WO2012070825A2 - 보습지속력이 우수한 메이크업 화장료 조성물 - Google Patents
보습지속력이 우수한 메이크업 화장료 조성물 Download PDFInfo
- Publication number
- WO2012070825A2 WO2012070825A2 PCT/KR2011/008896 KR2011008896W WO2012070825A2 WO 2012070825 A2 WO2012070825 A2 WO 2012070825A2 KR 2011008896 W KR2011008896 W KR 2011008896W WO 2012070825 A2 WO2012070825 A2 WO 2012070825A2
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- dimethicone
- makeup cosmetic
- cosmetic composition
- polyol
- emulsifier
- Prior art date
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/58—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
- A61K8/585—Organosilicon compounds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
- A61K8/892—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone modified by a hydroxy group, e.g. dimethiconol
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
Definitions
- the present invention relates to a makeup cosmetic composition excellent in moisturizing persistence, and more particularly, at least one selected from the group consisting of a branched type and a cross-linked polymer type polyglycerin modified dimethicone as an emulsifier.
- a makeup cosmetic composition excellent in moisturizing persistence and more particularly, at least one selected from the group consisting of a branched type and a cross-linked polymer type polyglycerin modified dimethicone as an emulsifier.
- a branched or crosslinked polyglycerin-based silicone emulsifier has a greater amount of polyol than a monomer type emulsifier or a PEG-based silicone emulsifier. It was found that it could be stabilized and the present invention was completed.
- the present invention provides a makeup cosmetic composition prepared using at least one selected from the group consisting of branched and cross-linked polyglycerol-based modified dimethicone as an emulsifier.
- the makeup cosmetic composition according to the present invention was able to stabilize a large amount of polyol by using a branched or cross-linked polyglycerol-based silicone emulsifier, and thus, a large amount of polyol was held to prevent moisture from evaporating, thereby providing excellent moisturizing sustainability. Dryness could be improved.
- the present invention provides a makeup cosmetic composition that provides instant moisturization and excellent moisturizing durability by stabilizing a large amount of polyol by using a branched and crosslinked polyglycerin-based silicone alone or mixed as an emulsifier.
- a polyglycerol-based silicone emulsifier may be used as the emulsifier, and more preferably, branched and crosslinked polyglycerol modified dimethicone may be used alone or in combination of two or more thereof.
- the branched polyglycerol-based silicone used in the present invention has the structures of the following Chemical Formulas 1 and 2, and specific examples thereof include polyglyceryl-3 disiloxane dimethicone (trade name KF-6100) manufactured by Shin Etsu Co., Ltd .; Polyglyceryl-3 polydimethyldisiloxyethyl dimethicone (trade name KF-6104) or lauryl polyglyceryl-3 polydimethyldisiloxyethyl dimethicone (trade name KF-6105), but is not limited thereto. It is not:
- the cross-linked polyglycerol-based silicone used in the present invention has the structures of the following formulas (3) and (4), and specific examples thereof are Shin-Etsu dimethicone / polyglycerin-3 cross-polymer (trade name KSG-710) or lauryl dimethicone / poly Glycerin-3 crosspolymers (trade names KSG-810, KSG-820, KSG-830 or KSG-810) and the like, but are not limited to these:
- the emulsifier in an amount of 0.1 to 20% by weight based on the total weight of the composition, and when the content of the emulsifier is less than 0.1% by weight, the emulsion is very unstable and exceeds 20.0% by weight. If you do, slippery and sticky feeling worse.
- the makeup cosmetic composition according to the present invention may further contain at least one polyol selected from the group consisting of glycerin, butylene glycol, propylene glycol, dipropylene glycol, pentylene glycol, hexylene glycol, polyethylene glycol and sorbitol as a moisturizing agent.
- the polyol may be contained in 10 to 80% by weight, more preferably in 20 to 40% by weight relative to the total weight of the composition. When the content of the polyol is less than 10% by weight, a satisfactory moisturizing sustainability cannot be obtained, and when the content of the polyol is more than 80% by weight, the user experiences a sticky and damp feeling when used.
- composition according to the present invention may further contain a skin active ingredient or various oils known in the art, the content of such oil is preferably 1 to 50% by weight relative to the total weight of the composition.
- oils include silicone oils such as dimethicone or cyclomethicone; Ester oils such as cetyl ethyl hexanoate or C12-15 alkyl benzoate; Hydrocarbon-based oils such as Hydrogenated Polydecene or Squalane, and mixtures thereof, but are not limited thereto.
- the makeup cosmetic composition according to the present invention may further contain auxiliary components such as pigments, flavors, preservatives and thickeners commonly used in manufacturing makeup cosmetics, in an amount of 0 to 20% by weight based on the total weight of the cosmetic composition.
- Makeup cosmetic composition according to the present invention is not particularly limited in the formulation, for example, it may be formulated with a water-in-oil type or oil-in-water makeup base or foundation containing a pigment, but is not limited thereto.
- Examples 1 to 3 and Comparative Examples 1 to 5 were prepared using the compositions shown in Tables 1 and 2 below (unit: wt%).
- Examples 1 to 3 of the present invention are lauryl polyglyceryl-3 polydimethyldisiloxyethyl dimethicone, which is a branched polyglycerin-based silicone emulsifier, and dimethicone / polyglycerine-3 cross-polymer, which is a crosslinked polyglycerol-based silicone emulsifier.
- Comparative Examples 1 and 2 were lauryl fiji-9 polydimethylsiloxyethyl dimethicone, which is a branched PEG-based silicone emulsifier, and dimethicone / fiji-10 /, which was a cross-linked PEG-based silicone emulsifier. 15 crosspolymers were used, and Comparative Example 3 used a monomeric emulsifier. In addition, Comparative Examples 4 and 5, using the same emulsifier as Example 3, the content of the polyol was different. Polyol was prepared using glycerin and butylene glycol.
- each of Examples 1 to 3 and Comparative Examples 1 to 5 were taken in 10 g each, and the samples were placed in a cycle chamber at room temperature, a 55 ° C thermostat and -10 to 45 ° C, respectively.
- One week stability was confirmed, and the results are shown in Table 3 below.
- the glycerin group which is a hydrophilic bonding group of the polyglycerol-based silicone emulsifier used in the present invention, is chemically similar to the polyol in the inner phase, so that the polyol can be caught with a harder binding force than the PEG-based silicone emulsifier to stabilize a large amount of polyol. .
- Comparative Example 2 since only the cross-linked emulsifier was used, huge particles having an emulsified particle size more than five times larger than the conventional one were prepared. When a large amount of polyol was contained in the inner phase, the polyol became unstable at high temperatures and cycles. Particles were broken. In Comparative Example 3, since only the mono-type emulsifier was used, it was confirmed that the emulsified particles were easily broken because the emulsification ability was weak because the silicone oil used as the main oil was not well grasped.
- Example 3 using the branched and cross-linked polyglycerol-based emulsifier at the same time, since the two emulsifiers of different sizes form the interface film more densely, the stability is more excellent than Examples 1 to 2 using only one type of emulsifier It was confirmed.
- Moisture is measured by measuring the amount of moisture in the skin's epidermis using a sensor and quantifying the amount of moisture.
- test subjects were surveyed about the improvement effect on dry skin after using each makeup cosmetic composition, and the average value of the evaluated values (five-point scale) is shown in Table 5 below.
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Emergency Medicine (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
Abstract
Description
성분 | 원료명 | 실시예 1 | 실시예 2 | 실시예 3 |
유상 성분 | 사이클로펜타실록산 | 20.00 | 20.00 | 20.00 |
세틸에틸헥사노에이트 | 10.00 | 10.00 | 10.00 | |
라우릴 폴리글리세릴-3 폴리디메틸디실록시에틸 디메치콘 | 4.00 | - | 2.00 | |
디메치콘/폴리글리세린-3 크로스 폴리머 | - | 4.00 | 2.00 | |
다이스테아르모니움헥토라이트 | 1.00 | 1.00 | 1.00 | |
파라옥시안식향산에스테르 | 적량 | 적량 | 적량 | |
착색제 | 티타늄옥사이드 및아이런옥사이드 | 10.00 | 10.00 | 10.00 |
수상 성분 | 정제수 | 잔량 | 잔량 | 잔량 |
글리세린 | 20.00 | 20.00 | 20.00 | |
부틸렌글리콜 | 20.00 | 20.00 | 20.00 | |
디소듐이디티에이 | 0.05 | 0.05 | 0.05 | |
소듐클로라이드 | 1.00 | 1.00 | 1.00 | |
페녹시에탄올 | 적량 | 적량 | 적량 |
성분 | 원료명 | 비교예 1 | 비교예 2 | 비교예 3 | 비교예 4 | 비교예 5 |
유상 성분 | 사이클로펜타실록산 | 20.00 | 20.00 | 20.00 | 20.00 | 20.00 |
세틸에틸헥사노에이트 | 10.00 | 10.0 | 10.00 | 10.00 | 10.00 | |
라우릴 폴리글리세릴-3 폴리디메틸디실록시에틸 디메치콘 | - | - | - | 2.00 | 2.00 | |
디메치콘/폴리글리세린-3 크로스 폴리머 | - | 2.00 | - | 2.00 | 2.00 | |
라우릴 피이지-9 폴리디메틸실록시에틸 디메치콘 | 2.00 | - | - | - | - | |
디메치콘/피이지-10/15 크로스폴리머 | 2.00 | 2.00 | - | - | - | |
폴리글리세릴-2 다이폴리하이드록시스테아레이트(모노머형 유화제) | - | - | 4.00 | - | - | |
다이스테아르모니움헥토라이트 | 1.00 | 1.00 | 1.00 | 1.00 | 1.00 | |
파라옥시안식향산에스테르 | 적량 | 적량 | 적량 | 적량 | 적량 | |
착색제 | 티타늄옥사이드 및아이런옥사이드 | 1.00 | 10.00 | 1.00 | 10.00 | 10.00 |
수상 성분 | 정제수 | 잔량 | 잔량 | 잔량 | 잔량 | 잔량 |
글리세린 | 20.00 | 20.00 | 20.00 | 2.50 | 4.50 | |
부틸렌글리콜 | 20.00 | 20.00 | 20.00 | 2.50 | 4.50 | |
디소듐이디티에이 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | |
소듐클로라이드 | 1.00 | 1.00 | 1.00 | 1.00 | 1.00 | |
페녹시에탄올 | 적량 | 적량 | 적량 | 적량 | 적량 |
시험물질 | 상온 안정도 | 고온 안정도 | 사이클 안정도 |
실시예 1 | ○ | △ | ○ |
실시예 2 | △ | △ | ○ |
실시예 3 | ○ | ○ | ○ |
비교예 1 | △ | X | △ |
비교예 2 | X | X | X |
비교예 3 | X | X | X |
비교예 4 | ○ | ○ | ○ |
비교예 5 | ○ | ○ | ○ |
<안정도 평가 기준> X: 매우 안 좋음 (일주일 안에 분리)△: 약간 안 좋음 (한달 안에 분리)○: 좋음 (한달 이상 안정) |
시험물질 | 피부 수분량(%) | ||||
도포 전 | 도포 직후 | 2시간 후 | 4시간 후 | 8시간 후 | |
실시예 1 | 34 | 48 | 47 | 45 | 43 |
실시예 2 | 36 | 49 | 43 | 44 | 42 |
실시예 3 | 35 | 50 | 44 | 39 | 45 |
비교예 4 | 36 | 35 | 36 | 34 | 34 |
비교예 5 | 34 | 42 | 38 | 36 | 37 |
시험물질 | 건조증 개선 효과 |
실시예 1 | 4.4 |
실시예 2 | 4.3 |
실시예 3 | 4.6 |
비교예 4 | 1.8 |
비교예 5 | 2.1 |
<평가기준> 5점: 매우 효과가 있다.4점: 조금 효과가 있다.3점: 보통이다.2점: 거의 효과가 없다.1점: 전혀 효과가 없다. |
Claims (6)
- 폴리글리세린계 변성 디메치콘을 함유하는 메이크업 화장료 조성물.
- 제 1항에 있어서, 상기 폴리글리세린계 변성 디메치콘은 가지형 및 가교형 폴리글리세린계 변성 디메치콘으로 이루어진 군에서 선택된 1종 이상임을 특징으로 하는 메이크업 화장료 조성물.
- 제 1항 또는 제 2항에 있어서, 상기 폴리글리세린계 변성 디메치콘은 유화제로 사용된 것임을 특징으로 하는 메이크업 화장료 조성물.
- 제 1항에 있어서, 상기 가지형 및 가교형 폴리글리세린계 변성 디메치콘은 폴리글리세릴-3 디실록산 디메치콘, 폴리글리세릴-3 폴리디메틸디실록시에틸 디메치콘, 라우릴 폴리글리세릴-3 폴리디메틸디실록시에틸 디메치콘, 디메치콘/폴리글리세린-3 크로스 폴리머 또는 라우릴 디메치콘/폴리글리세린-3 크로스폴리머임을 특징으로 하는 메이크업 화장료 조성물.
- 제 1항에 있어서, 상기 조성물은 조성물 총 중량에 대하여 10∼80 중량%의 폴리올을 더 함유하는 것임을 특징으로 하는 메이크업 화장료 조성물.
- 제 5항에 있어서, 상기 폴리올은 글리세린, 부틸렌글리콜, 프로필렌 글리콜, 디프로필렌글리콜, 펜틸렌글리콜, 헥실렌글리콜, 폴리에틸렌글리콜 및 솔비톨로 이루어진 군에서 선택된 1종 이상임을 특징으로 하는 유중수형 메이크업 화장료 조성물.
Priority Applications (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201180056672.9A CN103228260B (zh) | 2010-11-26 | 2011-11-22 | 具有良好的持久保湿性能的化妆品组合物 |
US13/988,961 US20130243714A1 (en) | 2010-11-26 | 2011-11-22 | Cosmetic makeup composition having an excellent moisture-sustaining capability |
HK13114370.6A HK1186964A1 (zh) | 2010-11-26 | 2013-12-30 | 具有良好的持久保濕性能的化妝品組合物 |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
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KR1020100119053A KR101737397B1 (ko) | 2010-11-26 | 2010-11-26 | 보습지속력이 우수한 메이크업 화장료 조성물 |
KR10-2010-0119053 | 2010-11-26 |
Publications (2)
Publication Number | Publication Date |
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WO2012070825A2 true WO2012070825A2 (ko) | 2012-05-31 |
WO2012070825A3 WO2012070825A3 (ko) | 2012-09-27 |
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PCT/KR2011/008896 WO2012070825A2 (ko) | 2010-11-26 | 2011-11-22 | 보습지속력이 우수한 메이크업 화장료 조성물 |
Country Status (5)
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US (1) | US20130243714A1 (ko) |
KR (1) | KR101737397B1 (ko) |
CN (1) | CN103228260B (ko) |
HK (1) | HK1186964A1 (ko) |
WO (1) | WO2012070825A2 (ko) |
Families Citing this family (4)
Publication number | Priority date | Publication date | Assignee | Title |
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KR101665756B1 (ko) * | 2013-12-31 | 2016-10-12 | 주식회사 풀무원 | 고함량 실리콘 유도체를 함유하는 피부 보습용 저점도 수중유형 에멀젼 상 화장료 조성물 |
WO2016069556A2 (en) | 2014-10-29 | 2016-05-06 | University Of Maryland | Methods of treating age-related symptoms in mammals and compositions therefor |
KR102453365B1 (ko) * | 2017-09-22 | 2022-10-07 | (주)아모레퍼시픽 | 고내상 유중수형 화장료 조성물 |
KR102559599B1 (ko) | 2023-03-08 | 2023-07-26 | (주)젠퓨어 | 상온 유화 공정을 이용한 화장료 조성물 제조방법 |
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JP4073389B2 (ja) * | 2003-10-31 | 2008-04-09 | 株式会社資生堂 | 油中水型乳化組成物 |
EP1579845B1 (en) * | 2004-03-22 | 2017-04-19 | L'Oréal | Cosmetic composition comprising a polyglycerolated silicone elastomer |
US20100092408A1 (en) * | 2008-10-14 | 2010-04-15 | Laurie Ellen Breyfogle | Resilient personal care composition comprising polyalkyl ether containing siloxane elastomers |
CN102223874B (zh) * | 2008-11-24 | 2014-12-31 | 宝洁公司 | 化妆品组合物 |
US20110301247A1 (en) * | 2010-06-08 | 2011-12-08 | Hayakawa Chihiro | Cosmetic product containing film-forming polymer |
-
2010
- 2010-11-26 KR KR1020100119053A patent/KR101737397B1/ko active IP Right Grant
-
2011
- 2011-11-22 CN CN201180056672.9A patent/CN103228260B/zh not_active Expired - Fee Related
- 2011-11-22 US US13/988,961 patent/US20130243714A1/en not_active Abandoned
- 2011-11-22 WO PCT/KR2011/008896 patent/WO2012070825A2/ko active Application Filing
-
2013
- 2013-12-30 HK HK13114370.6A patent/HK1186964A1/zh not_active IP Right Cessation
Patent Citations (4)
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US20060013791A1 (en) * | 2004-07-16 | 2006-01-19 | L'oreal | Cosmetic composition comprising a defined silicone polymer and a film former |
US20060013793A1 (en) * | 2004-07-16 | 2006-01-19 | Agnes Themens | Solid water-in-oil cosmetic emulsion |
US20060013843A1 (en) * | 2004-07-16 | 2006-01-19 | L'oreal | Cosmetic composition comprising a defined silicone polymer and a surfactant |
US20090252698A1 (en) * | 2008-04-03 | 2009-10-08 | L'oreal S.A. | Emulsion compositions for eyelashes |
Also Published As
Publication number | Publication date |
---|---|
CN103228260B (zh) | 2016-08-10 |
US20130243714A1 (en) | 2013-09-19 |
WO2012070825A3 (ko) | 2012-09-27 |
HK1186964A1 (zh) | 2014-03-28 |
KR20120057360A (ko) | 2012-06-05 |
KR101737397B1 (ko) | 2017-05-22 |
CN103228260A (zh) | 2013-07-31 |
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