静态乳化敏化无装药泵的连续生产方法， 其特征在 于， 所述内芯的喷射口设置在内芯的管壁上， 孔板设置在内芯的管尾， 水相由分流口再经喷 射口进入内芯， 与经油相进口进入内芯的油相混合乳化， 再经孔板进入下一个内芯。
5、 根据权利要求 2或 3所述的乳化炸药静态乳化敏化无装药泵的连续生产方法， 其特 征在于， 所述的静态乳化器内芯为 3个以上， 优选为 5个。
6、 根据权利要求 1所述的乳化炸药静态乳化敏化无装药泵的连续生产方法， 其特征在 于， 所述静态敏化器包括外壳、 敏化剂加料口、 内芯、 多孔板。
7、 根据权利要求 6所述的乳化炸药静态乳化敏化无装药泵的连续生产方法， 其特征在 于， 所述内芯为 1个以上， 优选为 3个， 静态敏化器的敏化方式为， 敏化剂通过敏化剂加料 口后， 在第一级内芯上的敏化剂喷射口作用下， 进入内芯中， 乳胶基质通过第一级多孔板时 与敏化剂相混合， 之后经过第二级， 第三级等多孔板进行混匀。
8、 根据权利要求 7所述的乳化炸药静态乳化敏化无装药泵的连续生产方法， 其特征在 于， 静态敏化器的多孔板的小孔， 可以为圆形、 方形、 锥形和 /或花瓣形。
9、 根据权利要求 1所述的乳化炸药静态乳化敏化无装药泵的连续生产方法， 其特征在 于， 静态乳化敏化方式， 还可以为静态初乳加静态敏化加静态精乳， 静态敏化与静态精乳为 同一设备。
10、根据权利要求 1所述的乳化炸药静态乳化敏化无装药泵的连续生产方法， 其特征在 于， 乳化敏化装置与注药管直接连接。
PCT/CN2014/080735 2014-06-25 2014-06-25 一种静态乳化敏化无装药泵的乳化炸药连续生产方法 WO2015196390A1 (zh)

Priority Applications (4)

Application Number Priority Date Filing Date Title
AU2014399172A AU2014399172B2 (en) 2014-06-25 2014-06-25 Method for continuously producing emulsion explosive without charge pump by means of emulsification and sensitization in static state
US15/322,289 US10759718B2 (en) 2014-06-25 2014-06-25 Method for continuously producing emulsion explosive by emulsification and sensitization in a static state without a loading pump
EP14895829.1A EP3162785B1 (en) 2014-06-25 2014-06-25 Method for continuously producing emulsion explosive without charge pump by means of emulsification and sensitization in static state
PCT/CN2014/080735 WO2015196390A1 (zh) 2014-06-25 2014-06-25 一种静态乳化敏化无装药泵的乳化炸药连续生产方法

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PCT/CN2014/080735 WO2015196390A1 (zh) 2014-06-25 2014-06-25 一种静态乳化敏化无装药泵的乳化炸药连续生产方法

Publications (1)

Publication Number Publication Date
WO2015196390A1 true WO2015196390A1 (zh) 2015-12-30

Family

ID=54936459

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/CN2014/080735 WO2015196390A1 (zh) 2014-06-25 2014-06-25 一种静态乳化敏化无装药泵的乳化炸药连续生产方法

Country Status (4)

Country Link
US (1) US10759718B2 (zh)
EP (1) EP3162785B1 (zh)
AU (1) AU2014399172B2 (zh)
WO (1) WO2015196390A1 (zh)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107382638A (zh) * 2017-08-28 2017-11-24 福建省民爆化工股份有限公司 乳化炸药的静态敏化技术方法和装置
CN106748588B (zh) * 2017-03-03 2019-02-26 马鞍山江南化工有限责任公司 乳化炸药废药再利用的处理装置、处理系统及其处理方法
CN110183288A (zh) * 2019-06-16 2019-08-30 保利民爆哈密有限公司 一种现场混装炸药装药车
CN110436205A (zh) * 2019-06-26 2019-11-12 新疆天河化工有限公司 大直径乳化炸药输送装置及其制备方法
CN114230421A (zh) * 2021-12-20 2022-03-25 安徽瑞思迪恩科技有限公司 一种乳化炸药的非电全静态生产工艺

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10226745B2 (en) 2014-10-16 2019-03-12 Shijiazhuang Success Machinery Electrical Co., Ltd. Emulsion matrix ground station with intrinsic safety
CN107941103B (zh) * 2017-05-27 2023-04-28 湖北凯龙化工集团股份有限公司 一种循环式震源药柱自动装药生产线
CN112521238B (zh) * 2020-11-19 2022-11-18 安徽江南化工股份有限公司 一种高稳定胶状乳化炸药及其制备方法
CN112745177A (zh) * 2020-12-31 2021-05-04 湖南雷鸣西部民爆有限公司 一种深孔爆破乳化炸药的敏化方法
CN114591121B (zh) * 2022-03-15 2022-11-15 广东华威化工股份有限公司 一种基于近红外光谱的乳化炸药制备方法及系统
CN115259973A (zh) * 2022-08-03 2022-11-01 湖北东神天神实业有限公司 一种膏状乳化基质的敏化装置及方法

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102850149A (zh) * 2012-08-13 2013-01-02 湖北凯龙化工集团股份有限公司 静态乳化泵送乳胶基质在线连续敏化乳化炸药制造工艺
CN103304348A (zh) * 2013-07-05 2013-09-18 石家庄成功机电有限公司 一种包装乳化炸药的静态敏化方法及设备
CN103664424A (zh) * 2013-09-26 2014-03-26 石家庄成功机电有限公司 一种乳化炸药的乳化方法及设备
CN104109057A (zh) * 2014-06-25 2014-10-22 石家庄成功机电有限公司 一种静态乳化敏化无装药泵的乳化炸药连续生产方法

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4491489A (en) * 1982-11-17 1985-01-01 Aeci Limited Method and means for making an explosive in the form of an emulsion
US5346564A (en) * 1993-06-16 1994-09-13 Nelson Brothers, Inc. Method of safely preparing an explosive emulsion composition
CN203598760U (zh) 2013-09-26 2014-05-21 石家庄成功机电有限公司 一种制备乳化炸药乳胶基质的设备

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102850149A (zh) * 2012-08-13 2013-01-02 湖北凯龙化工集团股份有限公司 静态乳化泵送乳胶基质在线连续敏化乳化炸药制造工艺
CN103304348A (zh) * 2013-07-05 2013-09-18 石家庄成功机电有限公司 一种包装乳化炸药的静态敏化方法及设备
CN103664424A (zh) * 2013-09-26 2014-03-26 石家庄成功机电有限公司 一种乳化炸药的乳化方法及设备
CN104109057A (zh) * 2014-06-25 2014-10-22 石家庄成功机电有限公司 一种静态乳化敏化无装药泵的乳化炸药连续生产方法

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106748588B (zh) * 2017-03-03 2019-02-26 马鞍山江南化工有限责任公司 乳化炸药废药再利用的处理装置、处理系统及其处理方法
CN107382638A (zh) * 2017-08-28 2017-11-24 福建省民爆化工股份有限公司 乳化炸药的静态敏化技术方法和装置
CN110183288A (zh) * 2019-06-16 2019-08-30 保利民爆哈密有限公司 一种现场混装炸药装药车
CN110183288B (zh) * 2019-06-16 2024-03-01 保利民爆哈密有限公司 一种现场混装炸药装药车
CN110436205A (zh) * 2019-06-26 2019-11-12 新疆天河化工有限公司 大直径乳化炸药输送装置及其制备方法
CN114230421A (zh) * 2021-12-20 2022-03-25 安徽瑞思迪恩科技有限公司 一种乳化炸药的非电全静态生产工艺

Also Published As

Publication number Publication date
AU2014399172B2 (en) 2018-03-15
EP3162785A4 (en) 2018-02-07
AU2014399172A1 (en) 2017-01-12
US20170129824A1 (en) 2017-05-11
US10759718B2 (en) 2020-09-01
EP3162785B1 (en) 2020-05-13
EP3162785A1 (en) 2017-05-03

Similar Documents

Publication Publication Date Title
WO2015196390A1 (zh) 一种静态乳化敏化无装药泵的乳化炸药连续生产方法
EP1819429B1 (en) Dry polymer hydration apparatus and methods of use
WO2016045078A1 (zh) 本安型乳化炸药现场装药车
US10610838B2 (en) Method and device for emulsifying emulsion explosive
CN104109057B (zh) 一种静态乳化敏化无装药泵的乳化炸药连续生产方法
CN104315933B (zh) 本安型乳化炸药现场装药车
CA2807857C (en) Process for the production of intermediate emulsions for use in emulsion explosives
US20240122808A1 (en) Coaxial nozzle configuration and methods thereof
CN104803814A (zh) 一种中温敏化的乳化炸药及其制备方法
CN102976872A (zh) 一种安全制备乳胶基质的乳化装置及其方法
CN106313324B (zh) 一种用于制备泡沫水泥浆的装置
EP2817087B1 (en) Installation and process for preparing a water/diesel fuel emulsion
RU104551U1 (ru) Технологическая линия изготовления эмульсионного взрывчатого вещества типа "вода в масле"
AU2014409009B2 (en) Ground station for intrinsic safety-type latex matrix
AU2013251106B2 (en) Method for emulsion treatment
CN206762071U (zh) 一种压缩氮气泡沫混合器
CN110436205A (zh) 大直径乳化炸药输送装置及其制备方法
CN107382638A (zh) 乳化炸药的静态敏化技术方法和装置
CN102010276A (zh) 气动喷雾细化制备微球低感hmx工艺
RU137877U1 (ru) Пеногенератор эжекционного типа
CN113636900A (zh) 一种乳化炸药静态敏化装置及方法
RU90789U1 (ru) Линия изготовления обратных водомасляных эмульсий
EP0022442B1 (en) Method and apparatus for preparing emulsions
CN210786929U (zh) 一种高端制剂微包被模块
JPH07228783A (ja) 高濃度アスファルト水乳化物の製造方法

Legal Events

Date Code Title Description
121 Ep: the epo has been informed by wipo that ep was designated in this application

Ref document number: 14895829

Country of ref document: EP

Kind code of ref document: A1

NENP Non-entry into the national phase

Ref country code: DE

WWE Wipo information: entry into national phase

Ref document number: 15322289

Country of ref document: US

ENP Entry into the national phase

Ref document number: 2014399172

Country of ref document: AU

Date of ref document: 20140625

Kind code of ref document: A

REEP Request for entry into the european phase

Ref document number: 2014895829

Country of ref document: EP

WWE Wipo information: entry into national phase

Ref document number: 2014895829

Country of ref document: EP