WO2015005535A1 - Method for manufacturing weakly acidic natural dietary fiber jelly sponge for face washing and bathing, and weakly acidic natural dietary fiber jelly sponge manufactured thereby - Google Patents

Method for manufacturing weakly acidic natural dietary fiber jelly sponge for face washing and bathing, and weakly acidic natural dietary fiber jelly sponge manufactured thereby Download PDF

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Publication number
WO2015005535A1
WO2015005535A1 PCT/KR2013/009583 KR2013009583W WO2015005535A1 WO 2015005535 A1 WO2015005535 A1 WO 2015005535A1 KR 2013009583 W KR2013009583 W KR 2013009583W WO 2015005535 A1 WO2015005535 A1 WO 2015005535A1
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dietary fiber
sponge
weakly acidic
acid
resultant
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PCT/KR2013/009583
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French (fr)
Korean (ko)
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곽태용
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(주)케이린
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C44/00Shaping by internal pressure generated in the material, e.g. swelling or foaming ; Producing porous or cellular expanded plastics articles
    • B29C44/34Auxiliary operations
    • B29C44/56After-treatment of articles, e.g. for altering the shape
    • B29C44/5609Purging of residual gas, e.g. noxious or explosive blowing agents
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C44/00Shaping by internal pressure generated in the material, e.g. swelling or foaming ; Producing porous or cellular expanded plastics articles
    • B29C44/02Shaping by internal pressure generated in the material, e.g. swelling or foaming ; Producing porous or cellular expanded plastics articles for articles of definite length, i.e. discrete articles
    • AHUMAN NECESSITIES
    • A47FURNITURE; DOMESTIC ARTICLES OR APPLIANCES; COFFEE MILLS; SPICE MILLS; SUCTION CLEANERS IN GENERAL
    • A47KSANITARY EQUIPMENT NOT OTHERWISE PROVIDED FOR; TOILET ACCESSORIES
    • A47K7/00Body washing or cleaning implements
    • A47K7/02Bathing sponges, brushes, gloves, or similar cleaning or rubbing implements

Definitions

  • the present invention relates to a weakly acidic natural dietary fiber jelly sponge for use in face wash and bath and a method for producing the same.
  • Dietary fiber is an indigestible polymer material of polysaccharides and polysaccharide derivatives and has properties such as water retention, solubility, viscosity, gelling, cation exchange, and adsorption.
  • the dietary fiber absorbs water in our body to increase its volume and swell and gel it to take a three-dimensional network structure, which is insoluble in solvents, and promotes "bowel activity" as it passes through the intestine and absorbs oil to regulate "cholesterol.” It also helps to suppress postprandial blood sugar by adsorbing and releasing toxic substances, waste products and impurities.
  • the present invention has a transparent, moist and soft three-dimensional network structure, such as jelly when the gelled dietary fiber absorbs water by irreversible heating reaction and freezing / thawing process to have the same effect on the skin
  • a jelly sponge that does not irritate the skin and makes the jelly sponge slightly acidic again, it protects the human body's skin barrier which is weakly acidic when washing and bathing, and replenishes the skin while adsorbing oil, sebum and impurities.
  • Waste products and the like relates to a weakly acidic dietary fiber jelly sponge and a method for producing the same.
  • face wash and bath are the most important basic steps in skin care to clean the skin by removing waste, sweat, sebum, dust, cosmetics, etc. on the skin surface to clean the skin, including the face.
  • washing or bathing properly in the usual way can be said to be the beginning of all skin care to maintain healthy and beautiful skin that cannot be overemphasized.
  • washing or bathing properly should not irritate the skin, second, clean every corner of the skin, and third, protect the skin barrier and maintain the skin's moisture (pH) balance, Finally, fourth, it should be easy and simple to do it every day in your life.
  • washing your face with a cleansing foam with a cleanser on your hands is like brushing your teeth or washing your hands, so the cleansing effect will be as clear as a fire.
  • a familiar sponge form In view of the conditions of such a cleaning tool, first, it is preferable to have a familiar sponge form because it should be excellent in washing ability with abundant foam and easy to use daily in daily life. Second, it should be an eco-friendly natural product that has no skin irritation and no harm to human body. The use of synthetic sponges that can be irritating and harmful to the body when washing or bathing is harmful to skin health. Therefore, eco-friendly natural products should be used. Plant products that can be easily grown are preferable to animal products that can destroy the ecosystem. have. Third, in order to have no skin irritation than the hand, it must be softer than the hand physically, and it is natural that a weakly acidic cleaning sponge is needed so as not to damage the chemically weak skin protective film.
  • a natural sponge having such a function that is, a cleaning sponge having a jelly shape
  • a natural sponge having such a function that is, a cleaning sponge having a jelly shape
  • newborns, infants, atopic dermatitis and acne-sensitive skin are more alkaline outside the range of pH 4.5-6, which is normal skin pH of normal adults, so the use of alkaline cleaners deteriorates skin health.
  • Synthetic sponges for example, foam well but are irritating, weakly acidic, and chemically disinfecting, usually triclosan, to prevent bacteria and fungi. It is well foamed, but it is a natural pulp that is irritating and weakly acidic if used without detergent, and the foam is good and soft, but if it is used without detergent, it is irritating and weakly acidic, and it is an animal natural that is concerned about destroying the sea ecosystem by excessive collection. There are also sponges, and foams are soft and soft, and there are konjac sponges with weak alkali properties that are less physically irritating to the skin but chemically irritating.
  • the skin permeation barrier is maintained to protect the skin from the outside, the skin's binding strength and cohesion is maintained, it is elastic, and it has the antibacterial ability against bacteria, bacteria, hair follicles, etc. do.
  • alkalinity increases allergic reactions, more toxic substances enter the skin, various infectious diseases increase, skin's ability to retain moisture, and the epidermis becomes thicker, such as atopy, acne, rashes, troubles, dryness, dead skin, sensitive skin. And so on.
  • acidity is reached between 3.7 and 4.5, keratin, which is a skin protein, coagulates and the skin becomes crumbly and loses its elasticity.
  • the activity of the skin glands becomes difficult and the metabolic activity of the skin cells is impaired.
  • the present invention reflects these trends and desires, and relates to a weakly acidic dietary fiber jelly sponge and a manufacturing process that are harmless to the human body, which was born for the first time in the world.
  • the present invention has been made to solve the problems of the prior art as described above, the problem to be solved in the present invention is to select the weakly acidic dietary fiber through an eco-friendly process, to ensure an excellent cleaning effect and at the same time cleansing with water only without detergent Even when taking a bath, it creates a sponge with a transparent, moist and soft three-dimensional network like jelly to minimize skin irritation, replenish moisture, absorb oil, and remove impurities and wastes.
  • the tissue itself is the same as the acidity of the skin layer. It is to provide a method for producing a weakly acidic dietary fiber jelly sponge for washing and bathing, and a weakly acidic dietary fiber jelly sponge prepared therefrom to have weak acidity.
  • the present invention (1) mixing and stirring purified water, emulsifiers, foaming agents and dietary fiber to form an aqueous sol, and stirring by adding a gelling agent; (2) a dispensing step of forming a shape by pouring the resultant of the step (1) into a mold; (3) a ripening step of aging for 1 to 24 hours at room temperature to stably gel the product of step (2); (4) a heating step of steaming the resultant of step (3) at 85 to 120 ° C.
  • step (5) for 1 to 5 hours to spongy the same through an irreversible heating reaction; (5) a slow cooling step of cooling the resultant of step (4) for 1 to 5 hours at room temperature; (6) a freezing step of freezing the resultant of step (5) for 1 to 5 days at minus 20 ° C.
  • step (7) thawing washing step of thawing the resultant of step (6) to strengthen the sponge tissue and to participate in the reaction and to remove the remaining emulsifier, foaming agent and gelling agent; (8) an immersion step for 1 to 24 hours soaking in edible organic acid to completely remove the base that may remain in the product of step (7) and restore weakly acidic properties; (9) a drying step of washing, disinfecting, dehydrating and drying the resultant of step (8); And (10) provides a method for producing a weakly acidic dietary fiber jelly sponge for face wash and bath comprising a packaging step of sealing the resulting product of step (9).
  • the blending ratio of the step (1) is preferably mixed in a ratio of 0.1 ⁇ 1.0g foaming agent, 0.01 ⁇ 1ml emulsifier, dietary fiber 2 ⁇ 10g, gelling agent 0.005 ⁇ 1ml with respect to 100ml of purified water.
  • the dietary fiber of step (1) is (a) glucomannan; (b) guar gum or guar hydrolyzate, chaff, indigestible maltodextrin, soybean fiber, sore throat, wheat fiber, barley fiber, oats, gum arabic, inulin and chicory extract, polydextrose, cellulose, fenugreek seed and Vegetable dietary fiber selected from the group consisting of mixtures thereof; And (c) a gel body selected from the group consisting of agar, agaroid, agarose, alginic acid, carrageenan, curdlan, gellan, pectin, gel-forming chemical derivatives thereof, and mixtures thereof.
  • the ratio of the dietary fiber of step (1) is preferably (a) 100 to 100 parts by weight of glucomannan, (b) 10 to 100 parts by weight of the vegetable fiber and 10 to 200 parts by weight of the gel-forming body.
  • the edible organic acid of step (8) is selected from the group consisting of glycolic acid, lactic acid, malic acid, citric acid, tartaric acid, mandelic acid, salicylic acid and acetic acid.
  • the drying of the step (9) is preferably dried for 15 to 40 hours at a temperature of 35 ⁇ 55 °C to dry the moisture content to 15% or less.
  • the present invention provides a weakly acidic dietary fiber jelly sponge for washing and bathing, which is prepared by the method of the present invention.
  • the weakly acidic dietary fiber jelly sponge for washing and bathing according to the manufacturing method of the present invention is prepared to have weak acidity such as acidity of the skin layer using the dietary fiber as a raw material.
  • weak acidity such as acidity of the skin layer using the dietary fiber as a raw material.
  • water When water is absorbed, it swells and has a transparent, moist and soft three-dimensional network structure like jelly, ensuring excellent cleaning effect without skin irritation, minimizing skin irritation and replenishing moisture and oil even when washing or bathing with water alone without cleaning agent. Is adsorbed, and impurities and wastes can be effectively removed.
  • the skin moisture level is in the normal range (pH 4.5 ⁇ 6.0), it ensures moist and smooth cleansing and bathing through excellent cleansing and cleansing after rinsing, and atopy (pH8.0) and acne (pH7.
  • Figure 1 schematically shows the manufacturing process of the weak acid natural dietary fiber jelly sponge for washing and bathing of the present invention.
  • the inventors of the present invention compensate for the disadvantages of sponge products that are unsuitable for conventional cleansing and bathing, and in particular, the cleaning sponges for optimally acidic jelly properties for correct cleansing and bathing, which is the beginning of skin care for modern people who need skin moisture (pH degree) balance.
  • the sponges produced are weakly acidic by completely removing the residues of the bases in the process of gelling dietary fiber such as glucomannan, which has a weak acidity, by edible organic acid. It was confirmed that it is possible to wash and bath effectively without damage and completed the present invention.
  • step (5) for 1 to 5 hours to spongy the same through an irreversible heating reaction; (5) a slow cooling step of cooling the resultant of step (4) for 1 to 5 hours at room temperature; (6) a freezing step of freezing the resultant of step (5) for 1 to 5 days at minus 20 ° C.
  • thawing washing step of thawing the resultant of step (6) to strengthen the sponge tissue and to participate in the reaction and to remove the remaining emulsifier, foaming agent and gelling agent;
  • purified water, a foaming agent, an emulsifier, and a dietary fiber are combined to form a sol, and then a gelling agent is added and stirred and mixed with a stirrer.
  • the blending ratio of the above step is preferably mixed at a ratio of 0.1 to 1.0 g of foaming agent, 0.01 to 1 ml of emulsifier, 2 to 10 g of dietary fiber, and 0.005 to 1 ml of gelling agent with respect to 100 ml of purified water.
  • the purified water serves as a medium for solvating dietary fiber in the stirring step.
  • the foaming agent is added to allow the bubbles to be formed smoothly when the fiber is stirred in the heating step to be described later as a natural foaming agent as described above, 0.1 ⁇ 1.0g is added to 100ml of purified water as described above do.
  • the emulsifier is added to smoothly mix the above-mentioned purified water, foaming agent, dietary fiber, and gelling agent, and does not inhibit the mixing ratio of other mixtures, and 0.01 to 1 ml is added with respect to 100 ml of water so as to obtain the efficacy of the emulsifier. .
  • the gelling agent is added to gel the solvated dietary fiber, so that the pH of the sol may be added to 0.05 ml to 100 ml of purified water so that the pH of the sol can be adjusted to about 9.0 to 12.0 by adding the gelling agent.
  • the gelling agent are not particularly limited, but may be one or more selected from the group consisting of ammonium hydroxide, alkali metal hydroxides or carbonates and alkaline earth metal hydroxides or carbonates.
  • the dietary fiber of step (1) comprises (a) glucomannan derived from konjac; (b) guar gum or guar hydrolyzate, chaff, indigestible maltodextrin, soybean fiber, sore throat, wheat fiber, barley fiber, oats, gum arabic, inulin and chicory extract, polydextrose, cellulose, fenugreek seed and Vegetable dietary fiber selected from the group consisting of mixtures thereof; And (c) a gel body selected from the group consisting of agar, agaroid, agarose, alginic acid, carrageenan, curdlan, gellan, pectin, gel-forming chemical derivatives thereof, and mixtures thereof.
  • the ratio of the dietary fiber of step (1) may be (a) 100 to 100 parts by weight of glucomannan, (b) 10 to 100 parts by weight of the vegetable fiber and 10 to 200 parts by weight of the gel forming body.
  • the dietary fiber is 2 ⁇ 10g with respect to 100ml of purified water.
  • the dispensing step of the step (2) is to pour the dough mixed through the stirring step to form a mold.
  • a molding die that forms a heat-resistant temperature of more than 90 °C made of polypropylene material so that the molding die is harmless to environmental hormones, the shape of the molding die is changed in various ways according to the user's selection It is applicable.
  • the aging step of step (3) is a step of aging for 1 to 24 hours at room temperature in an enclosed space so that the solvated dietary fiber can be stably gelled.
  • the heating step of step (4) is to put the gelated dietary fiber into a steam heater forming 85 ⁇ 120 °C steam heating for 1 to 5 hours to form a sponge shape of the three-dimensional net structure through an irreversible heating reaction will be.
  • the gelated dietary fiber is subjected to a bubble generation step to maintain the bubble and to fix the tissue through a process of hardening the sponge to be sponged.
  • the cooling step of the step (5) is a step of slowly cooling the sponge formed through the steam heating step for 1 to 4 hours at room temperature.
  • the freezing step of the step (6) is to freeze the sponge after the cooling step 1-5 days at below zero °C.
  • the thawing and washing step of the step (7) is thawed in the water of 25 ⁇ 35 °C frozen sponge through the freezing step to discharge the moisture and the net structure of the sponge separated in the freezing process to strengthen the tissue and in the stirring step Removing the added purified water, foaming agent, emulsifier, gelling agent.
  • the immersion step of step (8) is a step of immersing in edible organic acid for 1 to 24 hours to completely remove the gelling agent that may remain even after the thawing and washing step and to restore the original weak acidity of the sponge.
  • the edible organic acid is preferably one or more selected from the group consisting of glycolic acid, lactic acid, malic acid, citric acid, tartaric acid, mandelic acid, salicylic acid and acetic acid, and may be used in a mixture of 10 to 100 parts by weight based on 100 parts by weight of purified water.
  • the drying step of the step (9) is a step of washing, disinfecting, dehydrating and drying the sponge which has undergone the immersion step. Dry 15 to 40 hours at 35 ⁇ 55 °C temperature of the dryer to dry the moisture content below 15%.
  • the packaging step of the step (10) is a step of sealing the dried sponge so that moisture can not penetrate.

Abstract

The present invention relates to a weakly acidic dietary fiber jelly sponge used for face washing and bathing, and a manufacturing method therefor, and more specifically, to: a weakly acidic dietary fiber jelly sponge capable of protecting the skin protective layer during face washing and bathing, controlling the oil-water balance and effectively removing only waste matter by manufacturing a sponge of a jelly property by using a dietary fiber material and making the sponge be weakly acidic; and a manufacturing method therefor.

Description

세안 및 목욕용 약산성 천연 식이섬유 젤리 스폰지의 제조 방법 및 이로부터 제조되는 약산성 천연 식이섬유 젤리 스폰지Method for preparing weakly acidic natural fiber jelly sponge for face wash and bath and weakly acidic natural fiber jelly sponge prepared therefrom
본 발명은 세안 및 목욕에 사용되는 약산성 천연 식이섬유 젤리 스폰지 및 그 제조 방법에 관한 것이다.The present invention relates to a weakly acidic natural dietary fiber jelly sponge for use in face wash and bath and a method for producing the same.
식이섬유는 다당류와 다당류 유도체의 난소화성 고분자 물질로 보수성, 용해성, 점질성, 겔화, 양이온 교환성, 흡착성 등의 특성이 있다. 즉 식이섬유는 우리 몸 속에서 물을 흡수하여 체적 증가 및 팽윤하여 겔화하면 3차원적 그물구조를 취하여 용매에 녹지 않게 되어 장을 통과하면서 “배변활동”을 촉진하고, 유분을 흡수하여 “콜레스테롤 조절”하며, 독성물질, 노폐물, 불순물을 흡착, 배출하여 “식후혈당상승억제”에 도움을 주게 된다. Dietary fiber is an indigestible polymer material of polysaccharides and polysaccharide derivatives and has properties such as water retention, solubility, viscosity, gelling, cation exchange, and adsorption. In other words, the dietary fiber absorbs water in our body to increase its volume and swell and gel it to take a three-dimensional network structure, which is insoluble in solvents, and promotes "bowel activity" as it passes through the intestine and absorbs oil to regulate "cholesterol." It also helps to suppress postprandial blood sugar by adsorbing and releasing toxic substances, waste products and impurities.
본 발명은 이러한 기능을 피부에도 동일한 작용을 할 수 있도록 겔화된 식이섬유를 비가역적 가열반응 및 냉동/해동 과정을 통하여 스폰지화 하여 물을 흡수하였을 경우 젤리처럼 투명하고 촉촉하고 부드러운 3차원 그물구조를 갖게 되어 피부에 자극을 주지 않는 젤리 스폰지를 제조하고, 다시 젤리 스폰지가 약산성을 갖게 함으로써 세안과 목욕 시 약산성인 인체의 피부보호막은 보호하고, 피부에 수분은 보충하면서 유분, 피지는 흡착하고 불순물, 노폐물 등은 효율적으로 제거할 수 있는 약산성 식이섬유 젤리 스폰지 및 그 제조 방법에 관한 것이다.The present invention has a transparent, moist and soft three-dimensional network structure, such as jelly when the gelled dietary fiber absorbs water by irreversible heating reaction and freezing / thawing process to have the same effect on the skin By producing a jelly sponge that does not irritate the skin and makes the jelly sponge slightly acidic again, it protects the human body's skin barrier which is weakly acidic when washing and bathing, and replenishes the skin while adsorbing oil, sebum and impurities. Waste products and the like relates to a weakly acidic dietary fiber jelly sponge and a method for producing the same.
일반적으로 세안 및 목욕이란 얼굴을 포함한 피부를 깨끗이 하기 위하여 피부 표면의 노폐물, 땀, 피지, 먼지, 화장품 등을 제거함으로써 피부를 청결히 하는 것으로 피부 관리에서 가장 중요한 기본 단계이다.In general, face wash and bath are the most important basic steps in skin care to clean the skin by removing waste, sweat, sebum, dust, cosmetics, etc. on the skin surface to clean the skin, including the face.
그러나, 화장이나 자외선 크림을 바르고 낮 동안 열심히 활동한 이후에 피부 곳곳을 모공 속까지 딥클렌징 해주지 않으면 화장찌꺼기와 낮 동안 활동으로 쌓인 먼지, 대기오염, 땀, 각질, 피지는 물론 세정제 찌꺼기까지 어우러져, 피부에 흡수되거나 자체적으로 서서히 분해 혹은 산화되어 피부자극을 일으키며, 피부의 산화와 과산화지질을 형성하여 피부 노화를 재촉하게 된다. 또한, 노화되고 막힌 모공은 제대로 된 영양을 공급하여도 효율적인 흡수가 이루어지지 않아 아무리 좋고 값비싼 화장품, 영양성분을 공급해 준다고 하여도 그 효능을 제대로 전달하지 못하게 된다. 또, 어떤 경우에는 세균, 박테리아, 모낭충 등이 번식할 수 있는 환경을 제공하게 되어 또 다른 피부 트러블의 원인이 되기도 한다. However, after applying makeup or UV cream and working hard during the day, if you do not deep cleanse your skin all the way to the pores, you will be able to mix the debris with dust, air pollution, sweat, keratin, sebum and detergent residues accumulated during the day, It is absorbed by the skin or decomposed or oxidized by itself, causing skin irritation, and it promotes skin aging by forming oxidation and lipid peroxide. In addition, the aging and clogged pores do not provide effective nutrition absorption even if properly supplied, no matter how good and expensive cosmetics, even if it provides the nutritional ingredients will not deliver the effect properly. In some cases, bacteria, bacteria, Demodex, etc., can provide an environment for breeding, causing other skin problems.
따라서 평소에 세안이나 목욕을 제대로 하는 것은 거듭 강조하여도 지나치지 않는 건강하고 아름다운 피부를 유지하기 위한 모든 피부 관리의 시작이라고 할 수 있다.Therefore, washing or bathing properly in the usual way can be said to be the beginning of all skin care to maintain healthy and beautiful skin that cannot be overemphasized.
평소 올바로 세안이나 목욕을 한다는 것은, 첫째, 피부에 자극을 주지 않아야 하고, 둘째, 피부 구석구석 깨끗하게 세정이 이루어져야 하며, 셋째, 피부보호막을 보호하고 피부 유수분(pH도) 밸런스를 유지할 수 있어야 하고, 마지막으로 넷째, 생활 속에서 날마다 하기 쉽고 간편해야 한다는 것이다.Washing or bathing properly, first, should not irritate the skin, second, clean every corner of the skin, and third, protect the skin barrier and maintain the skin's moisture (pH) balance, Finally, fourth, it should be easy and simple to do it every day in your life.
대부분의 사람들의 경우, 손에 세정제를 묻혀서 거품을 내서 세안이나 목욕을 하는 것을 선호하는 데, 그 이유는 손을 대신해서 피부에 자극을 주지 않고 세안이나 목욕을 할 수 있는 도구가 없다는 것과 손으로 하는 것이 간단하고 쉽다는 것을 들 수 있다. Most people prefer to wash or bathe in their hands with foam and foam, because there are no tools for washing or bathing with hands instead of irritating the skin. It's simple and easy to do.
하지만 손에 세정제를 묻혀서 거품을 내서 세안이나 목욕을 하는 것은 마치 양치질을 손으로 하거나 설거지를 손으로 하는 것과 같아서 세정 효과가 떨어질 것은 불을 보듯 명확하다고 할 수 있다. However, washing your face with a cleansing foam with a cleanser on your hands is like brushing your teeth or washing your hands, so the cleansing effect will be as clear as a fire.
따라서, 양치질을 할 때 손대신 칫솔을 사용하고 설거지를 할 때 손대신 스폰지를 사용하는 것과 같이 세안이나 목욕을 할 때, 세정효과를 높일 수 있도록 손대신 사용할 수 있으며 손보다 더 피부에 자극이 없고 날마다 사용하기에 쉽고 간편한 세정도구의 개발이 절실하다고 하겠다.Therefore, you can use it instead of your hands to clean your face, such as using a toothbrush instead of your hands when brushing your teeth and a sponge instead of your hands when washing your face or washing your face. It is urgent to develop a cleaning tool that is easy to use every day.
이러한 세정도구의 조건을 보면, 첫째, 풍부한 거품에 의한 세정 능력이 우수해야 하고 생활 속에서 날마다 사용하기 쉽고 간편해야 하므로 이미 익숙한 스폰지 형태를 갖는 것이 바람직하다. 둘째, 피부에 자극이 없고 인체에 해가 없는 친환경 천연제품이어야 한다. 세안이나 목욕 시 몸에 자극이 되고 해로울 수 있는 합성스폰지를 사용하는 것은 오히려 피부 건강을 해치는 것이니 반드시 친환경 천연제품을 사용해야 하며 생태계를 파괴할 수 있는 동물성 제품보다는 쉽게 재배 가능한 식물성 제품이 바람직하다고 할 수 있다. 셋째, 손보다 더 피부에 자극이 없기 위해서는 물리적으로 손보다 더 부드러워야 하는 것은 물론이고 화학적으로도 약산성인 피부보호막을 손상시키지 않도록 약산성인 세정스폰지가 필요한 것은 당연하다고 하겠다. 넷째, 건강한 피부를 위해서는 세안이나 목욕 후에 피부의 유수분(pH도) 밸런스가 유지되어야 하기 때문에 그러한 기능을 가지고 있는 천연 식이섬유 즉 젤리 성상의 세정스폰지가 바람직하다. 특히, 신생아, 영유아, 아토피, 여드름 등 민감피부의 경우, 정상적인 성인의 피부 pH도 범위인 pH4.5~6의 범위를 벗어나 더 알칼리화되어 있어서 알칼리성 세정제의 사용은 피부 건강을 더 악화시키기 때문에 세정제를 사용하지 않고 물만으로 세안이나 목욕을 해야 하며, 정상적인 성인이라 할지라도 알칼리성 세정제를 사용한 세안이나 목욕 후에는 피부 pH도가 급격하게 알칼리화하기 때문에 남은 세정제 찌꺼기를 제거하고 피부 유수분 균형을 유지하기 위해서 물만으로 정리세안을 해주는 것이 좋다. 이와 같이 물과 세정스폰지 만을 사용해서 세안이나 목욕을 해야하는 상황과 욕구가 증가하고 있다. 이때 피부에 수분은 보충하고 여분의 유분(피지, 기름기)은 흡착하고 불순물이나 노폐물은 원할하게 제거할 수 있는 천연 식이섬유(젤리)의 특성을 갖춘 세정스폰지라면 더욱 바람직할 것이다. In view of the conditions of such a cleaning tool, first, it is preferable to have a familiar sponge form because it should be excellent in washing ability with abundant foam and easy to use daily in daily life. Second, it should be an eco-friendly natural product that has no skin irritation and no harm to human body. The use of synthetic sponges that can be irritating and harmful to the body when washing or bathing is harmful to skin health. Therefore, eco-friendly natural products should be used. Plant products that can be easily grown are preferable to animal products that can destroy the ecosystem. have. Third, in order to have no skin irritation than the hand, it must be softer than the hand physically, and it is natural that a weakly acidic cleaning sponge is needed so as not to damage the chemically weak skin protective film. Fourth, in order to maintain healthy skin, the skin's oil and water (pH degree) balance should be maintained after washing or bathing, and thus, a natural sponge having such a function, that is, a cleaning sponge having a jelly shape, is preferable. In particular, newborns, infants, atopic dermatitis and acne-sensitive skin are more alkaline outside the range of pH 4.5-6, which is normal skin pH of normal adults, so the use of alkaline cleaners deteriorates skin health. You should wash your face or bath with water without using it. Even after a normal adult, after washing or bathing with alkaline detergent, the pH level of your skin will be rapidly alkalinized. It is good to wash your face. As such, the situation and desire to wash or bathe using only water and a cleaning sponge are increasing. At this time, it would be more desirable to have a sponge that has the characteristics of natural dietary fiber (jelly) that replenishes the skin with moisture, absorbs excess oil (sebum, greasy), and removes impurities and waste products.
따라서 이러한 조건들을 모두 충족시키기 위해서는, 보수성, 용해성, 점질성, 겔화,양이온 교환성, 흡착성 등의 특성이 있는 식이섬유 가운데 한가지 혹은 혼합물을 원료로 하는 약산성 천연 식이섬유 젤리 스폰지의 개발이 절실하게 되는 것이다.Therefore, in order to satisfy all of these conditions, development of a weakly acidic natural dietary fiber jelly sponge based on one or a mixture of dietary fibers having water retention, solubility, viscosity, gelling, cation exchangeability, and adsorption properties is urgently needed. will be.
종래의 세정스폰지들이 시판되고 있으나 세안, 목욕용으로서 꼭 갖춰야 할 위와 같은 조건들 가운데 기본적인 일부만 갖추고 있어서 올바른 세안, 목욕이 불가능하다. 예를 들어 합성스폰지들은 거품은 잘 나지만 피부에 자극이 있고 약산성이 아니며 박테리아나 곰팡이 방지를 위하여 보통 트라이클로산과 같은 화학 살균성분이 투입되어 있다. 거품은 잘 나지만 세정제 없이 사용하면 피부에 자극이 있고 약산성도 아닌 천연 펄프도 있고, 거품은 잘나고 부드럽지만 세정제 없이 사용하면 피부에 자극이 있고 약산성도 아니며 과도한 채취로 바다 생태계 파괴가 우려되는 동물성 천연 해면도 있으며, 거품은 잘나고 부드럽고 피부에 물리적인 자극은 적으나 화학적으로 자극이 되는 약알칼리 특성을 가진 곤약스폰지 등도 있다. Conventional cleaning sponges are commercially available, but because they have only a basic part of the above conditions that must be provided for face wash and bath, proper face wash and bath are impossible. Synthetic sponges, for example, foam well but are irritating, weakly acidic, and chemically disinfecting, usually triclosan, to prevent bacteria and fungi. It is well foamed, but it is a natural pulp that is irritating and weakly acidic if used without detergent, and the foam is good and soft, but if it is used without detergent, it is irritating and weakly acidic, and it is an animal natural that is concerned about destroying the sea ecosystem by excessive collection. There are also sponges, and foams are soft and soft, and there are konjac sponges with weak alkali properties that are less physically irritating to the skin but chemically irritating.
피부가 정상범위 pH4.5~6인 경우에는 피부투과장벽이 유지되어 외부로부터 피부를 보호하고 피부의 결합력과 응집력이 유지되어 탄력이 있고 세균, 박테리아, 모낭충 등에 대한 항균력이 있어서 건강한 피부 상태를 유지한다. 그러나 알칼리화되면 알레르기 반응이 증가하거나 유독물질이 피부에 더 많이 유입되거나 각종 감염질환이 증가하게 되고 피부의 수분 보유능력은 떨어지고 표피는 두꺼워지는 등 아토피, 여드름, 뾰루지, 트러블, 건성, 각질, 민감피부 등이 되게 된다. 반대로 산성화하여 pH가 3.7~4.5 사이가 되면 피부단백질인 케라틴이 응고되면서 피부가 푸석푸석하고 탄력을 잃게 된다. 또한 피부 분비선의 활동이 어렵게 되며 피부세포의 대사활동에 장애를 받게 된다.When the skin is in the normal range of pH4.5 ~ 6, the skin permeation barrier is maintained to protect the skin from the outside, the skin's binding strength and cohesion is maintained, it is elastic, and it has the antibacterial ability against bacteria, bacteria, hair follicles, etc. do. However, alkalinity increases allergic reactions, more toxic substances enter the skin, various infectious diseases increase, skin's ability to retain moisture, and the epidermis becomes thicker, such as atopy, acne, rashes, troubles, dryness, dead skin, sensitive skin. And so on. On the contrary, when acidity is reached between 3.7 and 4.5, keratin, which is a skin protein, coagulates and the skin becomes crumbly and loses its elasticity. In addition, the activity of the skin glands becomes difficult and the metabolic activity of the skin cells is impaired.
따라서 현대인의 건강한 아름다운 피부에 대한 열망과 약산성에 대한 요구는 날로 증가하고 있어서 화장품, 자외선차단제는 물론 물비누, 심지어 고체비누 조차 세정력의 핵심인 알칼리성을 포기한 약산성 고체비누가 인기를 끌고 있는 추세이다. 하물며 세정제와 함께 풍성한 거품을 내야 할 세정스폰지가 약산성이어야 하는 것은 너무도 당연한 결과이고, 신생아/영유아 목욕, 아토피, 여드름, 민감피부 세안/목욕 등과 정상인의 아침 세안, 정리세안 등 세정제를 사용하지 않고 세안이나 목욕을 해야하는 경우와 상황이 더욱 많아지는 추세에서 세안과 목욕을 도와주는 유일한 도구인 약산성이면서 식이섬유 젤리 성상의 세정스폰지는 반드시 필요한 발명이라고 할 수 있다.Accordingly, the desire for healthy and beautiful skin and the demand for weak acidity are increasing day by day, and the cosmetics, sunscreen, water soap, and even solid soap have become popular. In addition, it is a natural result that the cleaning sponge, which should be foamed with the detergent, should be weakly acidic. In the trend of more and more situations when you need to take a bath, washing sponges, which are weakly acidic and dietary fiber jelly, are the only necessary tools to help cleansing and bathing.
본 발명은 이러한 시대적 추세와 욕구를 반영하여 세계 최초로 탄생한 인체에 해가 없는 약산성 식이섬유 젤리 스폰지 및 제조공정에 대한 것이다.The present invention reflects these trends and desires, and relates to a weakly acidic dietary fiber jelly sponge and a manufacturing process that are harmless to the human body, which was born for the first time in the world.
본 발명은 상기와 같은 종래 기술의 문제점을 해결하기 위하여 안출된 것으로서, 본 발명에서 해결하고자 하는 과제는 약산성 식이섬유를 선택해서 친환경 공정을 통하여, 탁월한 세정효과를 보장하고 동시에 세정제 없이 물만으로 세안이나 목욕하는 경우에도 피부자극은 최소화하고 수분은 보충하고 유분은 흡착하고 불순물, 노폐물은 제거할 수 있도록 젤리처럼 투명하고 촉촉하고 부드러운 3차원 그물구조를 갖춘 스폰지를 만들고, 조직 자체가 피부층의 산성도와 동일한 약산성을 갖도록 만드는, 세안 및 목욕용 약산성 식이섬유 젤리 스폰지의 제조 방법 및 이로부터 제조되는 약산성 식이섬유 젤리 스폰지를 제공하고자 하는 것이다.The present invention has been made to solve the problems of the prior art as described above, the problem to be solved in the present invention is to select the weakly acidic dietary fiber through an eco-friendly process, to ensure an excellent cleaning effect and at the same time cleansing with water only without detergent Even when taking a bath, it creates a sponge with a transparent, moist and soft three-dimensional network like jelly to minimize skin irritation, replenish moisture, absorb oil, and remove impurities and wastes.The tissue itself is the same as the acidity of the skin layer. It is to provide a method for producing a weakly acidic dietary fiber jelly sponge for washing and bathing, and a weakly acidic dietary fiber jelly sponge prepared therefrom to have weak acidity.
상기와 같은 과제를 해결하기 위하여, 본 발명은 (1) 정제수, 유화제, 기포제 및 식이섬유를 혼합 및 교반하여 수성 졸을 형성시키고, 겔화제를 첨가하여 교반하는 교반단계; (2) 상기 단계 (1)의 결과물을 성형틀에 부어 넣어 형상을 형성하는 분주단계; (3) 상기 단계 (2)의 결과물이 안정적으로 겔화하도록 상온에서 1~24시간 동안 숙성하는 숙성단계; (4) 상기 단계 (3)의 결과물을 85~120℃에서 1~5시간 동안 증기가열하여 비가역적 가열반응을 통하여 스폰지화하는 가열단계; (5) 상기 단계 (4)의 결과물을 상온에서 1~5시간 동안 냉각시키는 서냉단계; (6) 상기 단계 (5)의 결과물을 영하 20℃ 이하에서 1~5일 동안 냉동시키는 냉동단계; (7) 상기 단계 (6)의 결과물을 해동시켜서 스폰지 조직을 강화하고 반응에 참여하고 남은 유화제, 기포제, 겔화제를 제거하기 위하여 세척하는 해동세척단계; (8) 상기 단계 (7)의 결과물에 남아있을 수 있는 염기를 완전히 제거하고 약산성 특성을 복구하기 위하여 식용 유기산에 1~24시간 담가두는 침지단계; (9) 상기 단계 (8)의 결과물을 세척, 소독, 탈수, 건조하는 건조단계; 및 (10) 상기 단계 (9)의 결과물을 밀봉 포장하는 포장단계를 포함하는 것을 특징으로 하는 세안 및 목욕용 약산성 식이섬유 젤리 스폰지의 제조 방법을 제공한다.In order to solve the above problems, the present invention (1) mixing and stirring purified water, emulsifiers, foaming agents and dietary fiber to form an aqueous sol, and stirring by adding a gelling agent; (2) a dispensing step of forming a shape by pouring the resultant of the step (1) into a mold; (3) a ripening step of aging for 1 to 24 hours at room temperature to stably gel the product of step (2); (4) a heating step of steaming the resultant of step (3) at 85 to 120 ° C. for 1 to 5 hours to spongy the same through an irreversible heating reaction; (5) a slow cooling step of cooling the resultant of step (4) for 1 to 5 hours at room temperature; (6) a freezing step of freezing the resultant of step (5) for 1 to 5 days at minus 20 ° C. or less; (7) thawing washing step of thawing the resultant of step (6) to strengthen the sponge tissue and to participate in the reaction and to remove the remaining emulsifier, foaming agent and gelling agent; (8) an immersion step for 1 to 24 hours soaking in edible organic acid to completely remove the base that may remain in the product of step (7) and restore weakly acidic properties; (9) a drying step of washing, disinfecting, dehydrating and drying the resultant of step (8); And (10) provides a method for producing a weakly acidic dietary fiber jelly sponge for face wash and bath comprising a packaging step of sealing the resulting product of step (9).
상기 단계 (1)의 배합비율은 정제수 100ml에 대하여, 기포제 0.1~1.0g, 유화제 0.01~1ml, 식이섬유 2~10g, 겔화제 0.005~1ml의 비율로 혼합되는 것이 바람직하다.The blending ratio of the step (1) is preferably mixed in a ratio of 0.1 ~ 1.0g foaming agent, 0.01 ~ 1ml emulsifier, dietary fiber 2 ~ 10g, gelling agent 0.005 ~ 1ml with respect to 100ml of purified water.
상기 단계 (1)의 식이섬유는 (a) 글루코만난; (b) 구아검 또는 구아검가수분해물, 차전자피, 난소화성 말토덱스트린, 대두식이섬유, 목이, 밀식이섬유, 보리식이섬유, 귀리, 아라비아검, 이눌린 및 치커리 추출물, 폴리덱스트로스, 셀룰로스, 호로파종자 및 이들의 혼합물로 이루어지는 군으로부터 선택되는 식물성 식이섬유; 및 (c) 아가, 아가로이드, 아가로즈, 알긴산, 카라기난, 커들란, 겔란, 펙틴, 이들의 겔 형성 화학 유도체 및 이들의 혼합물로 이루어지는 군으로부터 선택되는 겔 형성체로 이루어지는 것이 바람직하다.The dietary fiber of step (1) is (a) glucomannan; (b) guar gum or guar hydrolyzate, chaff, indigestible maltodextrin, soybean fiber, sore throat, wheat fiber, barley fiber, oats, gum arabic, inulin and chicory extract, polydextrose, cellulose, fenugreek seed and Vegetable dietary fiber selected from the group consisting of mixtures thereof; And (c) a gel body selected from the group consisting of agar, agaroid, agarose, alginic acid, carrageenan, curdlan, gellan, pectin, gel-forming chemical derivatives thereof, and mixtures thereof.
상기 단계 (1)의 식이섬유의 비율은 (a) 글루코만난 100중량부에 대하여, (b) 식물성 식이섬유 10~100중량부 및 겔 형성체 10~200중량부인 것이 바람직하다.The ratio of the dietary fiber of step (1) is preferably (a) 100 to 100 parts by weight of glucomannan, (b) 10 to 100 parts by weight of the vegetable fiber and 10 to 200 parts by weight of the gel-forming body.
상기 단계 (8)의 식용 유기산이 글리콜산, 락트산, 사과산, 구연산, 주석산, 만델산, 살리실산 및 초산으로 이루어지는 군으로부터 1종 이상 선택되는 것이 바람직하다.Preferably, the edible organic acid of step (8) is selected from the group consisting of glycolic acid, lactic acid, malic acid, citric acid, tartaric acid, mandelic acid, salicylic acid and acetic acid.
상기 단계 (9)의 건조는 35~55℃ 온도에서 15~40 시간 동안 건조하여 수분 함량을 15% 이하로 건조하는 것이 바람직하다.The drying of the step (9) is preferably dried for 15 to 40 hours at a temperature of 35 ~ 55 ℃ to dry the moisture content to 15% or less.
또한, 본 발명은 본 발명의 상기 제조 방법으로 제조되는 것을 특징으로 하는 세안 및 목욕용 약산성 식이섬유 젤리 스폰지를 제공한다.In addition, the present invention provides a weakly acidic dietary fiber jelly sponge for washing and bathing, which is prepared by the method of the present invention.
본 발명의 제조 방법에 따른 세안 및 목욕용 약산성 식이섬유 젤리 스폰지는 식이섬유를 원료로 하여 피부층의 산성도와 같은 약산성을 갖도록 제조된다. 물을 흡수하면 팽윤하여 젤리처럼 투명하고 촉촉하고 부드러운 3차원 그물구조를 갖게 되어 피부 자극 없이 탁월한 세정효과를 보장하고, 세정제 없이 물만으로 세안이나 목욕하는 경우에도 피부자극은 최소화하고 수분은 보충하고 유분은 흡착하고 불순물, 노폐물들은 효과적으로 제거할 수 있다. 피부 유수분도가 정상범위(pH 4.5~6.0)에 있는 경우는 탁월한 세정과 행굼 후 정리세안을 통하여 촉촉하고 매끄러운 세안 및 목욕을 보장하고, 정상범위를 벗어난 아토피(pH8.0), 여드름(pH7.5), 신생아/영유아(pH6.5~6.8), 뾰루지, 트러블, 건성, 각질, 민감피부 등 피부가 알칼리화되어 세안이나 목욕 시 알칼리 세정제 영향을 많이 받는 경우에는, 알칼리세정제 사용 없이 본 발명품만으로 물세안이나 물목욕을 하게 되면 피부 pH도를 낮추는 데 도움을 주면서도 유분은 흡착하고 이물질은 제거하여 충분한 세정효과를 기대할 수 있어서 피부 건강에 획기적인 도움이 될 것이다.The weakly acidic dietary fiber jelly sponge for washing and bathing according to the manufacturing method of the present invention is prepared to have weak acidity such as acidity of the skin layer using the dietary fiber as a raw material. When water is absorbed, it swells and has a transparent, moist and soft three-dimensional network structure like jelly, ensuring excellent cleaning effect without skin irritation, minimizing skin irritation and replenishing moisture and oil even when washing or bathing with water alone without cleaning agent. Is adsorbed, and impurities and wastes can be effectively removed. If the skin moisture level is in the normal range (pH 4.5 ~ 6.0), it ensures moist and smooth cleansing and bathing through excellent cleansing and cleansing after rinsing, and atopy (pH8.0) and acne (pH7. 5) When newborns / infants (pH6.5 ~ 6.8), rashes, troubles, dryness, dead skin, sensitive skin are alkalinized and affected by alkaline detergents when washing or bathing, use only the present invention without using alkaline cleaners. Washing or bathing will help lower skin pH, while adsorbing oil and removing foreign substances, which can be expected to provide a sufficient cleansing effect.
도 1은 본 발명의 세안 및 목욕용 약산성 천연 식이섬유 젤리 스폰지의 제조 공정을 모식적으로 나타낸 것이다.Figure 1 schematically shows the manufacturing process of the weak acid natural dietary fiber jelly sponge for washing and bathing of the present invention.
이하, 본 발명을 상세하게 설명한다.EMBODIMENT OF THE INVENTION Hereinafter, this invention is demonstrated in detail.
본 발명의 발명자는 종래 세안 및 목욕에 부적합한 스폰지 제품들의 단점을 보완하고 특히 피부 유수분(pH도) 밸런스가 필요한 현대인들의 피부 관리의 시작인 올바른 세안과 목욕을 위한 최적의 약산성 젤리 성상의 세정스폰지를 위한 연구를 거듭한 결과, 본래 재료 자체가 약산성을 가진 글루코만난과 같은 식이섬유를 겔화하는 과정에서 투입된 염기의 잔여물을 식용 유기산으로 처리하여 완벽히 제거하므로써, 제조된 스폰지가 약산성을 띄게 되어 피부 보호막의 손상이 없이 효과적으로 세안 및 목욕이 가능함을 확인하고 본 발명을 완성하였다.The inventors of the present invention compensate for the disadvantages of sponge products that are unsuitable for conventional cleansing and bathing, and in particular, the cleaning sponges for optimally acidic jelly properties for correct cleansing and bathing, which is the beginning of skin care for modern people who need skin moisture (pH degree) balance. As a result of repeated studies, the sponges produced are weakly acidic by completely removing the residues of the bases in the process of gelling dietary fiber such as glucomannan, which has a weak acidity, by edible organic acid. It was confirmed that it is possible to wash and bath effectively without damage and completed the present invention.
본 발명의 세안 및 목욕용 약산성 식이섬유 젤리 스폰지의 제조 방법은 도 1에서 도시된 바와 같이, (1) 정제수, 유화제, 기포제 및 식이섬유를 혼합 및 교반하여 수성 졸을 형성시키고, 겔화제를 첨가하여 교반하는 교반단계; (2) 상기 단계 (1)의 결과물을 성형틀에 부어 넣어 형상을 형성하는 분주단계; (3) 상기 단계 (2)의 결과물이 안정적으로 겔화하도록 상온에서 1~24시간 동안 숙성하는 숙성단계; (4) 상기 단계 (3)의 결과물을 85~120℃에서 1~5시간 동안 증기가열하여 비가역적 가열반응을 통하여 스폰지화하는 가열단계; (5) 상기 단계 (4)의 결과물을 상온에서 1~5시간 동안 냉각시키는 서냉단계; (6) 상기 단계 (5)의 결과물을 영하 20℃ 이하에서 1~5일 동안 냉동시키는 냉동단계; (7) 상기 단계 (6)의 결과물을 해동시켜서 스폰지 조직을 강화하고 반응에 참여하고 남은 유화제, 기포제, 겔화제를 제거하기 위하여 세척하는 해동세척단계; (8) 상기 단계 (7)의 결과물에 남아있을 수 있는 염기를 완전히 제거하고 약산성 특성을 복구하기 위하여 식용 유기산에 1~24시간 담가두는 침지단계; (9) 상기 단계 (8)의 결과물을 세척, 소독, 탈수, 건조하는 건조단계; 및 (10) 상기 단계 (9)의 결과물을 밀봉 포장하는 포장단계로 이루어진다.In the manufacturing method of the weakly acidic dietary fiber jelly sponge for washing and bathing of the present invention, as shown in Figure 1, (1) by mixing and stirring purified water, emulsifier, foaming agent and dietary fiber to form an aqueous sol, and adding a gelling agent A stirring step of stirring; (2) a dispensing step of forming a shape by pouring the resultant of the step (1) into a mold; (3) a ripening step of aging for 1 to 24 hours at room temperature to stably gel the product of step (2); (4) a heating step of steaming the resultant of step (3) at 85 to 120 ° C. for 1 to 5 hours to spongy the same through an irreversible heating reaction; (5) a slow cooling step of cooling the resultant of step (4) for 1 to 5 hours at room temperature; (6) a freezing step of freezing the resultant of step (5) for 1 to 5 days at minus 20 ° C. or less; (7) thawing washing step of thawing the resultant of step (6) to strengthen the sponge tissue and to participate in the reaction and to remove the remaining emulsifier, foaming agent and gelling agent; (8) an immersion step for 1 to 24 hours soaking in edible organic acid to completely remove the base that may remain in the product of step (7) and restore weakly acidic properties; (9) a drying step of washing, disinfecting, dehydrating and drying the resultant of step (8); And (10) a packing step of sealingly packing the resultant of step (9).
상기 단계 (1)의 교반단계는 정제수, 기포제, 유화제, 식이섬유를 배합하여 졸을 형성시킨 후 겔화제를 넣고 교반기로 교반하며 혼합하는 것이다.In the stirring step of (1), purified water, a foaming agent, an emulsifier, and a dietary fiber are combined to form a sol, and then a gelling agent is added and stirred and mixed with a stirrer.
상기 단계의 배합비율은 정제수 100ml에 대하여, 기포제 0.1~1.0g, 유화제 0.01~1ml, 식이섬유 2~10g, 겔화제 0.005~1ml의 비율로 혼합되는 것이 바람직하다.The blending ratio of the above step is preferably mixed at a ratio of 0.1 to 1.0 g of foaming agent, 0.01 to 1 ml of emulsifier, 2 to 10 g of dietary fiber, and 0.005 to 1 ml of gelling agent with respect to 100 ml of purified water.
상기 정제수는 상기 교반단계에서 식이섬유를 졸화하는 매질 역할을 한다.The purified water serves as a medium for solvating dietary fiber in the stirring step.
상기 기포제는 천연기포제로 교반단계를 거친 식이섬유를 후술할 가열단계에서 스폰지화할 때 기포가 원활하게 형성될 수 있도록 하기 위하여 첨가되는 것으로서 상기에서 설명한 바와 같이, 정제수 100ml에 대하여 0.1~1.0g이 첨가된다.The foaming agent is added to allow the bubbles to be formed smoothly when the fiber is stirred in the heating step to be described later as a natural foaming agent as described above, 0.1 ~ 1.0g is added to 100ml of purified water as described above do.
상기 유화제는 상술한 정제수, 기포제, 식이섬유, 겔화제가 원활하게 혼합되도록 하기 위하여 첨가되는 것으로서 다른 혼합물의 혼합비율을 저해하지 않으며 유화제 본연의 효능을 얻을 수 있도록 물 100ml에 대하여 0.01~1ml가 첨가된다.The emulsifier is added to smoothly mix the above-mentioned purified water, foaming agent, dietary fiber, and gelling agent, and does not inhibit the mixing ratio of other mixtures, and 0.01 to 1 ml is added with respect to 100 ml of water so as to obtain the efficacy of the emulsifier. .
상기 겔화제는 졸화된 식이섬유를 겔화하기 위하여 첨가되는 것으로 상기 졸의 pH가 상기 겔화제를 첨가하므로써 약 9.0 내지 12.0으로 조정될 수 있도록 정제수 100ml에 대하여 0.05~1g이 첨가된다. 상기 겔화제의 예는 특별히 한정되는 것은 아니나, 수산화 암모늄, 알칼리 금속 하이드록사이드 또는 카보네이트 및 알칼리 토금속 하이드록사이드 또는 카보네이트로 이루어지는 군으로부터 1종 이상 선택될 수 있다.The gelling agent is added to gel the solvated dietary fiber, so that the pH of the sol may be added to 0.05 ml to 100 ml of purified water so that the pH of the sol can be adjusted to about 9.0 to 12.0 by adding the gelling agent. Examples of the gelling agent are not particularly limited, but may be one or more selected from the group consisting of ammonium hydroxide, alkali metal hydroxides or carbonates and alkaline earth metal hydroxides or carbonates.
상기 단계 (1)의 식이섬유는 (a) 곤약(konjac)으로부터 유도되는 글루코만난; (b) 구아검 또는 구아검가수분해물, 차전자피, 난소화성 말토덱스트린, 대두식이섬유, 목이, 밀식이섬유, 보리식이섬유, 귀리, 아라비아검, 이눌린 및 치커리 추출물, 폴리덱스트로스, 셀룰로스, 호로파종자 및 이들의 혼합물로 이루어지는 군으로부터 선택되는 식물성 식이섬유; 및 (c) 아가, 아가로이드, 아가로즈, 알긴산, 카라기난, 커들란, 겔란, 펙틴, 이들의 겔 형성 화학 유도체 및 이들의 혼합물로 이루어지는 군으로부터 선택되는 겔 형성체로 이루어진다.The dietary fiber of step (1) comprises (a) glucomannan derived from konjac; (b) guar gum or guar hydrolyzate, chaff, indigestible maltodextrin, soybean fiber, sore throat, wheat fiber, barley fiber, oats, gum arabic, inulin and chicory extract, polydextrose, cellulose, fenugreek seed and Vegetable dietary fiber selected from the group consisting of mixtures thereof; And (c) a gel body selected from the group consisting of agar, agaroid, agarose, alginic acid, carrageenan, curdlan, gellan, pectin, gel-forming chemical derivatives thereof, and mixtures thereof.
상기 단계 (1)의 식이섬유의 비율은 (a) 글루코만난 100중량부에 대하여, (b) 식물성 식이섬유 10~100중량부 및 겔 형성체 10~200중량부일 수 있다. 또한, 상기 식이섬유는 정제수 100ml에 대하여 2~10g이다.The ratio of the dietary fiber of step (1) may be (a) 100 to 100 parts by weight of glucomannan, (b) 10 to 100 parts by weight of the vegetable fiber and 10 to 200 parts by weight of the gel forming body. In addition, the dietary fiber is 2 ~ 10g with respect to 100ml of purified water.
상기 단계 (2)의 분주단계는 상기 교반단계를 통하여 혼합된 반죽을 성형틀에 부어 넣어 형상을 형성하는 것이다. The dispensing step of the step (2) is to pour the dough mixed through the stirring step to form a mold.
이는 상기 교반단계를 통하여 졸화된 식이섬유가 분부 및 숙성 단계를 거쳐 후술할 가열단계를 통하여 기포를 형성하여 원하는 스폰지의 형상을 형성하기 위하여 진행되는 것이다.This is to proceed to form the desired sponge by forming a bubble through the heating step to be described later through the portion of the fiber fiber solving and aging through the stirring step.
이때, 상기 성형틀은 인체에 환경호르몬으로 인한 해가 없도록 폴리프로필렌재질로 90℃ 이상의 내열온도를 이루는 성형틀을 사용하는 것이 바람직하며, 상기 성형틀의 형상은 사용자의 선택에 따라 다양하게 변경하여 적용할 수 있는 것이다.In this case, it is preferable to use a molding die that forms a heat-resistant temperature of more than 90 ℃ made of polypropylene material so that the molding die is harmless to environmental hormones, the shape of the molding die is changed in various ways according to the user's selection It is applicable.
상기 단계 (3)의 숙성단계는 졸화된 식이섬유가 안정적으로 겔화할 수 있도록 밀폐된 공간에서 상온으로 1~24시간 동안 숙성하는 단계이다. The aging step of step (3) is a step of aging for 1 to 24 hours at room temperature in an enclosed space so that the solvated dietary fiber can be stably gelled.
상기 단계 (4)의 가열단계는 겔화된 식이섬유를 85~120℃를 이루는 증기가열기에 넣고 1~5시간 동안 증기가열하여 비가역적 가열반응을 통하여 3차원 그물구조의 스폰지 형상을 이루도록 형성하는 것이다.The heating step of step (4) is to put the gelated dietary fiber into a steam heater forming 85 ~ 120 ℃ steam heating for 1 to 5 hours to form a sponge shape of the three-dimensional net structure through an irreversible heating reaction will be.
이때, 겔화된 식이섬유는 기포 발생단계를 거쳐 기포를 유지하고 고착화하는 단계를 거쳐 조직이 단단해지는 과정을 거쳐 스폰지화하게 된다. At this time, the gelated dietary fiber is subjected to a bubble generation step to maintain the bubble and to fix the tissue through a process of hardening the sponge to be sponged.
상기 단계 (5)의 냉각단계는 상기 증기가열단계를 통하여 형성된 스폰지를 상온에서 1~4시간 동안 서냉하는 단계이다. The cooling step of the step (5) is a step of slowly cooling the sponge formed through the steam heating step for 1 to 4 hours at room temperature.
상기 단계 (6)의 냉동단계는 상기 냉각단계를 거친 스폰지를 영하 20℃ 이하에서 1~5일 냉동시키는 것이다. The freezing step of the step (6) is to freeze the sponge after the cooling step 1-5 days at below zero ℃.
이는 스폰지의형상과 식이섬유의 3차원 그물 구조가 견고하게 유지되고 질겨지도록 하기 위한 것이다. 냉동을 시키게 되면 스폰지에 남아있던 수분과 그물 구조가 분리되게 된다. 이때 냉동시간과 스폰지의 질김, 내구성은 큰 연관이 있다. This is to ensure that the shape of the sponge and the three-dimensional mesh structure of the fiber are firmly maintained and tough. Freezing separates the water and the net structure from the sponge. At this time, the freezing time, the toughness of the sponge, the durability has a big relationship.
상기 단계 (7)의 해동세척단계는 상기 냉동단계를 거쳐 냉동된 스폰지를 25~35℃의 물속에서 해동시켜 냉동과정에서 분리된 스폰지의 수분과 그물조직을 배출시켜 조직을 강화하고 상기 교반단계에서 첨가된 정제수, 기포제, 유화제, 겔화제를 제거하는 단계이다.The thawing and washing step of the step (7) is thawed in the water of 25 ~ 35 ℃ frozen sponge through the freezing step to discharge the moisture and the net structure of the sponge separated in the freezing process to strengthen the tissue and in the stirring step Removing the added purified water, foaming agent, emulsifier, gelling agent.
스폰지를 깨끗한 정수에 침수시켜 해동시키고 꺼내어 탈수하는 과정을 반복 수행함으로써 스폰지에 남아있을 수 있는 첨가물 및 각종 불순물을 완전히 제거하여 사용자의 피부와 접촉하여 피부 트러블을 일으킬 수 있는 문제를 미연에 방지할 수 있게 되는 것이다.By repeatedly immersing the sponge in clean water, thawing, removing and dehydrating it, it is possible to completely remove the additives and other impurities that may remain in the sponge, thereby preventing the problem of contact with the user's skin and causing skin trouble. Will be.
상기 단계 (8)의 침지단계는 상기 해동세척단계 이후에도 잔류할 수 있는 겔화제를 완전히 제거하고 스폰지가 원래의 약산성을 회복할 수 있도록 식용유기산에 1~24시간 침지하는 단계이다. The immersion step of step (8) is a step of immersing in edible organic acid for 1 to 24 hours to completely remove the gelling agent that may remain even after the thawing and washing step and to restore the original weak acidity of the sponge.
식용 유기산은 글리콜산, 락트산, 사과산, 구연산, 주석산, 만델산, 살리실산 및 초산으로 이루어지는 군으로부터 1종 이상 선택되는 것이 바람직하며, 정제수 100중량부에 대하여 10 내지 100중량부로 혼합하여 사용할 수 있다.The edible organic acid is preferably one or more selected from the group consisting of glycolic acid, lactic acid, malic acid, citric acid, tartaric acid, mandelic acid, salicylic acid and acetic acid, and may be used in a mixture of 10 to 100 parts by weight based on 100 parts by weight of purified water.
상기 단계 (9)의 건조단계는 상기 침지 단계를 거친 스폰지를 세척, 소독, 탈수, 건조하는 단계이다. 건조기의 35~55℃ 온도에서 15~40 시간 동안 건조하여 수분 함량을 15% 이하로 건조한다.The drying step of the step (9) is a step of washing, disinfecting, dehydrating and drying the sponge which has undergone the immersion step. Dry 15 to 40 hours at 35 ~ 55 ℃ temperature of the dryer to dry the moisture content below 15%.
상기 단계 (10)의 포장단계는 수분이 침투할 수 없도록 상기 건조된 스폰지를 밀봉 포장하는 단계이다.The packaging step of the step (10) is a step of sealing the dried sponge so that moisture can not penetrate.
본 발명은 특정한 실시예에 관련하여 도시하고 설명하였지만, 이하의 특허청구범위에 의해 제공되는 본 발명의 정신이나 분야를 벗어나지 않는 한도 내에서 본 발명이 다양하게 개량 및 변화될 수 있다는 것을 당 업계에서 통상의 지식을 가진 자에게 있어서 자명할 것이다.While the invention has been shown and described with respect to specific embodiments thereof, it will be appreciated that various changes and modifications can be made in the art without departing from the spirit or scope of the invention as provided by the following claims. It will be self-evident for those of ordinary knowledge.

Claims (7)

  1. 다음의 단계들을 포함하는 것을 특징으로 하는 세안 및 목욕용 약산성 식이섬유 젤리 스폰지의 제조 방법:A method for preparing a weakly acidic dietary fiber jelly sponge for cleansing and bathing comprising the following steps:
    (1) 정제수, 유화제, 기포제 및 식이섬유를 혼합 및 교반하여 수성 졸을 형성시키고, 겔화제를 첨가하여 교반하는 교반단계;(1) a stirring step of mixing and stirring purified water, an emulsifier, a foaming agent, and dietary fiber to form an aqueous sol, and adding and stirring a gelling agent;
    (2) 상기 단계 (1)의 결과물을 성형틀에 부어 넣어 형상을 형성하는 분주단계; (2) a dispensing step of forming a shape by pouring the resultant of the step (1) into a mold;
    (3) 상기 단계 (2)의 결과물이 안정적으로 겔화하도록 상온에서 1~24시간 동안 숙성하는 숙성단계;(3) a ripening step of aging for 1 to 24 hours at room temperature to stably gel the product of step (2);
    (4) 상기 단계 (3)의 결과물을 85~120℃에서 1~5시간 동안 증기가열하여 비가역적 가열반응을 통하여 스폰지화하는 가열단계; (4) a heating step of steaming the resultant of step (3) at 85 to 120 ° C. for 1 to 5 hours to spongy the same through an irreversible heating reaction;
    (5) 상기 단계 (4)의 결과물을 상온에서 1~5시간 동안 냉각시키는 서냉단계; (5) a slow cooling step of cooling the resultant of step (4) for 1 to 5 hours at room temperature;
    (6) 상기 단계 (5)의 결과물을 영하 20℃ 이하에서 1~5일 동안 냉동시키는 냉동단계;(6) a freezing step of freezing the resultant of step (5) for 1 to 5 days at minus 20 ° C. or less;
    (7) 상기 단계 (6)의 결과물을 해동시켜서 스폰지 조직을 강화하고 반응에 참여하고 남은 유화제, 기포제, 겔화제를 제거하기 위하여 세척하는 해동세척단계; (7) thawing washing step of thawing the resultant of step (6) to strengthen the sponge tissue and to participate in the reaction and to remove the remaining emulsifier, foaming agent and gelling agent;
    (8) 상기 단계 (7)의 결과물에 남아있을 수 있는 염기를 완전히 제거하고 약산성 특성을 복구하기 위하여 식용 유기산에 1~24시간 담가두는 침지단계;(8) an immersion step for 1 to 24 hours soaking in edible organic acid to completely remove the base that may remain in the product of step (7) and restore weakly acidic properties;
    (9) 상기 단계 (8)의 결과물을 세척, 소독, 탈수, 건조하는 건조단계; 및 (9) a drying step of washing, disinfecting, dehydrating and drying the resultant of step (8); And
    (10) 상기 단계 (9)의 결과물을 밀봉 포장하는 포장단계.(10) a packing step of sealingly packing the resultant of step (9).
  2. 제 1항에 있어서,The method of claim 1,
    상기 단계 (1)의 배합비율은 정제수 100ml에 대하여, 기포제 0.1~1.0g, 유화제 0.01~1ml, 식이섬유 2~10g, 겔화제 0.005~1ml의 비율로 혼합되는 것을 특징으로 하는 제조 방법.The blending ratio of step (1) is a production method, characterized in that the mixing ratio of 0.1 ~ 1.0g foaming agent, 0.01 ~ 1ml, emulsifier 0.01 ~ 1ml, dietary fiber 2 ~ 10g, gelling agent 0.005 ~ 1ml with respect to 100ml of purified water.
  3. 제 1항에 있어서,The method of claim 1,
    상기 단계 (1)의 식이섬유는 (a) 글루코만난; (b) 구아검 또는 구아검가수분해물, 차전자피, 난소화성 말토덱스트린, 대두식이섬유, 목이, 밀식이섬유, 보리식이섬유, 귀리, 아라비아검, 이눌린 및 치커리 추출물, 폴리덱스트로스, 셀룰로스, 호로파종자 및 이들의 혼합물로 이루어지는 군으로부터 선택되는 식물성 식이섬유; 및 (c) 아가, 아가로이드, 아가로즈, 알긴산, 카라기난, 커들란, 겔란, 펙틴, 이들의 겔 형성 화학 유도체 및 이들의 혼합물로 이루어지는 군으로부터 선택되는 겔 형성체로 이루어지는 것을 특징으로 하는 제조 방법.The dietary fiber of step (1) is (a) glucomannan; (b) guar gum or guar hydrolyzate, chaff, indigestible maltodextrin, soybean fiber, sore throat, wheat fiber, barley fiber, oats, gum arabic, inulin and chicory extract, polydextrose, cellulose, fenugreek seed and Vegetable dietary fiber selected from the group consisting of mixtures thereof; And (c) a gel body selected from the group consisting of agar, agaroid, agarose, alginic acid, carrageenan, curdlan, gellan, pectin, gel-forming chemical derivatives thereof, and mixtures thereof.
  4. 제 3항에 있어서,The method of claim 3, wherein
    상기 단계 (1)의 식이섬유의 비율은 (a) 글루코만난 100중량부에 대하여, (b) 식물성 식이섬유 10~100중량부 및 겔 형성체 10~200중량부인 것을 특징으로 하는 제조 방법.The ratio of the dietary fiber of step (1) is (a) to 100 parts by weight of glucomannan, (b) 10 to 100 parts by weight of vegetable fiber and 10 to 200 parts by weight of gel-forming body.
  5. 제 1항에 있어서,The method of claim 1,
    상기 단계 (8)의 식용 유기산이 글리콜산, 락트산, 사과산, 구연산, 주석산, 만델산, 살리실산 및 초산으로 이루어지는 군으로부터 1종 이상 선택되는 것을 특징으로 하는 제조 방법.The edible organic acid of step (8) is at least one selected from the group consisting of glycolic acid, lactic acid, malic acid, citric acid, tartaric acid, mandelic acid, salicylic acid and acetic acid.
  6. 제 1항에 있어서,The method of claim 1,
    상기 단계 (9)의 건조는 35~55℃ 온도에서 15~40 시간 동안 건조하여 수분 함량을 15% 이하로 건조하는 것을 특징으로 하는 제조 방법.The drying of the step (9) is a drying method for 15 to 40 hours at a temperature of 35 ~ 55 ℃ to dry the water content to 15% or less.
  7. 제 1항 내지 제 6항 중 어느 한 항의 제조 방법으로 제조되는 것을 특징으로 하는 세안 및 목욕용 약산성 식이섬유 젤리 스폰지.A weakly acidic dietary fiber jelly sponge for washing and bathing, which is prepared by the method of any one of claims 1 to 6.
PCT/KR2013/009583 2013-07-10 2013-10-25 Method for manufacturing weakly acidic natural dietary fiber jelly sponge for face washing and bathing, and weakly acidic natural dietary fiber jelly sponge manufactured thereby WO2015005535A1 (en)

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