WO2010081640A3 - Verfahren und vorrichtung zur abtrennung von argon aus einem gasgemisch - Google Patents

Verfahren und vorrichtung zur abtrennung von argon aus einem gasgemisch Download PDF

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Publication number
WO2010081640A3
WO2010081640A3 PCT/EP2010/000003 EP2010000003W WO2010081640A3 WO 2010081640 A3 WO2010081640 A3 WO 2010081640A3 EP 2010000003 W EP2010000003 W EP 2010000003W WO 2010081640 A3 WO2010081640 A3 WO 2010081640A3
Authority
WO
WIPO (PCT)
Prior art keywords
gas mixture
separating
argon
separating argon
drying
Prior art date
Application number
PCT/EP2010/000003
Other languages
English (en)
French (fr)
Other versions
WO2010081640A2 (de
Inventor
Michael Wanner
Herbert Nickel
Original Assignee
Reicat Gmbh
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Reicat Gmbh filed Critical Reicat Gmbh
Priority to US13/144,330 priority Critical patent/US9139436B2/en
Priority to CN2010800046467A priority patent/CN102282100A/zh
Publication of WO2010081640A2 publication Critical patent/WO2010081640A2/de
Publication of WO2010081640A3 publication Critical patent/WO2010081640A3/de

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B23/00—Noble gases; Compounds thereof
    • C01B23/001—Purification or separation processes of noble gases
    • C01B23/0094—Combined chemical and physical processing
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/0228—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream
    • F25J3/028—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream separation of noble gases
    • F25J3/0285—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream separation of noble gases of argon
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/08—Separating gaseous impurities from gases or gaseous mixtures or from liquefied gases or liquefied gaseous mixtures
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2210/00—Purification or separation of specific gases
    • C01B2210/0001—Separation or purification processing
    • C01B2210/0003—Chemical processing
    • C01B2210/0006—Chemical processing by reduction
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2210/00—Purification or separation of specific gases
    • C01B2210/0001—Separation or purification processing
    • C01B2210/0009—Physical processing
    • C01B2210/0014—Physical processing by adsorption in solids
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2210/00—Purification or separation of specific gases
    • C01B2210/0029—Obtaining noble gases
    • C01B2210/0034—Argon
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2210/00—Purification or separation of specific gases
    • C01B2210/0043—Impurity removed
    • C01B2210/0045—Oxygen
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2210/00—Purification or separation of specific gases
    • C01B2210/0043—Impurity removed
    • C01B2210/0062—Water
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2200/00—Processes or apparatus using separation by rectification
    • F25J2200/02—Processes or apparatus using separation by rectification in a single pressure main column system
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2205/00—Processes or apparatus using other separation and/or other processing means
    • F25J2205/40—Processes or apparatus using other separation and/or other processing means using hybrid system, i.e. combining cryogenic and non-cryogenic separation techniques
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2205/00—Processes or apparatus using other separation and/or other processing means
    • F25J2205/60—Processes or apparatus using other separation and/or other processing means using adsorption on solid adsorbents, e.g. by temperature-swing adsorption [TSA] at the hot or cold end
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2205/00—Processes or apparatus using other separation and/or other processing means
    • F25J2205/82—Processes or apparatus using other separation and/or other processing means using a reactor with combustion or catalytic reaction
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2215/00—Processes characterised by the type or other details of the product stream
    • F25J2215/58—Argon
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2245/00—Processes or apparatus involving steps for recycling of process streams
    • F25J2245/58—Processes or apparatus involving steps for recycling of process streams the recycled stream being argon or crude argon
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2290/00—Other details not covered by groups F25J2200/00 - F25J2280/00
    • F25J2290/50—Arrangement of multiple equipments fulfilling the same process step in parallel

Abstract

Die vorliegende Erfindung betrifft ein Verfahren und eine Vorrichtung zur Abtrennung von Argon aus einem Gasgemisch. Das Verfahren beinhaltet die Verfahrensschritte Sammlung des Gasgemisches, Abtrennung des in dem Gasgemisch enthaltenen Sauerstoffes, Trocknung des Gasgemisches und Kryoreinigung des verbliebenen Gasgemisches zur flüssigen Abtrennung des Argons. Die Vorrichtung zur Durchführung des erfindungsgemäßen Verfahrens beinhaltet einen Sammelbehälter für das Gasgemisch, eine Baugruppe zur katalytischen und/oder adsorptiven Abtrennung von Sauerstoff aus dem Gasgemisch, eine Baugruppe zur Trocknung des Gasgemisches und eine Anlage zur Kryoreinigung des Gasgemisches und flüssigen Abtrennung des Argons.
PCT/EP2010/000003 2009-01-14 2010-01-04 Verfahren und vorrichtung zur abtrennung von argon aus einem gasgemisch WO2010081640A2 (de)

Priority Applications (2)

Application Number Priority Date Filing Date Title
US13/144,330 US9139436B2 (en) 2009-01-14 2010-01-04 Method and device for separating argon from a gas mixture
CN2010800046467A CN102282100A (zh) 2009-01-14 2010-01-04 用于分离混合气体中的氩气的方法和装置

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102009003350.5A DE102009003350C5 (de) 2009-01-14 2009-01-14 Verfahren und Vorrichtung zur Abtrennung von Argon aus einem Gasgemisch
DE102009003350.5 2009-01-14

Publications (2)

Publication Number Publication Date
WO2010081640A2 WO2010081640A2 (de) 2010-07-22
WO2010081640A3 true WO2010081640A3 (de) 2010-10-21

Family

ID=42260410

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP2010/000003 WO2010081640A2 (de) 2009-01-14 2010-01-04 Verfahren und vorrichtung zur abtrennung von argon aus einem gasgemisch

Country Status (4)

Country Link
US (1) US9139436B2 (de)
CN (2) CN105084329A (de)
DE (1) DE102009003350C5 (de)
WO (1) WO2010081640A2 (de)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102009003350C5 (de) 2009-01-14 2017-02-09 Reicat Gmbh Verfahren und Vorrichtung zur Abtrennung von Argon aus einem Gasgemisch
DE102009044249B3 (de) * 2009-10-14 2011-06-30 ReiCat GmbH, 63571 Verfahren und Vorrichtung zur Abtrennung von Argon aus einem Gasgemisch
DE102011050247B4 (de) * 2011-05-10 2019-02-21 Reicat Gmbh Verfahren und Vorrichtung zur Abtrennung von Argon aus einem Gasgemisch
JP5991330B2 (ja) * 2014-01-29 2016-09-14 信越半導体株式会社 シリコン単結晶製造装置からのアルゴンガス回収精製方法及びアルゴンガス回収精製装置
CN104383784B (zh) * 2014-11-27 2016-03-02 中国科学技术大学 从环境气体中分离提取惰性气体的系统和方法
CN110608367A (zh) * 2019-09-30 2019-12-24 苏州苏净保护气氛有限公司 一种氩气循环利用系统及方法
CN111663176B (zh) * 2020-06-18 2022-03-15 眉山博雅新材料股份有限公司 一种晶体生长方法及装置
GB2597545A (en) * 2020-07-28 2022-02-02 Edwards Ltd A noble gas recovery system
CN113277488B (zh) * 2021-07-23 2021-10-08 苏州市兴鲁空分设备科技发展有限公司 氩尾气的回收提纯方法和装置

Citations (5)

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Also Published As

Publication number Publication date
WO2010081640A2 (de) 2010-07-22
DE102009003350B3 (de) 2010-08-19
US9139436B2 (en) 2015-09-22
CN102282100A (zh) 2011-12-14
US20120085125A1 (en) 2012-04-12
CN105084329A (zh) 2015-11-25
DE102009003350C5 (de) 2017-02-09

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