WO2007063028A3 - Verfahren zur herstellung von sulfonamiden - Google Patents

Verfahren zur herstellung von sulfonamiden Download PDF

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Publication number
WO2007063028A3
WO2007063028A3 PCT/EP2006/068832 EP2006068832W WO2007063028A3 WO 2007063028 A3 WO2007063028 A3 WO 2007063028A3 EP 2006068832 W EP2006068832 W EP 2006068832W WO 2007063028 A3 WO2007063028 A3 WO 2007063028A3
Authority
WO
WIPO (PCT)
Prior art keywords
formula
equivalents
base
nitro
reacted
Prior art date
Application number
PCT/EP2006/068832
Other languages
English (en)
French (fr)
Other versions
WO2007063028A2 (de
Inventor
Thomas Schmidt
Joachim Gebhardt
Sandra Loehr
Michael Keil
Jan Hendrik Wevers
Michael Rack
Guido Mayer
Axel Pleschke
Original Assignee
Basf Ag
Thomas Schmidt
Joachim Gebhardt
Sandra Loehr
Michael Keil
Jan Hendrik Wevers
Michael Rack
Guido Mayer
Axel Pleschke
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from DE200510057681 external-priority patent/DE102005057681A1/de
Priority to CA002631113A priority Critical patent/CA2631113A1/en
Priority to KR1020137020659A priority patent/KR101422433B1/ko
Priority to EA200801432A priority patent/EA200801432A1/ru
Priority to CN2006800502073A priority patent/CN101351443B/zh
Priority to JP2008542731A priority patent/JP5555426B2/ja
Priority to US12/095,582 priority patent/US8263806B2/en
Priority to KR1020137020660A priority patent/KR101422434B1/ko
Application filed by Basf Ag, Thomas Schmidt, Joachim Gebhardt, Sandra Loehr, Michael Keil, Jan Hendrik Wevers, Michael Rack, Guido Mayer, Axel Pleschke filed Critical Basf Ag
Priority to AU2006319263A priority patent/AU2006319263B2/en
Priority to EP06830101A priority patent/EP1957443A2/de
Priority to BRPI0619760-4A priority patent/BRPI0619760A2/pt
Priority to KR1020087015883A priority patent/KR101430949B1/ko
Publication of WO2007063028A2 publication Critical patent/WO2007063028A2/de
Publication of WO2007063028A3 publication Critical patent/WO2007063028A3/de
Priority to IL191503A priority patent/IL191503A/en
Priority to IL215279A priority patent/IL215279A0/en
Priority to IL215280A priority patent/IL215280A0/en
Priority to US13/584,213 priority patent/US20120310010A1/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/36—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of amides of sulfonic acids
    • C07C303/38—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of amides of sulfonic acids by reaction of ammonia or amines with sulfonic acids, or with esters, anhydrides, or halides thereof
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/06—Preparation of nitro compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/06—Preparation of nitro compounds
    • C07C201/12—Preparation of nitro compounds by reactions not involving the formation of nitro groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/06—Preparation of nitro compounds
    • C07C201/16—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C205/00—Compounds containing nitro groups bound to a carbon skeleton
    • C07C205/13—Compounds containing nitro groups bound to a carbon skeleton the carbon skeleton being further substituted by hydroxy groups
    • C07C205/20—Compounds containing nitro groups bound to a carbon skeleton the carbon skeleton being further substituted by hydroxy groups having nitro groups and hydroxy groups bound to carbon atoms of six-membered aromatic rings
    • C07C205/21—Compounds containing nitro groups bound to a carbon skeleton the carbon skeleton being further substituted by hydroxy groups having nitro groups and hydroxy groups bound to carbon atoms of six-membered aromatic rings having nitro groups and hydroxy groups bound to carbon atoms of the same non-condensed six-membered aromatic ring
    • C07C205/22—Compounds containing nitro groups bound to a carbon skeleton the carbon skeleton being further substituted by hydroxy groups having nitro groups and hydroxy groups bound to carbon atoms of six-membered aromatic rings having nitro groups and hydroxy groups bound to carbon atoms of the same non-condensed six-membered aromatic ring having one nitro groups bound to the ring
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/36—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of amides of sulfonic acids
    • C07C303/40—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of amides of sulfonic acids by reactions not involving the formation of sulfonamide groups

Abstract

Verfahren zur Herstellung von Sulfonamiden (I) wobei die Variablen die in der Beschreibung genannten Bedeutungen haben, durch Umsetzung von m-Nitro-Benzoesäurechloriden II mit Aminosulfonen III, unter dem Einfluß von B Äquivalenten Base IV, dadurch gekennzeichnet, dass in Schritt a) das Aminosulfon III mit B1 Äquivalenten Base IV umgesetzt wird, und in Schritt b) die aus Schritt a) resultierende Reaktionsmischung mit m-Nitro- Benzoesäurechloriden II und B2 Äquivalenten Base IV umgesetzt wird; wobei B, B1 und B2 die in der Beschreibung genannten Bedeutungen haben.
PCT/EP2006/068832 2005-12-01 2006-11-23 Verfahren zur herstellung von sulfonamiden WO2007063028A2 (de)

Priority Applications (15)

Application Number Priority Date Filing Date Title
AU2006319263A AU2006319263B2 (en) 2005-12-01 2006-11-23 Method for producing sulfonamides
EP06830101A EP1957443A2 (de) 2005-12-01 2006-11-23 Verfahren zur herstellung von sulfonamiden
KR1020137020659A KR101422433B1 (ko) 2005-12-01 2006-11-23 불소화 ｍ-니트로벤조일 클로라이드의 제조 방법
BRPI0619760-4A BRPI0619760A2 (pt) 2005-12-01 2006-11-23 processo para preparar compostos
JP2008542731A JP5555426B2 (ja) 2005-12-01 2006-11-23 スルホンアミド類の製造方法
US12/095,582 US8263806B2 (en) 2005-12-01 2006-11-23 Method for producing sulfonamides
KR1020137020660A KR101422434B1 (ko) 2005-12-01 2006-11-23 불소화 ｍ-니트로벤조일 클로라이드의 제조 방법
CA002631113A CA2631113A1 (en) 2005-12-01 2006-11-23 Method for producing sulfonamides
KR1020087015883A KR101430949B1 (ko) 2005-12-01 2006-11-23 술폰아미드의 제조 방법
EA200801432A EA200801432A1 (ru) 2005-12-01 2006-11-23 Способ получения сульфонамидов
CN2006800502073A CN101351443B (zh) 2005-12-01 2006-11-23 制备磺酰胺的方法
IL191503A IL191503A (en) 2005-12-01 2008-05-15 Methods to generate sulfonamides
IL215279A IL215279A0 (en) 2005-12-01 2011-09-21 Method for producing sulfonamides
IL215280A IL215280A0 (en) 2005-12-01 2011-09-21 Method for producing sulfonamides
US13/584,213 US20120310010A1 (en) 2005-12-01 2012-08-13 Method for producing sulfonamides

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
DE102005057681.8 2005-12-01
DE200510057681 DE102005057681A1 (de) 2005-12-01 2005-12-01 Verfahren zur Herstellung fluorierter m-Nitro-Benzoesäurechloride
EP06123569 2006-11-07
EP06123569.3 2006-11-07

Related Child Applications (1)

Application Number Title Priority Date Filing Date
US13/584,213 Division US20120310010A1 (en) 2005-12-01 2012-08-13 Method for producing sulfonamides

Publications (2)

Publication Number Publication Date
WO2007063028A2 WO2007063028A2 (de) 2007-06-07
WO2007063028A3 true WO2007063028A3 (de) 2007-08-23

Family

ID=37697933

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP2006/068832 WO2007063028A2 (de) 2005-12-01 2006-11-23 Verfahren zur herstellung von sulfonamiden

Country Status (11)

Country Link
US (2) US8263806B2 (de)
EP (1) EP1957443A2 (de)
JP (1) JP5555426B2 (de)
KR (3) KR101422434B1 (de)
AR (1) AR057211A1 (de)
AU (1) AU2006319263B2 (de)
BR (1) BRPI0619760A2 (de)
CA (3) CA2821517A1 (de)
EA (2) EA200801432A1 (de)
IL (3) IL191503A (de)
WO (1) WO2007063028A2 (de)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8263806B2 (en) * 2005-12-01 2012-09-11 Basf Se Method for producing sulfonamides
EP2200978A1 (de) 2007-10-12 2010-06-30 Basf Se Verfahren zur herstelung von sulfonsäurediamiden
IL271962B (en) 2017-07-28 2022-08-01 Basf Se Preparation of 3-aryl-5-trifluoromethyl-4,2,1-converted oxadiazoles
EP3587396A1 (de) * 2018-06-27 2020-01-01 Basf Se Eine methode zur isolierung eines n-(3-nitrobenzoyl)sulfamides
CN111499506B (zh) * 2020-03-23 2021-03-30 浙江本立科技股份有限公司 一种2,4-二氯-5-氟苯甲酰氯绿色生产工艺

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5238908A (en) * 1989-08-31 1993-08-24 Rohm And Haas Company Herbicidal glutaramic acids and derivatives
WO2004039768A1 (de) * 2002-10-30 2004-05-13 Basf Aktiengesellschaft Bifunktionelle phenyliso(thio)cyanate; verfahren und zwischenprodukte zu ihrer herstellung
WO2006090210A1 (en) * 2005-02-22 2006-08-31 Miteni S.P.A. Process for the preparation of benzoic acid derivatives via a new intermediate of synthesis

Family Cites Families (26)

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DE1240853B (de) 1962-12-06 1967-05-24 Smith Kline French Lab Verfahren zur Herstellung von Sulfurylamiden
US3198785A (en) * 1964-04-17 1965-08-03 Sandoz Ag Sulfamoyl azabicyclononanes and derivatives thereof
NL175521C (nl) * 1973-04-26 1984-11-16 Hoechst Ag Werkwijze voor het bereiden van carbonzuurchloriden.
DE2933148A1 (de) * 1979-08-16 1981-02-26 Bayer Ag Verfahren zur herstellung von aromatischen dicarbonsaeuredichloriden iv
DE3040295A1 (de) * 1980-10-25 1982-06-03 Bayer Ag, 5090 Leverkusen Verfahren zur herstellung von aromatischen carbonsaeurechloriden
JPS61155350A (ja) * 1984-12-28 1986-07-15 Ihara Nikkei Kagaku Kogyo Kk 脂肪酸クロライド及び芳香族酸クロライドの製造方法
US4941909A (en) * 1987-06-19 1990-07-17 Hoffmann-La Roche Inc. Heterocyclic compounds
BR8807217A (pt) * 1987-09-23 1989-10-17 Hoffmann La Roche Compostos heterocilicos
DE3812175A1 (de) * 1988-04-13 1989-10-26 Bayer Ag Verfahren zur herstellung von carbonsaeurehalogeniden
JPH04117344A (ja) * 1990-09-05 1992-04-17 Res Assoc Util Of Light Oil 芳香族カルボン酸塩化物の製造方法
EP0721451A1 (de) * 1993-09-28 1996-07-17 Novartis AG Acylierte sulfonamide als insektizide und akarizide
KR100675245B1 (ko) * 1999-12-07 2007-01-29 바스프 악티엔게젤샤프트 Ｏ-클로로메틸벤조산 클로라이드의 제조 방법
DE19958758A1 (de) * 1999-12-07 2001-07-05 Basf Ag Verfahren zur Herstellung von o-Chlormethylbenzoesäurechloriden
JP2001187762A (ja) * 1999-12-28 2001-07-10 Nippon Light Metal Co Ltd 高純度芳香族酸クロライドの製造方法
DE60043397D1 (de) * 1999-12-28 2010-01-07 Pharmacopeia Inc Cytokine, insbesondere tnf-alpha, hemmer
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EP2200978A1 (de) 2007-10-12 2010-06-30 Basf Se Verfahren zur herstelung von sulfonsäurediamiden

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5238908A (en) * 1989-08-31 1993-08-24 Rohm And Haas Company Herbicidal glutaramic acids and derivatives
WO2004039768A1 (de) * 2002-10-30 2004-05-13 Basf Aktiengesellschaft Bifunktionelle phenyliso(thio)cyanate; verfahren und zwischenprodukte zu ihrer herstellung
WO2006090210A1 (en) * 2005-02-22 2006-08-31 Miteni S.P.A. Process for the preparation of benzoic acid derivatives via a new intermediate of synthesis

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Also Published As

Publication number Publication date
CA2821517A1 (en) 2007-06-07
KR101430949B1 (ko) 2014-08-18
US20120310010A1 (en) 2012-12-06
KR101422433B1 (ko) 2014-07-22
AR057211A1 (es) 2007-11-21
IL191503A (en) 2014-09-30
KR20080072093A (ko) 2008-08-05
US8263806B2 (en) 2012-09-11
CA2631113A1 (en) 2007-06-07
JP5555426B2 (ja) 2014-07-23
AU2006319263B2 (en) 2012-06-28
AU2006319263A1 (en) 2007-06-07
IL215280A0 (en) 2011-10-31
BRPI0619760A2 (pt) 2012-02-22
KR20130093696A (ko) 2013-08-22
EP1957443A2 (de) 2008-08-20
WO2007063028A2 (de) 2007-06-07
CA2821516A1 (en) 2007-06-07
EA201100377A1 (ru) 2011-08-30
KR20130093695A (ko) 2013-08-22
EA200801432A1 (ru) 2008-12-30
US20100228054A1 (en) 2010-09-09
JP2009517440A (ja) 2009-04-30
KR101422434B1 (ko) 2014-07-22
IL215279A0 (en) 2011-10-31

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