WO2005103329A3 - Manufacturing method - Google Patents

Manufacturing method Download PDF

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Publication number
WO2005103329A3
WO2005103329A3 PCT/GB2005/001524 GB2005001524W WO2005103329A3 WO 2005103329 A3 WO2005103329 A3 WO 2005103329A3 GB 2005001524 W GB2005001524 W GB 2005001524W WO 2005103329 A3 WO2005103329 A3 WO 2005103329A3
Authority
WO
WIPO (PCT)
Prior art keywords
electrode
solution
mixture
making
substrate
Prior art date
Application number
PCT/GB2005/001524
Other languages
French (fr)
Other versions
WO2005103329A2 (en
Inventor
Jan Augustynski
Martine Ulmann
Renata Solarska
Original Assignee
Hydrogen Solar Ltd
Jan Augustynski
Martine Ulmann
Renata Solarska
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hydrogen Solar Ltd, Jan Augustynski, Martine Ulmann, Renata Solarska filed Critical Hydrogen Solar Ltd
Priority to AU2005235787A priority Critical patent/AU2005235787A1/en
Publication of WO2005103329A2 publication Critical patent/WO2005103329A2/en
Publication of WO2005103329A3 publication Critical patent/WO2005103329A3/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
    • C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
    • C23C18/1225—Deposition of multilayers of inorganic material
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
    • C03C17/22—Surface treatment of glass, not in the form of fibres or filaments, by coating with other inorganic material
    • C03C17/23—Oxides
    • C03C17/25—Oxides by deposition from the liquid phase
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
    • C03C17/34—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions
    • C03C17/3411—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions with at least two coatings of inorganic materials
    • C03C17/3417—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions with at least two coatings of inorganic materials all coatings being oxide coatings
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
    • C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
    • C23C18/1204—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material inorganic material, e.g. non-oxide and non-metallic such as sulfides, nitrides based compounds
    • C23C18/1208—Oxides, e.g. ceramics
    • C23C18/1216—Metal oxides
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
    • C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
    • C23C18/1229—Composition of the substrate
    • C23C18/1245—Inorganic substrates other than metallic
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
    • C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
    • C23C18/125—Process of deposition of the inorganic material
    • C23C18/1287—Process of deposition of the inorganic material with flow inducing means, e.g. ultrasonic
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C2217/00—Coatings on glass
    • C03C2217/20—Materials for coating a single layer on glass
    • C03C2217/21—Oxides
    • C03C2217/219—CrOx, MoOx, WOx
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C2218/00—Methods for coating glass
    • C03C2218/10—Deposition methods
    • C03C2218/11—Deposition methods from solutions or suspensions
    • C03C2218/113—Deposition methods from solutions or suspensions by sol-gel processes
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/30—Hydrogen technology
    • Y02E60/36—Hydrogen production from non-carbon containing sources, e.g. by water electrolysis

Abstract

An embodiment of the invention pertains to a method of making an electrode which comprises a WO3 film, the method comprising the steps of: (a) forming a colloidal solution of a mixture of tungstic acid and at least one organic material, (b) ultrasonically stirring said colloidal solution; (c) applying a layer of said solution to a conductive substrate, and (d) heat­treating the said substrate at a temperature of at least 350°C. Another embodiment of the invention pertains to a method of making an electrode which comprises a WO3 film, the method comprising the steps of: (a) forming a colloidal solution of a mixture of tungstic acid and at least organic material, (b) adding to said mixture a solution comprised of a soluble Lithium salt; (c) applying a layer of said solution to a conductive substrate, and (d) heat­treating the said substrate at a temperature of at least 350°C. An electrode and photoelectrical systems using that electrode are also disclosed in conjunction with methods for making colloidal solutions for use in the aforementioned electrode manufacturing methods.
PCT/GB2005/001524 2004-04-21 2005-04-21 Manufacturing method WO2005103329A2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
AU2005235787A AU2005235787A1 (en) 2004-04-21 2005-04-21 Manufacturing method

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
GB0408887.8 2004-04-21
GB0408887A GB2413337A (en) 2004-04-21 2004-04-21 Electrodes with tungsten oxide films

Publications (2)

Publication Number Publication Date
WO2005103329A2 WO2005103329A2 (en) 2005-11-03
WO2005103329A3 true WO2005103329A3 (en) 2006-08-10

Family

ID=32344144

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/GB2005/001524 WO2005103329A2 (en) 2004-04-21 2005-04-21 Manufacturing method

Country Status (3)

Country Link
AU (1) AU2005235787A1 (en)
GB (1) GB2413337A (en)
WO (1) WO2005103329A2 (en)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AU2007289219B2 (en) 2006-08-29 2012-07-12 The Regents Of The University Of Colorado, A Body Corporate Rapid solar-thermal conversion of biomass to syngas
CN102211789B (en) * 2010-04-08 2013-02-27 中国科学院合肥物质科学研究院 Method for preparing tungsten trioxide nano material
CN101891396B (en) * 2010-07-21 2012-05-23 陕西科技大学 Method for preparing inorganic/organic composite electrochromic film
CN101891401B (en) * 2010-07-21 2012-06-27 陕西科技大学 Method for preparing inorganic-organic composite electrochromic film
CN105481264B (en) * 2016-01-24 2018-03-20 上海应用技术学院 A kind of WO of morphology controllable3The preparation method of film
CN110803707B (en) * 2019-11-04 2022-08-12 湖南工业大学 Preparation method of titanium-doped hierarchical porous silica/nano tungsten oxide composite electrochromic film
CN110935440B (en) * 2019-12-11 2022-01-28 南昌航空大学 Preparation method and application of self-thinned porous tungsten trioxide nano sheet material
CN112047641A (en) * 2020-09-17 2020-12-08 山东金晶科技股份有限公司 Gray cover plate glass for building integrated photovoltaic and preparation method thereof
CN112047642A (en) * 2020-09-17 2020-12-08 山东金晶科技股份有限公司 Yellow cover plate glass for building integrated photovoltaic and preparation method thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3505108A (en) * 1964-06-26 1970-04-07 Corning Glass Works Tungsten bronze films
US5034246A (en) * 1990-08-15 1991-07-23 General Motors Corporation Method for forming tungsten oxide films
WO1999067181A1 (en) * 1998-06-22 1999-12-29 Universite De Geneve Method for making an electrode comprising a tungsten oxide film
WO2001002624A1 (en) * 1999-07-05 2001-01-11 Ecole Polytechnique Federale De Lausanne (Epfl) Tandem cell for water cleavage by visible light

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1191450B (en) * 1961-02-02 1965-04-22 Siemens Ag Thermoelectric semiconductor device
GB1032574A (en) * 1962-06-06 1966-06-08 Daystrom Inc Electrical resistors
DE1442437C3 (en) * 1965-03-19 1975-07-24 Efa Entwicklungs- Und Forschungs Ag, Schaan (Liechtenstein) Process for the separation of mineral oils from oil in water emulsions, suspensions, dispersions by adsorption on surface-active substances
NL7001443A (en) * 1969-02-05 1970-08-07
DE3408238A1 (en) * 1984-03-07 1985-09-19 Licentia Patent-Verwaltungs-Gmbh, 6000 Frankfurt Process for preparing a metal oxide paste for electrical discharge configurations
JPH0334931A (en) * 1989-06-30 1991-02-14 Hokkaido Togyo Kk Anti-retrovirus agent
EP0492417B1 (en) * 1990-12-21 1996-11-20 Matsushita Electric Industrial Co., Ltd. Method of manufacturing chemically adsorbed film
JPH05287539A (en) * 1992-04-10 1993-11-02 Tokyo Gas Co Ltd Coating method for conductive oxide and metal-ceramic composite separator of solid electrolyte type fuel battery produced by this method
KR100230832B1 (en) * 1997-03-21 1999-11-15 박찬구 Method for manufacturing limno2 anodization material for lithium battery
FR2774087B1 (en) * 1998-01-29 2000-02-25 Seva METHOD FOR DEPOSITING A MAGNESIUM OXIDE LAYER ON A SUBSTRATE, SUBSTRATE OBTAINED AND USE OF SAID SUBSTRATE

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3505108A (en) * 1964-06-26 1970-04-07 Corning Glass Works Tungsten bronze films
US5034246A (en) * 1990-08-15 1991-07-23 General Motors Corporation Method for forming tungsten oxide films
WO1999067181A1 (en) * 1998-06-22 1999-12-29 Universite De Geneve Method for making an electrode comprising a tungsten oxide film
WO2001002624A1 (en) * 1999-07-05 2001-01-11 Ecole Polytechnique Federale De Lausanne (Epfl) Tandem cell for water cleavage by visible light

Also Published As

Publication number Publication date
GB0408887D0 (en) 2004-05-26
WO2005103329A2 (en) 2005-11-03
GB2413337A (en) 2005-10-26
AU2005235787A1 (en) 2005-11-03

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