WO2011008938A1 - Céramiques composites de titanate d'aluminium et de magnésium - Google Patents
Céramiques composites de titanate d'aluminium et de magnésium Download PDFInfo
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- WO2011008938A1 WO2011008938A1 PCT/US2010/042115 US2010042115W WO2011008938A1 WO 2011008938 A1 WO2011008938 A1 WO 2011008938A1 US 2010042115 W US2010042115 W US 2010042115W WO 2011008938 A1 WO2011008938 A1 WO 2011008938A1
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- C—CHEMISTRY; METALLURGY
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- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/46—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on titanium oxides or titanates
- C04B35/462—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on titanium oxides or titanates based on titanates
- C04B35/478—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on titanium oxides or titanates based on titanates based on aluminium titanates
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- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/64—Burning or sintering processes
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- C04B38/00—Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof
- C04B38/0006—Honeycomb structures
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- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/00474—Uses not provided for elsewhere in C04B2111/00
- C04B2111/00793—Uses not provided for elsewhere in C04B2111/00 as filters or diaphragms
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3205—Alkaline earth oxides or oxide forming salts thereof, e.g. beryllium oxide
- C04B2235/3206—Magnesium oxides or oxide-forming salts thereof
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3217—Aluminum oxide or oxide forming salts thereof, e.g. bauxite, alpha-alumina
- C04B2235/3222—Aluminates other than alumino-silicates, e.g. spinel (MgAl2O4)
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3418—Silicon oxide, silicic acids, or oxide forming salts thereof, e.g. silica sol, fused silica, silica fume, cristobalite, quartz or flint
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3427—Silicates other than clay, e.g. water glass
- C04B2235/3463—Alumino-silicates other than clay, e.g. mullite
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/36—Glass starting materials for making ceramics, e.g. silica glass
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- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/44—Metal salt constituents or additives chosen for the nature of the anions, e.g. hydrides or acetylacetonate
- C04B2235/441—Alkoxides, e.g. methoxide, tert-butoxide
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/44—Metal salt constituents or additives chosen for the nature of the anions, e.g. hydrides or acetylacetonate
- C04B2235/449—Organic acids, e.g. EDTA, citrate, acetate, oxalate
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/50—Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
- C04B2235/54—Particle size related information
- C04B2235/5418—Particle size related information expressed by the size of the particles or aggregates thereof
- C04B2235/5436—Particle size related information expressed by the size of the particles or aggregates thereof micrometer sized, i.e. from 1 to 100 micron
Definitions
- coefficient x satisfies 0.1 ⁇ x ⁇ 1.
- Alkali feldspar ((Na y Ki -y )AISi3 ⁇ 8, wherein y satisfies 0 ⁇ y ⁇ 1 ) is added to enhance sintering of aluminum magnesium titatane because of its low melting point.
- Mg x Al2(i- x ) Ti(i +X ) ⁇ 5 (wherein coefficient x satisfies 0 ⁇ x ⁇ 0.1 ) as a result of firing a mixture comprising TiO 2 , AI 2 O 3 , MgO, and SiO 2 , as expressed on a weight percent oxide basis of 36.0 - 57.0 % of TiO 2 ; 41.5 - 62.0% of AI 2 O 3 ; and 0 - 2.2 % of MgO with the sum total of the TiO 2 , AI 2 O 3 , MgO adding up to 100%, and the addition of 0 - 10% Of SiO 2 .
- Another embodiment of the present invention is a process for producing a ceramic comprising the following steps: a) combining TiO 2 , AI 2 O 3 , MgO, and SiO 2 to form a mixture, as expressed on a weight percent oxide basis of 36.0 - 57.0 % Of TiO 2 ; 41.5 - 62.0% Of AI 2 O 3 ; and 0 - 2.2 % of MgO with the sum total of the TiO 2 , AI 2 O 3 , MgO adding up to 100%, and the addition of 0 - 10% of SiO 2 ; b) mixing the mixture; b) drying the mixture, c) firing the mixture at a temperature in a range from 1200 0 C to 1700 0 C.
- the silica source is a compound to give a silicon ingredient to be in the aluminium magnesium titanate composite ceramic, and for example, includes silicon oxide (silica) such as silicon dioxide, silicon monoxide, etc.
- the silica source also includes a powder of a compound capable of being led into silica by firing alone in air.
- the compound includes, for example, silicic acid, silicon carbide, silicon nitride, silicon sulfide, silicon tetrachloride, silicon acetate, sodium silicate, sodium orthosilicate, glass frit, etc. Preferred are glass frit and the like, from the viewpoint of industrial availability.
- silica source also usable is a compound additionally serving as a titanate source, an alumina source, and magnesium source.
- Example of such compound includes any of titanate source, alumina source and/or Magnesium source, coated with silica source on a surface thereof.
- an alumina source, a magnesia source and a titania source may be mixed, preferably with stirring and grinding along with grinding media in a grinding container for producing an aluminium magnesium titanate composite ceramic having a uniform composition.
- the firing temperature may be generally from 1200 0 C to 1700 0 C from the viewpoint of easy production of aluminium magnesium titanate and from the practicability, preferably from 1400 0 C to 1600 0 C.
- the heating rate up to the firing temperature may be generally from 10°C/hr to 500°C/hr
- the firing may be attained by batch process or by continuous process, and may be attained in a static mode or a fluidized mode.
- the time to be taken for the firing may be a time enough for production of aluminium magnesium titanate from the mixture, and may vary depending on the amount of the mixture used, the type of the firing furnace, the firing temperature, the firing atmosphere and others, but may be generally from 10 minutes to 24 hours.
- the firing temperature is at least 1 ,200 0 C.
- the composite ceramic can have a coefficient of thermal expansion (RT30-1000 0 C) of less than 3x10 "6 (1 /K).
- the CTE (30 -
- the obtained sintered material was ground and classified to get grind powder with average grain size of about 24 micron meter.
- 10 g of the obtained grind powder was taken out, and put into a rectangular mold with the size of 10 mm x 10 mm x 50 mm, and pressed under a shaping pressure of 120 kgf/cm 2 , thereby giving a shaped ceramic.
- the shaped ceramic was again fired in air in a boxy electric furnace under the firing temperature and time as shown in the Table 1 , thereby giving a second sintered shaped ceramic.
- composition range of 41.5 to 62.0 wt% Of AI 2 O 3 and 36.0 to 57.0 wt% of TiO 2 is preferred.
- Application Example 3 is preferred.
- Application Example 6 and 7 and Comparative Example 4 were carried out in the same manner as in Example 1 and 2, except that, the compositions and firing temperatures of shaped ceramics were as shown in Table 3.
- Application Example 8 was carried out in the same manner as in Example 1 and 2, except that, TiO2 powder with SiO2 coating (about 5wt%) was used instead the silica powder and the composition and firing temperature of shaped ceramics were as shown in Table 3.
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Compositions Of Oxide Ceramics (AREA)
- Inorganic Chemistry (AREA)
Abstract
Priority Applications (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN2010800322274A CN102471170A (zh) | 2009-07-15 | 2010-07-15 | 钛酸铝镁复合陶瓷 |
AU2010273362A AU2010273362A1 (en) | 2009-07-15 | 2010-07-15 | Aluminium magnesium titanate composite ceramics |
EP10734423A EP2454214A1 (fr) | 2009-07-15 | 2010-07-15 | Céramiques composites de titanate d'aluminium et de magnésium |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US22560809P | 2009-07-15 | 2009-07-15 | |
US61/225,608 | 2009-07-15 |
Publications (1)
Publication Number | Publication Date |
---|---|
WO2011008938A1 true WO2011008938A1 (fr) | 2011-01-20 |
Family
ID=42827318
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/US2010/042115 WO2011008938A1 (fr) | 2009-07-15 | 2010-07-15 | Céramiques composites de titanate d'aluminium et de magnésium |
Country Status (4)
Country | Link |
---|---|
EP (1) | EP2454214A1 (fr) |
CN (1) | CN102471170A (fr) |
AU (1) | AU2010273362A1 (fr) |
WO (1) | WO2011008938A1 (fr) |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2012102003A (ja) * | 2010-10-12 | 2012-05-31 | Sumitomo Chemical Co Ltd | チタン酸アルミニウム質ハニカム構造体 |
WO2012101285A1 (fr) * | 2011-01-28 | 2012-08-02 | Mann+Hummel Gmbh | Corps céramique constitué d'un mélange de titanate d'aluminium |
WO2014104179A1 (fr) * | 2012-12-27 | 2014-07-03 | 住友化学株式会社 | Filtre en nid-d'abeilles et procédé de production associé, et céramique à base de titanate d'aluminium et procédé de production associé |
WO2018178436A1 (fr) | 2017-03-27 | 2018-10-04 | Torrecid, S.A | Composition et formation de matière céramique à faible coefficient de dilatation thermique et résistance élevée au choc thermique |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP6756530B2 (ja) * | 2016-07-05 | 2020-09-16 | イビデン株式会社 | ハニカム構造体及びハニカム構造体の製造方法 |
CN111675532A (zh) * | 2020-05-29 | 2020-09-18 | 秦皇岛松浦工业炉有限公司 | 一种陶瓷保温炉制造工艺 |
Citations (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS573767A (en) * | 1980-06-04 | 1982-01-09 | Nippon Toki Kk | High temperature-stable high strength aluminium titanate sintered body |
EP0335681A2 (fr) * | 1988-03-31 | 1989-10-04 | Kabushiki Kaisha Toshiba | Pièce façonnée céramique en titanate d'aluminium |
EP0506475A2 (fr) * | 1991-03-29 | 1992-09-30 | Ngk Insulators, Ltd. | Structure en titanate d'aluminium et son procédé de préparation |
US5153153A (en) | 1990-06-22 | 1992-10-06 | Bayer Aktiengesellschaft | Sintered ceramic materials based on aluminium titanate, a process for their production and their use |
US6197248B1 (en) * | 1997-08-18 | 2001-03-06 | Tsutomo Fukuda | Process for preparing aluminum titanate powder and sintered body |
WO2004039747A1 (fr) | 2002-11-01 | 2004-05-13 | Ohcera Co., Ltd. | Procede de production d'un produit fritte en titanate double de magnesium et d'aluminium |
EP1514857A1 (fr) * | 2002-04-26 | 2005-03-16 | Tsutomu Fukuda | Procede de production de briquette de titanate d'aluminium frittee |
CN1762900A (zh) * | 2004-10-18 | 2006-04-26 | 成都理工大学 | 一种合成热稳定性钛酸铝的工艺方法 |
WO2009063997A1 (fr) * | 2007-11-14 | 2009-05-22 | Hitachi Metals, Ltd. | Structure en nid d'abeilles en céramique à base de titanate d'aluminium, son procédé de production et poudre de matériau brut destinée à sa production |
WO2009093560A1 (fr) * | 2008-01-21 | 2009-07-30 | Sumitomo Chemical Company, Limited | Céramique composite d'alumine-titanate d'aluminium-magnésium |
WO2009122535A1 (fr) * | 2008-03-31 | 2009-10-08 | イビデン株式会社 | Procédé de production d'une structure en nid d'abeilles |
WO2009154219A1 (fr) * | 2008-06-18 | 2009-12-23 | 住友化学株式会社 | Procédé de production d’une céramique à base de titanate d’aluminium |
WO2010053122A1 (fr) * | 2008-11-07 | 2010-05-14 | 住友化学株式会社 | Procédé de fabrication d’une céramique à base de titanate d’aluminium |
WO2010074260A1 (fr) * | 2008-12-26 | 2010-07-01 | 住友化学株式会社 | Procédé de fabrication d'un corps fritté céramique en titanate d'aluminium, et corps fritté céramique en titanate d'aluminium |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN1233594C (zh) * | 2001-12-20 | 2005-12-28 | 罗海甦 | 一种型煤结合还原剂陶瓷煅烧方法 |
FR2857009A1 (fr) * | 2003-04-16 | 2005-01-07 | Sicat | Materiau ceramique a base de carbure de silicium pour utilisation dans des milieux agressifs |
-
2010
- 2010-07-15 WO PCT/US2010/042115 patent/WO2011008938A1/fr active Application Filing
- 2010-07-15 CN CN2010800322274A patent/CN102471170A/zh active Pending
- 2010-07-15 AU AU2010273362A patent/AU2010273362A1/en not_active Abandoned
- 2010-07-15 EP EP10734423A patent/EP2454214A1/fr not_active Withdrawn
Patent Citations (16)
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JPS573767A (en) * | 1980-06-04 | 1982-01-09 | Nippon Toki Kk | High temperature-stable high strength aluminium titanate sintered body |
EP0335681A2 (fr) * | 1988-03-31 | 1989-10-04 | Kabushiki Kaisha Toshiba | Pièce façonnée céramique en titanate d'aluminium |
US5153153A (en) | 1990-06-22 | 1992-10-06 | Bayer Aktiengesellschaft | Sintered ceramic materials based on aluminium titanate, a process for their production and their use |
EP0506475A2 (fr) * | 1991-03-29 | 1992-09-30 | Ngk Insulators, Ltd. | Structure en titanate d'aluminium et son procédé de préparation |
US6197248B1 (en) * | 1997-08-18 | 2001-03-06 | Tsutomo Fukuda | Process for preparing aluminum titanate powder and sintered body |
EP1514857A1 (fr) * | 2002-04-26 | 2005-03-16 | Tsutomu Fukuda | Procede de production de briquette de titanate d'aluminium frittee |
WO2004039747A1 (fr) | 2002-11-01 | 2004-05-13 | Ohcera Co., Ltd. | Procede de production d'un produit fritte en titanate double de magnesium et d'aluminium |
EP1559696A1 (fr) * | 2002-11-01 | 2005-08-03 | Ohcera Co., Ltd. | Procede de production d'un produit fritte en titanate double de magnesium et d'aluminium |
CN1762900A (zh) * | 2004-10-18 | 2006-04-26 | 成都理工大学 | 一种合成热稳定性钛酸铝的工艺方法 |
WO2009063997A1 (fr) * | 2007-11-14 | 2009-05-22 | Hitachi Metals, Ltd. | Structure en nid d'abeilles en céramique à base de titanate d'aluminium, son procédé de production et poudre de matériau brut destinée à sa production |
EP2221287A1 (fr) * | 2007-11-14 | 2010-08-25 | Hitachi Metals, Ltd. | Structure en nid d'abeilles en céramique à base de titanate d'aluminium, son procédé de production et poudre de matériau brut destinée à sa production |
WO2009093560A1 (fr) * | 2008-01-21 | 2009-07-30 | Sumitomo Chemical Company, Limited | Céramique composite d'alumine-titanate d'aluminium-magnésium |
WO2009122535A1 (fr) * | 2008-03-31 | 2009-10-08 | イビデン株式会社 | Procédé de production d'une structure en nid d'abeilles |
WO2009154219A1 (fr) * | 2008-06-18 | 2009-12-23 | 住友化学株式会社 | Procédé de production d’une céramique à base de titanate d’aluminium |
WO2010053122A1 (fr) * | 2008-11-07 | 2010-05-14 | 住友化学株式会社 | Procédé de fabrication d’une céramique à base de titanate d’aluminium |
WO2010074260A1 (fr) * | 2008-12-26 | 2010-07-01 | 住友化学株式会社 | Procédé de fabrication d'un corps fritté céramique en titanate d'aluminium, et corps fritté céramique en titanate d'aluminium |
Non-Patent Citations (2)
Title |
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DATABASE WPI Week 198207, Derwent World Patents Index; AN 1982-12815E, XP002604122 * |
DATABASE WPI Week 200662, Derwent World Patents Index; AN 2006-595826, XP002604123 * |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2012102003A (ja) * | 2010-10-12 | 2012-05-31 | Sumitomo Chemical Co Ltd | チタン酸アルミニウム質ハニカム構造体 |
WO2012101285A1 (fr) * | 2011-01-28 | 2012-08-02 | Mann+Hummel Gmbh | Corps céramique constitué d'un mélange de titanate d'aluminium |
US9061271B2 (en) | 2011-01-28 | 2015-06-23 | Mann+Hummel Gmbh | Ceramic body composed of an aluminum titanate mixture |
WO2014104179A1 (fr) * | 2012-12-27 | 2014-07-03 | 住友化学株式会社 | Filtre en nid-d'abeilles et procédé de production associé, et céramique à base de titanate d'aluminium et procédé de production associé |
WO2018178436A1 (fr) | 2017-03-27 | 2018-10-04 | Torrecid, S.A | Composition et formation de matière céramique à faible coefficient de dilatation thermique et résistance élevée au choc thermique |
Also Published As
Publication number | Publication date |
---|---|
CN102471170A (zh) | 2012-05-23 |
AU2010273362A1 (en) | 2011-12-01 |
EP2454214A1 (fr) | 2012-05-23 |
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