WO2015022699A1 - An improved novel process to reduce anti-nutritional agents in de-oiled cake of cotton seed meal/castor seed meal or any oil seeds meal/biomass thereof - Google Patents
An improved novel process to reduce anti-nutritional agents in de-oiled cake of cotton seed meal/castor seed meal or any oil seeds meal/biomass thereof Download PDFInfo
- Publication number
- WO2015022699A1 WO2015022699A1 PCT/IN2014/000513 IN2014000513W WO2015022699A1 WO 2015022699 A1 WO2015022699 A1 WO 2015022699A1 IN 2014000513 W IN2014000513 W IN 2014000513W WO 2015022699 A1 WO2015022699 A1 WO 2015022699A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- meal
- solventized
- toasted
- oiled
- dried
- Prior art date
Links
- 235000012054 meals Nutrition 0.000 title claims abstract description 35
- 238000000034 method Methods 0.000 title claims description 19
- 230000000433 anti-nutritional effect Effects 0.000 title claims description 11
- 239000002028 Biomass Substances 0.000 title claims description 8
- 239000003795 chemical substances by application Substances 0.000 title claims description 4
- 229920000742 Cotton Polymers 0.000 title description 4
- 235000004443 Ricinus communis Nutrition 0.000 title description 3
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 claims abstract description 46
- 239000000463 material Substances 0.000 claims abstract description 28
- 235000012343 cottonseed oil Nutrition 0.000 claims abstract description 16
- 241001465754 Metazoa Species 0.000 claims abstract description 14
- 235000004977 Brassica sinapistrum Nutrition 0.000 claims abstract description 13
- 235000015097 nutrients Nutrition 0.000 claims abstract description 13
- 240000002791 Brassica napus Species 0.000 claims abstract description 11
- 238000011282 treatment Methods 0.000 claims abstract description 11
- 229910001854 alkali hydroxide Inorganic materials 0.000 claims abstract description 8
- 150000008044 alkali metal hydroxides Chemical class 0.000 claims abstract description 8
- 239000000654 additive Substances 0.000 claims abstract description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 7
- 150000001875 compounds Chemical class 0.000 claims abstract description 6
- 238000013019 agitation Methods 0.000 claims abstract description 5
- 238000001035 drying Methods 0.000 claims abstract description 5
- 238000010411 cooking Methods 0.000 claims abstract description 4
- 244000144977 poultry Species 0.000 claims abstract description 4
- 239000002002 slurry Substances 0.000 claims abstract description 4
- 159000000000 sodium salts Chemical class 0.000 claims abstract description 4
- 238000000638 solvent extraction Methods 0.000 claims abstract description 4
- 239000000470 constituent Substances 0.000 claims description 7
- 150000001720 carbohydrates Chemical class 0.000 claims description 6
- 235000019198 oils Nutrition 0.000 claims description 6
- 239000002585 base Substances 0.000 claims description 5
- 235000014633 carbohydrates Nutrition 0.000 claims description 5
- 239000004615 ingredient Substances 0.000 claims description 5
- 239000003513 alkali Substances 0.000 claims description 4
- 238000006243 chemical reaction Methods 0.000 claims description 4
- 230000007062 hydrolysis Effects 0.000 claims description 4
- 238000006460 hydrolysis reaction Methods 0.000 claims description 4
- 150000001413 amino acids Chemical class 0.000 claims description 3
- 102000004196 processed proteins & peptides Human genes 0.000 claims description 3
- 108090000765 processed proteins & peptides Proteins 0.000 claims description 3
- 235000019779 Rapeseed Meal Nutrition 0.000 claims description 2
- 150000004679 hydroxides Chemical class 0.000 claims description 2
- 239000004456 rapeseed meal Substances 0.000 claims description 2
- 239000000344 soap Substances 0.000 claims description 2
- 239000000835 fiber Substances 0.000 claims 1
- 230000007065 protein hydrolysis Effects 0.000 claims 1
- 102000004169 proteins and genes Human genes 0.000 claims 1
- 108090000623 proteins and genes Proteins 0.000 claims 1
- 239000003921 oil Substances 0.000 description 5
- QBKSWRVVCFFDOT-UHFFFAOYSA-N gossypol Chemical compound CC(C)C1=C(O)C(O)=C(C=O)C2=C(O)C(C=3C(O)=C4C(C=O)=C(O)C(O)=C(C4=CC=3C)C(C)C)=C(C)C=C21 QBKSWRVVCFFDOT-UHFFFAOYSA-N 0.000 description 4
- 235000008935 nutritious Nutrition 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- 244000188595 Brassica sinapistrum Species 0.000 description 2
- QHOPXUFELLHKAS-UHFFFAOYSA-N Thespesin Natural products CC(C)c1c(O)c(O)c2C(O)Oc3c(c(C)cc1c23)-c1c2OC(O)c3c(O)c(O)c(C(C)C)c(cc1C)c23 QHOPXUFELLHKAS-UHFFFAOYSA-N 0.000 description 2
- 235000014113 dietary fatty acids Nutrition 0.000 description 2
- 229930195729 fatty acid Natural products 0.000 description 2
- 239000000194 fatty acid Substances 0.000 description 2
- 150000004665 fatty acids Chemical class 0.000 description 2
- 229930000755 gossypol Natural products 0.000 description 2
- 229950005277 gossypol Drugs 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 229930195730 Aflatoxin Natural products 0.000 description 1
- 235000019750 Crude protein Nutrition 0.000 description 1
- 230000003213 activating effect Effects 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 239000005409 aflatoxin Substances 0.000 description 1
- 239000013566 allergen Substances 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 239000006184 cosolvent Substances 0.000 description 1
- 230000009849 deactivation Effects 0.000 description 1
- 235000019621 digestibility Nutrition 0.000 description 1
- 239000008157 edible vegetable oil Substances 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
- 239000002657 fibrous material Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 125000004383 glucosinolate group Chemical group 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 230000003050 macronutrient Effects 0.000 description 1
- 235000021073 macronutrients Nutrition 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 235000013369 micronutrients Nutrition 0.000 description 1
- 238000003801 milling Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 239000004465 oilseed meal Substances 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 235000005985 organic acids Nutrition 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000000575 pesticide Substances 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000003053 toxin Substances 0.000 description 1
- 231100000765 toxin Toxicity 0.000 description 1
- 230000009261 transgenic effect Effects 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K50/00—Feeding-stuffs specially adapted for particular animals
- A23K50/80—Feeding-stuffs specially adapted for particular animals for aquatic animals, e.g. fish, crustaceans or molluscs
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K10/00—Animal feeding-stuffs
- A23K10/30—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms
- A23K10/37—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms from waste material
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K40/00—Shaping or working-up of animal feeding-stuffs
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K50/00—Feeding-stuffs specially adapted for particular animals
- A23K50/70—Feeding-stuffs specially adapted for particular animals for birds
- A23K50/75—Feeding-stuffs specially adapted for particular animals for birds for poultry
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
- Y02A40/80—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in fisheries management
- Y02A40/81—Aquaculture, e.g. of fish
- Y02A40/818—Alternative feeds for fish, e.g. in aquacultures
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P60/00—Technologies relating to agriculture, livestock or agroalimentary industries
- Y02P60/80—Food processing, e.g. use of renewable energies or variable speed drives in handling, conveying or stacking
- Y02P60/87—Re-use of by-products of food processing for fodder production
Definitions
- the present invention is to produce Cottonseed/ Rapeseed/ Castorseed/any kind of vegetable oilseed meal (oiled or de-oiled) or Biomass or in combination thereof to improve or modify the availability of valuable constituents and nutrients, detoxify by deactivating the anti-nutritional factors, and thereby improving their availability in a easily digestible or in dis-integrated form as an easy consumable and hence the applicability of said cake (oiled or de-oiled wetted with hexane or without wetted with hexane) for improving the health and productivity of animals, aqua etc and after application.
- This invention relates to a highly nutritious, easy digestible feed product/ingredients which is highly essential feeding product/ingredients required for feeding animals and poultry as the growing demands increases day by day for improving the quality and time bound weight development ,an essential requirement in the animal husbandry industry.
- novel and inventive feed product/ingredients which is easily digestible and high energetic as well as high nutritious compositions, which also provides instant energy for to the end users, as the invented process demonstrates and putting more efforts for breaking the high molecular
- the product also provides more bioavailability to the end users, and internal nourishing components of cotton seed meal, rape seed meal or castormeal or biomass or in combinations thereof having de-oiled cakes with or without solvent extraction of using normal hexane.
- the object of the present invention which enhances the bio- availability of these ingredients effectively and gives full energy source of conversion and ultimately an all- round growth and health.
- Further object of the present invention is that, it is essential to break down and/ or deactivate an anti-nutritional factors like Gossypol / Glucocinates / Resinins/ allergens components / and all its derivaties.
- the feed product can be effectively utilised by the end user without any wastage , but instantly releases of energy due to deactivation of anti-nutritional values of the de-oiled meal.
- the present invention pertains to improve or modify the availability of valuable constituents and nutrients, same time detoxify and deactivate the anti-nutritional factors, and thereby improving their availability in a easily digestible or in dis-integrated form as an easy consumable and hence the applicability of said eake/meai (oiied or de-oiied with hexane or without hexane) for improving the health and productivity of animals,
- the said nutritious feed product comprising a solvent wetted de-oiled meal or direct de-oiled meal will be treated in the desolventization/ toasting equipment which is operating with an central agitator in a single or multiple staged, compartmentalised equipment while intake would be from its top & discharge at its bottom stage with any given rated capacity per hour, prior to this cooking of material would be done as well.
- the agitator speed could be fixed at constant or varying in order to maintain the variable or fixed residence time for the material from inlet to outlet.
- the compartmentalized equipment had single or multiple number of stages where the material passes from top to down through a level controller device fitted either with mechanical or pneumatically system.
- the cake material would go through an indirect steam heating through each compartment's double bottom arrangement at a varying pressure & flow rate as per the required quantity to heat the materials from 40 to 130 degree centigrade temperature
- the de-oiled meal(with or without hexane) material would be treated with alkali metallic hydroxides (week or strong base) at a feed rate of 1kgs to 50 kgs per each ton of cake material besides with or without the sodium salts of soapy slurry material to be added.
- the aqueous solution fed and mixed with the cake would react and break the bonds of all the available amino acids, peptides, crude proteins, saccharides (mono, di, oligo, poly etc.), carbohydrates ,fatty acids, organic acids, vitamins, micro or macro nutrients and fibrous material into individual activative centers and the disintegrated components are be available to the animal at an easy form rather than using its energy & time to break in its gut which may not take place effectively as the above prevailing conditions are not exist.
- the aim of the present invention is to device a multi-objective process for treatment of said Cottonseed cake/ Rapeseed cake/ Castorseed cake / de-oiled meal (with or without hexane) to improve or modify the availability of valuable constituents and nutrients, detoxify and deactivate the anti-nutritional factors, and thereby improving their availability in a easily digestible or in dis-integrated form as an easy consumable and hence the applicability of said cake/meal (oiled or de-oiled with hexane or without hexane) for improving the health and productivity of animals, aqua etc and after application.
- the Cottonseed/ Rapeseed/ Castprseed-cake/meal or other material is obtained from Cottonseed/ Rapeseed/ Castorseed-/ de-oiled cake or oil cake an agricultural sources and is natural or modified (such as but not limited to hybrids, transgenic, genetically modified).
- Cotton seed/ Rapeseed/ Castorseed- cake is subjected to one or more treatments selected from a group but not limited to micronization, pulverization, grinding, crushing , dehulling, flaking, expanding, extrusion, milling, expelling/extraction or suitable combinations thereof: with or without heating and / or wetting; in presence or absence of aqueous, organic, aqueous-organic solvent/s optionally containing an additive/s and / or co-solvent/s.
- the present inventors have developed an unique method of making nutritional feed product comprising the following steps :- a) The grinded de-oiled meal are taken into the single or multi-stage cooking device followed by agitation. b) To the processed meal obtained at step (a) a required quantity of water is been added at a single stage or at all the stages. c) After addition of water, an indirect steam treatment to be introduced in any one of the stage or at all the stages and more number of treatments at different stages as depicted above. d) One can also have de-oiled meal after solvent extraction with hexane and perform the below steps to get the same result without performing steps a,b&c.
- step a-c/d Subjected de-oiled cake/meal of step a-c/d are treated in a DE-SOLVENTIZTION / TOASTER EQUIPMENT in presence of alkali hydroxides/ acides of strong or weak nature, in presence of direct heat and or steam, and thereby producing disintegrated, hydrolyzed, detoxified , de-solventized or dried and toasted Cottonseed/ Rapeseed/ Castorseed/ Rapeseen/ Castorseed de oiled cake or Cottonseed/ Rapeseed/ Castorseed-oil cakes as the case may be.
- step "e” Drying the disintegrated hydrolyzed, detoxified, de-solventized or dried and toasted material obtained to step "e” to obtain dried, de-solventized and toasted cake with improved properties.
- g) Alternatively, fortifying the dried , -de-solventized and toasted cakes with one or more nutrients and energy rich compounds/additives either with or without adding of sodium salts of soapy slurry material and further.
- the present invention pertains to treatment with alkali (weak or stong base) to improve or modify the availability of valuable constituents and nutrients, detoxify and deactivate the anti-nutritional factors, and thereby improving their availability in a easily digestible or in dis-integrated form as an easy consumable and hence the applicability of said cake/meal (oiled or de-oiled with hexane or without hexane) for improving the health and productivity of animals, aqua etc and after application there of which the process established in large commercial scale ;
- alkali weak or stong base
- alkali (weak or strong base) shall have a different concentration varying from 1 to 60% (%w/w),the reaction of hydrolysis takes place while during the toasting / drying temperatures duly maintained at 80 °C to 100 °C in particular and could be varying from 40 °C to 130 °C. Also it is to be noted that the feed rate of quantity of metallic alkali hydroxides would be added at 1 kgs / ton to 50 kg/ton of de-oiled cakes / bio mass with or without addition of soap stock material produced during neutralization of edible oils, same time .
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Polymers & Plastics (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Zoology (AREA)
- Birds (AREA)
- Animal Husbandry (AREA)
- Marine Sciences & Fisheries (AREA)
- Insects & Arthropods (AREA)
- Health & Medical Sciences (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Molecular Biology (AREA)
- Mycology (AREA)
- Physiology (AREA)
- Fodder In General (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
IN2684/MUM/2013 | 2013-08-16 | ||
IN2684MU2013 IN2013MU02684A (enrdf_load_stackoverflow) | 2013-08-16 | 2013-08-16 |
Publications (1)
Publication Number | Publication Date |
---|---|
WO2015022699A1 true WO2015022699A1 (en) | 2015-02-19 |
Family
ID=51871119
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/IN2014/000513 WO2015022699A1 (en) | 2013-08-16 | 2014-08-05 | An improved novel process to reduce anti-nutritional agents in de-oiled cake of cotton seed meal/castor seed meal or any oil seeds meal/biomass thereof |
Country Status (2)
Country | Link |
---|---|
IN (1) | IN2013MU02684A (enrdf_load_stackoverflow) |
WO (1) | WO2015022699A1 (enrdf_load_stackoverflow) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112358912A (zh) * | 2020-09-29 | 2021-02-12 | 新疆希普生物科技股份有限公司 | 一种烘烤棉籽的制备方法及其应用 |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2934431A (en) * | 1957-09-09 | 1960-04-26 | Ranchers Cotton Oil | Process for forming meal from cottonseed edible by animals and poultry |
US2958600A (en) * | 1956-11-23 | 1960-11-01 | Benjamin Clayton | Animal feeds and methods of producing same |
EP0006654A2 (en) * | 1978-06-26 | 1980-01-09 | Unilever N.V. | A process for producing a detoxified rapeseed protein concentrate |
GB1575506A (en) * | 1976-02-06 | 1980-09-24 | Unilever Ltd | Process for the detoxification of rapeseed meal |
-
2013
- 2013-08-16 IN IN2684MU2013 patent/IN2013MU02684A/en unknown
-
2014
- 2014-08-05 WO PCT/IN2014/000513 patent/WO2015022699A1/en active Application Filing
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2958600A (en) * | 1956-11-23 | 1960-11-01 | Benjamin Clayton | Animal feeds and methods of producing same |
US2934431A (en) * | 1957-09-09 | 1960-04-26 | Ranchers Cotton Oil | Process for forming meal from cottonseed edible by animals and poultry |
GB1575506A (en) * | 1976-02-06 | 1980-09-24 | Unilever Ltd | Process for the detoxification of rapeseed meal |
EP0006654A2 (en) * | 1978-06-26 | 1980-01-09 | Unilever N.V. | A process for producing a detoxified rapeseed protein concentrate |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112358912A (zh) * | 2020-09-29 | 2021-02-12 | 新疆希普生物科技股份有限公司 | 一种烘烤棉籽的制备方法及其应用 |
Also Published As
Publication number | Publication date |
---|---|
IN2013MU02684A (enrdf_load_stackoverflow) | 2015-06-19 |
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