WO2005065378A2 - Drop ejection assembly - Google Patents
Drop ejection assembly Download PDFInfo
- Publication number
- WO2005065378A2 WO2005065378A2 PCT/US2004/043946 US2004043946W WO2005065378A2 WO 2005065378 A2 WO2005065378 A2 WO 2005065378A2 US 2004043946 W US2004043946 W US 2004043946W WO 2005065378 A2 WO2005065378 A2 WO 2005065378A2
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- fluid
- nozzle opening
- apertures
- aperture
- control
- Prior art date
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
- B41J—TYPEWRITERS; SELECTIVE PRINTING MECHANISMS, i.e. MECHANISMS PRINTING OTHERWISE THAN FROM A FORME; CORRECTION OF TYPOGRAPHICAL ERRORS
- B41J2/00—Typewriters or selective printing mechanisms characterised by the printing or marking process for which they are designed
- B41J2/005—Typewriters or selective printing mechanisms characterised by the printing or marking process for which they are designed characterised by bringing liquid or particles selectively into contact with a printing material
- B41J2/01—Ink jet
- B41J2/135—Nozzles
- B41J2/14—Structure thereof only for on-demand ink jet heads
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
- B41J—TYPEWRITERS; SELECTIVE PRINTING MECHANISMS, i.e. MECHANISMS PRINTING OTHERWISE THAN FROM A FORME; CORRECTION OF TYPOGRAPHICAL ERRORS
- B41J2/00—Typewriters or selective printing mechanisms characterised by the printing or marking process for which they are designed
- B41J2/005—Typewriters or selective printing mechanisms characterised by the printing or marking process for which they are designed characterised by bringing liquid or particles selectively into contact with a printing material
- B41J2/01—Ink jet
- B41J2/135—Nozzles
- B41J2/14—Structure thereof only for on-demand ink jet heads
- B41J2/14201—Structure of print heads with piezoelectric elements
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
- B41J—TYPEWRITERS; SELECTIVE PRINTING MECHANISMS, i.e. MECHANISMS PRINTING OTHERWISE THAN FROM A FORME; CORRECTION OF TYPOGRAPHICAL ERRORS
- B41J2/00—Typewriters or selective printing mechanisms characterised by the printing or marking process for which they are designed
- B41J2/005—Typewriters or selective printing mechanisms characterised by the printing or marking process for which they are designed characterised by bringing liquid or particles selectively into contact with a printing material
- B41J2/01—Ink jet
- B41J2/015—Ink jet characterised by the jet generation process
- B41J2/04—Ink jet characterised by the jet generation process generating single droplets or particles on demand
- B41J2/045—Ink jet characterised by the jet generation process generating single droplets or particles on demand by pressure, e.g. electromechanical transducers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
- B41J—TYPEWRITERS; SELECTIVE PRINTING MECHANISMS, i.e. MECHANISMS PRINTING OTHERWISE THAN FROM A FORME; CORRECTION OF TYPOGRAPHICAL ERRORS
- B41J2/00—Typewriters or selective printing mechanisms characterised by the printing or marking process for which they are designed
- B41J2/005—Typewriters or selective printing mechanisms characterised by the printing or marking process for which they are designed characterised by bringing liquid or particles selectively into contact with a printing material
- B41J2/01—Ink jet
- B41J2/135—Nozzles
- B41J2/14—Structure thereof only for on-demand ink jet heads
- B41J2/1433—Structure of nozzle plates
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
- B41J—TYPEWRITERS; SELECTIVE PRINTING MECHANISMS, i.e. MECHANISMS PRINTING OTHERWISE THAN FROM A FORME; CORRECTION OF TYPOGRAPHICAL ERRORS
- B41J2/00—Typewriters or selective printing mechanisms characterised by the printing or marking process for which they are designed
- B41J2/005—Typewriters or selective printing mechanisms characterised by the printing or marking process for which they are designed characterised by bringing liquid or particles selectively into contact with a printing material
- B41J2/01—Ink jet
- B41J2/135—Nozzles
- B41J2/14—Structure thereof only for on-demand ink jet heads
- B41J2002/14475—Structure thereof only for on-demand ink jet heads characterised by nozzle shapes or number of orifices per chamber
Definitions
- This invention relates to ejecting drops.
- Inkjet printers are one type of apparatus for depositing drops on a substrate.
- Inkjet printers typically include an ink path from an ink supply to a nozzle path. The nozzle path terminates in a nozzle opening from which ink drops are ejected.
- Ink drop ejection is typically controlled by pressurizing ink in the ink path with an actuator, which may be, for example, a piezoelectric deflector, a thermal bubble jet generator, or an electrostatically deflected element.
- a typical print assembly has an array of ink paths with corresponding nozzle openings and associated actuators. Drop ejection from each nozzle opening can be independently controlled.
- each actuator is fired to selectively eject a drop at a specific pixel location of an image as the print assembly and a printing substrate are moved relative to one another.
- the nozzle openings typically have a diameter of 50 microns or less, e.g. around 25 microns, are separated at a pitch of 100-300 nozzles/inch, have a resolution of 100 to 3000 dpi or more, and provide drops with a volume of about 1 to 120 picoliters (pL) or less.
- Drop ejection frequency is typically 10 kHz or more.
- 5,265,315 describes a print assembly that has a semiconductor body and a piezoelectric actuator.
- the body is made of silicon, which is etched to define ink chambers. Nozzle openings are defined by a separate nozzle plate, which is attached to the silicon body.
- the piezoelectric actuator has a layer of piezoelectric material, which changes geometry, or bends, in response to an applied voltage. The bending of the piezoelectric layer pressurizes ink in a pumping chamber located along the ink path.
- Piezoelectric ink jet print assemblies are also described in Fishbeck et al. U.S. Patent No. 4,825,227, Hine U.S. Patent No. 4,937,598, Moynihan et al. U.S. Patent No. 5,659,346 and Hoisington U.S. Patent No. 5,757,391, the entire contents of which are hereby incorporated by reference.
- the invention features a drop ejection device that includes a flow path in which fluid is pressured to eject drops from a nozzle opening, a piezoelectric actuator for pressurizing the fluid, and one or more waste fluid control apertures proximate the nozzle opening.
- the aperture is in communication with a vacuum source.
- the invention features an ejecting fluid by providing a fluid drop ejection apparatus including a nozzle opening and at least one waste fluid control aperture, the waste fluid control aperture in communication with a vacuum, and ejection of fluid at a frequency of about 10 KHZ or greater, and drawing waste fluid through said apparatus in an amount of about 5% or less of the fluid ejected at an operating vacuum of about 5 inwg or less.
- Vacuum pressures herein are in inches of water gauge, inwg.
- the invention features an ejecting fluid providing a fluid drop ejection apparatus including a nozzle opening and at least one waste fluid control aperture, and without ejecting a drop, directing a bolus of said fluid through the nozzle opening in a manner to communicate with the aperture.
- the invention features a drop ejection device with a flow path in which fluid is pressurized to eject drops from a nozzle opening, a piezoelectric actuator, and one or more fluid control apertures.
- the fluid control apertures are spaced from the nozzle opening by a distance of about 200% of the nozzle opening width or less, and each aperture has an aperture width of about 30% or less than the width of the nozzle opening.
- Other aspects or embodiments may include combinations of the features in the aspects above and/or one or more of the following.
- the fluid control apertures are spaced from the nozzle opening by about 200% of the nozzle opening width or less.
- the fluid control apertures are spaced from the nozzle opening by about 200% to about 1000% of the nozzle opening width or less.
- the control apertures are in communication with the flow path in which fluid is pressurized. Each control aperture has a fluid resistance of about 25 times or more than the fluidic resistance of the nozzle opening.
- the average total flow through the apertures is about 10% or less than the average flow through the nozzle opening.
- Each aperture has a width of about 30% or less than the width of the nozzle opening.
- the width of the nozzle opening is about 200 microns or less.
- Each control aperture has a diameter of about 10 microns or less.
- a nonwetting coating is applied proximate the nozzle opening.
- the flow path, nozzle opening, and control aperture are defined in common body.
- the body is a silicon material.
- the control apertures are isolated from the flow path.
- the control apertures include a wicking material.
- the control apertures communicate with a waste container.
- the drop ejector includes at least three apertures.
- the method includes drawing about 2% of fluid ejected at about 2 inches of water or less.
- the control aperture and the nozzle opening are in comminication with a common fluid supply and the fluid supply and the vacuum are comminicated through the fluid supply.
- the control aperture is about 30% or less the diameter of the nozzle opening.
- the method includes periodically directing a bolus of fluid to maintain fluid in the aperture.
- Embodiments may include one or more of the following advantages. Printing errors can be reduced by controlling waste ink that collects adjacent ejection nozzles, where it could interfere with ink ejection, or become disposed on the substrate and obscure an image.
- the waste ink can be controlled by directing and containing it in controlled locations by using vacuum, capillary forces, gravity and/or surface tension effects.
- the waste ink can be recycled to an ink supply, or directed to a waste container off the nozzle plate surface.
- the waste control aperture features can be formed accurately on a nozzle plate by, e.g., etching a semiconductor material such as a silicon material.
- Fig. 1 is a schematic of a drop ejection assembly.
- Fig. 2 is a top view of a portion of a nozzle plate.
- Figs. 3-3C are cross-sectional views of a nozzle illustrating drop ejection.
- Figs. 4-4A are cross-sectional views of a nozzle.
- Figs. 5-5A are cross-sectional views of a nozzle.
- Fig. 6 is a cross-sectional view of a nozzle.
- DETAILED DESCRIPTION Referring to Fig. 1, an ink jet apparatus 10 includes a reservoir 11 containing a supply of ink 12 and a passage 13 leading from the reservoir 11 to a pressure chamber 14.
- An actuator 15, e.g., a piezoelectric transducer covers the pressure chamber 14.
- the actuator is operable to force ink from the pressure chamber 14 through a passage 16 leading to a nozzle opening 17 in an nozzle plate 18, causing a drop of ink 19 to be ejected from the nozzle 17 toward a substrate 20.
- the ink jet apparatus 10 and the substrate 20 can be moved relative to one another.
- the substrate can be a continuous web that is moved between rolls 22 and 23.
- the inkjet apparatus also controls the operating pressure at the ink meniscus proximate the nozzle openings when the system is not ejecting drops.
- pressure control is provided by a vacuum source 30 such as a mechanical pump that applies a vacuum to the headspace 9 over the ink 12 in the reservoir 11.
- the vacuum is communicated through the ink to the nozzle opening 17 to prevent ink from weeping through the nozzle opening by force of gravity.
- a controller 31 e.g. a computer controller, monitors the vacuum over the ink in the reservoir 11 and adjusts the source 30 to maintain a desired vacuum in the reservoir.
- a vacuum source is provided by arranging the ink reservoir below the nozzle openings to create a vacuum proximate the nozzle openings.
- An ink level monitor (not shown) detects the level of ink, which falls as ink is consumed during a printing operation and thus increases the vacuum at the nozzles.
- a controller monitors the ink level and refills the reservoir from a bulk container when ink falls below a desired level to maintain vacuum within a desired operation range.
- the ink in which the reservoir is located far enough below the nozzles that the vacuum of the meniscus overcomes the capillary force in the nozzle, the ink can be pressurized to maintain a meniscus proximate the nozzle openings. Variations in meniscus can cause variations in drop velocity and can lead to air injection or weeping.
- the operating vacuum maintained at the meniscus is about 0.5 to about 10 inwg, e.g., about 2 to about 6 inwg.
- nozzle 17, having a nozzle width, W N is surrounded by waste ink control apertures 32, having an aperture width, W A -
- the apertures generally surround the nozzle and are spaced a distance, S, from the periphery of the nozzle.
- the apertures communicate through a lumen 34 and an opening 36 with an ink passage upstream of the nozzle opening.
- ink may collect on the nozzle plate. Over time, ink can form puddles which cause printing errors. For example, puddles near the edge of a nozzle opening can effect the trajectory, velocity or volume of the ejected drops. Also, a puddle could become large enough so that it drips onto printing substrate causing an extraneous mark.
- the puddle could also protrude far enough off the nozzle plate surface that the printing substrate comes into contact with it, causing a smear on the printing substrate.
- the apertures 32 provide a region in which waste ink can collect to avoid forming excessive puddles. Ink can be drawn into the apertures 32 by capillary force and/or by vacuum produced by the piezoelectric actuator 15 and/or the vacuum source 30.
- Figs. 3-3C the operation of the ink control apertures during drop ejection is illustrated.
- the nozzle 17 is illustrated in a non-jetting condition in which an ink meniscus 24 forms in nozzle 17.
- ink on actuation, ink is directed out of the nozzle opening 17 and a drop 19 is formed and ejected.
- ink may also protrude from apertures 32, but it is not ejected from the apertures.
- waste ink 38 may be deposited onto nozzle plate 18.
- waste ink can be disposed on the nozzle plate as the drop separates from the ink or back-splashes in flight or satellites drops can be directed back to the nozzle plate.
- Fig. 3C after drop ejection or in preparation for ejection of the next drop, the meniscus 24 is withdrawn by a vacuum.
- the vacuum may be created the vacuum source 30 and/or by the piezoelectric actuator as it is actuated from a pressurizing condition, in which the actuator pressurizes ink 12 in chamber 14 to eject a drop, to a neutral or negative condition in preparation for the next drop ejection.
- the vacuum on nozzle 17 is also communicated to ink control openings 32 so that waste ink is drawn into the openings 32 and through lumens 34 in a direction indicated by arrows 35. As a result, waste ink does not pool excessively on the nozzle plate.
- the nozzle plate, particularly the region 33 between the nozzle opening and the aperture includes a nonwetting coating, e.g. a polymer such as a fluoropolymer (e.g.
- the vacuum can also be produced by controlling the vacuum over the ink reservoir 11.
- a relatively wettable nozzle plate surface can be provided between the nozzle and the apertures and a nonwetting coating can terminate outside the circle of apertures to discourage ink flow beyond the apertures.
- the size, number, spacing and pattern of the apertures are selected to prevent excessive waste ink pooling. For example, the size and number of apertures can be selected to prevent ejection of ink from the apertures while drawing a desired amount of waste ink without requiring large additional jetting forces for drop ejection.
- the apertures have a flow resistance sufficiently greater than the nozzle opening to prevent ink ejection from the apertures during drop ejection.
- the resistance of each aperture is about 25 times or more, e.g. 100 times or 200 times or more than the resistance of the nozzle.
- the total resistance of all the actuators is selected to withdraw a desired volume of waste ink without needing to significantly increase actuator displacement.
- the increase in actuator deflection can be estimated by comparing the average flow through the apertures with the nozzle flow.
- the average flow through the apertures is about 10% or less, e.g. 5% or 2% or less of the flow through the nozzle.
- the apertures are arranged to draw, 5%, 1%, 0.5%, 0.1% or less of the ink jetted.
- the flow resistance of a round cross sectioned channel is:
- I c is the length of the channel, re is the radius, ⁇ is the fluid viscosity and R e is the resistance.
- the average flow through a channel is obtained by dividing the average pressure by this resistance.
- a system including twelve 3 micron apertures, each of which corresponds to 20% of the nozzle width, would have the following features. Because fluidic resistance varies inversely with the fourth power of diameter, apertures that have 20% of the nozzle diameter have 625 times the resistance. Twelve apertures surrounding the nozzle have a total resistance that is 52 times the resistance of the nozzle. The average flow through the apertures will be about 1/52, or 2% of the flow through the nozzle. For a piezoelectric actuator, actuation voltage, which causes the actuator displacement, increases by about 2%.
- the apertures are provided in a pattern that surrounds the nozzle opening.
- the apertures are spaced a distance, S, so that fluid does not collect adjacent the nozzle opening where it would influence drop ejection.
- the apertures are spaced closely adjacent the nozzle periphery.
- spacing is about 200 % or less, e.g., 50%) or less, e.g. 20% or less of the nozzle width.
- apertures are positioned at greater spacing from the nozzle periphery, e.g., 200 % to 1000 % or more of the nozzle diameter.
- the apertures can be provided at various spacings, including closely spaced apertures and apertures of greater spacing.
- the apertures have a width of about 30% or less, e.g. 20% or less or 5% or less than the nozzle width.
- the vacuum on the apertures during fluid withdrawal is about 0.5 to 10 inwg or more.
- the nozzle width is about 200 micron or less, e.g. 10 to 50 micron.
- the ink or other jetting fluid has a viscosity of about 1 to 40 cps.
- Multiple nozzles are provided in a nozzle plate at a pitch of about 25 nozzles/inch or more, e.g. 100-300 nozzles/inch.
- the drop volume is about 1 to 70 pL.
- a system can be operated to continuously direct ink into the control apertures 32 when not ejecting drops to avoid ink stagnation or ink drying in the apertures 32.
- the actuator 15 is controlled to cause an ink bolus 27 to extend from the nozzle 17, but without sufficient energy to eject a drop.
- control apertures 40 are in communication with a vacuum source that is isolated from the ink supply.
- apertures 40 are in communication with a channel 42 that leads to a vacuum source such as a mechanical vacuum apparatus (not shown) that intermittently or continuously creates a vacuum.
- control apertures 50 include an absorbent material 52 to encourage waste ink 38 flow by wicking or capillary action.
- the absorbent material 52 can be disposed in a channel 54 which leads to a bulk container of ink (not shown). The material 52 can protrude slightly above the surface of the nozzle plate 18.
- Suitable wicking materials include polymeric foams, e.g., a polyurethane foam, or other porous material.
- the polyurethane precursor material can be delivered to the apertures as a low viscosity fluid which polymerizes in- situ within the apertures, forming the wicking material.
- the apertures and/or the nozzle opening in any of the above described embodiments can be formed by machining, laser ablation, or chemical or plasma etching.
- the apertures can also be formed by molding, e.g., injection molding.
- the apertures and nozzle opening can be formed in a common body or in separate bodies that are assembled. For example, the nozzle opening can be formed in a body that defines other components of an ink flow path, e.g.
- a pumping chamber and the aperture can be formed in a separate body which is assembled to the body defining the nozzle opening.
- the apertures, nozzle opening, and pressure chamber are formed in a common body.
- the body can be a metal, carbon or an etchable material such as silicon material, e.g., silicon, silicon dioxide, a silicon nitride, or other etchable materials.
- Forming printhead components using etching techniques is further described in U.S. Serial No. 10/189,947, filed July 3, 2002, and U.S. Serial No. 60/510,459, filed October 10, 2003, the entire contents of both of which are hereby incorporated by reference.
- the apertures can be used in combination with other waste fluid control features such as projections described in U.S.
- a series of channels can be included on the nozzle face proximate the apertures.
- the apertures can be provided within a well or channel or proximate projections.
- the cleaning structures can be combined with a manual or automatic washing and wiping system in which a cleaning fluid is applied to the nozzle plate and wiped clean.
- the cleaning structures can collect cleaning fluid and debris rather than jetted waste ink.
- the drop ejection system can be utilized to eject fluids other than ink.
- the deposited droplets may be a UV or other radiation curable material or other material, for example, chemical or biological fluids, capable of being delivered as drops.
- the apparatus described could be part of a precision dispensing system.
- the actuator can be an electromechanical or thermal actuator.
- the actuator can be electrostatic. Other embodiments are within the scope of the following claims.
Landscapes
- Particle Formation And Scattering Control In Inkjet Printers (AREA)
- Ink Jet (AREA)
- Nozzles (AREA)
- Coating Apparatus (AREA)
- Jet Pumps And Other Pumps (AREA)
Abstract
Description
Claims
Priority Applications (4)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP04817071A EP1706270B1 (en) | 2003-12-30 | 2004-12-29 | Drop ejection assembly |
AT04817071T ATE538934T1 (en) | 2003-12-30 | 2004-12-29 | DROP EJECTION ARRANGEMENT |
KR1020067015519A KR101222582B1 (en) | 2003-12-30 | 2004-12-29 | Drop ejection assembly |
JP2006547572A JP2007516879A (en) | 2003-12-30 | 2004-12-29 | Droplet ejection assembly |
Applications Claiming Priority (8)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US10/749,816 US7121646B2 (en) | 2003-12-30 | 2003-12-30 | Drop ejection assembly |
US10/749,622 US7168788B2 (en) | 2003-12-30 | 2003-12-30 | Drop ejection assembly |
US10/749,829 US7237875B2 (en) | 2003-12-30 | 2003-12-30 | Drop ejection assembly |
US10/749,816 | 2003-12-30 | ||
US10/749,829 | 2003-12-30 | ||
US10/749,622 | 2003-12-30 | ||
US10/749,833 US7303259B2 (en) | 2003-12-30 | 2003-12-30 | Drop ejection assembly |
US10/749,833 | 2003-12-30 |
Publications (2)
Publication Number | Publication Date |
---|---|
WO2005065378A2 true WO2005065378A2 (en) | 2005-07-21 |
WO2005065378A3 WO2005065378A3 (en) | 2006-02-23 |
Family
ID=34753903
Family Applications (3)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/US2004/043776 WO2005065331A2 (en) | 2003-12-30 | 2004-12-29 | Drop ejection assembly |
PCT/US2004/043577 WO2005065294A2 (en) | 2003-12-30 | 2004-12-29 | Drop ejection assembly |
PCT/US2004/043946 WO2005065378A2 (en) | 2003-12-30 | 2004-12-29 | Drop ejection assembly |
Family Applications Before (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/US2004/043776 WO2005065331A2 (en) | 2003-12-30 | 2004-12-29 | Drop ejection assembly |
PCT/US2004/043577 WO2005065294A2 (en) | 2003-12-30 | 2004-12-29 | Drop ejection assembly |
Country Status (5)
Country | Link |
---|---|
EP (4) | EP2415606A3 (en) |
JP (4) | JP2007516878A (en) |
KR (3) | KR101220272B1 (en) |
AT (2) | ATE538933T1 (en) |
WO (3) | WO2005065331A2 (en) |
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JP5764312B2 (en) * | 2010-11-05 | 2015-08-19 | 富士フイルム株式会社 | Ink jet recording apparatus and nozzle plate cleaning method |
US8517518B2 (en) | 2010-11-09 | 2013-08-27 | Canon Kabushiki Kaisha | Recording apparatus and liquid ejection head |
JP5863337B2 (en) * | 2011-08-25 | 2016-02-16 | キヤノン株式会社 | Inkjet recording head |
FR2968597A1 (en) * | 2010-12-13 | 2012-06-15 | Centre Nat Rech Scient | INKJET DEVICE HAVING FLUID EXTRACTION MEANS AND INK JET METHOD THEREOF |
JP5934161B2 (en) * | 2013-09-09 | 2016-06-15 | 武蔵エンジニアリング株式会社 | Nozzle and liquid material discharge apparatus including the nozzle |
JP6193442B2 (en) * | 2016-05-06 | 2017-09-06 | 武蔵エンジニアリング株式会社 | Liquid material discharge device |
JP7008270B2 (en) | 2017-04-24 | 2022-01-25 | ブラザー工業株式会社 | Liquid discharger and inkjet printer |
WO2023223196A1 (en) * | 2022-05-16 | 2023-11-23 | Merxin Ltd | Nozzle arrangement |
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2004
- 2004-12-29 KR KR1020067015516A patent/KR101220272B1/en active IP Right Grant
- 2004-12-29 WO PCT/US2004/043776 patent/WO2005065331A2/en active Application Filing
- 2004-12-29 AT AT04815778T patent/ATE538933T1/en active
- 2004-12-29 EP EP11183973A patent/EP2415606A3/en not_active Withdrawn
- 2004-12-29 KR KR1020067015517A patent/KR101154554B1/en active IP Right Grant
- 2004-12-29 EP EP04815609A patent/EP1706269B1/en active Active
- 2004-12-29 KR KR1020067015519A patent/KR101222582B1/en active IP Right Grant
- 2004-12-29 JP JP2006547520A patent/JP2007516878A/en active Pending
- 2004-12-29 JP JP2006547448A patent/JP2007516876A/en active Pending
- 2004-12-29 JP JP2006547572A patent/JP2007516879A/en active Pending
- 2004-12-29 EP EP04817071A patent/EP1706270B1/en active Active
- 2004-12-29 WO PCT/US2004/043577 patent/WO2005065294A2/en active Application Filing
- 2004-12-29 EP EP04815778A patent/EP1706266B1/en active Active
- 2004-12-29 WO PCT/US2004/043946 patent/WO2005065378A2/en active Application Filing
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2011
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Non-Patent Citations (1)
Title |
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See references of EP1706270A4 * |
Also Published As
Publication number | Publication date |
---|---|
ATE538933T1 (en) | 2012-01-15 |
JP2011161926A (en) | 2011-08-25 |
EP2415606A3 (en) | 2012-05-09 |
JP2007516878A (en) | 2007-06-28 |
JP2007516876A (en) | 2007-06-28 |
EP1706270A4 (en) | 2009-08-19 |
WO2005065378A3 (en) | 2006-02-23 |
EP1706266A4 (en) | 2009-08-12 |
KR101220272B1 (en) | 2013-01-09 |
WO2005065294A3 (en) | 2005-11-17 |
EP1706269A2 (en) | 2006-10-04 |
EP1706266A2 (en) | 2006-10-04 |
WO2005065294A2 (en) | 2005-07-21 |
WO2005065331A3 (en) | 2006-12-28 |
EP1706269B1 (en) | 2012-06-13 |
JP2007516879A (en) | 2007-06-28 |
KR20060127955A (en) | 2006-12-13 |
EP1706269A4 (en) | 2009-08-19 |
JP4959013B2 (en) | 2012-06-20 |
WO2005065331A2 (en) | 2005-07-21 |
KR101222582B1 (en) | 2013-01-16 |
EP1706270A2 (en) | 2006-10-04 |
EP1706266B1 (en) | 2011-12-28 |
KR101154554B1 (en) | 2012-06-14 |
KR20060127954A (en) | 2006-12-13 |
ATE538934T1 (en) | 2012-01-15 |
KR20060127957A (en) | 2006-12-13 |
EP1706270B1 (en) | 2011-12-28 |
EP2415606A2 (en) | 2012-02-08 |
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