WO2007062276A3 - Processeur de biodiesel a ecoulement continu - Google Patents

Processeur de biodiesel a ecoulement continu Download PDF

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Publication number
WO2007062276A3
WO2007062276A3 PCT/US2006/045743 US2006045743W WO2007062276A3 WO 2007062276 A3 WO2007062276 A3 WO 2007062276A3 US 2006045743 W US2006045743 W US 2006045743W WO 2007062276 A3 WO2007062276 A3 WO 2007062276A3
Authority
WO
WIPO (PCT)
Prior art keywords
continuous flow
biodiesel processor
flow biodiesel
processor
flow
Prior art date
Application number
PCT/US2006/045743
Other languages
English (en)
Other versions
WO2007062276A2 (fr
Inventor
Randall Ames
Original Assignee
Randall Ames
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Randall Ames filed Critical Randall Ames
Publication of WO2007062276A2 publication Critical patent/WO2007062276A2/fr
Publication of WO2007062276A3 publication Critical patent/WO2007062276A3/fr

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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/1806—Stationary reactors having moving elements inside resulting in a turbulent flow of the reactants, such as in centrifugal-type reactors, or having a high Reynolds-number
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D17/00—Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/02—Separation of non-miscible liquids
    • B01D17/0208—Separation of non-miscible liquids by sedimentation
    • B01D17/0211—Separation of non-miscible liquids by sedimentation with baffles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D17/00—Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/02—Separation of non-miscible liquids
    • B01D17/0217—Separation of non-miscible liquids by centrifugal force
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D63/00—Apparatus in general for separation processes using semi-permeable membranes
    • B01D63/02—Hollow fibre modules
    • B01D63/025—Bobbin units
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/1812—Tubular reactors
    • B01J19/1818—Tubular reactors in series
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2415—Tubular reactors
    • B01J19/242—Tubular reactors in series
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/26—Nozzle-type reactors, i.e. the distribution of the initial reactants within the reactor is effected by their introduction or injection through nozzles
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/02—Liquid carbonaceous fuels essentially based on components consisting of carbon, hydrogen, and oxygen only
    • C10L1/026—Liquid carbonaceous fuels essentially based on components consisting of carbon, hydrogen, and oxygen only for compression ignition
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
    • C11C3/003—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fatty acids with alcohols
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/27—Mixers with stator-rotor systems, e.g. with intermeshing teeth or cylinders or having orifices
    • B01F27/271—Mixers with stator-rotor systems, e.g. with intermeshing teeth or cylinders or having orifices with means for moving the materials to be mixed radially between the surfaces of the rotor and the stator
    • B01F27/2711—Mixers with stator-rotor systems, e.g. with intermeshing teeth or cylinders or having orifices with means for moving the materials to be mixed radially between the surfaces of the rotor and the stator provided with intermeshing elements
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/27—Mixers with stator-rotor systems, e.g. with intermeshing teeth or cylinders or having orifices
    • B01F27/272—Mixers with stator-rotor systems, e.g. with intermeshing teeth or cylinders or having orifices with means for moving the materials to be mixed axially between the surfaces of the rotor and the stator, e.g. the stator rotor system formed by conical or cylindrical surfaces
    • B01F27/2721—Mixers with stator-rotor systems, e.g. with intermeshing teeth or cylinders or having orifices with means for moving the materials to be mixed axially between the surfaces of the rotor and the stator, e.g. the stator rotor system formed by conical or cylindrical surfaces provided with intermeshing elements
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002—Chemical plants
    • B01J2219/00004—Scale aspects
    • B01J2219/00006—Large-scale industrial plants
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/0009—Coils
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00761—Details of the reactor
    • B01J2219/00763—Baffles
    • B01J2219/00765—Baffles attached to the reactor wall
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/18—Details relating to the spatial orientation of the reactor
    • B01J2219/185—Details relating to the spatial orientation of the reactor vertical
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/19—Details relating to the geometry of the reactor
    • B01J2219/194—Details relating to the geometry of the reactor round
    • B01J2219/1941—Details relating to the geometry of the reactor round circular or disk-shaped
    • B01J2219/1943—Details relating to the geometry of the reactor round circular or disk-shaped cylindrical
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/19—Details relating to the geometry of the reactor
    • B01J2219/194—Details relating to the geometry of the reactor round
    • B01J2219/1941—Details relating to the geometry of the reactor round circular or disk-shaped
    • B01J2219/1946—Details relating to the geometry of the reactor round circular or disk-shaped conical
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00—Technologies for the production of fuel of non-fossil origin
    • Y02E50/10—Biofuels, e.g. bio-diesel

Abstract

L'invention concerne un processeur de biodiesel à écoulement continu qui utilise le mélange à haute turbulence de l'huile en cours de traitement et une cuve de séparation traversée par l'écoulement et dotée de zones distinctes et de tubes d'extraction pour la recirculation, ainsi que des procédés d'utilisation de ce processeur.
PCT/US2006/045743 2005-11-28 2006-11-28 Processeur de biodiesel a ecoulement continu WO2007062276A2 (fr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US74034605P 2005-11-28 2005-11-28
US60/740,346 2005-11-28

Publications (2)

Publication Number Publication Date
WO2007062276A2 WO2007062276A2 (fr) 2007-05-31
WO2007062276A3 true WO2007062276A3 (fr) 2009-04-23

Family

ID=38067995

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/US2006/045743 WO2007062276A2 (fr) 2005-11-28 2006-11-28 Processeur de biodiesel a ecoulement continu

Country Status (2)

Country Link
US (1) US20070175092A1 (fr)
WO (1) WO2007062276A2 (fr)

Families Citing this family (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100799597B1 (ko) * 2006-04-07 2008-01-30 (주)두웰테크놀로지 고효율 환형 반응기를 이용한 대체 연료 제조 장치 및 방법
GB2438403B (en) * 2006-05-25 2011-02-23 Viktor Fedorovych Dekhtiaruk Manufacture of biodiesel
US20100132251A1 (en) * 2006-11-07 2010-06-03 Ulrich Sohling Method for purification of biodiesel
EP1920829A1 (fr) * 2006-11-07 2008-05-14 Süd-Chemie Ag Adsorbant amorphe, procédé pour sa préparation et son utilisation pour la décolorisation des graisses et/ou huiles
US20080115407A1 (en) * 2006-11-22 2008-05-22 Hoffman Mark A System and method for producing biodiesel
DE102007019379A1 (de) * 2007-04-23 2008-10-30 Bayer Technology Services Gmbh Verfahren zur Aufreinigung von Produktgemischen aus Umesterungsreaktionen
US8052848B2 (en) * 2007-06-26 2011-11-08 The Penn State Research Foundation Ultrasonic and microwave methods for enhancing the rate of a chemical reaction and apparatus for such methods
US8901330B2 (en) * 2007-08-29 2014-12-02 Sauber Llc Method for production of biofuel
AU2014240324B2 (en) * 2007-08-29 2016-06-30 Agron Bioenergy Llc Method for production of biofuel
US20100205853A1 (en) * 2007-10-09 2010-08-19 Council Of Scientific & Industrial Research Process for the Preparation of Biodiesel from Vegetable Oils Containing High FFA
US7452515B1 (en) * 2007-11-06 2008-11-18 Biofuels Allied, Inc. System for creating a biofuel
US9080117B2 (en) * 2008-01-22 2015-07-14 GER Enterprises, LLC Biofuel production method and system
US8097049B2 (en) * 2008-02-07 2012-01-17 The Dallas Group Of America, Inc. Biodiesel purification by a continuous regenerable adsorbent process
CZ305086B6 (cs) * 2008-09-16 2015-04-29 Univerzita Pardubice Způsob výroby bionafty z rostlinných olejů, zejména z řepkového oleje
US8232419B2 (en) * 2008-10-02 2012-07-31 The Dallas Group Of America Triacylglycerol purification by a continuous regenerable adsorbent process
WO2010081063A2 (fr) * 2009-01-12 2010-07-15 Arisdyne Systems Inc. Procédé de préparation de biodiesel amélioré
BRPI1008508A2 (pt) * 2009-02-10 2018-03-13 Bio Alternative Llc "instalação móvel para a produção de biodiesel"
WO2010107446A1 (fr) * 2009-03-19 2010-09-23 Green Earth Fuels, Llc Système de filtration par trempage à froid de biodiesel
AR074573A1 (es) * 2009-12-09 2011-01-26 Biocombustibles Y En Alternativas Als S A Un procedimiento continuo para producir combustible biodiesel
US9028697B2 (en) * 2011-02-01 2015-05-12 Masatoshi Matsumura Methods and apparatus for controlling moisture in plant oils and liquid biofuels
CA2768717C (fr) * 2011-12-20 2021-03-02 The Biofuel Partnership Limited Un systeme et un appareil de fabrication de biodiesel
US8304566B2 (en) 2012-03-09 2012-11-06 Antonio Cantizani Processes and apparatus for small-scale in situ biodiesel production
US9475029B2 (en) * 2013-08-28 2016-10-25 Louisiana Eco Green, L.L.C. Method of manufacturing bio-diesel and reactor
NL2017029B1 (en) * 2016-06-23 2018-01-17 Flowid Holding B V Spinning disc reactor

Citations (5)

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US1670593A (en) * 1923-12-03 1928-05-22 Barrett Co Mixing machine and process
US3738492A (en) * 1972-03-17 1973-06-12 Brunswick Corp Oil-water separator
EP0249463A2 (fr) * 1986-06-11 1987-12-16 Bio-Energy Technology Ltd. Production d'un biocombustible
US5514820A (en) * 1989-09-29 1996-05-07 Henkel Kommanditgesellschaft Auf Aktien Continuous process for the production of lower alkyl esters
US6015440A (en) * 1997-10-31 2000-01-18 Board Of Regents Of The University Of Nebraska Process for producing biodiesel fuel with reduced viscosity and a cloud point below thirty-two (32) degrees fahrenheit

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DE4209779C1 (fr) * 1992-03-26 1993-07-15 Oelmuehle Leer Connemann Gmbh & Co., 2950 Leer, De
US6174501B1 (en) * 1997-10-31 2001-01-16 The Board Of Regents Of The University Of Nebraska System and process for producing biodiesel fuel with reduced viscosity and a cloud point below thirty-two (32) degrees fahrenheit
NZ504648A (en) * 1997-11-24 2002-02-01 Energea Umwelttechnologie Gmbh Method and equipment for producing fatty acid methyl ester to produce diesel fuel where the fatty acids are transesterified to fatty acid methyl ester
DE59813936D1 (de) * 1998-04-29 2007-04-19 Sulzer Chemtech Ag Verfahren zum Trennen einer ersten von einer zweiten Flüssigkeit
US20030032826A1 (en) * 2001-07-20 2003-02-13 The Board Of Regents Of The University Of Nebraska Transesterification process for production of biodiesel
WO2003022961A1 (fr) * 2001-09-09 2003-03-20 Bio-Clean Fuels, Inc. Procede et appareil de fabrication de biodiesel
DE50309376D1 (de) * 2002-08-23 2008-04-24 Gapes J Richard Um- und veresterung von fetts uren und triglycerid herstellung von fettsäuremethylestern
DE10243700A1 (de) * 2002-09-20 2004-04-01 Oelmühle Leer Connemann Gmbh & Co. Verfahren und Vorrichtung zur Herstellung von Biodiesel
US20050027137A1 (en) * 2003-07-29 2005-02-03 Hooker Jeffrey D. Apparatus and method for the production of fatty acid alkyl ester

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1670593A (en) * 1923-12-03 1928-05-22 Barrett Co Mixing machine and process
US3738492A (en) * 1972-03-17 1973-06-12 Brunswick Corp Oil-water separator
EP0249463A2 (fr) * 1986-06-11 1987-12-16 Bio-Energy Technology Ltd. Production d'un biocombustible
US5514820A (en) * 1989-09-29 1996-05-07 Henkel Kommanditgesellschaft Auf Aktien Continuous process for the production of lower alkyl esters
US6015440A (en) * 1997-10-31 2000-01-18 Board Of Regents Of The University Of Nebraska Process for producing biodiesel fuel with reduced viscosity and a cloud point below thirty-two (32) degrees fahrenheit

Also Published As

Publication number Publication date
US20070175092A1 (en) 2007-08-02
WO2007062276A2 (fr) 2007-05-31

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